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Meso-Scale Strain Measurements in Fiber Reinforced Composites 纤维增强复合材料的细观尺度应变测量
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26028
B. Koohbor, C. Montgomery, S. White, N. Sottos
Effective bulk properties of fiber-reinforced composites can be determined from individual constituent properties through spatial homogenization. Homogenization, in this regard, is conducted over a specifically selected volume of the material that is sufficiently small to capture complex local deformation response, while large enough to encompass all individual components, i.e. fibers and matrix. The physical dimension of such homogenization volumes is a key parameter in multiscale studies. Experimental measurement of the length scale at which the transition from micro to macroscale response occurs is challenging. In the present study, we propose a systematic approach to estimate the physical dimensions of a micro-to-macro transition length scale in terms of the number of fibers in the transverse plane of a cross-ply laminate subjected to remote tensile load. In-house fabricated cross-ply composite samples are loaded in tension in a miniature tensile frame inside a scanning electron microscope, while images are acquired from a small area of interest located on the transverse ply. Digital Image Correlation (DIC) is utilized to obtain full-field strain distribution within the area of interest at various global stress/strain intervals. Spatial averaging of strains at mesoscale is used to determine the micro-to-macro transition scale.
纤维增强复合材料的有效体积性能可以通过空间均匀化从单个组分的性能来确定。在这方面,均质化是在特定选择的材料体积上进行的,该体积足够小以捕获复杂的局部变形响应,同时足够大以包含所有单个组件,即纤维和基质。这种均质体积的物理尺寸是多尺度研究中的一个关键参数。从微观尺度到宏观尺度反应发生转变的长度尺度的实验测量是具有挑战性的。在本研究中,我们提出了一种系统的方法来估计微观到宏观过渡长度尺度的物理尺寸,根据受远程拉伸载荷的交叉层合板横向平面上的纤维数量。内部制造的交叉层复合材料样品在扫描电子显微镜内的微型拉伸框架中以张力加载,同时从横向层上的小区域获取图像。利用数字图像相关技术(DIC)在不同的全局应力/应变区间获得感兴趣区域内的全场应变分布。采用中尺度应变的空间平均来确定微观到宏观的过渡尺度。
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引用次数: 1
On The Use of Multifunctional Z-Pins for Sensing Internal Damage in Composite Laminates Based on Electrical Resistance Measurements 基于电阻测量的多功能z型引脚在复合材料层合板内部损伤检测中的应用
Pub Date : 2018-11-07 DOI: 10.12783/asc33/26120
R. Hart
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引用次数: 0
Experimental and Numerical Characterization of the Intra-Laminar Fracturing Behavior in Discontinuous Fiber Composite Structures 不连续纤维复合材料结构层内断裂行为的实验与数值表征
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26079
S. Ko, K. Chan, Reed Hawkins, Rohith Jayaram, C. Lynch, Reda El Mamoune, M. Nguyen, Nicolay Pekhotin, N. Stokes, Daniel N. Wu, M. Tuttle, Jinkyu Yang, M. Salviato
In this paper, we investigate the intra-laminar size effect of discontinuous fiber composites (DFCs) with three different unidirectional prepreg platelet sizes (75×12, 50×8, and 25×4 mm). Experimentally, we test five different sizes of single edge notched specimens, geometrically scaled (1:2/3:1/3:1/6:1/20), with the constant thickness. We observe notch insensitivity meaning that the crack initiate away from the notch, when the structure sizes are small (from the ratio 1/20 to 1/6). However, the crack always initiate for the ratio of 2/3 and 1. Bazants size effect law is used to analyze such unconventional fracturing behaviors. The experimental results are fitted using the linear regression analysis follow by the size effect law. The transition behavior of the DFCs from the strength based criteria to the energy based criteria is clearly observed. Also, as the platelet size increases, the fracture behaviors shift away from the energy based criteria, which implies a decrease in brittleness. To obtain the intra-laminar fracture energy, Gf , we have developed a finite element model based on the stochastic laminate analogy. The platelet size of 75×12 mm shows 96.8% increase in the fracture energy compared to the platelet size of 25×4 mm while behaves less brittle way. In conclusion, this study examines the effect of the platelet sizes of the DFCs in the presence of the notch. In this process, capturing the quasi-brittleness of the material using the nonlinear fracture mechanics is essential and we accomplish this using the simple size effect law. This work expands on an earlier SAMPE conference proceeding [1], and thus, there is a significant overlap in texts and figures between this and the SAMPE conference proceedings.
