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Thermal Cycling Induced Bond-Coat Rumpling as a Precursor to TBC Failure 热循环诱导的粘结层皱褶是TBC失效的前兆
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2682
D. Clarke, V. Tolpygo
Microstructural observations of TBCs failed under thermal cycling conditions reveal that failure is associated with extensive local separations between either the thermally grown oxide and the TBC or within the TBC itself close to the thermally grown oxide. Based on extensive microstructural characterization and measurements of concentration profiles within the bond-coat, we present a new model for the cause of these separations based on local increases in the density of the bond coat associated with the beta-NiAl to gamma-prime Ni3Al phase transformation. The phase transformation, driven by aluminum depletion required to form the protective alumina thermally grown oxide, is constrained by the overlying TBC thereby generating tensile stresses across the TBC/TGO interface and its vicinity. The observations and evidence for the new model will be described together with the role of thermal cycling.
热循环条件下TBC失效的显微结构观察表明,失效与热生长氧化物和TBC之间或靠近热生长氧化物的TBC内部广泛的局部分离有关。基于广泛的微观结构表征和对键合层内浓度分布的测量,我们提出了一个新的分离原因模型,该模型基于与β - nial到γ -prime Ni3Al相变相关的键合层密度的局部增加。形成保护性氧化铝热生长氧化物所需的铝耗尽驱动的相变受到上覆TBC的限制,从而在TBC/TGO界面及其附近产生拉伸应力。新模式的观测和证据将与热循环的作用一起描述。
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引用次数: 0
Fatigue Reliability Under Corrosion, Creep, and Fretting Damage 腐蚀、蠕变和微动损伤下的疲劳可靠性
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2670
S. Mahadevan
This paper presents probabilistic methodologies being developed at Vanderbilt University for the reliability analysis of aging structures. Several deterioration mechanisms such as fatigue, corrosion, creep, and fretting are considered, and probabilistic models are developed. Interactions between the different mechanisms are considered. The effects of various uncertain parameters on the overall life prediction estimates are quantified. The fatigue damage process induced by pitting corrosion in aging aircraft is composed of seven stages: pitting nucleation, pit growth, transition from pit growth to short crack, short crack growth, transition from short crack to long crack, long crack growth and fracture. A comprehensive mechanics-based probabilistic model for pitting corrosion fatigue life prediction by including all the stages is presented. Analytical FORM/SORM methods as well as advanced Monte Carlo simulation methods are implemented with the proposed model, and probabilistic sensitivity analysis and parametric studies are performed. Fretting fatigue is one of the main mechanisms of the formation of cracks in riveted lap joint assemblies in aging aircraft and can reduce the fatigue life significantly. A macro-mechanics-based probabilistic model is developed to give the quantitative description of crack nucleation life. Fretting conditions in an idealized, cyclic-loaded pinned connection having dimensions typical of riveted panels are studied. ANSYS finite element analysis is applied to provide the stress, displacement and strain fields in the neighborhood of the contacts between the panel and pin. Creep is one of the principal damage mechanisms for materials operating at elevated temperatures, such as in aircraft and space propulsion engines. It can produce larger strain deformation, stress relaxation, and crack initiation and growth. Current creep-fatigue life prediction methods use a code-specified bilinear model that has several uncertainties and assumptions regarding material behavior. A new continuous creep-fatigue failure criterion function is introduced directly based on experimental data to facilitate analytical reliability approximations. Such a model is advantageous for new high performance materials where previous experience is limited. A linear damage accumulation rule is used. The use of analytical and simulation methods for reliability analysis with the proposed model is investigated. The effects of the scatter and distributions of different random variables on the creep-fatigue life are studied. This study is supported by funds from the National Science Foundation.
