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Anisotropic hardening of MS1180 steel plate: Experimental and analytical modeling Anisotrope Härtung von Stahlblechen aus MS1180: Experimentelle und analytische Modellierung MS1180 钢板的各向异性硬化:实验和分析建模 MS1180 钢板的各向异性硬化:实验和分析建模
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300155
Y. Tang, C. Zhou, P. Wu, X. Fang, Y. Wang, Y. Lou, T. Pan, J. Wang

This work is carried out to investigate the anisotropic hardening behavior of MS1180 steel through experiment and analytical modeling. Dogbone and hydraulic bulging specimens were machined to test the mechanical behavior of MS1180 steel plate under different loading directions and stress states. The loading process was recorded by the three-dimensional digital image correction system. The result uncovers that the strength under equi-biaxial tension is larger than that under uniaxial tension. Mechanical behavior under different loading directions presents the obvious difference related to the plastic strain. Hardening behavior under uniaxial tension and equi-biaxial tension is characterized by the Swift-Voce and polynomial equations, respectively. Three yield functions are adopted to describe the anisotropic behavior, including Yld2000-2d, S-Y2009, and CQN-Chen. A convexity analysis method based on geometric definition is used to determine the convex region of the CQN-Chen yield surface under large strain. By comparing the yield surfaces of the three yield functions under different plastic strain, the CQN-Chen yield function possesses a more flexible and reasonable characterization ability than the Yld2000-2d and S-Y2009 yield functions. The anisotropic hardening behavior of MS1180 steel plate is modeled with an error of less than 0.03 by the CQN-Chen yield function, showing high prediction accuracy.

本研究通过实验和分析模型研究了 MS1180 钢的各向异性硬化行为。为测试 MS1180 钢板在不同加载方向和应力状态下的力学行为,加工了狗骨试样和液压鼓包试样。加载过程由三维数字图像校正系统记录。结果表明,等轴拉伸下的强度大于单轴拉伸下的强度。不同加载方向下的力学行为呈现出与塑性应变相关的明显差异。单轴拉伸和等轴拉伸下的硬化行为分别由 Swift-Voce 和多项式方程表征。采用了三种屈服函数来描述各向异性行为,包括 Yld2000-2d、S-Y2009 和 CQN-Chen。基于几何定义的凸性分析方法用于确定大应变下 CQN-Chen 屈服面的凸区域。通过比较三种屈服函数在不同塑性应变下的屈服面,CQN-Chen 屈服函数比 Yld2000-2d 和 S-Y2009 屈服函数具有更灵活、更合理的表征能力。CQN-Chen 屈服函数对 MS1180 钢板各向异性硬化行为的建模误差小于 0.03,显示了较高的预测精度。
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引用次数: 0
Properties of polyamide epichlorohydrin resin-modified wood fibers/soybean straw powder copolymerization enhanced soy protein biomass composites Eigenschaften von mit Polyamid-Epichlorhydrin-Harz-modifizierten Holzpulvern/Sojabohnenstrohpulver durch Copolymerisation verstärkten Sojaprotein Biomasse-Verbundwerkstoffen 聚酰胺环氧氯丙烷树脂改性木纤维/大豆秸秆粉共聚增强型大豆蛋白生物质复合材料的性能 聚酰胺环氧氯丙烷树脂改性木纤维/大豆秸秆粉共聚增强型大豆蛋白生物质复合材料的性能
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300145
L. Feng, C. Hou, J. X. Wang, Y. Liu

The biomass composites were prepared by hot molding with a pressure of 10 MPa, a temperature of 125 °C, a time of 15 minutes using soybean straw powder, poplar wood fibers, and soy protein as raw materials. The effects of different straw species, the ratio of soybean straw powder to poplar wood fibers, the particle size of soybean straw powder, and the theoretical density on the performance of biomass composites were investigated. The experimental results show that under the condition that the ratio of soybean straw powder and poplar wood fibers is 1 : 1, 20 mesh to 40 mesh soybean straw powder and 20 mesh to 60 mesh wood fibers are selected to copolymerize and strengthen the soy protein biomass composites when the theoretical density is 0.80 g/cm3, the actual density of the biomass composites is 0.90 g/cm3, the tensile strength was up to 22.04 MPa, and the bending strength was up to 44.92 MPa. Biomass composites have good water resistance while obtaining excellent mechanical properties. The above figures not only meet the relevant technical requirements of automotive interior parts but also enable the lightweight design of automobiles and the sustainable development concept of green, low carbon, and environmental protection.