在本文中,我们研究了具有三种不同单向预浸料血小板尺寸(75×12, 50×8和25×4 mm)的不连续纤维复合材料(dfc)的层内尺寸效应。实验中,我们测试了五种不同尺寸的单边缺口试样,几何缩放(1:2/3:1/3:1/6:1/20),厚度不变。我们观察到缺口不敏感,这意味着当结构尺寸较小(从1/20到1/6的比例)时,裂纹从缺口处开始。在2/3和1的比例下,裂纹总是产生的。利用Bazants尺寸效应定律对非常规压裂行为进行了分析。采用线性回归分析,根据尺寸效应规律对实验结果进行拟合。可以清楚地观察到DFCs从基于强度的准则到基于能量的准则的转变行为。此外,随着血小板尺寸的增加,断裂行为偏离了基于能量的标准,这意味着脆性的降低。为了得到层间断裂能Gf,我们建立了基于随机层压类比的有限元模型。当血小板尺寸为75×12 mm时,其断裂能比25×4 mm时提高96.8%,但脆性较弱。总之,本研究考察了缺口存在时dfc血小板大小的影响。在此过程中,利用非线性断裂力学捕获材料的准脆性是必不可少的,我们使用简单的尺寸效应定律来实现这一点。这项工作扩展了早先的SAMPE会议论文集[1],因此,在文本和数字上,这与SAMPE会议论文集之间有很大的重叠。
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引用次数: 5
Improvement of Durability Property by Using Low Diameter Glass Chopped Strands 利用小直径玻璃短切线提高玻璃耐久性能
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/25968
Yosuke Nukui, Shunsuke Harashima, A. Takenaga, T. Mochizuki
The diameter of glass fiber chopped strands used for injection molding is usually from 10μm to 15μm. On the other hand, some reports have stated that the mechanical property is improved by slimming the diameter of the glass fiber chopped strands. By increasing the surface area between the glass fiber and matrix resin, in other words, an increase in the interface to bear the load is the main factor of this improvement. However, their report focused on the short-term load, so the effect on the durability strength has not been reported. This study was made to investigate the effect on the durability property by using low diameter fibers. In addition, we investigated the effect of using high strength and high modulus glass composition fibers on the durability property.
用于注塑成型的玻璃纤维短切线直径一般为10μm ~ 15μm。另一方面,一些报道指出,通过减小玻璃纤维切割股的直径,其机械性能得到改善。通过增加玻璃纤维和基体树脂之间的表面积,换句话说,增加承受载荷的界面是这种改善的主要因素。然而,他们的报告侧重于短期载荷,因此对耐久性强度的影响尚未报道。研究了低直径纤维对复合材料耐久性能的影响。此外,我们还研究了使用高强高模玻璃复合纤维对耐久性能的影响。
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引用次数: 0
Mechanics of Edge-Cracking and Toughness Determination for Strain Locking Composite Materials 应变锁定复合材料边缘开裂力学及韧性测定
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/25950
N. Payne, K. Pochiraju
In this paper, we describe the mechanics of edge cracking and methods for determining the fracture toughness of strain locking materials using homogenized constitutive models for strain locking materials. We implemented a thermodynamically consistent constitutive model for a strain locking material into a plane stress finite element model and determined the energy release rate for a single-edge cracked configuration. Using material parameters suitable for a copper-clad polymer flexible circuit board and for a biological material, we determined the relationship between the strain energy release rate and the crack length for an applied load history using crackadvance methodology. The change of total potential energy (П = - (U-W)) as an edge crack propagates through a prismatic bar loaded in tension is determined. A polynomial is fitted to П where U is the total strain energy stored and W is the work done by the external loads for the purpose of differentiating with respect to the crack length, a. The energy release rate, G, is derived from the slope Π as a function of crack length from these numerical results. Additionally, an additively manufactured strain locking composite material specimen is produced and tensile tested. The results are used to fit the material constants to a previously derived implicit nonlinear elastic model.
