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Using an acoustic levitator to investigate the drying kinetics and solids forming process of individual droplets during spray drying 利用声学悬浮仪研究喷雾干燥过程中单个液滴的干燥动力学和固体形成过程
Q3 Agricultural and Biological Sciences Pub Date : 2020-11-03 DOI: 10.1556/446.2020.00011
Ramona Huelsmann, G. Esper, R. Kohlus
Spray drying is a widely used process to turn slurries into dry powders and is especially important for thermally-sensitive materials, that are often found in the food or pharmaceutical industry. However, detailed insight into the drying kinetics during spray drying is difficult to investigate due to the boundary conditions in a spray drying tower. As a result, there is a lack of important information on the drying process and subsequent solidification of individual droplets. In this context, an experimental setup for a droplet positioned in a stationary ultrasonic field of an acoustic levitator is designed to enable a non-contacting measurement of the drying kinetics and the subsequent solidification process. To generate a comparable situation like in a real spray drying process, the droplet is positioned in an airflow, where air temperature, humidity, and velocity can be adjusted over wide range. Using an infrared camera to measure the surface temperature and a Complementary Metal Oxide Semiconductor (CMOS) camera for object recognition, the droplet can be observed continuously and drying kinetics of the droplet can be determined from the measured surface temperature and decreasing droplet size. Result of a 10 wt.% aqueous micro particle TiO2 suspension are reported and show that the investigated method is a very valuable and fast tool to safely scale-up spray drying systems very close to real process conditions. Especially when only small sample amounts are available in an early development stage.
喷雾干燥是一种广泛使用的将浆料转化为干粉的工艺,对于食品或制药行业中常见的热敏材料尤其重要。然而,由于喷雾干燥塔中的边界条件,很难详细了解喷雾干燥过程中的干燥动力学。因此,缺乏关于单个液滴的干燥过程和随后固化的重要信息。在这种情况下,设计了一种用于定位在声学悬浮器的固定超声场中的液滴的实验装置,以实现干燥动力学和随后固化过程的非接触测量。为了产生类似于真实喷雾干燥过程的类似情况,液滴位于气流中,在气流中,空气温度、湿度和速度可以在宽范围内调节。使用红外相机测量表面温度,使用互补金属氧化物半导体(CMOS)相机进行物体识别,可以连续观察液滴,并且可以根据测量的表面温度和液滴尺寸的减小来确定液滴的干燥动力学。报道了10wt.%水性微粒TiO2悬浮液的结果,并表明所研究的方法是一种非常有价值和快速的工具,可以在非常接近实际工艺条件的情况下安全地扩大喷雾干燥系统的规模。尤其是在早期开发阶段只有少量样品可用的情况下。
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引用次数: 3
Examination of the effect of type and quantity of sugar on main sensory parameters of homemade oat-flakes biscuit 糖的种类和用量对自制燕麦饼干主要感官参数的影响
Q3 Agricultural and Biological Sciences Pub Date : 2020-11-02 DOI: 10.1556/446.2020.10004
T. Kaszab, Blanka Halasi, Z. Kovács
The fiber intake is an important part of the human diet. The fiber-deficient nutrition may have long-term health problems. Oat (Avena sativa) is an excellent source of fiber and it has many health benefits due to its rich vitamin and mineral composition. Oats are used as flour and flakes in the food industry. The oat-flakes can be used in a variety of cakes, but it can be also consumed as breakfast cereals or porridge.The objective of our work was to determine the effect of the sugar content and sugar types on main sensory parameters of oat-flakes biscuit. During the experiments, six different types of biscuit were made with the addition of white or brown sugar at three different concentration levels. The moisture content, color, and the frangibility of the samples were analyzed during the 4-day storage period. The sensory evaluation of the biscuit samples was also performed on the first day of storage.The parameters of the rupture test and color measurement did not show significant changes during the storage, but the individual types of biscuits made of different types and quantities of sugar could be well distinguished. Results of sensory evaluation showed significant differences in frangibility, structure and stickiness parameters.
