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Impressum: Materialwiss. Werkstofftech. 7/2024 版本说明:Materialwiss.材料技术 7/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480721
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引用次数: 0
Effect of aging temperature on the microstructure and properties of alloyed high-manganese steel Einfluss der Alterungstemperatur auf das Gefüge und die Eigenschaften von legiertem hochmanganhaltigem Stahl 时效温度对合金高锰钢微观结构和性能的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-25 DOI: 10.1002/mawe.202300074
J. Sun, M. Jiang, L. Dong, Z. Ding, Y. Bao, S. Luo

This paper describes an aging treatment based on alloying the traditional high-carbon high-manganese steel to improve its initial wear resistance (wear resistance after water toughening treatment only). The changes in structure and mechanical properties of alloyed high-manganese steel after aging treatment at different temperatures were investigated using various experimental methods such as metallographic analysis, mechanical property testing, and fracture morphology observation.

The austenite grain boundary began to have the appearance of grain carbide at 550 °C; a large number of pearlites nucleated at the grain boundary and within grain at 600 °C, most phase transitions occur at 650 °C; and the pearlite and carbide began to revert to a soluble state at 700 °C, leaving only a small amount of pearlite in the austenite grain boundary. The hardness and yield strength of alloyed high-manganese steel increase and then decrease with the increasing aging temperature, and the high peaks appear in the range of 600 °C–650 °C; while the tensile strength and plasticity decrease and then slightly increase, with the highest and lowest peaks being approximately 550 °C and 650 °C, respectively.

At the aging temperature of 550 °C, the alloy high manganese steel has good comprehensive mechanical and deformation strengthening properties, with yield strength, tensile strength, elongation, and section shrinkage of 536 MPa, 1058 MPa, 51 % and 35 %, respectively. The changes in the properties of alloyed high-manganese steel are related to the pattern of structural changes that occur during the aging process.

本文介绍了一种基于传统高碳高锰钢合金化的时效处理方法,以提高其初始耐磨性(仅水韧化处理后的耐磨性)。采用金相分析、力学性能测试和断口形貌观察等多种实验方法,研究了合金化高锰钢在不同温度下进行时效处理后的组织和力学性能变化。550 ℃时,奥氏体晶界开始出现晶粒碳化物;600 ℃时,大量珠光体在晶界和晶粒内部成核,大部分相变发生在650 ℃;700 ℃时,珠光体和碳化物开始恢复到可溶状态,奥氏体晶界只剩下少量珠光体。随着时效温度的升高,合金高锰钢的硬度和屈服强度先增大后减小,在600 ℃-650 ℃范围内出现较高的峰值;而抗拉强度和塑性先减小后略有增大,最高和最低峰值分别约为550 ℃和650 ℃。在 550 ℃ 的时效温度下,合金高锰钢具有良好的综合力学性能和变形强化性能,屈服强度、抗拉强度、伸长率和断面收缩率分别为 536 MPa、1058 MPa、51 % 和 35 %。合金高锰钢性能的变化与时效过程中发生的结构变化规律有关。
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引用次数: 0
Features of the structure and properties of stone mastic asphalt Merkmale der Struktur und Eigenschaften von Steinmastixasphalt 石硫合剂沥青的结构和性能特点
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300181
A. Bieliatynskyi, S. Yang, V. Pershakov, M. Shao, M. Ta

The purpose of this study is to investigate the features and properties of stone mastic asphalt in the context of its potential for practical application in road repair works, aiming to create a high-quality road surface and replace outdated structural materials with newer alternatives. The leading approach combines a systematic analysis of the issues submitted for consideration and an experimental study of the properties of stone mastic asphalt, which are important in the context of the practical use of this building material to ensure high quality parameters of the roadway and the timeliness of its repair, if necessary. Within the framework of this study, results were obtained that indicate a significant variety of approaches to determining the characteristics and properties of the material under consideration, clearly demonstrating current solutions to the problem of improving the performance of stone mastic asphalt by introducing special admixtures into its composition. The findings and conclusions of this research are valuable for road service employees and developers of modern construction materials, aiding in high-quality road surface repair and creating durable asphalt for safe road use in the future.

