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Characterizing surface roughness evolution in copper conductors under mechanical strain using power spectral density analysis Charakterisierung der Entwicklung der Oberflächenrauheit in Kupferleitern unter mechanischer Beanspruchung mit Hilfe der Leistungsspektraldichteanalyse 利用功率谱密度分析,在机械应力下铜导体表面粗糙度的表征
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-03 DOI: 10.1002/mawe.70029
C. Maier, P. Rachwalsky, A. Wittmann, K. P. Koch, G. Fischer

This study investigates the effects of mechanical strain on the surface roughness of copper conductors, focusing on the electrolyte-refined copper (Cu-ETP, CW004A) used in H07V-U 1.5 mm2 single-core cables. For the first time, the surface roughness evolution is characterized using the power spectral density (PSD) function, enabling a detailed roughness analysis across different spatial length scales. Conductors were subjected to mechanical stress, with measurements taken at multiple stages of service life. The study confirms the results from other studies that surface roughness increases significantly in the early stages of loading, with a plateau observed in 50 % - 75 % of cycles to failure. Micro crack formation and material extrusion are identified as key mechanisms driving roughness growth, especially at small length scales, with a shift towards larger length scales as strain intensifies. The increasing Hurst exponent suggests a transformation from a random to a more persistent and correlated surface. The results underscore the potential of power spectral density analysis in understanding surface behavior in copper conductors.

本研究研究了机械应变对铜导体表面粗糙度的影响,重点研究了H07V-U 1.5 mm2单芯电缆中使用的电解精铜(Cu-ETP, CW004A)。首次使用功率谱密度(PSD)函数来表征表面粗糙度的演变,从而可以在不同的空间长度尺度上进行详细的粗糙度分析。导体承受机械应力,并在使用寿命的多个阶段进行测量。该研究证实了其他研究的结果,即表面粗糙度在加载的早期阶段显著增加,在50% - 75%的循环中观察到一个平台。微裂纹形成和材料挤压被认为是驱动粗糙度增长的关键机制,特别是在小长度尺度下,随着应变的加剧,粗糙度会向大长度尺度转变。赫斯特指数的增加表明一个从随机到更持久和相关的表面的转变。结果强调了功率谱密度分析在理解铜导体表面行为方面的潜力。
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引用次数: 0
Structural integrity and morphology of glass fibre-aluminium foam epoxy sandwich composites Strukturelle Integrität und Morphologie von Glasfaser-Aluminiumschaum-Epoxid-Sandwichverbundwerkstoffen 玻璃纤维-铝泡沫环氧夹层复合材料的结构完整性和形态
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-03 DOI: 10.1002/mawe.70025
K. G. Chandrashekhar, S. K. Bhoi, D. R. Srinivasan, A. K. Singh, K. A. Razak

Sandwich composites are used in automobiles, aerospace, shipbuilding and structural applications in civil engineering. In the present investigation, glass fibre reinforced aluminium foam (AA6061-T6) sandwich laminates are fabricated in four different layers of 1 mm-thickened aluminium foam (0, 1, 2 and 3) that have been combined with epoxy resin in the hand layup method. The four different combination samples were indexed as S1 – S4. The tensile, flexural, impact strength and hardness test were performed to study the mechanical properties of the developed sandwich composites, and the morphological study of tensile fractured specimens was carried out using scanning electron microscopy (SEM). The results indicated that the morphologies of the sandwich composites enhanced their mechanical characteristics by increasing the bonding between the epoxy and aluminium foam. The two-layer aluminium foam sandwich composite (S2) has better mechanical properties than the other three aluminium foam sandwich composites, including tensile (102.3 MPa), flexural (7.7 kN), impact strength (11.9 kJ/m2) and hardness (242 HV 10), which indicates its enhanced structural performance. The mechanical strength of the aluminium foam sandwich composite is further supported by the findings of scanning electron microscopy scans. This work advances engineering in the real world by offering a useful guideline for improving aluminium foam layers in sandwich composites.

