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Creep Behaviour of Hot Isostatically Pressed Metal-Matrix Composite 热等静压金属基复合材料的蠕变行为
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0496
C. S. Lim, N. P. Hung, Y. C. Tan, N. Loh
Castings usually contain defects such as shrinkage cavities and internal gas porosity. The application of hot isostatic pressing (HIPping) to cast metals can remove such defects through the synergistic effect of high isostatic pressure and high temperature. This paper investigates the effects of HIPping on creep of cast A359/SiC/20p composite. Although creep life was expected to improve due to removal of internal porosity in the castings, the creep results were contrary to expectations. Activation energy calculated for the cast composite, showed a decrease in activation energy for the material after HIPping. Creep life was noted to have improved with higher tensile strength as for the cast composite while creep strain at failure improved with an increase in elongation for the cast-HIPped composite. The effect of stress on creep properties are reported to show a decrease in creep life and creep strain at failure with an increase in stress, temperature remaining constant.
铸件通常含有缩孔和内部气孔等缺陷。将热等静压(HIPping)技术应用于铸造金属,可以通过高等静压和高温的协同作用来消除这些缺陷。研究了HIPping对铸造A359/SiC/20p复合材料蠕变的影响。尽管由于消除了铸件内部孔隙,蠕变寿命有望提高,但蠕变结果与预期相反。对铸态复合材料的活化能计算表明,HIPping后材料的活化能降低。随着拉伸强度的提高,铸造复合材料的蠕变寿命得到改善,而随着伸长率的增加,铸造hipped复合材料的失效蠕变应变得到改善。据报道,应力对蠕变特性的影响表明,随着应力的增加,温度保持不变,蠕变寿命和蠕变应变会减少。
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引用次数: 0
Effects of High Heat on the Strength and Fatigue Life of Unidirectional Polymer-Matrix Composites 高热对单向聚合物基复合材料强度和疲劳寿命的影响
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0495
P. Mclaughlin, Henry A. McShane, R. Cochran, E. Armstrong-Carroll
An analysis of local fiber/matrix interface damage growth in unidirectional composites under tension-tension loading is modified to include thermal residual stresses and subsequent temperature histories with the goal of estimating the loss of strength and fatigue life occurring when a graphite/epoxy composite structure is subjected to flame or hot exhaust gasses. Tests show that epoxy thermomechanical and strength properties degrade rapidly from 200 to 300°C, and that time-at-temperature is important. Using properties estimated from these tests, two mechanisms of static strength and fatigue life reduction are studied: thermal-stress-induced interface cracking parallel to fibers, and degradation of room-temperature interface properties. The effects of heat on static strength and constant-amplitude fatigue life of a particular graphite/epoxy material system are then analytically determined for two heat exposure scenarios: one, a relatively short-time exposure of five minutes; and two, a long-time exposure of more than an hour. Strength and life loss are found to be dependent on temperature, time-at-temperature, and length of damage zone, with severe reductions in static and fatigue strengths at temperatures above 200°C.
