首页 > 最新文献

Materialwissenschaft und Werkstofftechnik最新文献

英文 中文
Sound absorption characteristics of 3-dimensional printed biodegradable structure backed with luffa fiber Schallabsorptionseigenschaften einer 3-dimensional gedruckten, biologisch abbaubaren Struktur mit Luffa-Faser-Rückseite 以丝瓜纤维为背衬的三维印刷生物可降解结构的吸音特性 以丝瓜纤维为背衬的三维印刷生物可降解结构的吸音特性
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300279
R. Tyagi, N. K. Jha, A. Tripathi, N. Ranjan, A. K. Srivastava, S. Kumar, R. Kumar

In this work, an investigation has been carried out on the sound absorption properties of the microperforated composites prepared by filling natural luffa fiber and synthetic luffa fiber. These composite structures are created by 3-dimensional printing of polylactic acid, which exhibits excellent biodegradability. After preparing the structure, the micro-perforation is done at the top of the composite with the help of a heated cylindrical drill. During the printing process, the infill density (printing parameter) and type of luffa fiber (natural and synthetic) have been varied to find out its effect on acoustic properties. Finally, a comparative study is carried out among natural luffa fiber and without using natural luffa fiber. The results showed excellent sound absorption of luffa filled structure compared to an unfilled structure. Out of three different infilled densities, the density of 5 % revealed a maximum amount of absorption, suggesting the potential applications of these structures in the field of sound absorption.

在这项工作中,对通过填充天然丝瓜纤维和合成丝瓜纤维制备的微穿孔复合材料的吸音特性进行了研究。这些复合材料结构是通过三维印刷聚乳酸制成的,聚乳酸具有良好的生物降解性。在准备好结构后,利用加热的圆柱形钻头在复合材料的顶部进行微穿孔。在印刷过程中,改变填充密度(印刷参数)和丝瓜纤维类型(天然和合成),以找出其对声学特性的影响。最后,对天然丝瓜纤维和不使用天然丝瓜纤维进行了比较研究。结果表明,与未填充的结构相比,填充了丝瓜纤维的结构具有极佳的吸音效果。在三种不同的填充密度中,5% 的密度具有最大的吸声量,这表明这些结构在吸声领域具有潜在的应用价值。
{"title":"Sound absorption characteristics of 3-dimensional printed biodegradable structure backed with luffa fiber\u0000 Schallabsorptionseigenschaften einer 3-dimensional gedruckten, biologisch abbaubaren Struktur mit Luffa-Faser-Rückseite","authors":"R. Tyagi,&nbsp;N. K. Jha,&nbsp;A. Tripathi,&nbsp;N. Ranjan,&nbsp;A. K. Srivastava,&nbsp;S. Kumar,&nbsp;R. Kumar","doi":"10.1002/mawe.202300279","DOIUrl":"https://doi.org/10.1002/mawe.202300279","url":null,"abstract":"<p>In this work, an investigation has been carried out on the sound absorption properties of the microperforated composites prepared by filling natural luffa fiber and synthetic luffa fiber. These composite structures are created by 3-dimensional printing of polylactic acid, which exhibits excellent biodegradability. After preparing the structure, the micro-perforation is done at the top of the composite with the help of a heated cylindrical drill. During the printing process, the infill density (printing parameter) and type of luffa fiber (natural and synthetic) have been varied to find out its effect on acoustic properties. Finally, a comparative study is carried out among natural luffa fiber and without using natural luffa fiber. The results showed excellent sound absorption of luffa filled structure compared to an unfilled structure. Out of three different infilled densities, the density of 5 % revealed a maximum amount of absorption, suggesting the potential applications of these structures in the field of sound absorption.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041581","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Microstructure, thermal and radiation shielding properties of aluminium-silicon-boron alloy prepared by mechanical alloying Gefüge, thermische und strahlungsabschirmende Eigenschaften einer durch mechanisches Legieren hergestellten Al-Si-B-Legierung 机械合金化制备的铝硅硼合金的微观结构、热性能和辐射屏蔽性能 机械合金化制备的铝硅硼合金的微观结构、热性能和辐射屏蔽性能
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300262
H. Yaykaşlı, H. Eskalen, M. Göğebakan, A. Sünbül, Y. Kavun