纤维的摄入是人类饮食的重要组成部分。缺乏纤维的营养可能会造成长期的健康问题。燕麦(燕麦)是一种极好的纤维来源,由于其丰富的维生素和矿物质成分,它对健康有很多好处。燕麦在食品工业中用作面粉和燕麦片。燕麦片可以用来做各种蛋糕,但也可以作为早餐谷物或粥食用。研究了含糖量和含糖量对燕麦片饼干主要感官参数的影响。在实验过程中,用三种不同浓度的白糖或红糖制作了六种不同类型的饼干。在4天的贮藏期内,对样品的含水量、颜色和脆性进行了分析。饼干样品的感官评价也在储存的第一天进行。在贮藏过程中,饼干的破裂试验和颜色测量参数没有明显变化,但不同种类和不同糖量的饼干可以很好地区分出不同种类的饼干。感官评价结果显示,脆性、结构和粘性参数存在显著差异。
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引用次数: 0
Food quality attributes of melon (Cucumis melo L.) influenced by grafting 嫁接对甜瓜食品品质特性的影响
Q3 Agricultural and Biological Sciences Pub Date : 2020-11-02 DOI: 10.1556/446.2020.10006
Dzsenifer Németh, G. Balázs, Z. Bodor, J. Z. Zaukuu, Z. Kovács, N. Kappel
Melon (Cucumis melo L.) is an important and valuable vegetable crop that nowadays has a 550ha cultivation area in Hungary. The use of grafting for cucurbits is a growing technique of interest to the food industry. Nevertheless, for melons the practice of grafting is not widespread, in contrast grafted seedlings are widely used by the watermelon growers. On the other hand, it should be mentioned that the food quality attributes can change, due to the grafting. Globally there are not many scientific articles available in this topic. The goal of our study is to provide a systematic review of literature with emphasis on the influence of grafting on melon fruit quality variations and the major advantages of this technique. Over the last few years, the near infrared spectroscopy (NIRS) and electronic tongue method became popular to measure food attributes.
甜瓜(Cucumis melo L.)是一种重要而有价值的蔬菜作物,目前在匈牙利拥有550公顷的种植面积。嫁接葫芦是食品工业日益关注的一项技术。然而,对于甜瓜来说,嫁接的做法并不普遍,相反,嫁接苗被西瓜种植者广泛使用。另一方面,应该提到的是,由于嫁接,食品质量属性可能会发生变化。在全球范围内,关于这一主题的科学文章并不多。我们研究的目的是对文献进行系统综述,重点介绍嫁接对甜瓜果实质量变化的影响以及该技术的主要优势。近几年来,近红外光谱(NIRS)和电子舌法开始流行于测量食物属性。
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引用次数: 1
Betalains, total polyphenols, and antioxidant contents in red beetroot peel (Cylindra type) 红甜菜根皮(圆柱形)中甜菜素、总多酚和抗氧化剂含量
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-30 DOI: 10.1556/446.2020.20004
M. Zin, F. Borda, E. Márki, Szilvia Bánvölgyi
Since significant percentage of fruits and vegetables go to waste during processing, investigation of how to improve the valuable products of extraction from the wastes is an undeniably effective way to save the planet. Beetroot (root, peel, and stalk) is a chief source of natural betalain color compounds and phenolic compounds with copious radical scavenging activity. The major emphasis of this work is to optimize process variables which are extraction time (10–60 min), operating temperature (20–50 °C), and aqueous ethanol solvent with the concentration of (25–75%) for effective extraction of valuable compounds such as betalains, total polyphenols, and antioxidant activity from beetroot peel. Spectrophotometric analysis was applied for quantification of those compounds. Amongst which, lowest solvent concentration (25% v/v) together with the highest temperature (50 °C) and extraction time (50 min) brought yielded higher results. The process optimization was carried out using Design Expert (11.0.3) statistical software. Overall, it can be noted that extraction process can be improved by controlling operating time and temperature, avoiding unnecessary overuse of costly solvent.