以大豆秸秆粉、杨木纤维和大豆蛋白为原料,在压力为 10 兆帕、温度为 125 °C、时间为 15 分钟的条件下通过热成型制备了生物质复合材料。研究了不同秸秆种类、大豆秸秆粉与杨木纤维的比例、大豆秸秆粉的粒度以及理论密度对生物质复合材料性能的影响。实验结果表明,在大豆秸秆粉与杨木纤维的比例为 1 :1 的条件下,选择 20 目至 40 目大豆秸秆粉和 20 目至 60 目木质纤维共聚增强大豆蛋白生物质复合材料,当理论密度为 0.80 g/cm3 时,生物质复合材料的实际密度为 0.90 g/cm3,拉伸强度达到 22.04 MPa,弯曲强度达到 44.92 MPa。生物质复合材料在获得优异机械性能的同时,还具有良好的耐水性。上述数据不仅满足了汽车内饰件的相关技术要求,还实现了汽车的轻量化设计和绿色、低碳、环保的可持续发展理念。
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引用次数: 0
Development of a robust welding process for electron beam welding of thick plates for construction of offshore wind turbines Entwicklung eines robusten Schweißverfahrens zum Elektronenstrahlschweißen von Dickblechen für den Windenergieanlagenbau 开发用于海上风力涡轮机建造的厚板电子束焊接的稳健焊接工艺 开发用于风力涡轮机建造的厚板电子束焊接的稳健焊接工艺
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300194
U. Reisgen, S. Olschok, T. Evers

Due to its high energy intensity and the associated high welding depth, electron beam welding is particularly suitable for welding steel plates with high wall thicknesses. These are used, for example, in offshore wind power systems. However, due to the cooling conditions, the required cold toughness for offshore applications is often not achieved. The aim is to develop S355 ML steels – within the EN10025 4 standard – for welding monopiles for wind turbines. For this purpose, three parameters with different energy input are developed on three steels. The tests are carried out on plates with a wall thickness of 80 mm, whereby a full penetration weld must be achieved. The resulting top and bottom bead of the welds meet the standard DIN EN ISO 13919-1. The parameters have an energy per unit length of 9.5 kJ mm−1 to 15.5 kJ mm−1. The resulting weld seams have an average width of 5.5 mm to 7.5 mm, and burn-off of the manganese alloy element is observed, particularly on the top side of the seam. In addition, T8/5 times close to the weld seam of 11 s to 27 s are estimated using a simulation.

由于电子束焊接具有高能量强度和高焊接深度,因此特别适用于焊接壁厚较高的钢板。例如,这些钢板可用于海上风力发电系统。然而,由于冷却条件的限制,通常无法达到海上应用所需的冷韧性。我们的目标是开发符合 EN10025 4 标准的 S355 ML 钢,用于焊接风力涡轮机的单桩。为此,在三种钢材上开发了三种不同能量输入的参数。试验在壁厚为 80 毫米的钢板上进行,必须实现全熔透焊接。焊缝的顶部和底部焊缝符合 DIN EN ISO 13919-1 标准。参数的单位长度能量为 9.5 kJ mm-1 至 15.5 kJ mm-1。由此产生的焊缝平均宽度为 5.5 毫米至 7.5 毫米,并可观察到锰合金元素的烧损,尤其是在焊缝的顶部。此外,通过模拟估计,焊缝附近的 T8/5 时间为 11 秒至 27 秒。
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引用次数: 0
Cover Picture: (Materialwiss. Werkstofftech. 6/2024) 封面图片: (Materialwiss. Werkstofftech. 6/2024)
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202480601

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引用次数: 0
Magnesium-based nanocomposites developed through multi-pass friction stir processing and strengthening mechanisms exploration Entwicklung von magnesiumbasierten Nanoverbundwerkstoffen durch einen mehrstufigen Rührreibschweißprozess und Erforschung der Verfestigungsmechanismen 通过多道搅拌摩擦工艺开发的镁基纳米复合材料及强化机理探索 通过多道搅拌摩擦焊接工艺开发的镁基纳米复合材料及强化机理探索
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300291
P. Sagar, A. Handa, Sushma Sangwan

