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Production and characterization of titanium carbide particulate reinforced AA6061 aluminum alloy composites using stir casting 碳化钛颗粒增强AA6061铝合金复合材料的搅拌铸造制备及表征
Pub Date : 2021-01-01 DOI: 10.4149/KM_2016_3_257
J. Moses, I. Dinaharan, S. Sekhar
Stir casting is an economical method to produce aluminum matrix composites. In the present work, composites of aluminum alloy AA6061 reinforced with various amounts (0, 5, 10 and 15 wt.%) of TiC particles were prepared by stir casting technique. X-ray diffraction patterns of the prepared composites clearly revealed the incorporation of TiC particles without the presence of any other compounds. The microstructures of the composites were studied using optical and scanning electron microscopy. It was observed that the TiC particles distributed all over the composite and properly bonded to the matrix alloy. Local clusters of TiC particles were also seen in a few places. The result shows that the reinforcement of TiC particles enhances the microhardness, ultimate tensile strength and wear resistance of the composite. The details of fracture morphology, worn surface, and wear debris are also presented in this paper. K e y w o r d s: metal matrix composites, stir casting, microstructure, mechanical properties
搅拌铸造是一种经济的铝基复合材料生产方法。本文采用搅拌铸造技术制备了不同含量(0%、5%、10%和15% wt.%)的TiC颗粒增强AA6061铝合金复合材料。制备的复合材料的x射线衍射图清楚地显示TiC颗粒的掺入,而没有任何其他化合物的存在。利用光学显微镜和扫描电镜对复合材料的微观组织进行了研究。结果表明,TiC颗粒分布在复合材料的各个部位,并与基体结合良好。在一些地方也可以看到局部的TiC粒子团。结果表明,TiC颗粒的增强提高了复合材料的显微硬度、极限拉伸强度和耐磨性。文中还详细介绍了断裂形态、磨损面和磨损碎屑。金属基复合材料,搅拌铸造,显微组织,力学性能
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引用次数: 5
Influence of thermal and electrochemical oxidation on the mechanical and corrosion properties of titanium alloy 热氧化和电化学氧化对钛合金力学性能和腐蚀性能的影响
Pub Date : 2021-01-01 DOI: 10.4149/km_2013_4_251
V. Alar, Ž. Alar, S. Jakovljević, B. Runje
In this paper thermal oxidation and electrochemical anodizing processes were used to produce titanium oxide films on titanium alloy and to examine the effects of oxidation on mechanical and corrosion properties. The surface morphology oxide films, thickness and chemical composition of the surfaces were evaluated using scanning electron microscopy and energy dispersive spectroscopy. The microhardness of titanium oxide films prepared at different experimental conditions is maintained between 8, 2 GPa and 9, 6 GPa, measured by ultra micro hardness tester. The microhardness increased with temperature and voltage. The values of roughness parameters Rz, Rt and Ra indicate a somewhat less roughness of the anodized samples. The values of the roughness parameter Rk are nearly identical for both groups of samples. The cyclic polarization tests showed that none of the tested samples were susceptible to localized corrosion. The oxide films produced by anodic oxidation on titanium alloy showed a higher corrosion resistance than the ones produced by thermal oxidation.