夹层复合材料用于汽车、航空航天、造船和土木工程中的结构应用。在本研究中,玻璃纤维增强泡沫铝(AA6061-T6)夹层层压板由四层不同的1 mm增厚泡沫铝(0、1、2和3)制成,并与环氧树脂以手铺法组合。4种不同组合样品标为S1 - S4。通过拉伸、弯曲、冲击强度和硬度测试研究了复合材料的力学性能,并对拉伸断裂试样进行了扫描电镜(SEM)形貌研究。结果表明,夹层复合材料的形貌通过增强环氧树脂与泡沫铝之间的结合增强了其力学性能。两层泡沫铝夹层复合材料(S2)的拉伸性能(102.3 MPa)、弯曲性能(7.7 kN)、冲击强度(11.9 kJ/m2)和硬度(242 HV 10)均优于其他三种泡沫铝夹层复合材料,表明其结构性能有所提高。扫描电镜扫描结果进一步证实了泡沫铝夹层复合材料的机械强度。这项工作为改进夹层复合材料中的泡沫铝层提供了有用的指导方针,从而推动了现实世界中的工程。
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引用次数: 0
Accumulative roll bonded composites with highly uniform distribution of copper layers and wear properties Akkumulativ walzplattierte Verbundwerkstoffe mit hochgradig gleichmäßiger Verteilung der Kupferschichten und Verschleißeigenschaften 具有高度均匀铜层分布和磨损性能的累积卷合复合材料,具有高度均匀铜层分布和磨损性能的累积卷合复合材料
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-03 DOI: 10.1002/mawe.70033
Y. Huang, Z. Zhou

This study characterizes the wear behavior of an aluminum/copper laminated composite with a highly uniform distribution using a wear test under various sliding and loading conditions. The composite is processed through up to twelve accumulative roll bonding passes to achieve a uniform distribution. The microstructure, mechanical, and wear properties are characterized using optical microscopy, scanning electron microscopy, tensile testing, hardness testing, and wear tests. The ultimate tensile strength of 321 MPa, coupled with an elongation at a break of 9.7 %, is achieved after twelve passes. For lower loads and sliding distances, the amount of weight loss decreases due to the increase in hardness (154 % for aluminum and 174 % for copper compared to the raw sheets) in the strain-hardened layers. However, with an increase in the applied load (from 5 N to 10 N) and sliding distance (from 500 m to 1500 m), weight loss increases, which is due to the higher contact stress between the pin and wear surfaces, resulting in greater depth of deformation and surface temperature, which accelerates the recrystallization process in the plastically deformed region. Additionally, based on the wear test results, various wear mechanisms, including adhesion, abrasion, and delamination, are observed.

本文研究了一种分布高度均匀的铝/铜层合复合材料在不同滑动和加载条件下的磨损特性。复合材料经过多达12道累积滚接道来实现均匀分布。使用光学显微镜、扫描电子显微镜、拉伸测试、硬度测试和磨损测试来表征微观结构、机械和磨损性能。经过12道次后,拉伸强度达到321 MPa,断裂伸长率达到9.7%。对于较低的载荷和滑动距离,由于应变硬化层中硬度的增加(与原始板材相比,铝的硬度为154%,铜的硬度为174%),重量损失量减少。然而,随着外加载荷(从5 N到10 N)和滑动距离(从500 m到1500 m)的增加,失重增加,这是由于销与磨损面之间的接触应力增加,导致变形深度和表面温度增加,从而加速了塑性变形区域的再结晶过程。此外,根据磨损测试结果,观察到各种磨损机制,包括粘附、磨损和分层。
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引用次数: 0
Mechanical characterization and thermal conductivity of nanosilica reinforced Al6061 based nanocomposite Mechanische Charakterisierung und Wärmeleitfähigkeit von mit Nano-Siliziumdioxid verstärktem Nanoverbundwerkstoff auf Al6061-Basis 基于Al6061的纳米二氧化硅增强纳米复合材料的机械特性和导热性。
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-03 DOI: 10.1002/mawe.70027
S. R. Kumar, A. Sharma, D. K. Patel

In the form of bar, rod and plate, aluminum alloy Al6061 has been widely used as components in many applications. In the current investigation, the effect of silica nanoparticles on the physical and mechanical behavior of Al6061-based nanocomposite has been investigated. Al6061-based nanocomposites were prepared using stir casting machine. Characterization properties for the investigation taken were hardness, void content, tensile strength, flexural strength, fracture toughness, and thermal conductivity. The inclusion of 3 wt.-% silica nanoparticle increased the void content, hardness, tensile strength, flexural strength, and fracture toughness by 44 %, 5.1 %, 52 %, 8 %, and 18.6 % respectively. However, the composite made of Al6061 had a 4 % reduction in thermal conductivity. The best percentage of nanosilica for mechanical and thermal conductivity properties of Al6061 based composite was 9 wt.-%. Hence, nanosilica can be suggested as promising reinforcement for composite material applications requiring high strength and low thermal conductivity.