单向复合材料在拉伸-拉伸载荷下的局部纤维/基体界面损伤增长分析被修改为包括热残余应力和随后的温度历史,目的是估计当石墨/环氧复合材料结构受到火焰或热废气时发生的强度和疲劳寿命损失。试验表明,在200 ~ 300℃范围内,环氧树脂的热机械性能和强度性能迅速下降,温度下的时间是重要的。利用这些试验估计的性能,研究了静态强度和疲劳寿命降低的两种机制:热应力诱导的平行于纤维的界面开裂和室温界面性能的退化。热对特定石墨/环氧材料体系的静态强度和恒幅疲劳寿命的影响,然后分析确定了两种热暴露情景:一种,相对较短的暴露时间为5分钟;二是长时间暴露超过一小时。强度和寿命损失与温度、温度下的时间和损伤区长度有关,在200℃以上的温度下,静态强度和疲劳强度会严重降低。
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引用次数: 0
Microscopic Examination of Titanium Matrix Composites Subjected to Testing Designed to Cause Varying Dominant Damage Mechanisms 钛基复合材料在不同主要损伤机制下的显微检查
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0476
J. Calcaterra, W. S. Johnson
Titanium Matrix Composites (TMC’s) like SCS-6/Timetal 21S are envisioned for use as a structural material for advanced aircraft and in the next generation of turbine engine. In general, damage in representative temperature and load regimes can be dominated by either mechanical, environmental or time dependent deformation and damage mechanisms. Mechanical deformation, present under all load conditions, includes mechanisms such as matrix yielding and fiber/matrix debonding. Time dependent deformation refers to either the creep or relaxation of the matrix and will typically occur at moderately high elevated temperatures. Environmental damage is also time dependent but is distinguished by the fact that it describes the chemical interaction of the composite and the environment. Environmental damage in SCS-6/Timetal 21S composites is commonly thought to be caused by the oxygen embrittlement of the matrix. This damage type becomes prevalent at high elevated temperatures which are near the operational limit of the material. Testing has been completed at Georgia Tech to separate the three damage types listed above. This test matrix involved isothermal constant amplitude fatigue tests at temperatures of 400, 500 and 650°C with hold times at the maximum stress varying from 1 to 100 seconds. Testing was conducted on laminates with stacking sequences of both [0/±45/90]s and [90/±45/0]s. The changes in stacking sequence yielded significant differences in cyclic lives for identical test conditions. Fractographic examination of the specimens indicate that the true cause for environmental attack is not the formation of brittle oxides, but the coarsening of the alpha grains in the microstructure. This form of damage is shown to affect the fracture morphology of specimens at all temperatures, but proper selection of the stacking sequence can reduce the importance of this effect and increase cyclic lives.
像SCS-6/Timetal 21S这样的钛基复合材料(TMC)被设想用作先进飞机和下一代涡轮发动机的结构材料。一般来说,在具有代表性的温度和载荷情况下的损伤可以由机械、环境或时间相关的变形和损伤机制决定。机械变形存在于所有载荷条件下,包括基体屈服和纤维/基体脱粘等机制。时间相关变形是指基体的蠕变或松弛,通常发生在中等高温下。环境损害也与时间有关,但其区别在于它描述了复合材料与环境的化学相互作用。SCS-6/Timetal 21S复合材料的环境破坏通常被认为是由基体的氧脆引起的。这种损伤类型在接近材料工作极限的高温下变得普遍。佐治亚理工学院已经完成了对上述三种损伤类型的分离测试。该测试矩阵包括在400、500和650℃温度下的等温恒幅疲劳测试,在最大应力下保持时间从1到100秒不等。在[0/±45/90]s和[90/±45/0]s的叠加顺序下对层压板进行了测试。在相同的试验条件下,堆叠顺序的变化导致循环寿命的显著差异。试样的断口分析表明,环境攻击的真正原因不是脆性氧化物的形成,而是微观组织中α晶粒的粗化。这种形式的损伤在所有温度下都会影响试样的断裂形态,但适当选择堆叠顺序可以降低这种影响的重要性,并提高循环寿命。
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引用次数: 0
Damage Accumulation Mechanisms in Thermal Barrier Coatings 热障涂层的损伤积累机制
Pub Date : 1996-11-17 DOI: 10.1115/1.2807004
G. Newaz, S. Nusier, Z. Chaudhury
Spallation is a major failure condition experienced by thermal barrier coatings (TBCs) subjected to thermal and mechanical loads. Although evidence of spallation is substantiated and mechanistic models to describe the failure condition is prevalent in literature, the progressive nature of damage evolution leading to spallation has not been addressed adequately. In this paper, we investigated the damage evolution in partially stabilized zirconia TBC on Nickel-based single crystal superalloy, Rene N5. Thermal cycles were imposed on button specimens with Electron Beam - Plasma Vapor Deposition (EB-PVD) TBC coating. The bond coat was PtAl. The temperature range used was 200–1177C. Progressive damage evolution was tracked using microscopy on samples subjected to a series of thermal cycles. Fick’s law can describe the thermally grown oxide (TGO) buildup for early cycles. However, at higher number of thermal cycles, damage in the form of microcracks and their coalescence results in the loss of integrity of the TGO. Thus, both oxidation kinetics and damage appears to have significant roles to play as it relates to spallation. As these microcracks coalesce to form major delamination cracks or interlayer separation, the susceptibility for coating buckling is increased. The delamination cracks finally consume the TGO layer. The loss of TBC integrity from the bond coat and the substrate facilitates its buckling during cool down from elevated temperature. Our estimations show that a delamination crack length of about sixteen times the TBC thickness is needed for the current material system to initiate buckling. Progressive microcrack linking is a possible mechanism to develop such critical delamination crack lengths. Physical evidence of buckling was found in specimens prior to complete spallation.