In the current experimental work, using secondary phase hard nano titanium carbide (TiC) particles as reinforcement, two different magnesium metal matrices i. e., AZ31B/TiC and AZ61 A/TiC composite materials were synthesized by friction stir processing. Using the traditional testing approach for the developed materials, the simultaneous gain in metallurgical, mechanical, electrical, and tribological characteristics compared to the base substrate was examined. The microstructure study results for AZ31B/TiC and AZ61 A/TiC composites showed a uniform distribution of reinforced particles as well as an evolution in grain size, from 82 μm to 4.2 μm and from 74 μm to 3.7 μm, respectively, which consequently contribute in a significant gain in the microhardness of both composites i. e., around 2.2 times and 2.67 times respectively, greater than the base metal. When compared to monolithic alloys, the synthesized AZ31B/TiC and AZ61 A/TiC composites showed improvements in the areas of tensile strength, compressive strength, and coefficient of friction up to 1.81 times, and 1.64 times, 1.74 times and 1.58 times, and 57.92 % and 58.47 %, respectively. Furthermore, these improvements in characteristics also increase the final strengthening of the nanocomposite and reduce electrical conductivity.

在当前的实验工作中,使用二级硬质纳米碳化钛 (TiC) 颗粒作为增强材料,通过搅拌摩擦加工合成了两种不同的镁金属基材,即 AZ31B/TiC 和 AZ61 A/TiC 复合材料。采用传统的测试方法,对所开发的材料进行了冶金、机械、电气和摩擦学特性的同步增益测试。AZ31B/TiC 和 AZ61 A/TiC 复合材料的微观结构研究结果表明,增强颗粒分布均匀,晶粒大小也有所变化,分别从 82 μm 减小到 4.2 μm,从 74 μm 减小到 3.7 μm,因此这两种复合材料的显微硬度都有显著提高,分别是基体金属的 2.2 倍和 2.67 倍。与整体合金相比,合成的 AZ31B/TiC 和 AZ61 A/TiC 复合材料在抗拉强度、抗压强度和摩擦系数方面分别提高了 1.81 倍和 1.64 倍、1.74 倍和 1.58 倍,以及 57.92 % 和 58.47 %。此外,这些特性的改善还提高了纳米复合材料的最终强度并降低了导电率。
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引用次数: 0
Powder coating waste filler in high-density polyethylene – Variations in morphology, mechanical and thermal performance Variationen in Morphologie, mechanischer und thermischer Leistung von Pulverlackrecyclaten als Füllstoff in Polyethylen mit hoher Dichte 高密度聚乙烯中的粉末涂料废物填料--形态、机械和热性能的变化 Variationen in Morphologie, mechanischer und thermischer Leistung von Pulverlackrecyclaten als Füllstoff in Polyethylen mit hoher Dichte
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300257
Y. Kısmet

In the present study, electrostatic powder coating waste was recycled and employed to reinforce high-density polyethylene. The hydrolysis method was preferred to modify the powder coating waste of various systems, and they were mixed with high-density polyethylene at various weight ratios. The mixtures were prepared in a mechanical mixer and then in an extruder to obtain a homogeneous mixture. This homogeneous structure was pressed into molds with a plastic injection device to obtain standard tensile samples. Mechanical and thermal tests were conducted on the samples. It was determined that the tensile stress of the sample decreased with the increase in filler content. The changes in sample tensile strength were investigated after the samples were aged. Three-point bending strength of the samples was also investigated and it was observed that they became more resistant to vertical loads as the filler content increased. The Izod impact strength of the samples differed based on the filler type and weight ratio. Furthermore, mass loss in the produced mixtures was determined with thermogravimetric analysis. The matrix and filler bonding mechanisms were observed under an electron microscope.

本研究回收了静电粉末涂料废料,并将其用于增强高密度聚乙烯。首选水解法对各种体系的粉末涂料废料进行改性,并以不同的重量比将其与高密度聚乙烯混合。混合物在机械混合器中制备,然后在挤压机中挤出,以获得均匀的混合物。使用塑料注射装置将这种均质结构压入模具,以获得标准拉伸样品。对样品进行了机械和热测试。结果表明,样品的拉伸应力随着填料含量的增加而降低。在样品老化后,对样品拉伸强度的变化进行了研究。此外,还对样品的三点弯曲强度进行了研究,结果表明,随着填料含量的增加,样品对垂直载荷的抵抗力增强。根据填料类型和重量比,样品的伊佐德冲击强度也有所不同。此外,还利用热重分析测定了所制混合物的质量损失。在电子显微镜下观察了基体和填料的结合机制。
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引用次数: 0
Impressum: Materialwiss. Werkstofftech. 6/2024 版本说明:Materialwiss.6/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202480621
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引用次数: 0
Materialwiss. Werkstofftech. 6/2024 材料科学材料技术 6/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202480611
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引用次数: 0
Electrochemical hydrogen permeation measurement during cyclic stress testing of a ferritic chromium steel Elektrochemische Messung der Wasserstoffpermeation während einer mechanischen Wechselbelastung für einen ferritischen Chromstahl 铁素体铬钢循环应力测试期间的电化学氢渗透测量 铁素体铬钢循环机械应力测试期间的电化学氢渗透测量
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300093
J. M. Vatter, B. Jung, M. Oechsner