铝合金Al6061以棒材、棒材和板材的形式,在许多应用中被广泛用作构件。在本研究中,研究了二氧化硅纳米颗粒对al6061基纳米复合材料物理力学行为的影响。采用搅拌铸造法制备了al6061基纳米复合材料。研究的表征性能包括硬度、孔隙含量、拉伸强度、弯曲强度、断裂韧性和导热系数。3 wt.-%二氧化硅纳米颗粒的加入使孔隙含量、硬度、抗拉强度、抗弯强度和断裂韧性分别提高了44%、5.1%、52%、8%和18.6%。然而,由Al6061制成的复合材料的导热性降低了4%。纳米二氧化硅对Al6061基复合材料力学和导热性能的最佳影响为9 wt.-%。因此,纳米二氧化硅可以被认为是需要高强度和低导热性的复合材料应用的有前途的增强材料。
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引用次数: 0
Effect of surface boronizing on the zinc corrosion resistance of Fe-20Cr-5B-3Al alloy Einfluss der Oberflächenborierung auf die Zinkkorrosionsbeständigkeit der Legierung FeCr20B5Al3 表面硼化对FeCr20B5Al3合金锌耐腐蚀性的影响
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-03 DOI: 10.1002/mawe.70032
S.L. Zhu, Y. Liu, C.J. Wu, X.Y. Zhu, X.P. Su

This study systematically investigated boronizing treatment and its effect on the corrosion behavior and microstructure of the iron - 20 % chromium - 5 % boron - 3 % aluminum alloy in molten zinc. Diiron boride, α-iron, and dichromium boride exist in the as-cast iron - 20 % chromium - 5 % boron - 3 % aluminum alloy. The boronizing treatment was conducted using the pack cementation method, the α-iron phase on the alloy surface was transformed into the more zinc corrosion-resistant diiron boride phase. Boron diffusion and enrichment turned the original diiron boride and dichromium boride into iron boride and chromium boride. Performance of the alloy before and after boronizing treatment was compared through a 128 h molten zinc corrosion test. Although chromium and aluminium in alloy enhance its corrosion resistance in molten zinc, the α-iron phase is still prone to preferential corrosion. The less corrosion-resistant α-iron disappears and a complete boride layer forming on the surface of the alloy in boriding process significantly improves the overall corrosion resistance of the alloy in molten zinc. Since the newly formed iron-boron compounds are interleaved with the original iron-boron compounds, the adhesion property of surface boride layer is guaranteed.

本文系统地研究了渗硼处理对铁- 20%铬- 5%硼- 3%铝合金在锌液中的腐蚀行为和组织的影响。在铸铁- 20%铬- 5%硼- 3%铝合金中存在硼化二铁、α-铁和硼化二铬。采用填充渗硼法进行渗硼处理,使合金表面α-铁相转变为耐锌腐蚀的硼化二铁相。硼的扩散和富集使原来的硼化二铁和硼化二铬变成硼化铁和硼化铬。通过128 h的锌液腐蚀试验,比较了渗硼前后合金的性能。虽然合金中的铬和铝增强了合金在锌液中的耐蚀性,但α-铁相仍容易发生优先腐蚀。渗硼过程中抗蚀性较差的α-铁消失,合金表面形成完整的硼化物层,显著提高了合金在锌液中的整体耐蚀性。由于新形成的铁硼化合物与原有的铁硼化合物相互交织,保证了表面硼化物层的附着性能。
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引用次数: 0
Materialwiss. Werkstofftech. 8/2025 Materialwiss .Werkstofftech . 8/2025
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-25 DOI: 10.1002/mawe.70036
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引用次数: 0
Impressum: Materialwiss. Werkstofftech. 8/2025 刊头:Materialwiss .Werkstofftech . 8/2025
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-25 DOI: 10.1002/mawe.70034
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引用次数: 0
Cover Picture: (Materialwiss. Werkstofftech. 8/2025) 封面图片:(Materialwiss。Werkstofftech . 8/2025)
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-25 DOI: 10.1002/mawe.70035

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引用次数: 0
Effect of aluminum contents on the microstructure and mechanical properties of magnesium-aluminum-calcium alloys Einfluss von Aluminium auf das Gefüge und die mechanischen Eigenschaften von Magnesium-Aluminium-Calciumlegierungen 铝含量对镁-铝-钙合金的微观结构和机械性能的影响
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-17 DOI: 10.1002/mawe.70017
X. D. Yuan, C. Y. Zhang, H. P. Pan, Y. Liu, P. Liu, X. Y. Zhang

