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Processing and characterization of waste dolomite dust filled hemp-epoxy composites Verarbeitung und Charakterisierung von mit Dolomitabfall gefüllten Hanf-Epoxid-Verbundwerkstoffen 废白云石粉填充麻-环氧复合材料的加工和表征 废白云石粉填充麻-环氧复合材料的加工和表征
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-28 DOI: 10.1002/mawe.202300314
S. Maurya, S. K. Mahapatra, A. Satapathy

The necessity to adapt sustainable development, green chemistry and industrial ecology leads to the creation of newer materials and the utilization of waste. In this context, this work aims at exploring the feasibility of the fabrication of hybrid composites comprised of a polymeric resin reinforced with a natural fiber (hemp) and an industry waste filler (dolomite dust). While the hemp fiber content is kept constant, epoxy-based hybrid composites are fabricated with different weight percentages of dolomite dust using the conventional hand lay-up route. The microstructural features of the constituent materials are studied using stereo and scanning electron microscopes which show the shape and size of dolomite particles and the arrangement of fibers. An x-ray diffraction analysis revealed the presence of hematite, graphite, lime and manganite. The presence of functional groups like hydroxyl, carboxyl and azide is ascertained from the transmittance spectra of Fourier transform infrared spectroscopy. The density and void fractions are increasing with the amount of filler particles in the composite. It is observed that the tensile and flexural strengths of the composites marginally drop with increase in dolomite dust content, but there is a reasonable improvement in their inter-laminar shear strength, micro-hardness and impact strength values.

为了适应可持续发展、绿色化学和工业生态学的需要,必须创造出更新的材料并利用废弃物。在此背景下,本研究旨在探索用天然纤维(麻)和工业废料填料(白云石粉)增强聚合物树脂的混合复合材料制造的可行性。在保持麻纤维含量不变的情况下,采用传统的手糊工艺,用不同重量百分比的白云石粉制造环氧基混合复合材料。使用立体电子显微镜和扫描电子显微镜研究了组成材料的微观结构特征,显示了白云石颗粒的形状和大小以及纤维的排列。X 射线衍射分析显示了赤铁矿、石墨、石灰和锰矿的存在。从傅里叶变换红外光谱的透射光谱中可以确定存在羟基、羧基和叠氮等官能团。密度和空隙率随着复合材料中填料颗粒数量的增加而增加。据观察,随着白云石粉含量的增加,复合材料的拉伸强度和弯曲强度略有下降,但其层间剪切强度、微硬度和冲击强度值有了合理的改善。
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引用次数: 0
Influence of mixed particle sizes on shear yield stress of magnetorheological fluid Einfluss von gemischten Partikelgrößen auf die Scherfließspannung einer magnetorheologischen Flüssigkeit 混合颗粒尺寸对磁流变液剪切屈服应力的影响 混合颗粒尺寸对磁流变液剪切屈服应力的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-22 DOI: 10.1002/mawe.202400093
X. H. Liu, W. T. Zhou, P. P. Yan, Z. M. Fu, Y. Wu, X. Y. He, F. Li

This study investigated the effect of magnetic particle size and volume fraction on the shear yield stress and dynamic viscosity of magnetorheological fluids. Magnetorheological fluids with varying volume fractions of micro- and nanoscale magnetic particles were prepared. A plate-on-plate shear test bench was constructed to evaluate the fluids under a constant shear rate, with the applied current ranging from 0 A to 1.2 A. Results indicated that the shear yield stress initially increased and then decreased as the volume fraction of magnetic nanoparticles increased, reaching a maximum of 47 kPa at a volume fraction of 7 %. However, the excessive addition of magnetic particles or large-diameter particles led to settling and reduced stability of the fluids. The findings suggest that optimizing the size and volume fraction of magnetic particles is crucial for maximizing the shear yield stress of magnetorheological fluids.

本研究探讨了磁性颗粒尺寸和体积分数对磁流变液剪切屈服应力和动态粘度的影响。研究人员制备了具有不同体积分数的微米级和纳米级磁性颗粒的磁流变液。构建了一个板对板剪切试验台,以评估恒定剪切速率下的流体,施加的电流从 0 A 到 1.2 A 不等。结果表明,随着磁性纳米粒子体积分数的增加,剪切屈服应力先是增大,然后减小,在体积分数为 7% 时达到最大值 47 kPa。然而,过量添加磁性颗粒或大直径颗粒会导致沉降,降低流体的稳定性。研究结果表明,优化磁性颗粒的大小和体积分数对于最大限度地提高磁流变流体的剪切屈服应力至关重要。
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引用次数: 0
Evaluating storage conditions on the effect of peroxide content in acrylonitrile Bewertung der Lagerungsbedingungen und der Auswirkungen des Peroxidgehaltes in Acrylnitril 评估储存条件对丙烯腈中过氧化物含量的影响 评估储存条件和丙烯腈中过氧化物含量的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-22 DOI: 10.1002/mawe.202400068
X. Li, S. Zhang, T. Liu, H. Li, X. Sui

