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On the degree of influence of waterflooding on the oil recovery factor from productive formations of high-viscosity reservoirs X, represented by terrigenous reservoirs 以陆源油藏为代表的高黏度油藏X产层水驱对采收率的影响程度
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-02-24 DOI: 10.31643/2023/6445.28
A. Agzamov, G. Efendiyev, G. Moldabayeva, A. Syzdykov, R. Suleimenova, S. Tuzelbayeva, К. Zaurbekov
On the basis of the generalization of experience in the development of multilayer high-viscosity fields X the influence of waterflooding in the late stage on the oil recovery factor of productive formations has been studied. By applying statistical methods of data processing the dependence of the oil recovery factor on the reservoir flushing factor, with a sufficiently high correlation coefficient, has been obtained. The dependence obtained confirms the theoretical basis of oil recovery from productive formations developed with waterflooding and can be used when designing the process on similar objects. In many oil-producing regions of the world, the tendency of deteriorating quality of the resource base and incomplete replenishment of oil production by the growth of their reserves due to the discovery of new fields is observed. At the same time, the costs of prospecting and exploration works are increasing, and geological, andphysical conditions and specific reserves per each discovered field are worsening.
在总结多层高黏度油田开发经验的基础上,研究了后期注水对生产层采收率的影响。应用数据处理的统计方法,得到了采油系数与储层冲刷系数的相关性,并具有足够高的相关系数。所获得的相关性证实了采用水驱开发的生产层采油的理论基础,可用于类似对象的工艺设计。在世界上许多产油区,由于发现了新油田,资源基础的质量不断恶化,而且由于储量的增加而不能完全补充石油生产。与此同时,勘探和勘探工作的成本在增加,地质和物理条件以及每个已发现油田的具体储量都在恶化。
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引用次数: 1
Determination of the quality of special coke as a result of heat treatment of coal from the Shubarkolskoye field Shubarkolskoye矿区煤热处理后专用焦炭质量的测定
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-02-24 DOI: 10.31643/2023/6445.33
A. Aubakirov, A. G. Kaliakparov, L. Tolymbekova
To date, there is a tendency to increase the pace of production in the field of ferrous metallurgy. The constant demand for steel products is accompanied by an increase in prices for raw materials, including carbon reducing agents. In the conditions of the domestic market of Kazakhstan, of great interest is the study and the possibility of using low-baking and non-baking coal as a raw material for the production of special coke used as a reducing agent in metallurgy, the relevance and expediency of which is also due to the resource conservation and energy efficiency program in the use of raw materials put forward by the Government of the Republic of Kazakhstan. In this article, as a result of the search for high-quality, alternative types of reducing agents used in the production of ferroalloys, experimental data of thermal oxidation treatment (coking) of long-flame, non-baking coals of the Shubarkol deposit (Kazakhstan) are presented. In laboratory conditions, during the experiments, the tested grade D coals with a fraction of 70-80 mm were subjected to temperature exposure at temperatures of 800, 850, 900, 950 °C with various preset heating speeds to determine the quality characteristics that meet the requirements for reducing agents for the metallurgical industry, in particular for the production of ferroalloys, in electro thermal, steelmaking, for agglomeration of iron and non-ferrous ores, etc. A technical analysis of long–flame coal was carried out, the volatile and moisture content of which are Vdaf – 44.5%, W – 14.8%, respectively. Also, the obtained special coke was evaluated by the content of volatile components as a result of heat treatment of coals from the Shubarkol deposit: the volatile content averaged 1.73-3.15%, the moisture was 0.73-1.65%.Based on the results of the studies, the possibility of obtaining a special coke from these types of coals with appropriate characteristics was shown.