本文介绍了范德比尔特大学正在开发的用于老化结构可靠性分析的概率方法。考虑了疲劳、腐蚀、蠕变和微动等几种劣化机制,并建立了概率模型。考虑了不同机制之间的相互作用。量化了各种不确定参数对总体寿命预测估计的影响。时效飞机的点蚀疲劳损伤过程由点蚀成核、坑扩展、坑扩展向短裂纹过渡、短裂纹扩展、短裂纹向长裂纹过渡、长裂纹扩展和断裂七个阶段组成。提出了一种综合考虑各阶段的点腐蚀疲劳寿命预测的基于力学的概率模型。利用该模型实现了解析FORM/SORM方法以及先进的蒙特卡罗模拟方法,并进行了概率敏感性分析和参数化研究。微动疲劳是老化飞机铆接搭接件裂纹形成的主要机制之一,会显著降低其疲劳寿命。为了定量描述裂纹成核寿命,建立了基于宏观力学的概率模型。研究了具有典型铆接板尺寸的理想循环加载钉接中的微动条件。通过ANSYS有限元分析,给出了面板与销接触区域的应力场、位移场和应变场。蠕变是高温下材料的主要损伤机制之一,例如在飞机和空间推进发动机中。它能产生较大的应变变形、应力松弛和裂纹萌生和扩展。目前的蠕变疲劳寿命预测方法使用代码指定的双线性模型,该模型具有关于材料行为的几个不确定性和假设。基于试验数据,直接引入了一种新的连续蠕变-疲劳破坏准则函数,便于分析可靠性近似。这样的模型是有利于新的高性能材料,以前的经验是有限的。采用线性损伤累积规则。研究了用解析法和仿真法对该模型进行可靠性分析的方法。研究了不同随机变量的分散和分布对蠕变疲劳寿命的影响。这项研究由美国国家科学基金会资助。
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引用次数: 0
Microstructural Characterization of Micro-Textured Titanium Surfaces 微织构钛表面的微观结构表征
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2674
W. Soboyejo, C. Mercer, S. Allameh, B. Nemetski, N. Marcantonio, J. Ricci
This paper presents the results of a multi-scale microstructural characterization of micro-textured Ti-6Al-4V surfaces that are used in biomedical implants. The hierarchies of substructural and microstructural features associated with laser micro-texturing, polishing and surface blasting with alumina pellets are elucidated via atomic force microscopy (AFM), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and optical microscopy (OM). The nano-scale roughness profiles associated with the different surface textures are elucidated via AFM. Sub-micron precipitates and dislocation substructures associated with wrought processing and laser processing are revealed by TEM. Micro- and meso-scale images of the groove structures are then discussed using OM and SEM. The implications of the results are discussed for the optimization of laser processing schemes for the fabrication of micro-textured surfaces that will facilitate the self organization of proteins, and the attachment of mammalian cells to the Ti-6Al-4V surfaces in biomedical implants.
本文介绍了用于生物医学植入物的微纹理Ti-6Al-4V表面的多尺度微观结构表征结果。通过原子力显微镜(AFM)、透射电子显微镜(TEM)、扫描电子显微镜(SEM)和光学显微镜(OM)分析了氧化铝颗粒激光微纹理、抛光和表面爆破的亚结构和微观结构特征。通过原子力显微镜分析了不同表面结构的纳米尺度粗糙度分布。透射电镜观察了变形加工和激光加工的亚微米析出物和位错亚结构。然后用OM和SEM对沟槽结构的微观和中尺度图像进行了讨论。研究结果对优化激光加工方案的意义进行了讨论,以制造微纹理表面,促进蛋白质的自组织,以及哺乳动物细胞在生物医学植入物Ti-6Al-4V表面的附着。
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引用次数: 0
Probabilistic Micromechanical Fatigue Model for High Temperature Materials 高温材料的概率微机械疲劳模型
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2654
R. Tryon
The paper discusses an enhanced analytical modeling approach to characterize and understand fatigue crack initiation and growth in gas turbine engine intermetallics. It is recognized that the design of components subjected to fatigue cannot be based on average material behavior but that designs must consider −3σ or some other appropriate extreme value material properties. Thus, a life prediction capability useful in a design application must address the scatter inherent in material response to fatigue. The paper addresses the scatter in fatigue life of gamma titanium aluminide by investigating the microstructural variables responsible for the scatter and developing analytical and semi-analytical models to quantitatively relate the variables to the response. The model is general and considers the entire range of damage accumulation sequences; from crack nucleation of the initially unflawed structure to final fast fracture. However, the model also allows failure to be defined as any subset of damage accumulation i.e., crack initiation life to a particular crack size or the number of cycles to grow a crack from a particular size to final fracture. The models allows the structural engineer to systematically and quantitatively assess the influence of the material uncertainties on the overall reliability of the structure.