This study focused on developing microstructural, thermal, and radiation shielding changes in Al50Si25B25 powders using mechanical alloying techniques. Based on the x-ray powder diffraction data, the crystallite size and microstrain of the 100-hours milled powder were calculated as 0.25 nm and 50.33 %, respectively. The solubility of silicon in the α-aluminium matrix increased with longer mechanical alloying duration. Transmission electron microscope analyses further showed that the alloy particulates had an average size of 3 μm and an average grain size of 0.226 nm. The radiation shielding properties of the Al50Si25B25 powders indicated that the Linear Attenuation Coefficient value increased from 0.0554±0.1689 cm−1 to 1.0632±0.2425 cm−1 with an increase in the thickness of the Al50Si25B25 alloy. This work successfully demonstrated the potential of mechanical alloying techniques to enhance the microstructural and thermal properties of Al50Si25B25 powders. It highlighted their effectiveness in providing radiation shielding capabilities when varying the thickness of the alloy.

本研究的重点是利用机械合金化技术改变 Al50Si25B25 粉末的微观结构、热性能和辐射屏蔽性能。根据 X 射线粉末衍射数据,计算出 100 小时碾磨粉末的晶粒尺寸和微应变分别为 0.25 nm 和 50.33 %。硅在α-铝基体中的溶解度随着机械合金化时间的延长而增加。透射电子显微镜分析进一步表明,合金颗粒的平均尺寸为 3 μm,平均晶粒尺寸为 0.226 nm。Al50Si25B25 粉末的辐射屏蔽性能表明,随着 Al50Si25B25 合金厚度的增加,线性衰减系数值从 0.0554±0.1689 cm-1 增加到 1.0632±0.2425 cm-1。这项工作成功证明了机械合金化技术在提高 Al50Si25B25 粉末的微观结构和热性能方面的潜力。它强调了在改变合金厚度时,机械合金技术在提供辐射屏蔽能力方面的有效性。
{"title":"Microstructure, thermal and radiation shielding properties of aluminium-silicon-boron alloy prepared by mechanical alloying\u0000 Gefüge, thermische und strahlungsabschirmende Eigenschaften einer durch mechanisches Legieren hergestellten Al-Si-B-Legierung","authors":"H. Yaykaşlı,&nbsp;H. Eskalen,&nbsp;M. Göğebakan,&nbsp;A. Sünbül,&nbsp;Y. Kavun","doi":"10.1002/mawe.202300262","DOIUrl":"https://doi.org/10.1002/mawe.202300262","url":null,"abstract":"<p>This study focused on developing microstructural, thermal, and radiation shielding changes in Al<sub>50</sub>Si<sub>25</sub>B<sub>25</sub> powders using mechanical alloying techniques. Based on the x-ray powder diffraction data, the crystallite size and microstrain of the 100-hours milled powder were calculated as 0.25 nm and 50.33 %, respectively. The solubility of silicon in the α-aluminium matrix increased with longer mechanical alloying duration. Transmission electron microscope analyses further showed that the alloy particulates had an average size of 3 μm and an average grain size of 0.226 nm. The radiation shielding properties of the Al<sub>50</sub>Si<sub>25</sub>B<sub>25</sub> powders indicated that the Linear Attenuation Coefficient value increased from 0.0554±0.1689 cm<sup>−1</sup> to 1.0632±0.2425 cm<sup>−1</sup> with an increase in the thickness of the Al<sub>50</sub>Si<sub>25</sub>B<sub>25</sub> alloy. This work successfully demonstrated the potential of mechanical alloying techniques to enhance the microstructural and thermal properties of Al<sub>50</sub>Si<sub>25</sub>B<sub>25</sub> powders. It highlighted their effectiveness in providing radiation shielding capabilities when varying the thickness of the alloy.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041579","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The effect of tempering time and cooling environment on the corrosion behavior of AA5083-H111 alloy Der Einfluss der Anlasszeit und der Abkühlumgebung auf das Korrosionsverhalten der Aluminiumlegierung AA5083-H111 回火时间和冷却环境对 AA5083-H111 合金腐蚀行为的影响 回火时间和冷却环境对 AA5083-H111 铝合金腐蚀行为的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300217
İ. Karagöz, M. Buğdaycı, L. Öncel

The tempering process can increase the mechanical properties of the material, such as hardness and impact strength, as well as enhance the corrosion resistance. Therefore, the selection of appropriate tempering time and cooling environment is crucial. This study aims to investigate changes in properties such as hardness, tensile strength, corrosion resistance, and microstructure of AA5083-H111 alloy after a brief tempering process (30 minutes, 45 minutes and 60 minutes) at 320 °C, followed by cooling in air and water environments. The study found that tempering time and cooling environment significantly affect the mechanical properties and corrosion rate. The results show that samples labeled as S30 and S60 have the highest hardness and impact strength, but the best corrosion resistance is achieved in the S60 sample. This study demonstrates that even after a limited-term tempering process, the mechanical properties and corrosion resistance of AA5083-H111 alloy can be improved. This information is crucial data for use in the production and application of alloys. The findings of this study could have important implications for the production and application of AA5083-H111 alloy in industries such as aerospace, automotive, and marine engineering.