迄今为止,在黑色冶金领域有加快生产步伐的趋势。对钢铁产品的持续需求伴随着包括减碳剂在内的原材料价格的上涨。在哈萨克斯坦国内市场的条件下,研究和探讨使用低焙烧煤和非焙烧煤作为原料生产冶金还原剂专用焦炭的可能性是非常值得关注的,其相关性和便捷性也得益于哈萨克斯坦共和国政府提出的原料使用中的资源节约和能源效率计划。在本文中,作为寻找用于铁合金生产的高质量、可替代类型的还原剂的结果,提出了对长焰、未烘烤煤(哈萨克斯坦)的Shubarkol矿床进行热氧化处理(焦化)的实验数据。在实验室条件下,在实验过程中,将分数为70-80 mm的D级煤在800、850、900、950℃的温度下以不同的预设加热速度进行暴露,以确定满足冶金工业,特别是铁合金生产,电热,炼钢,铁和有色矿石团聚等还原剂要求的质量特性。对长焰煤进行了技术分析,其挥发分和水分含量分别为Vdaf - 44.5%和W - 14.8%。通过对Shubarkol矿床煤热处理后的挥发性组分含量进行评价,得到的特殊焦炭挥发性组分平均含量为1.73 ~ 3.15%,水分平均含量为0.73 ~ 1.65%。根据研究结果,指出了从这些煤中获得具有适当特性的特殊焦炭的可能性。
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引用次数: 0
An advanced method for the development of highly reliable asphalt concrete mixture 一种研制高可靠沥青混凝土混合料的先进方法
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-02-24 DOI: 10.31643/2023/6445.27
S. Kosparmakova, Zh. A. Shashpan, M. Guler
This paper introduces the new technology of road construction pavement Superpave. From the beginning of the technology, the method of calculation of road pavement temperature has been taken as an example on the Shymkent city road in Kazakhstan. The material calculation for high quality was conducted with the new climate data of the exact city. A new methodological approach will determine the most accurate selection of bitumen binder grades using a specifically developed PG Grade calculation based on the meteorological data for the period from 2000 to 2020 (20 years) for the specific city. This will be intended to establish requirements for bitumen binders testing by the traditional method for both original and modified bitumen, such as penetration, softening point, and flash and fire point tests, taking into account the climatic characteristics of the republic. Today, have to be accounted that the most common bitumen binder is a 70-100 penetration rating, which means that quite incorrect to use at the highest temperature in Shymkent at +41.3°C and with the lowest temperature at -17.8°C. The results will help to decide on the use of polymer modification of binders, taking into account the design temperatures and operating conditions of asphalt concrete surfaces.
介绍了路面超铺施工新技术。该技术从一开始就以哈萨克斯坦的奇姆肯特城市道路为例进行了路面温度的计算。高质量的材料计算是利用精确城市的新气候数据进行的。一种新的方法方法将根据2000年至2020年(20年)特定城市的气象数据,使用专门开发的PG等级计算来确定沥青粘合剂等级的最准确选择。本标准将考虑到共和国的气候特点,制定用传统方法对原始沥青和改性沥青进行沥青粘合剂测试的要求,如渗透、软化点、闪点和燃点测试。目前,最常见的沥青粘合剂的渗透等级为70-100,这意味着在奇姆肯特的最高温度(+41.3°C)和最低温度(-17.8°C)下使用是不正确的。考虑到沥青混凝土表面的设计温度和操作条件,研究结果将有助于决定聚合物改性粘合剂的使用。
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引用次数: 0
Fine-grаined fiber concrete using polypropylene аnd bаsаlt fibers 细颗粒纤维混凝土采用聚丙烯纤维和粗纤维
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-02-24 DOI: 10.31643/2023/6445.26
M. Nurbаyevа, L. Аruovа, R. Lukpаnov, S.А. Vаinberger, M. Gunasekaran
The purpose of the study is to evаluаte the effect of fibers on the bending strength of fine-grаined concrete sаmples. The results of experimentаl studies of polypropylene аnd bаsаlt fibers for dispersion reinforcement of concrete аre considered. The strength chаrаcteristics of fiber concrete of different compositions hаve been determined. The regulаrities of the influence of fiber type аnd concentrаtion on the strength chаrаcteristics of fiber concrete аre reveаled. The results of determining the bending strength of fine-grаined fiber concrete without аdding fiber (control composition) аnd with the аddition of polypropylene fiber 0.1, 0.5, 1.5, 2.5% of the weight of cement аnd bаsаlt 0.05, 0.1, 0.2, 0.5% of the weight of cement аre presented. It is shown thаt the optimаl limits of the introduction of polypropylene fiber in the mixture of fine-grаined concrete cаn be considered 0.5 % by weight of cement. The introduction of bаsаlt fiber in the mixture of fine-grаined concrete in аn аmount of 0.1 % of the weight of cement cаn increаse the bending tensile strength.