本研究的目的是根据石硫合剂沥青在道路维修工程中的实际应用潜力,对其特征和特性进行研究,旨在创造高质量的路面,并用更新的替代材料取代过时的结构材料。主要方法是对提交审议的问题进行系统分析,并对石硫合剂沥青的特性进行实验研究,这些特性在实际使用这种建筑材料时非常重要,可确保路面的高质量参数,并在必要时及时进行修复。在这项研究的框架内获得的结果表明,确定所考虑材料的特征和性能的方法多种多样,清楚地表明了通过在其成分中引入特殊外加剂来改善石硫合剂沥青性能问题的当前解决方案。这项研究的结果和结论对道路服务人员和现代建筑材料开发人员很有价值,有助于高质量的路面修复,并为未来道路的安全使用创造耐用的沥青。
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引用次数: 0
A-prori layer height determination for wire arc additive manufacturing based on weld geometry A-priori-Lagenhöhenbestimmung für drahtbasierte Lichtbogen-Additiv-Schweißverfahren auf Basis der Schweißnahtgeometrie 根据焊缝几何形状确定线弧快速成型制造的 A-prori 层高
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300158
K. Mäde, P. J. Kellerwessel, R. Sharma, U. Reisgen

The application of wire arc additive manufacturing (WAAM) for the production of large size components is currently limited, due to strong distortion and unprecise filling behavior. The resulting geometric and metallurgical irregularities pose a challenge to the process. The current approach of a layered structure cannot be adopted without adjustments when using wire arc additive manufacturing. Reasons include incompleteness, material accumulation and deformation. The combination of experimental weld geometry-determination and its numerical estimation is presented here as solution to this challenge. The procedure is based on the measurement of a weld bead cross-section-area. By convolution of a path matrix with a weld-geometry-function, the planned path is filled with the seam geometry. Subsequent summation of multiple matrices results in a height profile showing discontinuities and accumulations. Further validation tests show a good agreement between the method and experimentally determined problem areas. The presented optimisation procedure can be extended with material parameters. A local compensation for deformation can be achieved.

目前,线弧快速成型技术(WAAM)在大尺寸部件生产中的应用受到了限制,原因在于其强烈的变形和不精确的填充行为。由此产生的几何和冶金不规则性对工艺提出了挑战。在使用线弧快速成型技术时,如果不进行调整,就无法采用当前的分层结构方法。原因包括不完整、材料堆积和变形。本文介绍了焊接几何形状的实验确定和数值估算相结合的方法,作为应对这一挑战的解决方案。该程序基于焊缝横截面积的测量。通过路径矩阵与焊缝几何函数的卷积,用焊缝几何填充计划路径。随后对多个矩阵求和,得到一个显示不连续性和堆积的高度剖面图。进一步的验证测试表明,该方法与实验确定的问题区域之间具有良好的一致性。所介绍的优化程序可通过材料参数进行扩展。可以实现变形的局部补偿。
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引用次数: 0
Decreasing the electrostatic discharge generated from friction of polyester and polyamide sing carbon fiber Verringerung der durch Reibung von Polyester und Polyamid erzeugten elektrostatischen Entladung mithilfe von Kohlefasern 减少聚酯和聚酰胺与碳纤维摩擦产生的静电放电
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300084
H. Suaad, M. K. Mohamed, W. Y. Ali

The present work discusses the voltage difference as a measure for electrostatic charge generated from the contact-separation and sliding of polymeric textiles on polyamide textile. It is proposed to blend polyester by carbon fiber to decrease the electrostatic charge generated on the contact surfaces. Because polyester acquires a negative charge and polyamide gains a positive one, carbon fiber is proposed to conduct the negative electrostatic charge from polyester to polyamide and conducts the positive one from polyamide to polyester, so that the resultant electrostatic charge decreased. The effect of carbon fiber to decrease the electrostatic charge depends on its area of contact, interaction, and distribution with polyester. Polyester double weaved by carbon fiber showed the lowest voltage. Based on those observations, it can be recommended to use double weaves of carbon fiber with polyester. The reduction in voltage was relatively lower for braided polyester by carbon fiber than that detected for double-weaved polyester by carbon fiber.