本文讨论了一种改进的分析建模方法来表征和理解燃气涡轮发动机金属间化合物的疲劳裂纹萌生和扩展。人们认识到,构件的疲劳设计不能基于材料的平均性能,而必须考虑- 3σ或其他一些适当的极值材料性能。因此,在设计应用中有用的寿命预测能力必须解决材料对疲劳响应中固有的散射。本文通过研究造成散射的微观组织变量,并建立了定量地将这些变量与响应联系起来的分析和半分析模型,来解决γ铝化钛疲劳寿命中的散射问题。该模型具有通用性,考虑了损伤累积序列的全范围;从最初无缺陷组织的裂纹形核到最终的快速断裂。然而,该模型也允许将失效定义为损伤积累的任何子集,即裂纹起裂寿命到特定裂纹尺寸或裂纹从特定尺寸扩展到最终断裂的循环次数。这些模型使结构工程师能够系统和定量地评估材料不确定性对结构整体可靠性的影响。
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引用次数: 0
Synthesis and Characteristics of Interpenetrating Polymer Network Hydrogels Based on Silicone and Poly(vinyl alcohol) 有机硅-聚乙烯醇互穿聚合物网络水凝胶的合成及性能研究
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2700
S. J. Kim, M. Shin
Hydrogels have become increasingly important for use in the biomedical field. They are used diagnostic, therapeutic and implantable devices(e.g. catheter, biosensor, artificial skin, controlled release drug delivery system and contact lenses). Also silicone derivatives are widely used owing to their favorable properties such as low-glass transition temperature, high gas permeability, high thermal stability and good biocompatibility. We have studied the interpenetrating polymer networks(IPN) by previous reports, and to report on the preparation and properties of poly(vinyl alcohol), (PVA) and vinyl terminated polydimethylsiloxane(PDMS) IPN hydrogel in this presentation. The IPN composed of PVA and PDMS was synthesized by the following method. PVA was dissolved in the water to make 10wt% aqueous solution. And PDMS was mixed with 0.5wt% 2,2-dimethyl-2-phenylacetophenone(DMPAP) and 0.5mol% methylenebis acrylicamide(MBAAm). This mixture was added to PVA aqueous solution and heated at 90oC for 3hrs. Various IP{Ns were prepared from different mol ratios of PVA/PDMS. Hydrogels obtained were characterized by using FT-IR, wide angle X-ray diffractometry(WAXD), differential scanning calorimetry(DSC), dielectric analysis(DEA), and equilibrium water content(EWC).