由于相当大比例的水果和蔬菜在加工过程中被浪费,研究如何从废物中提取有价值的产品是拯救地球的一种不可否认的有效方法。甜菜根(根、皮和茎)是天然甜菜素颜色化合物和酚类化合物的主要来源,具有丰富的自由基清除活性。本工作的重点是优化提取时间(10-60 min)、操作温度(20-50℃)和乙醇水溶液(25-75%)的工艺变量,以有效地从甜菜根皮中提取甜菜碱、总多酚和抗氧化活性等有价值的化合物。采用分光光度法对这些化合物进行定量分析。其中,最低溶剂浓度(25% v/v)、最高萃取温度(50℃)和萃取时间(50 min)可获得较高的萃取效果。采用Design Expert(11.0.3)统计软件进行工艺优化。总的来说,可以注意到,通过控制操作时间和温度,可以改善提取过程,避免不必要的过度使用昂贵的溶剂。
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引用次数: 8
Heat treatment of liquid egg yolk 蛋黄液的热处理
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-30 DOI: 10.1556/446.2020.10013
E. Ayari, C. Németh, K. Hidas, A. Tóth, Dávid Láng, L. Friedrich
Starting from mechanical revolution, each day new methods and new equipment have emerged. Today, the Ultra Heat Treatment (UHT) is one of the important technologies that permits to the industry to reduce processing time while maintaining the same quality of the products. Egg and egg products are known as heat-sensitive products, so the UHT enables us to preserve their qualities after a heat treatment.Our aim is to study the effect of UHT treatment (approximately 67 °C for 190 s) on the Liquid Egg Yolk (LEY). For twenty-one days, the color and the apparent viscosity were measured every seven days, we also studied the damage of protein using DSC (Differential Scanning Calorimetry).Comparing the two graphs of DSC, the denaturation of protein is distinct. The endothermic peak decreased. This could be seen also on the rheological curves. The apparent viscosity is diminished from 231 mPa.s on the 1st day of storage to 224 mPa.s on 21st day. However, the treated LEY could be stored for longer period than the raw LEY.
从机械革命开始,每天都有新的方法和新的设备出现。如今,超高温处理(UHT)是一项重要技术,它使该行业能够在保持产品质量不变的同时缩短加工时间。鸡蛋和鸡蛋制品被称为热敏产品,因此超高温灭菌使我们能够在热处理后保持其品质。我们的目的是研究超高温处理(约67°C,持续190秒)对液态蛋黄(LEY)的影响。在21天的时间里,每7天测量一次颜色和表观粘度,我们还使用DSC(差示扫描量热法)研究了蛋白质的损伤。对比DSC的两张图,蛋白质的变性是不同的。吸热峰降低。这也可以在流变曲线上看到。表观粘度从储存第1天的231mPa.s降低到第21天的224mPa.s。然而,处理后的LEY可以比未处理的LEY储存更长的时间。
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引用次数: 0
Effects of combined HHP and heat treatment on viscosity attributes and microbiological condition of liquid egg yolk 高温高压复合热处理对蛋黄液粘度属性及微生物状况的影响
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-30 DOI: 10.1556/446.2020.10007
A. Tóth, C. Németh, I. Zeke, Annamária Barkói, K. Hidas, L. Friedrich
Minimal processing technologies, like High Hydrostatic Pressure (HHP), heat treatments at low temperatures have an increasing role in food industry. Eggs are considered as functional foods, but for high retention of biological active compounds adequate minimal processing technologies are needed during preservation procedure. In our study, liquid egg yolk (LEY) was examined to meet consumer's expectations.Combinations of pasteurization (57–63 °C, 5–7 min) and HHP (350–400 MPa, 5 min) were used to provide microbiological stability of LEY. After these treatments samples were examined for mesophyll aerobes and Enterobacteriaceae cell counts (using Nutrient agar an incubation of 30 °C, 48 h) and viscosity attributes (Anton Paar MCR 92).Our results show that microbiological stability is significantly influenced by the different parameters of heat treatments and HHP. Heat treatment effected at least 3 orders of magnitude decrease in cell count. Viscosity attributes point out that higher pressure of HHP have a stronger effect on viscosity than the temperature of pasteurization.The results point out a great opportunity for industrial use of minimal processing technologies for LEY. Microbiological safety is strongly influenced by the order of treatments, but viscosity may be independent from the order of the treatments.
