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Determination of oxide barrier-film thickness of anodized aluminum by electrochemical impedance spectroscopy at the nanometer scale 纳米级电化学阻抗光谱法测定阳极氧化铝的氧化障膜厚度
Pub Date : 2010-03-25 DOI: 10.1117/12.861960
K. Habib
In this study, the effect of the annealing treatment on electrochemical behavior and the oxide barrier-film thickness of anodized aluminum-magnesium (Al-Mg) alloy was investigated. Electrochemical parameters such as the polarization resistance (RP), solution resistance (RSol), alternating current impedance (Z), and the double layer capacitance (CdL) of the anodized Al-Mg alloy were determined in sulfuric acid solutions ranged from 0-10% H2SO4 by electrochemical impedance spectroscopy (EIS) methods. Then, the oxide film thickness of the anodized Al-Mg alloy was determined from the obtained electrochemical parameters as a function of the sulfuric acid concentration (0-10% H2SO4), in the as received sample and annealed sample conditions. The optimum thickness of the oxide film was determined for the as received samples (4.2nm) and for the annealed samples (0.63nm) in sulfuric acid concentrations of 4% and 2% H2SO4, respectively. The reason behind the oxide film thickness of the as received samples is greater than the one for the annealed samples, because the former samples are thermodynamically unstable (more chemically active) as compared to the annealed samples. A mathematical model was developed to interpret the mechanism of the oxide film build up on the aluminum substrate. The mathematical model of the oxide film build up on the aluminum substrate was proposed for the next challenge of the present work.
在本研究中,研究了退火处理对阳极氧化铝镁(Al-Mg)合金电化学行为和氧化阻挡膜厚度的影响。采用电化学阻抗谱法(EIS)测定了阳极氧化铝镁合金在0 ~ 10%硫酸溶液中的极化电阻(RP)、溶液电阻(RSol)、交流阻抗(Z)和双层电容(CdL)等电化学参数。然后,根据得到的电化学参数,在接收样品和退火样品条件下,测定了阳极氧化铝镁合金的氧化膜厚度与硫酸浓度(0-10% H2SO4)的关系。在硫酸浓度为4%和2% H2SO4的条件下,分别确定了接收样品(4.2nm)和退火样品(0.63nm)的最佳氧化膜厚度。接收样品的氧化膜厚度背后的原因大于退火样品的氧化膜厚度,因为与退火样品相比,接收样品的热力学不稳定(化学活性更强)。建立了一个数学模型来解释氧化膜在铝基体上形成的机理。提出了在铝基板上形成氧化膜的数学模型,为本工作的下一个挑战。
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引用次数: 0
Noninvasive vital signal monitoring 无创生命信号监测
Pub Date : 2010-03-25 DOI: 10.1117/12.862727
Zenan Wang, J. Chee, K. P. Chua, Z. Chen
Vital signals of patients, such as heart rate, temperature and movement are crucial to monitor patients in hospital. Current heart rate measurement is obtained by using Electrocardiograph, which normally applies electrodes to the patient's body. As electrodes are extremely uncomfortable to ware and hinder patient's movement, a non-invasive vital signal-monitoring device will be a better solution. Similar to Electrocardiograph, the device detects the voltage difference across the heart by using concept of capacitance, which can be obtained by two conductive fiber sewing on the bed sheet. Simultaneous temperature reading can also be detected by using surface mounted temperature sensor. This paper will mainly focus on the heart rate monitoring.
病人的生命信号,如心率、体温、运动等,是医院监测病人的关键。目前的心率测量是通过使用心电图仪获得的,心电图仪通常将电极放在患者的身体上。由于电极非常不舒服,并且会阻碍患者的运动,一种非侵入性的生命信号监测设备将是一个更好的解决方案。与心电图仪类似,该装置利用电容的概念检测心脏两端的电压差,通过在床单上缝两根导电纤维即可获得。同时温度读数也可以通过使用表面安装的温度传感器来检测。本文将主要研究心率监测。
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引用次数: 0
Fabrication of optical comb filter using tapered fiber based ring resonator 利用锥形光纤环形谐振器制备梳状光滤波器
Pub Date : 2010-03-25 DOI: 10.1117/12.862153
S. Harun, K. Lim, A. A. Jasim, H. Ahmad
A tapered fiber based ring resonator is fabricated and its optical characteristic is investigated. Fiber taper is firstly made by heating and stretching a piece of optical fiber, after the polymer protective cladding has been removed. The ring resonator is fabricated by twisting the tapered fiber and manipulating the two ends of the fiber. The comb filter with a constant spacing and an extinction ratio of 4.2dB can be obtained with the ring resonator. The free spectral range (FSR) of tapered fiber ring resonator can be varied from 0.08nm to 0.33nm by controlling the diameter of the ring. The filtering characteristic of the resonator is maintained after packaging with low index polymer.
制作了一种基于锥形光纤的环形谐振器,并对其光学特性进行了研究。光纤锥度首先是通过加热和拉伸一段光纤,然后去除聚合物保护包层。环形谐振器是通过扭转锥形光纤并操纵光纤的两端来制造的。利用环形谐振器可获得恒定间距、消光比为4.2dB的梳状滤波器。通过控制环的直径,锥形光纤环形谐振器的自由光谱范围可在0.08 ~ 0.33nm之间变化。用低折射率聚合物封装后,保持了谐振器的滤波特性。
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引用次数: 0
Numerical simulation of single electron transistor using master equation 利用主方程对单电子晶体管进行数值模拟
Pub Date : 2010-03-25 DOI: 10.1117/12.862848
R. Nuryadi, A. Haryono
In this work, simulation technique for single electron transistor (SET) based on master equation is presented. The SET is modeled as a circuit consisting of two tunnel junctions, one non-tunnel junction and two voltage sources of gate voltage and drain voltage. A tunneling electron is described as a discrete charge due to stochastic nature of a tunneling event. Simulated source-drain current versus drain voltage characteristics show the staircase behavior, while source-drain current is a periodic function of the gate voltage. Coulomb diamond region is also found, which means that the SET operation is based on single electron tunneling. These results reproduce the previous studies of the SET, indicating that the simulation technique achieves good accuration. Such simulation method is also useful in the application of single electron turnstile, single electron pump and the other more complex multiple tunnel junction circuits.
本文提出了基于主方程的单电子晶体管(SET)仿真技术。该电路由两个隧道结、一个非隧道结和两个栅极电压源和漏极电压源组成。由于隧穿事件的随机性,将隧穿电子描述为离散电荷。模拟的源极漏极电流对漏极电压的变化表现为阶梯特性,而源极漏极电流是栅极电压的周期函数。还发现了库仑钻石区域,这意味着SET操作是基于单电子隧穿的。这些结果再现了前人对SET的研究,表明模拟技术达到了较好的精度。这种仿真方法也适用于单电子转门、单电子泵和其他更复杂的多隧道结电路的应用。
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引用次数: 1
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Southeast Asian International Advances in Micro/Nano-technology
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