In the present work, the hydrogen diffusion during cyclic stress testing in the ferritic chromium steel 1.4521 (X2CrMoTi18-2) is investigated. Therefore, electrochemical hydrogen permeation measurements are carried out on a hollow cylinder geometry. Simultaneously an alternating stress is applied using a stress ratio of R=-1. At low stress amplitudes, no influence on the diffusion behaviour of hydrogen is found. At a higher stress amplitude, close to the macroscopic yield strength, a delayed hydrogen permeation by a factor of two is observed. It is postulated that this observation is a result of the nucleation of new hydrogen traps during the measurement. Hydrogen content measurements using carrier gas hot extraction support this hypothesis.

本研究调查了铁素体铬钢 1.4521 (X2CrMoTi18-2) 在循环应力测试过程中的氢扩散情况。因此,在空心圆柱体上进行了电化学氢渗透测量。同时施加交变应力,应力比为 R=-1。在低应力振幅下,氢的扩散行为不受影响。在接近宏观屈服强度的较高应力振幅下,氢的渗透延迟了 2 倍。据推测,这是由于在测量过程中产生了新的氢阱。使用载气热萃取法进行的氢含量测量也支持这一假设。
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引用次数: 0
Induktive Randschichtnachbehandlung zur Steigerung der Korrosionsschwingfestigkeit des Radsatzwellenwerkstoffes EA4T Inductive surface layer treatment to increase the corrosion fatigue strength of the wheelset shaft material EA4T 感应式表面层处理,提高轮轴材料的腐蚀疲劳强度 EA4T 感应式表面层处理,提高轮轴材料的腐蚀疲劳强度 EA4T
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-02 DOI: 10.1002/mawe.202300319
S. Schönborn, T. Melz, J. Hasnain, H. Scheerer, T. Engler, M. Oechsner, A. Schulz, M. Steinbacher

Wheelset shafts are usually coated to protect them from mechanical and corrosive influences. However, damage during operation requires close inspection intervals to check permissible damage depths. The focus of this research is to investigate a possible increase in corrosion fatigue strength through inductive surface layer treatment for the wheelset shaft material EA4T (25CrMo4+quenched and tempered). For this purpose, process parameters for inductive surface hardening were identified and optimized in order to achieve a sufficiently high hardening depth and hardness of the surface layer on lightly notched test specimens. Subsequently, fatigue strength tests were carried out in air and in 5 % NaCl solution for the initial state and the hardened state. By comparing the fatigue strength results determined, the expected potential for increasing fatigue strength and corrosion fatigue strength was confirmed. In order to demonstrate stone chipping and corrosion stress, further tests were repeated with damage specifically introduced into the surface layer. The findings indicate the potential of surface layer hardening for significantly lower-maintenance wheelset shafts in freight transport in the future.

轮轴通常涂有涂层,以保护其免受机械和腐蚀影响。然而,运行过程中的损坏需要密切的检查间隔,以检查允许的损坏深度。本研究的重点是探讨通过对轮轴材料 EA4T(25CrMo4+淬火和回火)进行感应式表面层处理来提高腐蚀疲劳强度的可能性。为此,确定并优化了感应式表面硬化的工艺参数,以便在轻度缺口试样上获得足够高的硬化深度和表层硬度。随后,在空气和 5 % 氯化钠溶液中对初始状态和硬化状态进行了疲劳强度测试。通过比较测定的疲劳强度结果,证实了提高疲劳强度和腐蚀疲劳强度的预期潜力。为了证明石块崩裂和腐蚀应力,在表层专门引入损伤的情况下重复了进一步的测试。研究结果表明,表层硬化具有在未来货运中大幅降低轮轴维护成本的潜力。
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引用次数: 0
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