水凝胶在生物医学领域的应用越来越重要。它们被用于诊断、治疗和植入式装置(例如:导管、生物传感器、人造皮肤、控释给药系统和隐形眼镜)。有机硅衍生物由于具有玻璃化转变温度低、透气性好、热稳定性好、生物相容性好等优点而得到广泛应用。我们在以前的报道中研究了互穿聚合物网络(IPN),并在本报告中报告了聚乙烯醇(PVA),聚二甲基硅氧烷(PDMS) IPN水凝胶的制备和性能。采用以下方法合成了由PVA和PDMS组成的IPN。将PVA溶于水中,制成10wt%的水溶液。PDMS与0.5wt% 2,2-二甲基-2-苯基苯乙酮(DMPAP)和0.5mol%亚甲基双丙烯酰胺(MBAAm)混合。将该混合物加入PVA水溶液中,在90℃下加热3h。采用不同的PVA/PDMS物质比制备了不同的IP{Ns。采用红外光谱(FT-IR)、广角x射线衍射(WAXD)、差示扫描量热法(DSC)、介电分析(DEA)和平衡含水量(EWC)对所得水凝胶进行表征。
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引用次数: 0
Clinical Performance: A Reflection of Damage Accumulation 临床表现:损伤积累的反映
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2662
E. Rekow, V. Thompson
Clinical performance of an prosthesis is directly dependent on damage introduced during fabrication and during fatigue loading associated with function. The relation between shaping damage and fatigue damage on clinical performance of all-ceramic dental crowns was investigated. Materials used commercially for all-ceramic crowns and investigated in this study included a series of different microstructures of machinable glass ceramics (Corning), aluminas and porcelains (Vita Zahnfabrik), and zirconias (Norton).
假肢的临床性能直接取决于制造过程中引入的损伤和与功能相关的疲劳载荷。研究了全瓷牙冠成形损伤和疲劳损伤对临床性能的影响。商业上用于全陶瓷冠的材料和本研究调查的材料包括一系列不同微观结构的可加工玻璃陶瓷(康宁),氧化铝和瓷器(Vita Zahnfabrik),以及氧化锆(诺顿)。
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引用次数: 0
Processing and Microstructure Evolution in EB-PVD TBCs EB-PVD tbc的加工与微观结构演变
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2683
S. G. Terry, Junghyun Cho, C. Levi
The connection between processing and performance in thermal barrier coatings produced by electron-beam physical-vapor-deposition is not well understood. A significant component of the problem is the limited understanding of the role that microstructure (including defects) plays in this connection, and the relationships between microstructure and process parameters. This presentation will review recent work aimed at understanding these relationships. The focus will be on the evolution of porosity within the TBC, which is of paramount importance to both thermal conductivity and strain tolerance. Porosity is a result of shadowing processes in the presence of insufficient surface diffusion, and thus deposition temperature and vapor incidence pattern are major parameters. The presentation will highlight the interplay between vapor flux and surface topography, illustrating the relevant phenomena with experimental and modeling results. (Work sponsored by ONR under Grant N00014-99-1-0471 and the UC-LANL Collaborative Research Program.)
电子束物理气相沉积热障涂层的工艺与性能之间的关系尚不清楚。问题的一个重要组成部分是对微观结构(包括缺陷)在这方面所起的作用的理解有限,以及微观结构和工艺参数之间的关系。本报告将回顾旨在理解这些关系的最新工作。重点将放在TBC内孔隙度的演变上,这对导热性和应变容限都至关重要。孔隙度是在表面扩散不足的情况下阴影过程的结果,因此沉积温度和蒸汽入射模式是主要参数。本报告将重点介绍蒸汽通量与表面形貌之间的相互作用,并以实验和模拟结果说明相关现象。(这项工作由美国国家研究中心在N00014-99-1-0471基金和加州大学洛杉矶分校合作研究计划下资助。)
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引用次数: 0
Advanced Stochastic Techniques for Jet Engine Component Life Prediction 喷气发动机部件寿命预测的先进随机技术
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2650
D. Ghiocel
The paper addresses significant aspects of stochastic modeling for jet engine component life prediction. Probabilistic life prediction for gas turbine engine components represents a very difficult engineering problem involving stochastic modeling of multiple, complex random phenomena. A key aspect for developing a probabilistic life prediction tool is to incorporate, and to be open to modeling advances related to dynamic complex random phenomena, including space-time random variabilities of mission environment and material parameters, aero-elastic interactions, friction at contact interfaces, multi-site fatigue, progressive damage mechanism, including loading interactions, etc.. The paper addresses the main aspects involved in stochastic modeling of component fatigue life prediction for jet engine rotating components, specifically fan blades. The paper highlights the need of the use of stochastic process and field models for including space-time varying random aspects. Mission speed profiles produced by pilot’s random maneuvers are modeled by pulse non-Gaussian stochastic processes. These pulse processes are approximated using linear recursive models when the cluster effects are not significant. A more general approach, useful when cluster effects are significant, based on a combination of two pulse processes is used. Aero-pressure distribution on blade as well as blade surface geometry deviations due to manufacturing are idealized by using factorable stochastic field models. Also, stochastic field models are used for modeling strain-life and damage accumulation curves. Stochastic damage accumulation models are based on randomized stress-dependent models (nonlinear damage rule models). The paper also addresses mathematical modeling of stochastic nonlinear responses in multidimensional parameter spaces. Stochastic response surface techniques based on factorable stochastic fields or optimum stochastic models are suggested. An illustrative example of a jet engine blade is used for discussion and to show the consequences of different modeling assumptions.