回火工艺可以提高材料的机械性能,如硬度和冲击强度,并增强耐腐蚀性。因此,选择合适的回火时间和冷却环境至关重要。本研究旨在探讨 AA5083-H111 合金在 320 °C 下进行短暂回火(30 分钟、45 分钟和 60 分钟),然后在空气和水环境中冷却后硬度、抗拉强度、耐腐蚀性和微观结构等性能的变化。研究发现,回火时间和冷却环境对机械性能和腐蚀速率有显著影响。结果表明,标为 S30 和 S60 的样品硬度和冲击强度最高,但 S60 样品的耐腐蚀性最好。这项研究表明,即使经过有限时间的回火处理,AA5083-H111 合金的机械性能和耐腐蚀性能也能得到改善。这些信息对于合金的生产和应用都是至关重要的数据。本研究的结果可能对 AA5083-H111 合金在航空航天、汽车和海洋工程等行业的生产和应用产生重要影响。
{"title":"The effect of tempering time and cooling environment on the corrosion behavior of AA5083-H111 alloy\u0000 Der Einfluss der Anlasszeit und der Abkühlumgebung auf das Korrosionsverhalten der Aluminiumlegierung AA5083-H111","authors":"İ. Karagöz,&nbsp;M. Buğdaycı,&nbsp;L. Öncel","doi":"10.1002/mawe.202300217","DOIUrl":"https://doi.org/10.1002/mawe.202300217","url":null,"abstract":"<p>The tempering process can increase the mechanical properties of the material, such as hardness and impact strength, as well as enhance the corrosion resistance. Therefore, the selection of appropriate tempering time and cooling environment is crucial. This study aims to investigate changes in properties such as hardness, tensile strength, corrosion resistance, and microstructure of AA5083-H111 alloy after a brief tempering process (30 minutes, 45 minutes and 60 minutes) at 320 °C, followed by cooling in air and water environments. The study found that tempering time and cooling environment significantly affect the mechanical properties and corrosion rate. The results show that samples labeled as S30 and S60 have the highest hardness and impact strength, but the best corrosion resistance is achieved in the S60 sample. This study demonstrates that even after a limited-term tempering process, the mechanical properties and corrosion resistance of AA5083-H111 alloy can be improved. This information is crucial data for use in the production and application of alloys. The findings of this study could have important implications for the production and application of AA5083-H111 alloy in industries such as aerospace, automotive, and marine engineering.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041583","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Research on arc evolution law of arc extin-ction device under high-speed large current Untersuchung des Lichtbogenverhaltens in Abhängigkeit des Lichtbogenabschaltgerätes bei hohen Geschwindigkeiten und hohen Stromstärken 高速大电流条件下灭弧装置的电弧演变规律研究 高速大电流条件下灭弧装置的电弧行为研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300218
M. C. Jia, T. Huang, K. X. Song, X. H. Guo, J. Feng, X. Wang, H. T. Song

The lifespan of the guide rail is a bottleneck restricting the operational life of electromagnetic railguns. A well-designed arc extinguishing device can reduce the arcing erosion caused by residual currents within the guide rail. The CuW alloy is widely used in the high-pressure arc extinction field due to its excellent electrical and thermal conductivity, high strength, and hardness. Based on the theory of equilibrium state arc plasma, a finite element model of the air arc-CuW electrode coupling in the arc extinction device was established to study millisecond-level arc initiation, evolution, extinguishing characteristics, and distribution patterns under extreme and harsh operational conditions with a current input of 110 kA. The highest temperature in the arc column region was found to exceed 50,000 K. The study elucidated the influence of arc extinction device parameters on arc evolution, breakdown time, and breakdown voltage. Consequently, it established that the R70 spherical electrode exhibits optimal arc extinguishing characteristics. The aim of this research is to provide theoretical support for optimizing the arc suppression device. Additionally, experiments on high-speed and high-current arc extinction device discharges were conducted to validate the finite element analysis results regarding arc diffusion patterns and electrode erosion.