本研究讨论了聚合纺织品在聚酰胺纺织品上接触分离和滑动时产生的静电荷的测量电压差。建议用碳纤维混合聚酯,以减少接触面上产生的静电荷。由于聚酯获得负电荷,而聚酰胺获得正电荷,因此建议用碳纤维将负静电荷从聚酯传导到聚酰胺,并将正静电荷从聚酰胺传导到聚酯,从而减少由此产生的静电荷。碳纤维降低静电荷的效果取决于其与聚酯的接触面积、相互作用和分布。碳纤维双层编织的聚酯显示的电压最低。根据上述观察结果,建议使用碳纤维与聚酯双层编织。与碳纤维双织聚酯相比,碳纤维编织聚酯的电压降低幅度相对较低。
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引用次数: 0
Nanosecond laser micromachining of graphene nanoplatelets reinforced ZK60 matrix composites Nanosekunden-Laserstrahl-Mikrobearbeitung von mit Graphen-Nanoplättchen verstärkten ZK60-Matrix-Verbundwerkstoffen 纳秒激光微加工石墨烯纳米片增强 ZK60 矩阵复合材料
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300283
Z. Wu, C. W. Li, Y. Zhang, Y. L. Liu, J. Y. Song, C. M. Yang

In this paper, a nanosecond laser was used to etch the surface of graphene nanoplatelets reinforced ZK60 (GNPs/ZK60) matrix composites, and the effects of different scanning speeds, pulse repetition frequency and laser power on the etched morphology of the machined surface were investigated. The experimental results show that the etched groove width and heat affected zone width of GNPs/ZK60 composites are significantly increased compared with ZK60 material due to the influence of graphene, and the growth rate of the difference in heat affected zone width between GNPs/ZK60 composites and ZK60 materials is most significantly affected by the pulse repetition frequency. In addition, the dross height increases with the increase of laser power, while the scaly dross structure becomes increasingly clear.

本文采用纳秒激光刻蚀石墨烯纳米片增强 ZK60(GNPs/ZK60)基复合材料表面,研究了不同扫描速度、脉冲重复频率和激光功率对加工表面刻蚀形貌的影响。实验结果表明,由于石墨烯的影响,GNPs/ZK60 复合材料的蚀刻沟槽宽度和热影响区宽度与 ZK60 材料相比明显增大,而 GNPs/ZK60 复合材料与 ZK60 材料热影响区宽度差异的增长率受脉冲重复频率的影响最为显著。此外,渣滓高度随激光功率的增加而增加,同时鳞片状渣滓结构变得越来越清晰。
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引用次数: 0
Hafnium surface changes during dissolution in concentrated sulfuric acid Veränderungen der Hafniumoberfläche während der Auflösung in konzentrierter Schwefelsäure 铪在浓硫酸中溶解时的表面变化
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300280
G. M. Carriello, G. M. Pegoraro, L. R. Alves, G. P. Mambrini

Scientific studies involving hafnium have grown significantly in recent years due to the potential applications that this metal has. These potential applications come from the properties of this element, which for many years since its discovery were neglected in research. Among the factors that contributed to this was the high cost of extracting its ores from nature. One of the properties is the solubility of this metal in concentrated sulfuric acid, reacting to form hafnium(IV) sulfate and hydrogen gas. This acid is one of the few that can dissolve this metal, since hafnium is highly resistant to corrosion. The present work reports a chemometrically planned study on the surface of hafnium metal during its dissolution in sulfuric acid at different temperatures (13 °C, 25 °C and 97 °C) and for different times (5 minutes, 60 minutes and 120 minutes). Samples of metallic hafnium were completely immersed in sulfuric acid, subsequently characterized by scanning electron microscopy and the mass variation of the samples was analyzed. The corrosion of hafnium occurs only after the rupture of the protective film of hafnium(IV) oxide of the material, this rupture being faster as the temperature increases.