在本文中,我们描述了边缘开裂的力学和方法来确定断裂韧性应变锁定材料的均质本构模型的应变锁定材料。我们将应变锁定材料的热力学一致本构模型转化为平面应力有限元模型,并确定了单侧裂纹结构的能量释放率。使用适合于覆铜聚合物柔性电路板和生物材料的材料参数,我们使用裂纹推进方法确定了应用载荷历史中应变能释放率与裂纹长度之间的关系。确定了边缘裂纹在拉伸载荷下通过棱柱杆扩展时总势能(П = - (U-W))的变化。在П中拟合了一个多项式,其中U是存储的总应变能,W是外部载荷所做的功,目的是对裂纹长度A进行微分。能量释放率G是从这些数值结果中作为裂纹长度函数的斜率Π中导出的。另外,制作一种增材制造的应变锁定复合材料试样并进行拉伸试验。结果用于拟合材料常数到先前推导的隐式非线性弹性模型。
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引用次数: 0
MoS2 Dispersed Epoxy Composite: Influence of Solvent Quality and Surface Chemistry to Local Chemical Network Formation and its Influence on Nanoscale Toughening Mechanism 二硫化钼分散环氧复合材料:溶剂质量和表面化学对局部化学网络形成的影响及其对纳米级增韧机理的影响
Pub Date : 2018-11-07 DOI: 10.12783/asc33/26142
J. Ryan, R. Wheeler, G. Kedziora, Andrew Sharits, Samit Roy, J. Moller, I. Sizemore, D. Nepal
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引用次数: 0
Non-Local Damage Modeling for Composite Laminates: Application to Isogeometric Analysis for Impact Simulations 复合材料层合板的非局部损伤建模:在冲击模拟等几何分析中的应用
Pub Date : 2018-11-07 DOI: 10.12783/asc33/26077
M. Pigazzini, D. Kamensky, D. Iersel, J. Remmers, Y. Bazilevs
High-fidelity progressive damage simulations of composite materials are important for advancements in damage tolerant design. We recently proposed a novel modeling approach for damage analysis of composite laminates, in which multi-layer structures are represented as individual plies connected through zero-Thickness cohesive interfaces. The model is developed in the framework of Isogeometric Analysis (IGA). By using Non-Uniform Rational B-Spline (NURBS) basis functions for representing geometries and discretizing the displacement field, IGA allows for a more direct connection between numerical simulation and CAD software. In addition, compared to traditional polynomial basis functions, NURBS functions allow for better representation of geometries and higher order inter-element continuity properties. The computational efficiency of the proposed modeling approach stems from the adoption of Kirchhoff-Love shell elements for the modeling of individual lamina. Intralaminar damage is introduced in the framework of continuum damage mechanics, in which a strain-softening damage model drives the degradation of material elastic properties. However, the use of local strain measures, in combination with strainsoftening degradation models, may lead to damage localization problems. These cause the governing equations to become ill-posed and their approximate solution to be highly mesh-sensitive. Our work aims to re-establish the objectivity with respect to the adopted discretization. We extend our analysis framework by introducing a smoothed strain field to re-place the local strain measures used in the damage model. Our approach builds on the Gradient-Enhanced Damage (GED) model and is specialized for the Kirchhoff-Love shell structural model. The smoothed strain field is obtained by solving an additional set of partial differential equations on each ply of the composite laminate. The GED model can be applied to smooth tensor-valued quantities, such as strains, on generic-shaped geometries in the three-dimensional space, including complex and curved aerospace structures modeled by means of shell elements. In this work, we propose numerical examples in order to illustrate the validity of the GED model.
复合材料的高保真渐进损伤模拟对于提高损伤容限设计具有重要意义。我们最近提出了一种新的复合材料层合板损伤分析建模方法,其中多层结构被表示为通过零厚度内聚界面连接的单个层。该模型是在等几何分析(IGA)框架下开发的。通过使用非均匀有理b样条(NURBS)基函数来表示几何形状和离散位移场,IGA允许数值模拟和CAD软件之间更直接的连接。此外,与传统的多项式基函数相比,NURBS函数可以更好地表示几何形状和更高阶的元素间连续性特性。所提出的建模方法的计算效率源于对单个层的建模采用了Kirchhoff-Love壳单元。在连续损伤力学的框架中引入了层间损伤,其中应变软化损伤模型驱动材料弹性性能的退化。然而,使用局部应变测量,结合应变软化退化模型,可能会导致损伤局部化问题。这导致控制方程变得不适定,其近似解对网格高度敏感。我们的工作旨在重新建立客观性关于采用离散化。我们通过引入平滑应变场来取代损伤模型中使用的局部应变测量来扩展我们的分析框架。我们的方法建立在梯度增强损伤(GED)模型的基础上,专门用于Kirchhoff-Love壳结构模型。通过求解复合材料层合板每一层上的一组偏微分方程,得到了光滑应变场。该模型可以应用于三维空间中一般几何形状的光滑张量,如应变,包括用壳单元建模的复杂和弯曲的航空航天结构。在这项工作中,我们提出了数值例子,以说明GED模型的有效性。
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引用次数: 0
Simulation on Kink-Band Formation Based On X-Ray Computed Tomography Modeling 基于x射线计算机断层成像模型的扭结带形成模拟
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26020
Takuya Takahashi, M. Ueda, K. Iizuka, A. Yoshimura
Kink-band failure is a representative failure mode of a unidirectional carbon fiber reinforced plastics (CFRP) under axial compressive loading. Unidirectional CFRP has initial fiber waviness, and it may trigger kink-band failure. However, initiation of kink-band is not clarified yet. In this paper, three-dimensional finite element model with an actual fiber waviness was constructed by means of X-ray computed tomography (XCT) imaging. Simulation on compression was carried out using the three-dimensional model. A small unidirectional CFRP cylinder was fabricated and scanned the internal fiber structure using an XCT system. The three-dimensional model of the unidirectional CFRP was developed from the XCT images by tracking each fiber positions along the longitudinal direction. Numerical simulation on compression was performed using the constructed three-dimensional finite element model. With increase of compressive loading, matrix deformation was increased locally at some volumes inside the unidirectional CFRP due to fiber random waviness. Matrix started to yield at the volumes, which was considered as an initiation of kink-band formation. The applied compressive load started to decrease after the matrix yielded showing snap-through behavior in the load-displacement relation. The yielded volume of the matrix expanded through the cross-section with rotation of carbon fibers, and kinkband was gradually formed. The numerical simulation revealed initiation and formation of kink-band in a unidirectional CFRP by the random fiber waviness model.