导轨的使用寿命是限制电磁轨道炮工作寿命的瓶颈。设计精良的灭弧装置可以减少导轨内残余电流造成的电弧侵蚀。CuW 合金因其优异的导电性、导热性、高强度和硬度而被广泛应用于高压灭弧领域。基于平衡态电弧等离子体理论,建立了灭弧装置中空气电弧-CuW 电极耦合的有限元模型,研究了在输入电流为 110 kA 的极端恶劣运行条件下毫秒级电弧的起弧、演化、熄灭特性和分布模式。发现弧柱区域的最高温度超过 50,000 K。研究阐明了灭弧装置参数对电弧演化、击穿时间和击穿电压的影响。因此,研究确定 R70 球形电极具有最佳灭弧特性。这项研究旨在为优化灭弧装置提供理论支持。此外,还进行了高速大电流灭弧装置放电实验,以验证有关电弧扩散模式和电极侵蚀的有限元分析结果。
{"title":"Research on arc evolution law of arc extin-ction device under high-speed large current\u0000 Untersuchung des Lichtbogenverhaltens in Abhängigkeit des Lichtbogenabschaltgerätes bei hohen Geschwindigkeiten und hohen Stromstärken","authors":"M. C. Jia,&nbsp;T. Huang,&nbsp;K. X. Song,&nbsp;X. H. Guo,&nbsp;J. Feng,&nbsp;X. Wang,&nbsp;H. T. Song","doi":"10.1002/mawe.202300218","DOIUrl":"https://doi.org/10.1002/mawe.202300218","url":null,"abstract":"<p>The lifespan of the guide rail is a bottleneck restricting the operational life of electromagnetic railguns. A well-designed arc extinguishing device can reduce the arcing erosion caused by residual currents within the guide rail. The CuW alloy is widely used in the high-pressure arc extinction field due to its excellent electrical and thermal conductivity, high strength, and hardness. Based on the theory of equilibrium state arc plasma, a finite element model of the air arc-CuW electrode coupling in the arc extinction device was established to study millisecond-level arc initiation, evolution, extinguishing characteristics, and distribution patterns under extreme and harsh operational conditions with a current input of 110 kA. The highest temperature in the arc column region was found to exceed 50,000 K. The study elucidated the influence of arc extinction device parameters on arc evolution, breakdown time, and breakdown voltage. Consequently, it established that the R70 spherical electrode exhibits optimal arc extinguishing characteristics. The aim of this research is to provide theoretical support for optimizing the arc suppression device. Additionally, experiments on high-speed and high-current arc extinction device discharges were conducted to validate the finite element analysis results regarding arc diffusion patterns and electrode erosion.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041586","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effects of current intensities on material removal rate, electrode wear rate, and surface roughness of machining high carbon high chromium steel Auswirkungen von Stromstärken auf die Spanvolumenrate, die Elektrodenverschleißrate und die Oberflächenrauheit bei der Bearbeitung von hochgekohltem Chromstahl 电流强度对加工高碳高铬钢的材料去除率、电极磨损率和表面粗糙度的影响 电流强度对加工高碳高铬钢的切屑率、电极磨损率和表面粗糙度的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300188
P. K. Rakesh, M. K. Gupta, J. N. Mahto, N. S. Rajput

The electrical discharge machining is very successful and generally recognized for producing complicated shapes and small openings with exceptional precision. The objective of this study is to assess the impact of different electrical discharge machining parameters on the attributes of the machining process. The evaluation of the machining process was conducted based on the workpiece‘s material removal rate, the rate at which the electrodes wear, and the level of surface roughness. Simultaneously achieving a high material removal rate, low electrode wear rate, and high surface roughness is not possible with a specific combination of approaches due to their contradicting nature. Frequently, it is necessary to independently apply many measures instantaneously in order to assess their impact on various responses. This research investigates the machining of high carbon high chromium steel making use of electrical discharge machining with aluminum, copper, and graphite electrodes. The study focuses on the impact of different current intensities on the rate of material removal, electrode wear, and surface roughness. The experimental results demonstrate that the highest material removal rate (mmcubicmin−1) is achieved at a current density of 12 A when using a copper electrode (54.67), as opposed to aluminum electrode (22.91) and graphite electrode (29.43).