近年来,由于铪的潜在应用,涉及铪的科学研究有了显著增长。这些潜在的应用来自于这种元素的特性,自发现以来的许多年里,这种特性在研究中一直被忽视。造成这种情况的因素包括从自然界中提取铪矿石的高昂成本。其中一个特性是这种金属在浓硫酸中的溶解性,反应生成硫酸铪(IV)和氢气。这种酸是少数几种能溶解这种金属的酸之一,因为铪具有很强的耐腐蚀性。本研究报告对金属铪在不同温度(13 °C、25 °C、97 °C)和不同时间(5 分钟、60 分钟、120 分钟)的硫酸溶解过程中的表面进行了化学计量学研究。将金属铪样品完全浸入硫酸中,然后用扫描电子显微镜对其进行表征,并分析样品的质量变化。只有在材料的氧化铪(IV)保护膜破裂后,铪才会发生腐蚀,这种破裂随着温度的升高而加快。
{"title":"Hafnium surface changes during dissolution in concentrated sulfuric acid\u0000 Veränderungen der Hafniumoberfläche während der Auflösung in konzentrierter Schwefelsäure","authors":"G. M. Carriello,&nbsp;G. M. Pegoraro,&nbsp;L. R. Alves,&nbsp;G. P. Mambrini","doi":"10.1002/mawe.202300280","DOIUrl":"10.1002/mawe.202300280","url":null,"abstract":"<p>Scientific studies involving hafnium have grown significantly in recent years due to the potential applications that this metal has. These potential applications come from the properties of this element, which for many years since its discovery were neglected in research. Among the factors that contributed to this was the high cost of extracting its ores from nature. One of the properties is the solubility of this metal in concentrated sulfuric acid, reacting to form hafnium(IV) sulfate and hydrogen gas. This acid is one of the few that can dissolve this metal, since hafnium is highly resistant to corrosion. The present work reports a chemometrically planned study on the surface of hafnium metal during its dissolution in sulfuric acid at different temperatures (13 °C, 25 °C and 97 °C) and for different times (5 minutes, 60 minutes and 120 minutes). Samples of metallic hafnium were completely immersed in sulfuric acid, subsequently characterized by scanning electron microscopy and the mass variation of the samples was analyzed. The corrosion of hafnium occurs only after the rupture of the protective film of hafnium(IV) oxide of the material, this rupture being faster as the temperature increases.</p>","PeriodicalId":18366,"journal":{"name":"Materialwissenschaft und Werkstofftechnik","volume":null,"pages":null},"PeriodicalIF":1.2,"publicationDate":"2024-07-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141812978","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Machinability study of stainless steel AISI 304 under the influence of copper oxide nanoparticles dispersed emulsifier cutting fluid Untersuchung der Zerspanbarkeit von rostfreiem Stahl X5CrNi18 10 unter dem Einfluss von mit Kupferoxid-Nanopartikeln dispergiertem Emulgator-Kühlschmierstoff 氧化铜纳米颗粒分散乳化剂切削液影响下 AISI 304 不锈钢的切削性研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-19 DOI: 10.1002/mawe.202300220
S. Ravi, P. Tamilselvam

Quality machining on stainless steel AISI 304 is achieved by reducing the interface temperature generated due to high hardness and compressive frictional force. Temperature rise during the turning operation was observed to cause a weak tool nose, and machining surface. Enhanced lubricant properties can alleviate these issues and help reduce tool nose wear while increasing machined surface quality. Nano-lubricants have been prepared to meet the functional requirements for machining. Emulsifier oil-based nanofluids perform exceptionally well in heat transfer during machining. The present investigation focuses on copper oxide nanoparticles addition in “Society of Automotive Engineers 30” emulsifier oil at two different weight percentage: 1.5 wt.-% and 2.25 wt.-%, aiming to improve heat transfer and machined surface quality. In this experimental study, a computer numerical control machine tool, DCMT120404 insert, tool dynamometer, and infrared pyrometer are utilized for the machining operation. It was observed that 2.25 wt.-% copper oxide mixed emulsifier-nano cutting fluid exhibited minimum cutting force and work-tool interface temperature while enhancing the surface quality.

对 AISI 304 不锈钢进行高质量加工的方法是降低由于高硬度和压缩摩擦力而产生的界面温度。据观察,车削操作过程中的温度升高会导致刀头和加工表面变薄。增强润滑剂的性能可以缓解这些问题,有助于减少刀头磨损,同时提高加工表面质量。纳米润滑剂的制备满足了机加工的功能要求。乳化剂油基纳米流体在加工过程中的传热性能特别好。本研究的重点是在 "美国汽车工程师协会 30 "乳化剂油中添加两种不同重量百分比的氧化铜纳米粒子:1.5 wt.-%和 2.25 wt.-%,旨在改善热传递和加工表面质量。在这项实验研究中,使用了计算机数控机床、DCMT120404 刀片、刀具测力计和红外线高温计进行加工操作。结果表明,2.25 wt.-%的氧化铜混合乳化剂-纳米切削液在提高表面质量的同时,切削力和工件-刀具界面温度也最小。
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引用次数: 0
Effect of tempering temperature on microstructure and properties of low silicon hypereutectic high chromium cast iron Auswirkung der Anlasstemperatur auf das Gefüge und die Eigenschaften von übereutektischem Gusseisen mit niedrigem Siliziumgehalt und hohem Chromgehalt 回火温度对低硅超共晶高铬铸铁显微组织和性能的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-19 DOI: 10.1002/mawe.202300235
J. Gu, S. Liu, J. Si, Z. Zhang, X. Wang