The content of peroxide in acrylonitrile is critical for the production of polyacrylonitrile-based carbon fibers. Peroxide-free acrylonitrile is used as a blank solution for testing the peroxide content of acrylonitrile, which storage conditions are important to the test. Of course, for the change of peroxide content in acrylonitrile stored for a period of time has an effect on the production of carbon fiber. In order to study the effect of storage conditions on peroxide in peroxide-free acrylonitrile and acrylonitrile, the changes at refrigerator and room temperature were studied, respectively. Studies have shown that storage at temperatures below 20 °C for 3 months hardly affect the use of either peroxide-free acrylonitrile or acrylonitrile. The experimental results obtained are useful for practical production and testing, which can improve the accuracy of testing and stability of production.

丙烯腈中的过氧化物含量对于聚丙烯腈基碳纤维的生产至关重要。不含过氧化物的丙烯腈被用作检测丙烯腈过氧化物含量的空白溶液,其储存条件对检测非常重要。当然,存放一段时间后,丙烯腈中过氧化物含量的变化会对碳纤维的生产产生影响。为了研究储存条件对无过氧化物丙烯腈和丙烯腈中过氧化物的影响,分别研究了在冰箱和室温下的变化。研究表明,在低于 20 °C 的温度下储存 3 个月,几乎不会影响无过氧化物丙烯腈或丙烯腈的使用。所获得的实验结果对实际生产和检测很有帮助,可以提高检测的准确性和生产的稳定性。
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引用次数: 0
Simulation and experimental study on surface modification of 6061-T651 aluminum alloy by machine hammer peening Simulation und experimentelle Studie zur Oberflächenmodifikation von der Aluminiumlegierung 6061-T651 durch maschinelles Hammerstrahlen 机器锤击强化 6061-T651 铝合金表面改性的模拟和实验研究 机器锤击强化 6061-T651 铝合金表面改性的模拟和实验研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-22 DOI: 10.1002/mawe.202400007
X. Lin, J. Xu, G. Sun

Machine hammer peening is a surface treatment technique employed to enhance the surface properties of the treated samples. In this present work, the theoretical analysis, finite element simulation and experiment of single peening are carried out to investigate the relationship between the machine hammer peening force and geometric dimensions of the single peening indentation deformation, including diameter and depth. The single peening experimental results are in accordance with theoretical and simulation analysis. The machine hammer peening experiment with grate tool path are done and the results including surface topography, surface roughness, surface hardness, x-ray diffraction analysis and wear resistance are discussed. This work seeks to explore the effects of process parameters like machine hammer peening force, indentation and pitch spacing on surface roughness and hardness. The results reveal that the surface hardness and roughness are positively associated with machine hammer peening force and small indentation and pitch spacing lead to high hardness. The x-ray diffraction analysis validate machine hammer peening is a mechanical treatment without new compound generated. The friction test results in an enhancement in wear resistance of treated samples.

机锤强化是一种表面处理技术,用于提高被处理样品的表面性能。本研究对单次强化进行了理论分析、有限元模拟和实验,以研究机锤强化力与单次强化压痕变形的几何尺寸(包括直径和深度)之间的关系。单次强化实验结果与理论和模拟分析结果相符。使用篦形刀具路径进行了机锤强化实验,并讨论了包括表面形貌、表面粗糙度、表面硬度、X 射线衍射分析和耐磨性在内的结果。这项工作旨在探索机器锤式强化力、压痕和间距等工艺参数对表面粗糙度和硬度的影响。结果表明,表面硬度和粗糙度与机器锤击强化力呈正相关,压痕和间距小则硬度高。X 射线衍射分析验证了机锤强化是一种机械处理方法,不会产生新的化合物。摩擦测试结果表明,经过处理的样品耐磨性有所提高。
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引用次数: 0
Optimization of laser powder bed fusion process parameter for the fabrication of AlSi12 using NSGA-II and Pareto search algorithm Optimierung der Prozessparameter für das Laserstrahl-Pulverbett-Schmelzen zur Herstellung von AlSi12 mit NSGA-II und Pareto-Suchalgorithmus 利用 NSGA-II 和帕累托搜索算法优化制造 AlSi12 的激光粉末熔床工艺参数 利用 NSGA-II 和帕累托搜索算法优化制造 AlSi12 的激光粉末熔床工艺参数
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-22 DOI: 10.1002/mawe.202400098
S. K. Balla, R. K. Konki, M. Manjaiah, A. Joshi