放电加工是一种非常成功的加工方法,在加工复杂形状和小开口时具有极高的精度,这一点已得到普遍认可。本研究的目的是评估不同放电加工参数对加工过程属性的影响。对加工过程的评估基于工件的材料去除率、电极磨损率和表面粗糙度水平。同时实现高材料去除率、低电极磨损率和高表面粗糙度是不可能的,因为它们之间存在矛盾。通常情况下,有必要在瞬间独立应用多种措施,以评估它们对各种反应的影响。本研究调查了使用铝、铜和石墨电极对高碳高铬钢进行放电加工的情况。研究重点是不同电流强度对材料去除率、电极磨损和表面粗糙度的影响。实验结果表明,使用铜电极(54.67)时,电流密度为 12 A 时的材料去除率(mmcubicmin-1)最高,而使用铝电极(22.91)和石墨电极(29.43)时的材料去除率(mmcubicmin-1)最低。
{"title":"Effects of current intensities on material removal rate, electrode wear rate, and surface roughness of machining high carbon high chromium steel\u0000 Auswirkungen von Stromstärken auf die Spanvolumenrate, die Elektrodenverschleißrate und die Oberflächenrauheit bei der Bearbeitung von hochgekohltem Chromstahl","authors":"P. K. Rakesh,&nbsp;M. K. Gupta,&nbsp;J. N. Mahto,&nbsp;N. S. Rajput","doi":"10.1002/mawe.202300188","DOIUrl":"https://doi.org/10.1002/mawe.202300188","url":null,"abstract":"<p>The electrical discharge machining is very successful and generally recognized for producing complicated shapes and small openings with exceptional precision. The objective of this study is to assess the impact of different electrical discharge machining parameters on the attributes of the machining process. The evaluation of the machining process was conducted based on the workpiece‘s material removal rate, the rate at which the electrodes wear, and the level of surface roughness. Simultaneously achieving a high material removal rate, low electrode wear rate, and high surface roughness is not possible with a specific combination of approaches due to their contradicting nature. Frequently, it is necessary to independently apply many measures instantaneously in order to assess their impact on various responses. This research investigates the machining of high carbon high chromium steel making use of electrical discharge machining with aluminum, copper, and graphite electrodes. The study focuses on the impact of different current intensities on the rate of material removal, electrode wear, and surface roughness. The experimental results demonstrate that the highest material removal rate (mm<sup>cubic</sup>min<sup>−1</sup>) is achieved at a current density of 12 A when using a copper electrode (54.67), as opposed to aluminum electrode (22.91) and graphite electrode (29.43).</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041544","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
In vitro degradation behavior of grain refined WE43 magnesium alloy for biodegradable temporary implant applications In vitro-Abbauverhalten einer kornverfeinerten Magnesiumlegierung (MgY4RE3) für biologisch abbaubare temporäre Implantate 用于生物可降解临时植入物的晶粒细化 WE43 镁合金的体外降解行为体外降解镁合金 (MgY4RE3) 用于生物可降解临时植入物的体外降解行为
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300296
V. S. S. H. Vardhan, A. Sharma

In the present work, grain-refined WE43 magnesium alloy was produced by friction stir processing to investigate the in vitro degradation behavior targeted for temporary bone implant applications. Friction stir processing resulted in significant grain refinement (from 46±4.2 μm to 16.1±5.4 μm) as observed from microstructural studies. Increased wettability was observed from the contact angle measurements in grain-refined WE43 alloy. The corrosion behavior of the base alloy and the grain refined alloy assessed by potentiodynamic polarization tests demonstrated the influence of the smaller grain size and decreased intermetallics on enhancing corrosion resistance. Immersion studies carried out in simulated body fluids for one week indicated a quick development of the protective magnesium hydroxide on the surface of grain-refined WE43 alloy compared with the base alloy. The deposition of the mineral phases from the immersed solution on the surface of the samples was studied by scanning electron microscopy and x-ray diffraction analysis to assess the effect of microstructure on the biomineralization. Promisingly, grain refined WE43 exhibited relatively excellent mineral deposition which further helped to control the degradation of the alloy. The weight loss measurements of the samples from the immersion tests were also in good agreement with the electrochemical test results. Hence, the results demonstrate the promising role of grain refinement by friction stir processing in tailoring WE43 magnesium alloy with better degradation behavior for temporary bone implant applications.