本文讨论了喷气发动机部件寿命预测随机建模的几个重要方面。燃气涡轮发动机部件的概率寿命预测是一个非常困难的工程问题,涉及多个复杂随机现象的随机建模。开发概率寿命预测工具的一个关键方面是纳入并开放与动态复杂随机现象相关的建模进展,包括任务环境和材料参数的时空随机变异性、气动弹性相互作用、接触界面摩擦、多点疲劳、包括载荷相互作用在内的渐进损伤机制等。本文讨论了喷气发动机旋转部件(特别是风扇叶片)疲劳寿命预测随机建模的主要方面。本文强调了使用随机过程和场模型来包含时空变化的随机方面的必要性。由飞行员随机机动产生的任务速度曲线采用脉冲非高斯随机过程建模。当集群效应不显著时,使用线性递归模型近似这些脉冲过程。一种基于两个脉冲过程的组合的更通用的方法在集群效应显著时很有用。采用可因子随机场模型理想化了叶片上的气动压力分布以及由于制造引起的叶片表面几何偏差。此外,随机场模型用于模拟应变-寿命和损伤累积曲线。随机损伤累积模型是基于随机应力依赖模型(非线性损伤规则模型)。本文还讨论了多维参数空间中随机非线性响应的数学建模。提出了基于可因子随机场或最优随机模型的随机响应面技术。本文以喷气发动机叶片为例进行了讨论,并说明了不同建模假设的结果。
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引用次数: 0
Damage Tolerance in Biomedical Implants: Cardiac Valves and Endovascular Stents 生物医学植入物的损伤容忍度:心脏瓣膜和血管内支架
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2671
R. Ritchie
The human heat rate is roughly 40 million beats per year. To prosthetic implants such as mechanical heart valves and endovascular stents, this means that they must endure almost 109 fatigue cycles during the patient’s lifetime. To prevent premature mechanical failures of such devices, which inevitably lead to patient fatalities, considerations of damage-tolerant design and life-prediction methodologies represent a preferred approach. In this presentation, a damage-tolerant approach to life prediction and “quality control” for both metallic and ceramic heart valve prostheses is presented, based on the notion that the useful life of the device is governed by the time for incipient defects in the material to propagate, by stress corrosion or more critically fatigue, to failure. Based on these analyses, the relative benefits of metallic (Co-Cr, Ti-6Al-4V) vs. ceramic (pyrolytic carbon) valves are discussed. Finally, analogous considerations are presented for endovascular stents, particularly those processed by laser cutting of the superelastic Ni-Ti alloy Nitinol. Again, the relative benefits of Nitinol vs. more traditional metallic implant materials (stainless steel, Co-Cr, titanium, titanium alloys) are discussed.