The effect of aluminum contents on the microstructure and mechanical properties of as-extruded magnesium-aluminum-calcium alloys was systematically investigated. The as-solid alloys with three aluminum contents contain block-shape calcium aluminide phases and aluminum-manganese intermetallic phases. Differently, the amounts of block-shape calcium aluminide phases and aluminum-manganese intermetallic phases increased with aluminum contents. During hot extrusion process, the block-shape calcium aluminide phases and aluminum-manganese intermetallic phases are fragmented into small pieces and aligned along the extrusion direction. Bimodal microstructures were obtained after extrusion, consisting of fine dynamically recrystallized grains and coarse deformed grains. The area fractions of dynamically recrystallized grains increased from 53 % to 65 % with aluminum contents increasing from 3.12 % to 5.21 %, due to the particle stimulated nucleation mechanism caused by block-shape aluminum-containing phases. The as-extruded magnesium-aluminum-calcium alloys show a strong basal fiber texture, which diminished as aluminum contents increase. The strength of as-extruded magnesium-aluminum-calcium alloys diminished as aluminum contents increased. The as-extruded magnesium-3.12 aluminum-2.65 calcium (wt.-%) alloy demonstrates a yield strength of 366 MPa and an ultimate tensile strength of 391 MPa. The exceptional high strengths are due to the ultrafine dynamically recrystallized grains stabilized by fragmented second phases, strong basal texture and high dislocation density.

系统研究了铝含量对挤压态镁铝钙合金组织和力学性能的影响。三种含铝量的固态合金含有块状的铝化钙相和铝锰金属间相。块状铝化钙相和铝锰金属间相的含量随铝含量的增加而增加。在热挤压过程中,块状的钙铝化物相和铝锰金属间相破碎成小块,并沿挤压方向排列。挤压后得到由细小动态再结晶晶粒和粗大变形晶粒组成的双峰组织。随着铝含量从3.12%增加到5.21%,动态再结晶晶粒的面积分数从53%增加到65%,这是由于块状含铝相引起的颗粒激发成核机制所致。挤压态镁铝钙合金呈现出较强的基纤维织构,随着铝含量的增加,基纤维织构逐渐减弱。挤压态镁铝钙合金的强度随铝含量的增加而降低。挤压态镁-3.12铝-2.65钙(wt.-%)合金的屈服强度为366 MPa,抗拉强度为391 MPa。超常的高强度是由破碎的第二相稳定的超细动态再结晶晶粒、强基织构和高位错密度造成的。
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引用次数: 0
Comparative study of physico-mechanical wear analysis of gravity die casting and centrifugal methods for waste/nanoparticle-filled polymer composites Untersuchung der physikalisch-mechanischen Verschleißanalyse zu Druckguss- und Schleudergussverfahren für mit Abfall/Nanopartikeln gefüllte Polymerverbundwerkstoffe 废物/纳米颗粒填充聚合物复合材料的物理机械磨损分析、铸造方法和离心方法的比较研究
IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-09 DOI: 10.1002/mawe.70018
B. Gangil, L. Ranakoti, P. Bhandari, A. Bisht, D. Biswas, S. K. Verma

The present investigation compares two fabrication techniques, gravity die casting and centrifugal casting, for fabricating homogeneous and functionally graded material composites based on their mechanical and wear characteristics. Therefore, composite samples were fabricated by incorporating different weights of silica nanoparticles in vinyl ester containing a fixed amount of walnut shell filler. The choice of walnut shell filler and vinyl ester as the reinforcing and matrix materials, respectively, was deliberate, as these materials possess unique characteristics that make them suitable for composite fabrication. Tests were conducted on fabricated samples of both gravity die casting and functionally graded material. It was found that gravity die casting composites exhibit better tensile strength and impact energy, while functionally graded material composites showed better hardness and wear resistance. In addition, void formation is much lower in functionally graded material composite, demonstrating the effectiveness of the centrifugal technique in producing composites with fewer defects.

本研究比较了重力压铸和离心铸造两种制造技术,基于它们的力学和磨损特性来制造均质和功能梯度复合材料。因此,将不同重量的二氧化硅纳米颗粒掺入含有一定量核桃壳填料的乙烯酯中制备复合样品。选择核桃壳填料和乙烯基酯分别作为增强材料和基体材料是经过深思熟虑的,因为这些材料具有独特的特性,使它们适合复合材料的制造。对重力压铸件和功能梯度材料的制备样品进行了试验。结果表明,重力压铸复合材料具有更好的抗拉强度和冲击能,而功能梯度材料复合材料具有更好的硬度和耐磨性。此外,在功能梯度材料复合材料中,孔隙形成率要低得多,这表明离心技术在生产缺陷较少的复合材料方面是有效的。
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引用次数: 0
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