本文采用热氧化法和电化学阳极氧化法在钛合金表面制备氧化钛膜,考察了氧化对钛合金力学性能和腐蚀性能的影响。利用扫描电镜和能量色散光谱对氧化膜的表面形貌、厚度和化学成分进行了表征。不同实验条件下制备的氧化钛膜的显微硬度均保持在8.2 ~ 9.6 GPa之间。显微硬度随温度和电压的升高而升高。粗糙度参数Rz, Rt和Ra的值表明阳极氧化样品的粗糙度有所降低。两组样品的粗糙度参数Rk值几乎相同。循环极化试验表明,试样均不受局部腐蚀的影响。在钛合金表面阳极氧化制备的氧化膜比热氧化制备的氧化膜具有更高的耐蚀性。
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引用次数: 1
Al-Cu alloy formation by aluminium underpotential deposition from AlCl3+NaCl melts on copper substrate AlCl3+NaCl熔体在铜基体上欠电位沉积形成铝铜合金
Pub Date : 2021-01-01 DOI: 10.4149/km_2010_3_159
B. Radović, V. Cvetković, R. A. Edwards, J. Jovićević
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引用次数: 1
Observations on the intersection between {1011} and {1012} twin in deformed magnesium alloy 变形镁合金中{1011}和{1012}孪晶交点的观察
Pub Date : 2021-01-01 DOI: 10.4149/km_2021_4_231
G. Xi, J. Zhang, J. Wu, J. Jia, Y. Zhi
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引用次数: 3
Study on the mechanical properties, wear resistance and microstructure of nano-SiCp/ZA38 composite material under the synergistic effects of thermal-force-acoustic field 热-力-声场协同作用下纳米sicp /ZA38复合材料的力学性能、耐磨性和微观结构研究
Pub Date : 2021-01-01 DOI: 10.4149/km_2021_5_303
S. Liu, Y. Sima, L. Zhang, J. Zhang, W. Qiao, Q. Yuan
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引用次数: 0
Effect of solidification parameters on microsegregation behaviour of main alloying elements in a peritectic TiAl based alloy 凝固参数对包晶TiAl基合金中主要合金元素微偏析行为的影响
Pub Date : 2021-01-01 DOI: 10.4149/km_2013_2_89
A. Klimová, J. Lapin, T. Pelachová, M. Nosko
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引用次数: 0
Investigating the effect of reinforcing particulates on the weight loss and worn surface of compocast AMCs
Pub Date : 2021-01-01 DOI: 10.4149/km_2013_1_11
A. Mazahery, M. Shabani
This paper aims to investigate the abrasive wear behavior of the sol-gel coated B4C particulate reinforced aluminum metal matrix composite. Sliding wear is related to asperity-to-asperity contact of two counter surfaces, which are in relative motion against each other. The effective wear from the specimen surface is due to the combined effect of a number of factors. An increase in the applied load leads to increase in penetration of hard asperities of the counter surface to the softer pin surface, increase in micro cracking tendency of the subsurface and also increase in the deformation and fracture of asperities of the softer surface. In general, composites offer superior wear resistance as compared to the alloy irrespective of applied load and B4C particles volume fraction. This is primarily due to the presence of the hard dispersoid which protects the matrix from severe contact with the counter surfaces, and thus results in less wear, lower coefficient friction and temperature rise in composite as compared to that in the alloy. The worn surfaces of all specimens were covered with grooves parallel to the sliding direction and some plastic deformations. These grooves are typical features associated with abrasive wear, in which hard asperities on the steel counter face or hard particles between the pin and disc, plough or cut into the pin cause wear by the removal of the material. Plastic deformation, material smearing, cavities and craters imply adhesive wear. K e y w o r d s: dry sliding, adhesive, mechanically mixed layer
研究溶胶-凝胶包覆B4C颗粒增强铝金属基复合材料的磨粒磨损性能。滑动磨损与两个相互相对运动的计数器表面的粗糙接触有关。试样表面的有效磨损是多种因素共同作用的结果。外加载荷的增加,导致计数器表面的硬突起向较软销表面的渗透增加,次表面的微裂纹倾向增加,软表面突起的变形和断裂也增加。一般来说,复合材料与合金相比,无论施加的载荷和B4C颗粒的体积分数如何,都具有优越的耐磨性。这主要是由于硬分散体的存在,它保护基体免受与计数器表面的严重接触,因此与合金相比,复合材料的磨损更小,摩擦系数更低,温升也更低。所有试件的磨损表面都覆盖着平行于滑动方向的沟槽和一些塑性变形。这些凹槽是与磨料磨损相关的典型特征,其中钢表面上的硬颗粒或销与盘之间的硬颗粒,犁或切入销,通过去除材料引起磨损。塑性变形、材料污迹、空洞和弹坑暗示黏着磨损。可分为:干滑、粘接、机械混合层
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引用次数: 1
Inhibitory effect of new azole derivative in the corrosion of aluminum in acidic medium: common electrochemical and electrochemical noise investigation 新型唑衍生物在酸性介质中对铝腐蚀的抑制作用:常见电化学和电化学噪声研究