最小加工技术,如高静压(HHP)、低温热处理,在食品工业中发挥着越来越大的作用。鸡蛋被认为是功能性食品,但为了高保留生物活性化合物,在保存过程中需要足够的最小加工技术。在我们的研究中,液态蛋黄(LEY)被检测以满足消费者的期望。巴氏灭菌(57–63°C,5–7分钟)和HHP(350–400 MPa,5分钟)的组合用于提供LEY的微生物稳定性。在这些处理后,检查样品的叶肉需氧菌和肠杆菌科细胞计数(使用营养琼脂培养30°C,48小时)和粘度特性(Anton Paar MCR 92)。我们的结果表明,热处理和HHP的不同参数对微生物稳定性有显著影响。热处理使细胞数量减少了至少3个数量级。粘度属性指出,较高的HHP压力比巴氏灭菌温度对粘度的影响更大。研究结果为LEY的最小加工技术的工业应用提供了一个巨大的机会。微生物安全性受到处理顺序的强烈影响,但粘度可能与处理顺序无关。
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引用次数: 2
Acoustic investigation of chocolate by changing temperature and cocoa content 通过改变温度和可可含量对巧克力的声学研究
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-27 DOI: 10.1556/446.2020.10012
K. Badak-Kerti, V. Zsom-Muha, T. Zsom, D. Nagy, J. Felföldi
In the experiments, the sound generated during the breaking of chocolate samples was examined. The fracture was performed by a precision penetrometer, the breaking sound was recorded. Texture index (TI) was calculated from the resulting signal. First the change of the resulting TI was monitored as a function of the samples' temperature. The sample groups of the same dark chocolate with different temperatures were completely separated from each other with statistical tool (LDA, linear discriminant analyses), but no trend was found to describe the change. Secondly, based on the TI, we could identify and classify the chocolate samples in the appropriate groups (based on cocoa content from 40 to 85%). According to linear discriminant analyses chocolates with different cocoa content were completely separated and showed a certain pattern. Based on the obtained results, it can be stated that the cocoa content of chocolate can be determined on the basis of TI obtained by acoustic method.
在实验中,对巧克力样品破碎过程中产生的声音进行了检测。用精密透度计进行断裂,记录断裂声。根据所得信号计算纹理指数(TI)。首先,将所得TI的变化作为样品温度的函数进行监测。使用统计工具(LDA,线性判别分析)将同一黑巧克力在不同温度下的样本组完全分离,但没有发现描述变化的趋势。其次,基于TI,我们可以将巧克力样品识别并分类为适当的组(基于可可含量从40%到85%)。根据线性判别分析,不同可可含量的巧克力被完全分离,并显示出一定的模式。基于所获得的结果,可以说巧克力中可可含量可以基于声学方法获得的TI来确定。
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引用次数: 1
Comparing different CFD software with NACA 2412 airfoil 不同CFD软件与NACA 2412翼型的比较
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-22 DOI: 10.1556/446.2020.00004
C. Hetyei, I. Molnár, F. Szlivka
The engineering application's design process starts with a concept, based on our theoretical knowledge and continues with a numerical simulation. In our paper, we review the finite volume method (FVM) which is used generally for heat and fluid dynamic simulations.We compare three different computational fluid dynamics (CFD) software (based in the fine volume method) for validating a NACA airfoil, which can be used for example in the aerospace industry for an airplane's wing profile, and it can be used for example in the renewable industry for a wind turbine's blade or a water turbine's impeller profile. At the end of this paper, the result of our simulations will be compared with a validation case and the difference between the CFD software and the measured data will be presented.