剥落是热障涂层在热载荷和机械载荷作用下的主要失效形式。尽管裂裂的证据是确凿的,并且描述破坏状态的机制模型在文献中普遍存在,但导致裂裂的损伤演化的渐进性尚未得到充分解决。本文研究了部分稳定氧化锆TBC对镍基单晶高温合金Rene N5的损伤演化过程。采用电子束-等离子体气相沉积(EB-PVD) TBC涂层对纽扣试样进行热循环处理。粘合层是PtAl。使用的温度范围为200 - 1177℃。使用显微镜对一系列热循环的样品进行了渐进式损伤演变。菲克定律可以描述早期循环中热生成氧化物(TGO)的积累。然而,在较高的热循环次数下,微裂纹形式的损伤及其合并导致TGO完整性的丧失。因此,氧化动力学和损伤似乎都有重要的作用,因为它涉及到剥落。当这些微裂纹合并形成大的脱层裂纹或层间分离时,涂层屈曲的易感性增加。分层裂纹最终消耗TGO层。粘结层和基材的TBC完整性的丧失使其在高温冷却时容易发生屈曲。我们的估计表明,脱层裂纹长度约为TBC厚度的16倍,目前的材料系统需要引起屈曲。渐进微裂纹连接可能是形成这种临界分层裂纹长度的机制。在完全剥落之前,在标本中发现了屈曲的物理证据。
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引用次数: 22
Fatigue Damage Modeling and Life Prediction of Titanium Matrix Composites 钛基复合材料疲劳损伤建模与寿命预测
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0472
P. C. Wang, J. Yang, A. Mal
The evolution of microstructural damage during fatigue loading, which includes matrix cracking, interfacial debonding, and fiber fracture results in the progressive degradation of mechanical properties of the fiber-reinforced titanium matrix composites. A mechanism-based fatigue life prediction methodology was developed to simulate the evolution of fatigue damage, degradation of mechanical properties, and distribution of fatigue lives under various applied stress levels. The simulated matrix crack propagation rates, residual stiffness, residual tensile strength, and fatigue life are also correlated with experimental results.
疲劳加载过程中基体开裂、界面剥离和纤维断裂等微观组织损伤的演化导致了纤维增强钛基复合材料力学性能的逐步退化。提出了一种基于力学的疲劳寿命预测方法,以模拟不同应力水平下疲劳损伤的演变、力学性能的退化和疲劳寿命的分布。模拟的基体裂纹扩展速率、残余刚度、残余抗拉强度和疲劳寿命也与实验结果相关。
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引用次数: 0
Dislocation Punching in Functionally-Graded Materials 功能梯度材料中的位错冲孔
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0473
M. Taya, J. Lee, T. Mori
A new dislocation punching model for a functionally graded material (FGM) subjected to a temperature change has been proposed, using Eshelby’s model. FGM, consisting of several layers, is deposited on a ceramic substrate. Two types of microstructures are examined for a layer: one consists of a metal matrix and ceramic particles and the other of a ceramic matrix and metal particles. An elastic energy is evaluated when plastic strain, in addition to thermal mismatch strain, is introduced in the metal phase. The work dissipated by the plastic deformation is also calculated. From the condition that the reduction in the elastic energy is larger than the work dissipated, a critical thermal mismatch strain to induce stress relaxation is determined. The magnitude of the plastic strain is also determined, when the relaxation occurs. The results of the present theory for a special case of FGM, i.e., the case of single interface coincide with those of our earlier work on a thin metal coating on ceramic substrate. The theory is applied to a model FGM consisting of mixtures of Pd and Al2O3 on an Al2O3 substrate.