本研究的目的是评估纤维对细粒混凝土试件抗弯强度的影响。本文考虑了聚丙烯纤维和粗纤维对混凝土分散性加固的试验研究结果。测定了不同成分纤维混凝土的强度特性。揭示了纤维类型和浓度对纤维混凝土强度特性影响的规律。给出了不添加纤维(对照成分)和添加水泥重量的0.1、0.5、1.5、2.5%的聚丙烯纤维和水泥重量的0.05、0.1、0.2、0.5%的细粒纤维混凝土的抗弯强度测定结果。结果表明,在细颗粒混凝土混合物中引入聚丙烯纤维的最佳限度可考虑为水泥重量的0.5%。在细颗粒混凝土混合料中掺入掺量为水泥重量0.1%的粗纤维,可提高混凝土的抗弯抗拉强度。
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引用次数: 0
Removal of Ferrous using Citric Acid in Patchouli Oil Purification by Complexometry 络合法纯化广藿香油中柠檬酸去除亚铁的研究
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-01-26 DOI: 10.31643/2023/6445.31
S. Primandari, Mulianti, A. Kaharudin, Y. Fernanda, Generousdi, B. Narayanan
This study is aimed to examine citric acids as a potential chelating agent to decrease colloidal impurities in patchouli oil to improve its quality. It covers colour, specific density, refractive index, acid value, iron content, oleoresin oil content, and patchouli alcohol. Complete Randomized Design with factorial design is used with two factors and repeated 3 times. Factors are (1) citric acid concentration consists of 0.25%, 0.5%, 1.0% and 1.50% (w/v), (2) stirring time of 30, 60 and 90 minutes. Further, purified oil by citric acid was compared to purified oil by Ethylene Diamine Tetra Acetate (EDTA). Findings show that the concentration of chelating agents and the time of stirring have an effect on the quality of patchouli oil. The higher the chelating concentration and the more the stirring time, the better the quality of purified patchouli oil in terms of colour, specific density, refractive index, acid value, and iron content. Findings also show that citric acid has almost the same performance as EDTA. The main components in patchouli oil (patchouli alcohol and oleoresin oil) are not affected by treatment. Purified patchouli oil by using citric acid meets Indonesian National Standard (SNI) requirements so citric acid is one of the potential chelating agents.
本研究旨在探讨柠檬酸作为一种潜在的螯合剂,可以减少广藿香油中的胶体杂质,从而提高广藿香油的质量。它包括颜色、比密度、折射率、酸值、铁含量、油树脂含量和广藿香醇。完全随机设计和因子设计采用两个因素,重复3次。影响因素为(1)柠檬酸浓度分别为0.25%、0.5%、1.0%和1.50% (w/v);(2)搅拌时间分别为30、60和90分钟。此外,还比较了柠檬酸纯化油和乙二胺四乙酸(EDTA)纯化油。结果表明,螯合剂的浓度和搅拌时间对广藿香油的质量有影响。螯合浓度越高,搅拌时间越长,纯化的广藿香油的颜色、比密度、折射率、酸值、铁含量等品质越好。研究结果还表明,柠檬酸与EDTA具有几乎相同的性能。广藿香油的主要成分(广藿香醇和油树脂油)不受处理的影响。用柠檬酸纯化广藿香油符合印尼国家标准(SNI)的要求,因此柠檬酸是一种很有潜力的螯合剂。
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引用次数: 0
Anchor bolt of rock massif in coal mines to decrease soil rock heaving of the workings 煤矿岩体锚杆,以减少工作间的土石隆起
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2022-11-28 DOI: 10.31643/2023/6445.21
V. Demin, V. Zhurov
During the maintenance of workings, the effects of soil rock heaving, caused by plastic deformation and extrusion into the excavation cavity under the action of the rock pressure, are usually eliminated. The identified patterns of change in the stress-strain state of coal-rock massifs (displacements, stresses, cracking zones), depending on the main mining-geological and mining-technical factors will allow to establish the optimal parameters of soil anchoring, technological schemes for decreasing soil rock heaving of mine workings to increase the stability of preparatory mine workings have been developed. The development and improvement of existing technologies of effective and safe stiffening of near-soil rocks at conducting mine workings on flat and inclined coal seams were substantiated. The modelling of the SSS shows that both side-rock and ground deformations are predominantly influenced by side anchorage which results in reduction of the effective deformations in the rocks surrounding the working and in a decrease of gas release from the coal massif. It is established that the deformations and stresses both side and in-soil rocks in the excavation are influenced by side anchors rather than near-soil ones.