Additive manufacturing, notably laser powder bed fusion (LPBF), excels in producing complex geometries and is widely used in the automotive, aerospace, and naval industries. Laser powder bed fusion enables the creation of components with the required stiffness and strength at a lighter weight than traditional manufacturing methods. Aluminium alloys are particularly promising for laser powder bed fusion in the automotive and aerospace sectors. To enhance the effectiveness of laser powder bed fusion-produced components, optimized process parameters must be designed for specific materials. This study investigates the influence of processing parameters, scan speed, scan strategy, and hatch space, on the relative density, surface roughness, and microhardness of AlSi12 samples fabricated by laser powder bed fusion. A Taguchi L27 orthogonal array was used to systematically analyze the effects of these parameters. A regression model was developed and evaluated through analysis of variance using signal-to-noise (S/N) ratios to identify optimal parameter values. Results indicated that the scan pattern significantly affects relative density, while hatch space impacts surface roughness and microhardness. Optimal solutions were obtained through multi-objective optimization using the non-dominated sorting genetic algorithm (NSGA-II) and Pareto search algorithms. Experimental validation showed average errors of 0.483 % and 0.461 % for NSGA-II and Pareto search algorithms, respectively.

快速成型技术,特别是激光粉末床熔融技术(LPBF),擅长制造复杂的几何形状,并广泛应用于汽车、航空航天和海军工业。与传统制造方法相比,激光粉末床熔融技术能以更轻的重量制造出具有所需刚度和强度的部件。在汽车和航空航天领域,铝合金在激光粉末床熔融技术中的应用前景尤为广阔。为了提高激光粉末床熔融技术生产部件的效果,必须针对特定材料设计优化的工艺参数。本研究探讨了加工参数、扫描速度、扫描策略和舱口空间对激光粉末床熔融技术制造的 AlSi12 样品的相对密度、表面粗糙度和显微硬度的影响。采用田口 L27 正交阵列系统分析了这些参数的影响。通过信噪比(S/N)进行方差分析,建立并评估了回归模型,以确定最佳参数值。结果表明,扫描模式对相对密度有显著影响,而舱口空间对表面粗糙度和显微硬度有影响。通过使用非支配排序遗传算法(NSGA-II)和帕累托搜索算法进行多目标优化,获得了最佳解决方案。实验验证表明,NSGA-II 和帕累托搜索算法的平均误差分别为 0.483 % 和 0.461 %。
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引用次数: 0
In situ digital image correlation study on the mechanical properties of GH4169 at different temperatures In-situ-Studie zur digitalen Bildkorrelation der mechanischen Eigenschaften von GH4169 bei verschiedenen Temperaturen 不同温度下 GH4169 力学性能的原位数字图像相关性研究 不同温度下 GH4169 力学性能的原位数字图像相关性研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-22 DOI: 10.1002/mawe.202300392
X. Y. Wu, J. Zhu, J. W. Liu, S. Y. Wang, X. H. Hou, X. Jiang, F. C. Lang, Y. M. Xing

GH4169 is a precipitation-strengthened nickel-based high-temperature alloy, and its mechanical behavior at different temperatures is of significant importance for practical applications. Here, an in situ study on the mechanical properties and microstructural evolution of the GH4169 alloy at different temperatures was conducted using scanning electron microscopy in combination with digital image correlation. The results demonstrate the existence of a linear relationship between the local average strain and the macroscopic strain. At temperatures of 20 °C, 100 °C, 180 °C, and 260 °C, the local average strain is 1.96, 2.13, 2.26, and 2.30 times the macroscopic strain, respectively, which shows a clear trend. This indicates that the temperature has a significant influence on the plasticity of the alloy. Additionally, the strain is concentrated below the notch, whereby at a macroscopic strain of 1.7 % at 20 °C and 260 °C, the local maximum strain at the notch is 52 % and 83 %, respectively. Furthermore, when the macroscopic strain reaches 2.12 %, the local maximum strain at the notch is 72 % and 103 %, respectively. At this point, cracks start to initiate and gradually propagate. In situ observations show that at the beginning of the tensile plasticity stage, the plastic strain rate in the grains is twice the rate at the grain boundaries; subsequently, both rates tend to stabilize, and a high-strain zone appears inside the grains and is coordinately transferred to the surrounding grains through the grain boundaries. The final stage of damage of the alloy consists of perforation fracture, and the presence of a large number of cracked carbides at the fracture results in specimen cracking.