High-chromium cast iron is a good wear-resistant material. Its heat treatment regime has an important influence on the evolution of its microstructure and properties. This study investigates the microstructural attributes and properties of Fe–4.0 C–35.0Cr–0.5Si (wt.%) low-silicon hypereutectic high-chromium cast iron subsequent to quenching at 1050 °C, followed by tempering at diverse temperatures. The microstructure was examined using optical microscopy, scanning electron microscopy, and X-ray diffractometry across varied tempering conditions. Furthermore, microhardness and wear resistance were conducted via a microhardness tester and a wear testing machine. The results show that the quenching heat treatment promotes the transformation of the matrix from austenite to martensite, while also promoting the precipitation of secondary carbides of M23C6-type. The subsequent tempering heat treatment engenders transformations involving retained austenite to martensite, amplifies the precipitation and enlargement of secondary carbides, and induces martensite decomposition. As the tempering temperature increases, primary and eutectic carbides exhibit minimal changes, while the secondary carbide morphology evolves from granular to reticular. The matrix composition predominantly comprises martensite, interspersed with a minor fraction of austenite. It is worth noting that the alloy has the highest hardness and wear resistance after quenching at 1050 °C and then tempering at 400 °C.

高铬铸铁是一种良好的耐磨材料。其热处理制度对其微观结构和性能的演变有重要影响。本研究调查了在 1050 °C 淬火后,在不同温度下回火的 Fe-4.0 C-35.0Cr-0.5Si (重量百分比)低硅高共晶高铬铸铁的微观结构属性和性能。使用光学显微镜、扫描电子显微镜和 X 射线衍射仪对不同回火条件下的微观结构进行了检测。此外,还通过显微硬度计和磨损试验机进行了显微硬度和耐磨性测试。结果表明,淬火热处理促进了基体从奥氏体到马氏体的转变,同时也促进了 M23C6 型二次碳化物的析出。随后的回火热处理会引起保留奥氏体向马氏体的转变,扩大二次碳化物的析出和增大,并诱导马氏体分解。随着回火温度的升高,一次碳化物和共晶碳化物的变化极小,而二次碳化物的形态则从颗粒状演变为网状。基体成分主要包括马氏体,中间夹杂少量奥氏体。值得注意的是,该合金在 1050 °C 淬火、400 °C 回火后具有最高的硬度和耐磨性。
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引用次数: 0
A novel sensor placement strategy based on an enhanced damage assessment method in beam-like structures: Saddle point criteria Eine neuartige Sensorplatzierungsstrategie basierend auf einer verbesserten Schadensbewertungsmethode in balkenähnlichen Strukturen: Sattelpunktkriterien 基于增强型梁状结构损伤评估方法的新型传感器安置策略:鞍点标准
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-19 DOI: 10.1002/mawe.202300175
T. Tufan

Sensor placement is one of the vital concerns in civil structure monitoring. A sensor placement strategy based on a damage assessment method has been introduced for beam-like structures. An existing damage detection method adapted to multi-modes and different types of beam-like structures. Then, it is numerically verified to be suitable for detecting any damage location in a 100 degrees of freedom mass-spring system. Depending on the noise in the response and the limited measurements, the results demonstrate the validity of using the multi-mode damage indicator. However, there are limitations to this method due to mode shape saddle points. Sensor deployment schemes have been proposed to address the restriction. In contrast to the corresponding procedure, this method does not rely on the optimization algorithm. Sensor placement strategies involve the simultaneous use of accelerometers and large-area electronics.

传感器的布置是土木工程结构监测的重要问题之一。针对类梁结构,引入了一种基于损伤评估方法的传感器布置策略。现有的损伤检测方法适用于多模式和不同类型的梁状结构。通过数值验证,该方法适用于检测 100 自由度质量弹簧系统中的任何损伤位置。根据响应中的噪声和有限的测量,结果证明了使用多模式损伤指标的有效性。然而,由于模式形状鞍点的存在,这种方法存在局限性。针对这一限制,提出了传感器部署方案。与相应的程序相比,这种方法不依赖于优化算法。传感器部署策略涉及同时使用加速度计和大面积电子设备。
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引用次数: 0
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Materialwissenschaft und Werkstofftechnik
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