在工程维护过程中,通常可以消除因岩石压力作用下塑性变形和挤压进入开挖腔体而引起的土石隆起的影响。根据主要采矿地质因素和采矿技术因素,确定煤岩体应力-应变状态(位移、应力、开裂区)的变化规律,确定最优锚固参数,并制定了减少矿山巷道围岩隆起以提高预备矿山稳定性的技术方案。论述了平斜煤层开采中有效、安全加固近土岩现有技术的发展和改进。SSS模型表明,边锚对边岩和地面变形均有显著影响,边锚降低了工作区周围岩石的有效变形,降低了煤体瓦斯释放量。研究结果表明,基坑两侧和土内岩石的变形和应力主要受侧锚的影响,而非近土锚的影响。
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引用次数: 0
Extraction of gold from low-sulfide gold-bearing ores by beneficiating method using a pressure generator for pulp microaeration 用压力发生器进行矿浆微曝气的选别法从低硫化物含金矿中提金
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2022-11-28 DOI: 10.31643/2023/6445.19
G. Toktar, D. Magomedov, A.K. Коizhanova, N. Abdyldaev, A.N. Bakraeva
Research results on the study of the material composition of low-sulfide gold-bearing ore from the East Kazakhstan deposit are presented. The main non-metallic minerals of the original sample and beneficiation products include quartz, chlorite (clinochlore), carbonates (calcite and dolomite). Pyrite is present predominantly in the form of cubic crystals, sometimes in the form of clusters. The grain size is from 0.03 to 0.40.5 mm, the size of the clusters reaches several mm. Iron oxides (goethite, hydrogoethite) were formed on pyrite, possibly magnetite and ilmenite. The assay test found that the test sample contains 6.04 g/t Au and 7.9 g/t Ag. The content of sulfide minerals is 11.81%. A significant part of gold (85.51%) is in a finely disseminated state in sulfides, as well as in rock-forming minerals 1.22%. The paper presents the results of laboratory studies of the gold- ore beneficiation ability using gravity concentration processes. Gravity enrichment tests were performed on laboratory equipment: Knelson KS-MD 3 centrifugal concentrator, SKO-05 concentration table, and a two-chamber diaphragm jig (OML TsNIGRI type (jig of Central Geological Research Institute for Nonferrous and Precious Metals)). The obtained results of ore beneficiation on the concentration table show the possibility of obtaining a gravity concentrate with a gold grade of 48.9 g/t with a gold recovery of 40.08%. When separating the gravity concentrate on a jig, the gold extraction was 31.6% at a content of 51.4 g/t. It was found that that according to a single-stage beneficiation scheme in a centrifugal concentrator, a gold-bearing concentrate with a gold content of 58.3 g/t was obtained with a recovery of 80.6%. The dependence of the gold extraction and its content in the gravity concentrate on the output at the Knelson centrifugal concentrator is shown. The results of ore flotation beneficiation show the possibility of obtaining waste grade flotation tailings with a gold grade of 0.8 g/t. The extraction of gold into the combined concentrate, with a gold content of 49.7 g/t, is 88.88%.