利用Eshelby模型,提出了一种温度变化下功能梯度材料的位错冲孔模型。FGM由几层组成,沉积在陶瓷衬底上。对一层进行两种类型的微观结构检查:一种由金属基体和陶瓷颗粒组成,另一种由陶瓷基体和金属颗粒组成。当在金属相中引入塑性应变和热失配应变时,计算弹性能。计算了塑性变形所耗散的功。从弹性能减少量大于功耗散的条件出发,确定了引起应力松弛的临界热失配应变。当松弛发生时,塑性应变的大小也被确定。本理论对于FGM的一种特殊情况,即单界面情况的结果与我们先前对陶瓷基板上薄金属涂层的研究结果一致。将该理论应用于由Al2O3衬底上的Pd和Al2O3混合物组成的FGM模型。
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引用次数: 0
Crack Deflection and Penetration Criteria for Brittle Matrix Composites 脆性基复合材料裂纹挠度和侵彻准则
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0479
N. Pagano
In this work, we will consider the three most crucial mechanisms that control the behavior of unidirectional brittle matrix composites (BMC) such that they display the desired characteristics of adequate strength and damage tolerance (or toughness). Composites made with uncoated silicon carbide fibers and two different glass matrices which differ principally in their thermal expansion coefficients were made and tested in order to determine matrix crack initiation stress (Fig. 1), fiber fracture (Fig. 2), and a lower bound interface fracture toughness (Fig. 3). Furthermore, these tests provide direct evidence to examine the quality of an axisymmetric damage model (ADM) derived earlier [1, 2]. Although there was no observed damage tolerance in that both stress-strain curves were linear to failure, a stable system of (apparently) full-cell matrix cracks (Fig. 1) develops prior to ultimate failure. It is not clear if the matrix cracks have arrested prior to entering the fiber or if they have penetrated the fiber itself.
在这项工作中,我们将考虑控制单向脆性基复合材料(BMC)行为的三个最关键的机制,使它们显示出足够的强度和损伤容限(或韧性)的所需特性。由未涂层碳化硅纤维和热膨胀系数主要不同的两种不同玻璃基体制成的复合材料进行了制作和测试,以确定基体裂纹起裂应力(图1)、纤维断裂(图2)和界面断裂韧性的下限(图3)。此外,这些测试为检验之前导出的轴对称损伤模型(ADM)的质量提供了直接证据[1,2]。虽然没有观察到损伤容限,因为应力-应变曲线与破坏呈线性关系,但在最终破坏之前,一个稳定的(显然)全细胞矩阵裂纹系统(图1)已经形成。目前还不清楚基质裂缝是在进入纤维之前就停止了,还是已经穿透了纤维本身。
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引用次数: 0
Mechanism-Based Design of Composite Structures 基于力学的复合材料结构设计
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0485
S. Adjerid, M. Beall, G. Dvorak, J. Fish, J. Flaherty, J. Hudson, K. Shek, M. Shephard, R. Wentorf
The paper introduces high temperature composite software developed for mechanism-based design of composite structures. Mechanism-based design is characterized by an understanding of the critical composite behaviors at several physical scales: the fibrous (micro) scale, the ply/weave (meso) scale and the laminated part (macro) scale, and by the specification of the available design parameters to achieve functionality by those behaviors. A software framework is described which integrates material modeling and analysis codes, provides automated assistance, and links to material databases. Elastic and inelastic material modeling codes suitable for high temperature composites with complex reinforcement and weave/lay-up configurations are presented and references to their underlying theories are given. Advanced analysis techniques are outlined for numerically efficient computational plasticity based on mathematical homogenization, idealization error indicators for material scale, three dimensional crack propagation in a fibrous composite, and modeling of reactive vapor infiltration and chemical vapor deposition processes.