Pub Date : 2021-01-01 DOI: 10.4149/KM_2016_3_233
A. Ehsani, H. M. Shiri, M. G. Mahjani, R. Moshrefi, R. Safari
1-(2,4-Dimethylphenyl)-5-amino-1H-tetrazole (DAT) nanoparticles were synthesized, and its inhibiting action on the corrosion of Aluminum AA1005 alloy (Al) in sulfuric acid was investigated using potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). Inhibition efficiency increases as inhibitor concentration increases. A good correlation was observed between the potentiodynamic studies and electrochemical impedance spectroscopy with electrochemical noise measurements. Hence, it seems that the electrochemical noise (EN) method can be applied as a complementary quantitative technique to study the corrosion behavior of inhibitors. The effect of inhibitor concentration on the interpretation of noise resistance and spectral noise impedance was evaluated. Furthermore, quantum chemical calculations were employed to provide further insight into the mechanism of inhibition by DAT. It was shown that the adsorption of inhibitors on the AA1005 surface takes place through both physical and chemical adsorption. The best fit to the experimental data was obtained using Langmuir adsorption isotherm. K e y w o r d s: aluminum, polarization, impedance, electrochemical noise, adsorption, nanostructure
合成了1-(2,4-二甲基苯基)-5-氨基- 1h -四唑(DAT)纳米颗粒,并利用动电位极化和电化学阻抗谱(EIS)研究了其对铝AA1005合金(Al)在硫酸中的腐蚀抑制作用。缓蚀剂浓度越大,缓蚀效率越高。在电位学研究和电化学阻抗谱与电化学噪声测量之间观察到良好的相关性。因此,电化学噪声(EN)方法可以作为一种补充的定量技术来研究缓蚀剂的腐蚀行为。评价了抑制剂浓度对噪声阻力和谱噪声阻抗解释的影响。此外,采用量子化学计算来进一步了解DAT的抑制机制。结果表明,抑制剂在AA1005表面的吸附主要通过物理吸附和化学吸附两种方式进行。Langmuir吸附等温线最符合实验数据。研究方向:铝、极化、阻抗、电化学噪声、吸附、纳米结构
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引用次数: 3
Isothermal oxidation kinetics of laser cladded NiCoCrAl/WC + La2O3 hybrid composite coatings at 700 °C 激光熔覆NiCoCrAl/WC + La2O3复合涂层700℃等温氧化动力学
Pub Date : 2021-01-01 DOI: 10.4149/km_2021_4_269
P. Ashtari, N. P. Ahmadi, S. Yazdani
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引用次数: 0
The effect of nozzle orifice diameter on penetration depth and mechanical properties of AISI430/AISI1040 dissimilar steel joined by keyhole PTA welding process 喷嘴孔径对AISI430/AISI1040异种钢锁孔PTA焊接熔深及力学性能的影响
Pub Date : 2021-01-01 DOI: 10.4149/km_2013_4_241
T. Teker, N. Özdemir
In this study, AISI 430/AISI 1040 steel couple 10 mm thick were welded in the butt position without any pre-treatment using keyhole plasma transferred arc (KPTA) process. Welded joints were manufactured selecting constant welding speed (0.01 mmin−1) and two different nozzle orifice diameters (2.4 and 3.2 mm), three different welding currents (130, 135 and 140 A), at a constant plasma gas flow (1.2 l min−1), a shielding gas flow (25 l min−1). The microstructural changes that occurred in the interface regions of the welded samples were examined by microhardness, scanning electron microscopy (SEM), X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). In order to determine mechanical properties of samples, the V-notch Charpy tests were performed. In addition, fracture types in the notch impact strength tests of samples were determined from the fractographic examinations using SEM. K e y w o r d s: plasma transferred arc welding, keyhole, AISI 430, AISI 1040, nozzle orifice diameter
在本研究中,采用不进行任何预处理的锁孔等离子转移电弧(KPTA)工艺,在对接位置焊接了10 mm厚的AISI 430/AISI 1040钢对。在恒定的等离子体气体流量(1.2 l min - 1)和保护气体流量(25 l min - 1)下,选择恒定的焊接速度(0.01 mm - 1)、两种不同的喷嘴直径(2.4 mm和3.2 mm)、三种不同的焊接电流(130、135和140 A)来制造焊接接头。采用显微硬度、扫描电子显微镜(SEM)、x射线衍射仪(XRD)和能谱仪(EDS)分析了焊接试样界面区微观组织的变化。为了确定试样的力学性能,进行了v形缺口夏比试验。此外,通过扫描电镜的断口分析,确定了试样缺口冲击强度试验中的断裂类型。焊接工艺:等离子转移弧焊,锁孔,AISI 430, AISI 1040,喷嘴孔径
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引用次数: 1
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Metallic Materials
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