介绍了东哈萨克斯坦矿床低硫化物含金矿石物质组成的研究成果。原样及选矿产品的主要非金属矿物有石英、绿泥石(斜绿石)、碳酸盐(方解石、白云石)。黄铁矿主要以立方晶体的形式存在,有时以团簇的形式存在。晶粒尺寸为0.03 ~ 0.0.4 mm,团簇尺寸达数mm。氧化铁(针铁矿、水针铁矿)在黄铁矿上形成,可能有磁铁矿和钛铁矿。经分析检测,样品中Au含量为6.04 g/t, Ag含量为7.9 g/t。硫化物矿物含量为11.81%。大部分金(85.51%)以微细浸染态存在于硫化物中,1.22%存在于造岩矿物中。本文介绍了采用重选工艺对金矿石进行选矿试验研究的结果。重力富集试验在实验室设备上进行:Knelson KS-MD 3离心式选矿机、SKO-05浓度表、双室隔膜跳汰机(OML TsNIGRI型(中央有色贵金属地质研究所跳汰机))。精矿选别结果表明,可获得金品位为48.9 g/t、金回收率为40.08%的重精矿。在跳汰机上分离重精矿时,金的提取率为31.6%,金的含量为51.4 g/t。结果表明,采用离心选矿厂单段选矿方案,可获得含金量为58.3 g/t、回收率为80.6%的含金精矿。给出了重精矿中金的提取率及其含量对Knelson离心选矿厂产量的依赖关系。矿石浮选选矿结果表明,有可能获得金品位为0.8 g/t的废级浮选尾矿。该组合精矿的金提取率为88.88%,金含量为49.7 g/t。
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引用次数: 2
Effect of microarc oxidation on the properties of aluminum alloy samples 微弧氧化对铝合金试样性能的影响
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2022-11-28 DOI: 10.31643/2023/6445.16
Z. Ramazanova, M. Zamalitdinova, M.Zh. Baidauletova, M. Kovalenko
Currently, modern manufacturing industries impose special requirements on structural materials such as aluminum, titanium, and their alloys. Various methods are used to improve the physicomechanical and corrosion properties of these materials. One of the promising ways to modify the surface in order to give it multifunctional properties is the treatment of micro-arc oxidation. A distinctive feature of the process is the formation of the oxide coatings on valve metals because of exposure to micro-arc discharges. At the same time, coatings with unique properties are formed. However, the effect of the micro-arc oxidation process on the properties of the base material has been little studied. The purpose of this work is to study the effect of the micro-arc process, implemented in pulsed mode, on the properties of oxide layers, and the base material. Modification of the alloy surface was carried out in the anode mode, with small values of the duration of the anode current pulse. An alkaline electrolyte solution was used as the electrolyte. Studies of the microhardness of the oxide layer, as well as the metal layer from the interface – oxide layer /metal deep into the metal, have shown that micro-arc discharges affect not only the properties of the oxide layer but also structural changes in the thickness of the metal. It is shown that the formed oxide coating is characterized by high microhardness. The oxide coatings obtained at the duration of the anode current pulse of 100 µs – 200 µs are wear-resistant, the coatings do not collapse, and do not wear to the ground under the accepted test conditions.
目前,现代制造业对结构材料如铝、钛及其合金提出了特殊要求。各种方法被用来改善这些材料的物理、机械和腐蚀性能。微弧氧化处理是一种很有前途的表面改性方法,使其具有多功能性能。该工艺的一个显著特点是由于暴露于微弧放电而在阀门金属上形成氧化物涂层。同时,形成具有独特性能的涂层。然而,微弧氧化工艺对基材性能的影响研究甚少。本工作的目的是研究微弧工艺在脉冲模式下对氧化层和基材性能的影响。在阳极模式下对合金表面进行改性,阳极电流脉冲持续时间很小。采用碱性电解质溶液作为电解液。对氧化层显微硬度的研究,以及从界面-氧化层/金属深入到金属的金属层的研究表明,微弧放电不仅影响氧化层的性能,还会影响金属厚度的结构变化。结果表明,所形成的氧化膜具有较高的显微硬度。在100µs ~ 200µs的阳极电流脉冲持续时间内得到的氧化膜耐磨,涂层不塌陷,在可接受的测试条件下不磨损到地面。
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引用次数: 0
Studies for hydrometallurgical processing of titanium-magnesium production sludge with niobium extraction in solution 溶液提铌法湿法处理钛镁生产污泥的研究
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2022-11-28 DOI: 10.31643/2023/6445.18
A. Ultarakova, Z. Karshyga, N. Lokhova, A. Yessengaziyev, P. Burns
The material composition of sludge deposits from titanium-magnesium production was studied by chemical, X-ray, and microprobe analysis methods. Studies of the phase composition of the collector sludge showed that niobium is mainly bound with aluminum and titanium in oxide compounds. The particles of these compounds are very small and surrounded by the clay and carbonate component of the sludge collector. The chemical and mechanical activation processes of the sludge from the titanium-magnesium production sludge collector were executed based on the data obtained on the material composition. Alkaline leaching of sludge from sludge collector after preliminary activation was executed. The optimum conditions for the niobium extraction from the sludge of the sludge dump from the titanium-magnesium production were determined: sodium hydroxide concentration of 200 g/dm3, glycerol 5 g/dm3, S:L = 1:10, temperature 95 °C, leaching process duration - 4 hours. The addition of glycerol during alkaline leaching of sludge inhibits the transition of hexaniobate into insoluble sodium metaniobate enabling to increase the niobium extraction by 1.3 times with transfer into the solution of up to 80% of the extracted metal.