介绍了为复合材料结构基于力学的设计而开发的高温复合材料软件。基于机制的设计的特点是理解几个物理尺度上的关键复合材料行为:纤维(微观)尺度,铺面/编织(中观)尺度和层压部分(宏观)尺度,并通过规范可用的设计参数来实现这些行为的功能。描述了一个软件框架,它集成了材料建模和分析代码,提供自动化辅助,并链接到材料数据库。提出了适用于具有复杂增强和编织/铺层结构的高温复合材料的弹性和非弹性材料建模规范,并给出了它们的基础理论参考。本文概述了基于数学均匀化、材料尺度的理想化误差指标、纤维复合材料的三维裂纹扩展以及反应蒸汽渗透和化学气相沉积过程建模的数值高效计算塑性的先进分析技术。
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引用次数: 0
An Approach to Characterize Nonlinear Viscoelastic Material Behavior Using Dynamic Mechanical Tests and Analyses 用动态力学试验和分析表征非线性粘弹性材料性能的方法
Pub Date : 1996-11-17 DOI: 10.1115/1.2791791
H. Golden, T. Strganac, Richard Schapery
Traditional methods of viscoelastic material characterization have not been able to rapidly characterize nonlinear viscoelastic materials. Dynamic mechanical analysis has been a method in which only linear viscoelastic material properties are rapidly identifying. Herein, dynamic mechanical analysis is extended to provide a method of nonlinear characterization. The proposed method is based on an extension of Schapery’s nonlinear viscoelastic model to dynamic mechanical theory. The oscillatory loading during a dynamic test is accounted for by expanding the nonlinear viscoelastic model on stress. An experimental protocol is established and utilized in the characterization of thin film polyethylene for validation of the nonlinear dynamic mechanical theory.
传统的粘弹性材料表征方法已不能快速表征非线性粘弹性材料。动态力学分析一直是一种只能快速识别材料线性粘弹性特性的方法。在此,将动态力学分析扩展为提供一种非线性表征方法。该方法是基于Schapery的非线性粘弹性模型在动力力学理论中的推广。通过扩展应力非线性粘弹性模型来解释动态试验过程中的振荡载荷。建立了一种实验方案,并将其应用于聚乙烯薄膜的表征中,以验证非线性动态力学理论。
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引用次数: 22
Failure Analysis of Fiber Composites at Phase Interface 纤维复合材料相界面失效分析
Pub Date : 1996-11-17 DOI: 10.1115/imece1996-0490
H. Edmiston, S. Nomura
Failure criteria of fiber reinforced composites expressed in terms of externally applied stresses are derived based on the interface stress distribution. The composite is modeled by a single inclusion surrounded by a matrix which possesses the properties of the composite. Using the Eshelby’s method and the self-consistent approximation, the interface stress can be derived analytically as a function of fiber and matrix properties and the fiber volume fraction. Using the proposed method, failure envelopes can be drawn that can properly reflect the effect of fiber shapes and anisotropy.
基于界面应力分布,导出了以外应力表示的纤维增强复合材料破坏准则。复合材料的模型是由具有复合材料特性的基体包围的单个夹杂物组成。利用Eshelby方法和自洽近似,可以解析地推导出界面应力作为纤维和基体性能以及纤维体积分数的函数。利用该方法,可以绘制出能较好地反映纤维形状和各向异性影响的失效包络。
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引用次数: 0
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Aerospace and Materials
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