在本研究中,通过搅拌摩擦加工制备了晶粒细化的 WE43 镁合金,以研究针对临时骨植入应用的体外降解行为。从微观结构研究中观察到,搅拌摩擦加工导致晶粒明显细化(从 46±4.2 μm 到 16.1±5.4 μm)。接触角测量结果表明,晶粒细化的 WE43 合金的润湿性有所提高。通过电位极化测试评估的基合金和晶粒细化合金的腐蚀行为表明,晶粒尺寸变小和金属间化合物减少对提高耐腐蚀性有影响。在模拟体液中进行的为期一周的浸泡研究表明,与基合金相比,晶粒细化的 WE43 合金表面迅速形成了氢氧化镁保护层。通过扫描电子显微镜和 X 射线衍射分析,研究了浸泡液中的矿物相在样品表面的沉积情况,以评估微观结构对生物矿化的影响。令人欣喜的是,晶粒细化的 WE43 表现出相对优异的矿物沉积,这进一步帮助控制了合金的降解。浸泡测试中样品的失重测量结果与电化学测试结果也十分吻合。因此,研究结果表明,通过搅拌摩擦加工进行晶粒细化,可使 WE43 镁合金具有更好的降解性能,从而有望用于临时骨植入物。
{"title":"In vitro degradation behavior of grain refined WE43 magnesium alloy for biodegradable temporary implant applications\u0000 In vitro-Abbauverhalten einer kornverfeinerten Magnesiumlegierung (MgY4RE3) für biologisch abbaubare temporäre Implantate","authors":"V. S. S. H. Vardhan,&nbsp;A. Sharma","doi":"10.1002/mawe.202300296","DOIUrl":"https://doi.org/10.1002/mawe.202300296","url":null,"abstract":"<p>In the present work, grain-refined WE43 magnesium alloy was produced by friction stir processing to investigate the in vitro degradation behavior targeted for temporary bone implant applications. Friction stir processing resulted in significant grain refinement (from 46±4.2 μm to 16.1±5.4 μm) as observed from microstructural studies. Increased wettability was observed from the contact angle measurements in grain-refined WE43 alloy. The corrosion behavior of the base alloy and the grain refined alloy assessed by potentiodynamic polarization tests demonstrated the influence of the smaller grain size and decreased intermetallics on enhancing corrosion resistance. Immersion studies carried out in simulated body fluids for one week indicated a quick development of the protective magnesium hydroxide on the surface of grain-refined WE43 alloy compared with the base alloy. The deposition of the mineral phases from the immersed solution on the surface of the samples was studied by scanning electron microscopy and x-ray diffraction analysis to assess the effect of microstructure on the biomineralization. Promisingly, grain refined WE43 exhibited relatively excellent mineral deposition which further helped to control the degradation of the alloy. The weight loss measurements of the samples from the immersion tests were also in good agreement with the electrochemical test results. Hence, the results demonstrate the promising role of grain refinement by friction stir processing in tailoring WE43 magnesium alloy with better degradation behavior for temporary bone implant applications.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041582","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Chemical treatment, fibre length, and fibre loading affecting the mechanical and morphological characteristics of flax fibre/polylactic acid (PLA) green composites developed by injection moulding Einfluss von chemischer Behandlung, Faserlänge und Faserbelastung auf die mechanischen und morphologischen Eigenschaften von im Spritzgiessverfahren hergestellten grünen Verbundwerkstoffen aus Flachsfasern/Polymilchsäure (PLA) 化学处理、纤维长度和纤维负载对注塑成型亚麻纤维/聚乳酸(PLA)绿色复合材料机械和形态特性的影响 化学处理、纤维长度和纤维负载对注塑成型亚麻纤维/聚乳酸(PLA)绿色复合材料机械和形态特性的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300316
M. Debnath, P. Chakraborti, G. S. Rao

This paper presents the parametric investigation and optimization of various chemical treatment parameters that affect the mechanical performance of the green composite. The injection moulding method was used to produce the green composites using flax fibre (FF) and polylactic acid (PLA). The chemical parameters chosen to investigate their effects are chemical type (sodium hydroxide, sodium carbonate, and potassium hydroxide), chemical concentrations (1 %, 2 %, and 3 % (w/v)), and duration for fibre treatment (2 h, 4 h, and 6 h). The mechanical performance of the green composites was assessed by evaluating the various properties namely strength, modulus, and elongation under tensile, share, flexural, and compression loading conditions. The morphological study was also performed to examine the failure behavior of the composite after mechanical testing. The effect of fibre length (2 mm, 3 mm, 4 mm, 5 mm, and 6 mm) and fibre loading (10 wt.%, 20 wt.%, and 30 wt.%) on the performance of the flax fibre (FF)/polylactic acid (PLA) composite was also investigated. The fibre dispersion, fibre orientation, and fibre length retention were investigated to assess the characteristics of fibre during injection moulding of the developed flax fibre (FF)/polylactic acid (PLA) composite.