GH4169 是一种沉淀强化镍基高温合金,其在不同温度下的力学性能对实际应用具有重要意义。本文利用扫描电子显微镜结合数字图像相关技术,对 GH4169 合金在不同温度下的力学性能和微观结构演变进行了现场研究。研究结果表明,局部平均应变与宏观应变之间存在线性关系。在温度为 20 ℃、100 ℃、180 ℃ 和 260 ℃ 时,局部平均应变分别是宏观应变的 1.96 倍、2.13 倍、2.26 倍和 2.30 倍,呈现出明显的趋势。这表明温度对合金的塑性有显著影响。此外,应变集中在切口下方,在 20 °C 和 260 °C 时,当宏观应变为 1.7 % 时,切口处的局部最大应变分别为 52 % 和 83 %。此外,当宏观应变达到 2.12 % 时,缺口处的局部最大应变分别为 72 % 和 103 %。此时,裂纹开始产生并逐渐扩展。现场观察表明,在拉伸塑性阶段开始时,晶粒中的塑性应变率是晶界应变率的两倍;随后,两种应变率趋于稳定,晶粒内部出现高应变区,并通过晶界协调地传递到周围的晶粒。合金破坏的最后阶段是穿孔断裂,断口处出现大量裂纹碳化物导致试样开裂。
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引用次数: 0
Impressum: Materialwiss. Werkstofftech. 9/2024 版本说明:Materialwiss.9/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-08 DOI: 10.1002/mawe.202480921
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引用次数: 0
Materialwiss. Werkstofftech. 9/2024 材料科学材料技术 9/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-08 DOI: 10.1002/mawe.202480911
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引用次数: 0
Cover Picture: (Materialwiss. Werkstofftech. 9/2024) 封面图片: (Materialwiss. Werkstofftech. 9/2024)
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-08 DOI: 10.1002/mawe.202480901

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引用次数: 0
Correction to “Use of a low transformation temperature effect for the targeted reduction of welding distortion in stainless chromium-nickel steel for an application in rail vehicle construction” 对 "利用低转变温度效应有针对性地减少不锈铬镍钢的焊接变形,以应用于轨道车辆制造 "的更正
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-08 DOI: 10.1002/mawe.202477164

M. Gamerdinger, F. Akyel, S. Olschok, C. Kahve, D.C. Fritsche, U. Elliesen, C. Hopmann, U. Reisgen. Use of a low transformation temperature effect for the targeted reduction of welding distortion in stainless chromium-nickel steel for an application in rail vehicle construction. Materialwiss. Werkstofftech. 2024, 55, 1005–1017.

In paragraph “Acknowledgements” the following text is missing:

“The presented investigations were carried out at RWTH Aachen University within the framework of the Collaborative Research Centre SFB1120-236616214 “Bauteilpräzision durch Beherrschung von Schmelze und Erstarrung in Produktionsprozessen” and funded by the Deutsche Forschungsgemeinschaft e. V. (DFG, German Research Foundation). The sponsorship and support is gratefully acknowledged. The data that support the findings of this study are available at http://hdl.handle.net/21.11102/777fe674-4446-445c-ab21-b38f5b0b37b5 upon request”

We apologize for this error.

M.Gamerdinger, F. Akyel, S. Olschok, C. Kahve, D.C. Fritsche, U. Elliesen, C. Hopmann, U. Reisgen.利用低转变温度效应有针对性地减少不锈铬镍钢的焊接变形,应用于轨道车辆制造。Materialwiss.Werkstofftech.2024, 55, 1005-1017.In paragraph "Acknowledgements" the following text is missing: "The presented investigations were carried out at RWTH Aachen University within the framework of the Collaborative Research Centre SFB1120-236616214 "Bauteilpräzision durch Beherrschung von Schmelze und Erstarrung in Produktionsprozessen" and funded by the Deutsche Forschungsgemeinschaft e. V. (DFG, German Research Foundation).(DFG, 德国研究基金会) 资助。衷心感谢赞助和支持。支持本研究结果的数据可向 http://hdl.handle.net/21.11102/777fe674-4446-445c-ab21-b38f5b0b37b5 索要。"我们对这一错误表示歉意。
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