采用化学、x射线和微探针等分析方法对钛镁生产污泥沉积物的物质组成进行了研究。对集热器污泥相组成的研究表明,铌主要与铝、钛以氧化物形式结合。这些化合物的颗粒非常小,被污泥收集器的粘土和碳酸盐成分所包围。根据所获得的材料组成数据,对钛镁生产污泥收集器产生的污泥进行了化学活化和机械活化处理。初步活化后污泥收集器产生的污泥进行碱性浸出。确定了从钛镁厂排土场污泥中提取铌的最佳工艺条件:氢氧化钠浓度200 g/dm3,甘油5 g/dm3, S:L = 1:10,浸出温度95℃,浸出时间4 h。在污泥的碱性浸出过程中,添加甘油抑制了己酸盐向不溶性的偏氨酸钠的转变,从而使铌的提取率提高了1.3倍,并转移到高达80%的提取金属的溶液中。
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引用次数: 0
Mathematical modeling of sulfuric acid leaching of pyrite cinders after preliminary chemical activation 初步化学活化后硫铁矿渣硫酸浸出的数学模型
IF 0.7 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2022-11-28 DOI: 10.31643/2023/6445.12
Y. Abikak, B. Kenzhaliyev, H. Retnawati, S. Gladyshev, A. Akcil
Pyrite cinders, waste products of pyrite concentrate processing by firing to produce sulfuric acid, can serve as raw materials for the extraction of precious, ferrous, and non-ferrous metals. The paper considers the possibilities of obtaining non-ferrous metal concentrate from pyrite cinders by sulfuric acid leaching. This operation is one of the stages in the integrated technology. To increase the extraction of non-ferrous metals during leaching, the method of preliminary chemical activation was used. Chemical activation was carried out in a solution containing 40-120 g/dm3 NaНCO3 at temperatures of 90-230 ° C and a duration of 30-300 minutes. Sulfuric acid leaching of pyrite cinder after activation was carried out in H2SO4 solutions with a concentration of 5-20 % at a temperature of 60 ° C, duration of 30 minutes, and pulp density of 33 %. To determine the optimal conditions for the sulfuric acid leaching of pyrite cinders, a mathematical planning method was used, which allows to assess with a high degree of reliability the influence of the main factors (temperature, pulp density, the concentration of the solution NaHCO3 and duration) and predict an increase in the efficiency of the process by analyzing the numerical values of the regression equations. As a result of sulfuric acid leaching of pyrite cinders after preliminary chemical activation under optimal conditions determined by a mathematical model, the extraction of iron and non-ferrous metals into a solution is 10-15% higher than without activation.
黄铁矿矿渣是黄铁矿精矿烧制硫酸的废产物,可作为提取贵重金属、黑色金属和有色金属的原料。探讨了用硫酸浸出法从黄铁矿渣中获得有色金属精矿的可能性。该操作是综合技术的一个阶段。为了提高浸出过程中有色金属的提取率,采用了初步化学活化法。化学活化在含有40-120 g/dm3 NaНCO3的溶液中进行,温度为90-230℃,持续时间为30-300分钟。对活化后的硫铁矿渣在浓度为5 ~ 20%的H2SO4溶液中进行硫酸浸出,浸出温度为60℃,浸出时间为30 min,矿浆密度为33%。为了确定硫铁矿渣硫酸浸出的最佳工艺条件,采用数学规划方法,对温度、矿浆密度、NaHCO3溶液浓度和浸出时间等主要因素的影响进行了高可靠性评估,并通过回归方程的数值分析预测了浸出效率的提高。在数学模型确定的最佳条件下,对硫铁矿渣进行初步化学活化后的硫酸浸出,铁和有色金属的提取率比未活化时高10-15%。
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引用次数: 0
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