本文对影响绿色复合材料机械性能的各种化学处理参数进行了参数研究和优化。采用注塑成型法生产亚麻纤维(FF)和聚乳酸(PLA)绿色复合材料。为研究其影响而选择的化学参数包括化学类型(氢氧化钠、碳酸钠和氢氧化钾)、化学浓度(1%、2% 和 3%(w/v))以及纤维处理时间(2 小时、4 小时和 6 小时)。通过评估绿色复合材料在拉伸、共用、弯曲和压缩加载条件下的各种性能,即强度、模量和伸长率,对其机械性能进行了评估。此外,还进行了形态学研究,以检查复合材料在机械测试后的失效行为。此外,还研究了纤维长度(2 毫米、3 毫米、4 毫米、5 毫米和 6 毫米)和纤维负载(10 wt.%、20 wt.% 和 30 wt.%)对亚麻纤维(FF)/聚乳酸(PLA)复合材料性能的影响。研究了纤维分散、纤维取向和纤维长度保持,以评估亚麻纤维(FF)/聚乳酸(PLA)复合材料在注塑成型过程中的纤维特性。
{"title":"Chemical treatment, fibre length, and fibre loading affecting the mechanical and morphological characteristics of flax fibre/polylactic acid (PLA) green composites developed by injection moulding\u0000 Einfluss von chemischer Behandlung, Faserlänge und Faserbelastung auf die mechanischen und morphologischen Eigenschaften von im Spritzgiessverfahren hergestellten grünen Verbundwerkstoffen aus Flachsfasern/Polymilchsäure (PLA)","authors":"M. Debnath,&nbsp;P. Chakraborti,&nbsp;G. S. Rao","doi":"10.1002/mawe.202300316","DOIUrl":"https://doi.org/10.1002/mawe.202300316","url":null,"abstract":"<p>This paper presents the parametric investigation and optimization of various chemical treatment parameters that affect the mechanical performance of the green composite. The injection moulding method was used to produce the green composites using flax fibre (FF) and polylactic acid (PLA). The chemical parameters chosen to investigate their effects are chemical type (sodium hydroxide, sodium carbonate, and potassium hydroxide), chemical concentrations (1 %, 2 %, and 3 % (w/v)), and duration for fibre treatment (2 h, 4 h, and 6 h). The mechanical performance of the green composites was assessed by evaluating the various properties namely strength, modulus, and elongation under tensile, share, flexural, and compression loading conditions. The morphological study was also performed to examine the failure behavior of the composite after mechanical testing. The effect of fibre length (2 mm, 3 mm, 4 mm, 5 mm, and 6 mm) and fibre loading (10 wt.%, 20 wt.%, and 30 wt.%) on the performance of the flax fibre (FF)/polylactic acid (PLA) composite was also investigated. The fibre dispersion, fibre orientation, and fibre length retention were investigated to assess the characteristics of fibre during injection moulding of the developed flax fibre (FF)/polylactic acid (PLA) composite.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041584","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative study on periodic immersion+infrared aging corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium Korrosionsverhalten der Stähle Q345qNH und Q420qNH bei zyklischer Immersion und Infrarotalterung in einem simulierten industriellen atmosphärischen Medium Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的周期性浸泡+红外老化腐蚀行为比较研究 Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的周期性浸泡和红外老化腐蚀行为研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1002/mawe.202300248
T. Guo, H. Yang, W. Wu, X. Liu, X. Nan, Y. Hu

The corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium was studied by periodic immersion+infrared aging corrosion experiment. The results show that the corrosion type of both samples is uneven comprehensive corrosion, and the rust layer formed in the later stage of corrosion is relatively dense. But average corrosion rate of Q345qNH steel is always lower than that of Q420qNH steel, and the ratio of Iα-FeOOH/Iγ-FeOOH in rust layer is always higher. Compared with Q420qNH steel, Q345qNH steel has fewer surface pits but deeper local pits. The self-corrosion potential of Q345qNH steel increases obviously, the resistance of the rust layer is larger, and protection to the matrix is stronger. This is because the formation of a large number of corrosion microcells induced by fine lamellar sorbite tissue that uneven distributed in Q420qNH steel, which increases the corrosion rate and makes corrosion uneven, while the larger pearlitic group in Q345qNH steel increases the local corrosion rate. However, the higher chromium/carbon ratio in Q345qNH steel promotes the conversion of lepidocrocite to goethite and inhibits the cathode reaction in the infrared drying stage, improving the density and stability of the rust layer.