工程应用程序的设计过程从一个概念开始,基于我们的理论知识,并以数值模拟继续。在我们的论文中,我们回顾了有限体积法(FVM),它通常用于热和流体动力学模拟。我们比较了三种不同的计算流体动力学(CFD)软件(基于精细体积法)来验证NACA翼型,该软件可用于航空航天工业中的飞机机翼轮廓,也可用于可再生工业中的风力涡轮机叶片或水轮机叶轮轮廓。在本文的最后,我们的模拟结果将与验证案例进行比较,并介绍CFD软件与测量数据之间的差异。
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引用次数: 3
Analysis of the grapevine (Vitis vinifera L.) berry shape by using elliptic Fourier descriptors 用椭圆傅立叶描述符分析葡萄浆果形状
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-22 DOI: 10.1556/446.2020.10009
P. Bodor, E. Somogyi, László Baranyai, J. Lazar, B. Báló
Grapevine berry shape has important marketing value in the table grape commerce, hence variability evaluation of this characteristic is highly important. In this study berry shape of 5 table grape genotypes: “Fanny”, “Lidi”, “Hamburgi muskotály”, “Moldova”, and “Orsi” were compared. To evaluate the shape variability graphic reconstruction and elliptic Fourier analysis have been carried out. Shape outlines have been investigated and Principal Component Analysis (PCA) has been performed with the SHAPE software package. PCA of the contours showed that 6 out of the 77 principal components were effective to describe shape attributes. The first 6 PCs explained 94.51% of the total variance. PC1 associated with the width and length of the berry. PC2 related to the shape of the top and bottom of the berries, while PC3 linked to the ratio of the top and the bottom width. ANOVA of the principal component scores revealed significant difference among the genotypes. Results suggest that morphology of the berry is a variable not only among but within the accessions. Our findings confirmed that elliptic Fourier descriptors (EFDs) would be a powerful tool for quantifying grapevine berry morphological diversity.
葡萄浆果形状在食用葡萄商业中具有重要的市场价值,因此对这一特性的变异性评估非常重要。本研究比较了“Fanny”、“Lidi”、“Hamburgi muscotály”、“Moldova”和“Orsi”5个食用葡萄基因型的浆果形状。为了评估形状变异性,进行了图形重建和椭圆傅立叶分析。对形状轮廓进行了研究,并使用Shape软件包进行了主成分分析(PCA)。轮廓的主成分分析表明,77个主成分中有6个能够有效地描述形状属性。前6个PC解释了94.51%的总方差。PC1与浆果的宽度和长度相关。PC2与浆果顶部和底部的形状有关,而PC3与顶部和底部宽度的比例有关。主成分得分的方差分析显示基因型之间存在显著差异。结果表明,浆果的形态不仅在材料之间而且在材料内部都是可变的。我们的研究结果证实,椭圆傅立叶描述符(EFDs)将是量化葡萄果实形态多样性的有力工具。
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引用次数: 4
Comparing microwave and convective heat treatment methods by applying colour parameters of wine 应用葡萄酒的颜色参数,对微波和对流热处理方法进行了比较
Q3 Agricultural and Biological Sciences Pub Date : 2020-10-17 DOI: 10.1556/446.2020.10011
P. Korzenszky, G. Géczi, T. Kaszab
This research aims to determine whether the treatment of food products in a microwave electromagnetic field is advantageous or disadvantageous compared to conventional technologies. In household practice, microwave energy transfer is used mostly for heating. One of the most important tangible benefits of microwave heat treatment is that it causes less damage to the nutritional value of the product due to its speed.Despite the fact that microwave technology was introduced more than 70 years ago, it is still not clear whether its application results in equivalent products in terms of quality and food safety.This study demonstrates how heat-treated wines with microwave energy transmission and with convective heating in a thermostatic water bath are affected. In the white, rose and red wine samples pasteurized at a temperature of 74 ± 0.5 °C, significant differences between the two heating methods regarding colour characteristics could be indicated.
这项研究旨在确定在微波电磁场中处理食品与传统技术相比是有利还是不利。在家庭实践中,微波能量转移主要用于加热。微波热处理最重要的实际好处之一是,由于其速度快,对产品营养价值的损害较小。尽管微波技术早在70多年前就被引入,但目前尚不清楚其应用是否会在质量和食品安全方面产生同等的产品。这项研究展示了微波能量传输和恒温水浴中对流加热对葡萄酒热处理的影响。在温度为74±0.5°C的巴氏灭菌白葡萄酒、玫瑰葡萄酒和红酒样品中,可以表明两种加热方法在颜色特征方面存在显著差异。
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引用次数: 4
期刊
Progress in Agricultural Engineering Sciences
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