人体的热率大约是每年4000万次。对于机械心脏瓣膜和血管内支架等假体植入物来说,这意味着它们在患者的一生中必须承受近109次疲劳循环。为了防止这些设备过早的机械故障,不可避免地导致患者死亡,考虑损伤容忍设计和寿命预测方法是首选的方法。在本报告中,提出了一种金属和陶瓷心脏瓣膜假体的寿命预测和“质量控制”的损伤容忍方法,该方法基于这样一种概念,即设备的使用寿命是由材料中早期缺陷传播的时间决定的,通过应力腐蚀或更关键的疲劳,直至失效。基于这些分析,讨论了金属(Co-Cr, Ti-6Al-4V)与陶瓷(热解碳)阀门的相对优势。最后,类似的考虑提出了血管内支架,特别是那些由激光切割的超弹性镍钛合金镍钛诺加工。本文再次讨论了镍钛诺与传统金属植入材料(不锈钢、钴铬合金、钛、钛合金)的相对优势。
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引用次数: 0
Probabilistic Fatigue Damage Assessment for Small Crack Growth 小裂纹扩展的概率疲劳损伤评估
Pub Date : 2000-11-05 DOI: 10.1115/imece2000-2647
Zhengwei Zhao, Irewole Wally Orisamolu
Fatigue and fracture are typical random phenomena due to various uncertainty sources, including material property, initial flaw and crack shape, structural configuration and geometry around crack tip, load fluctuation, and other environmental factors. As contrast to the most commonly used probabilistic fatigue growth models, which are built based on simplified fatigue crack growth law, a framework of probabilistic fracture mechanics based fatigue damage assessment methodology for small crack propagation is presented here. The proposed modeling is developed based on a comprehensive fatigue crack growth model, which accounts the effect of crack aspect ratio, stress ratio, and crack closure and retardation. Due to the complicated nature of the fatigue damage modeling adopted, a high non-linear limit state function with discontinuity resulted from physical domain jumping and overlapping are encountered. The advanced fast probability integration techniques in conjunction with response surface methodology and Monte Carlo simulation are used and the accuracy of the analysis is verified. The interface between probabilistic analysis package and the deterministic fracture mechanics analysis program is developed for the purpose of uncertainty propagation. The probability of failure of fatigue damage is computed first. The statistical characteristics of estimated fatigue life and critical crack size are obtained and presented through CDF/PDF curves. The sensitivity analysis is also performed, which provides an indication of the order of importance for the random variables considered. The results of the study have shown robustness and efficiency of the probabilistic analysis to deal with the real world challenge of uncertainty modelling, propagation, and quantification. Currently, possibility to combine the subject probabilistic damage assessment methodology with reliability updating techniques is under the investigation. The successfulness of the presented research activity will address an important issue of quantitative risk analysis for aging structures subjected to accumulative material damage.
疲劳断裂是一种典型的随机现象,其不确定性来源多种多样,包括材料性能、初始缺陷和裂纹形状、裂纹尖端周围的结构形态和几何形状、载荷波动等环境因素。针对目前常用的基于简化疲劳裂纹扩展规律的概率疲劳扩展模型,提出了一种基于概率断裂力学的小裂纹扩展疲劳损伤评估方法框架。该模型是在综合疲劳裂纹扩展模型的基础上建立的,该模型考虑了裂纹长径比、应力比以及裂纹闭合和延迟的影响。由于所采用的疲劳损伤模型的复杂性,会遇到由物理域跳跃和重叠引起的高度非线性的极限状态函数。采用响应面法和蒙特卡罗模拟相结合的先进快速概率积分技术,验证了分析的准确性。为了实现不确定性的传播,开发了概率分析包与确定性断裂力学分析程序之间的接口。首先计算疲劳损伤的失效概率。通过CDF/PDF曲线得到了预估疲劳寿命和临界裂纹尺寸的统计特征。灵敏度分析也被执行,它提供了一个重要的顺序为考虑的随机变量的指示。研究结果表明,概率分析在处理不确定性建模、传播和量化等现实挑战方面具有鲁棒性和有效性。目前,将主体概率损伤评估方法与可靠性更新技术相结合的可能性正在研究中。本研究的成功将解决累积材料损伤下老化结构的定量风险分析这一重要问题。
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引用次数: 0
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