通过周期性浸泡+红外老化腐蚀实验研究了 Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的腐蚀行为。结果表明,两种试样的腐蚀类型均为不均匀的全面腐蚀,腐蚀后期形成的锈层相对致密。但 Q345qNH 钢的平均腐蚀速率始终低于 Q420qNH 钢,锈层中 Iα-FeOOH/Iγ-FeOOH 的比值始终较高。与 Q420qNH 钢相比,Q345qNH 钢的表面凹坑较少,但局部凹坑较深。Q345qNH 钢的自腐蚀潜能明显增加,锈层的阻力更大,对基体的保护更强。这是因为 Q420qNH 钢中分布不均匀的细小片状索氏体组织诱导形成了大量的腐蚀微胞,从而增加了腐蚀速率并使腐蚀不均匀,而 Q345qNH 钢中较大的珠光体基团则增加了局部腐蚀速率。然而,Q345qNH 钢中较高的铬/碳比促进了鳞片闪长岩向闪长岩的转化,抑制了红外干燥阶段的阴极反应,提高了锈层的致密性和稳定性。
{"title":"Comparative study on periodic immersion+infrared aging corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium\u0000 Korrosionsverhalten der Stähle Q345qNH und Q420qNH bei zyklischer Immersion und Infrarotalterung in einem simulierten industriellen atmosphärischen Medium","authors":"T. Guo,&nbsp;H. Yang,&nbsp;W. Wu,&nbsp;X. Liu,&nbsp;X. Nan,&nbsp;Y. Hu","doi":"10.1002/mawe.202300248","DOIUrl":"https://doi.org/10.1002/mawe.202300248","url":null,"abstract":"<p>The corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium was studied by periodic immersion+infrared aging corrosion experiment. The results show that the corrosion type of both samples is uneven comprehensive corrosion, and the rust layer formed in the later stage of corrosion is relatively dense. But average corrosion rate of Q345qNH steel is always lower than that of Q420qNH steel, and the ratio of I<sub>α-FeOOH</sub>/I<sub>γ-FeOOH</sub> in rust layer is always higher. Compared with Q420qNH steel, Q345qNH steel has fewer surface pits but deeper local pits. The self-corrosion potential of Q345qNH steel increases obviously, the resistance of the rust layer is larger, and protection to the matrix is stronger. This is because the formation of a large number of corrosion microcells induced by fine lamellar sorbite tissue that uneven distributed in Q420qNH steel, which increases the corrosion rate and makes corrosion uneven, while the larger pearlitic group in Q345qNH steel increases the local corrosion rate. However, the higher chromium/carbon ratio in Q345qNH steel promotes the conversion of lepidocrocite to goethite and inhibits the cathode reaction in the infrared drying stage, improving the density and stability of the rust layer.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-08-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142041537","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Materialwiss. Werkstofftech. 7/2024 材料科学材料技术 7/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480711
{"title":"Materialwiss. Werkstofftech. 7/2024","authors":"","doi":"10.1002/mawe.202480711","DOIUrl":"https://doi.org/10.1002/mawe.202480711","url":null,"abstract":"","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-07-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141967648","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Cover Picture: (Materialwiss. Werkstofftech. 7/2024) 封面图片: (Materialwiss. Werkstofftech. 7/2024)
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480701

{"title":"Cover Picture: (Materialwiss. Werkstofftech. 7/2024)","authors":"","doi":"10.1002/mawe.202480701","DOIUrl":"https://doi.org/10.1002/mawe.202480701","url":null,"abstract":"<p>\u0000 <figure>\u0000 <div><picture>\u0000 <source></source></picture><p></p>\u0000 </div>\u0000 </figure>\u0000 </p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-07-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/mawe.202480701","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141967646","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Materialwissenschaft und Werkstofftechnik
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1