扭结带破坏是单向碳纤维增强塑料(CFRP)在轴向压缩载荷作用下的典型破坏模式。单向碳纤维布具有初始纤维波纹,可能引发扭结带破坏。然而,扭结带的起始机制尚不清楚。本文采用x射线计算机断层扫描(XCT)技术,建立了具有实际纤维波纹度的三维有限元模型。利用三维模型对压缩过程进行了仿真。制作了一个单向CFRP小圆柱体,并利用XCT系统对其内部纤维结构进行了扫描。利用XCT图像,沿纵向跟踪各纤维的位置,建立单向CFRP的三维模型。利用所建立的三维有限元模型对压缩过程进行了数值模拟。随着压缩载荷的增加,单向碳纤维布内部部分体积的基体变形由于纤维的无规波纹而局部增大。在体积处,基体开始屈服,这被认为是扭结带形成的开始。施加的压缩载荷在基体屈服后开始减小,在荷载-位移关系中表现出卡断行为。随着碳纤维的旋转,基体的屈服体积通过截面扩大,并逐渐形成扭结带。采用随机纤维波纹模型对单向碳纤维复合材料的扭结带的产生和形成进行了数值模拟。
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引用次数: 0
Dispersion and Properties of Graphene Oxide and Reduced Graphene Oxide in Nanocomposites 氧化石墨烯和还原氧化石墨烯在纳米复合材料中的分散与性能
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26082
Melanie Schneider, Pouria Khanbolouki, Nekoda van de Werken, Elijah Wade, R. Foudazi, M. Tehrani
Reducing graphene oxide (GO) is currently seen as one of the most cost effective and scalable methods to produce graphene sheets. This method takes exfoliated graphite in the form of graphene oxide (GO) and reduces it to reduced graphene oxide (rGO). This reduction process recovers the mechanical, thermal, and electrical properties of GO,1 making it more appealing for many applications including fillers in polymers. However, the reduction of oxygen functional groups tends to lead to lower dispersion quality and activity of rGO in polymers. This remains an issue as researchers search to produce graphene based nanocomposites for different applications. This study characterizes the thermal and mechanical properties of graphene oxide and reduced graphene oxide epoxy nanocomposites to determine the overall performance in relation to dispersion quality and nanoparticle loading. For this purpose, epoxy nanocomposites of GO (C:O ratio 1:1) and rGO (C:O ratio 5:1) with various loadings (0.5, 1.0, and 2.0 wt.%) and dispersion qualities (3 different combinations of shear mixing and horn sonication) were fabricated and characterized. Transmission optical microscopy (TOM) and scanning electron microscopy (SEM) were used to qualitatively asses the level of dispersion for each dispersion technique. Flash diffusivity analysis and differential scanning calorimetry (DSC) were employed to measure the thermal diffusivity and specific heat capacity, respectively, for each sample, from which the thermal conductivity was calculated. The thermal conductivity was then correlated to the level of dispersion and filler (GO or rGO) for the composites. Nanoindentation was utilized to assess the mechanical properties of the nanocomposites with respect to dispersion, loading, and filler type.
还原氧化石墨烯(GO)目前被认为是生产石墨烯片的最具成本效益和可扩展性的方法之一。该方法采用氧化石墨烯(GO)形式的剥落石墨,并将其还原为还原氧化石墨烯(rGO)。这种还原过程恢复了氧化石墨烯的机械、热学和电学性能,使其在包括聚合物填料在内的许多应用中更具吸引力。然而,氧官能团的减少往往会导致还原氧化石墨烯在聚合物中的分散质量和活性降低。这仍然是一个问题,因为研究人员正在为不同的应用寻找基于石墨烯的纳米复合材料。本研究表征了氧化石墨烯和还原氧化石墨烯环氧纳米复合材料的热性能和力学性能,以确定与分散质量和纳米颗粒负载相关的整体性能。为此,制备了不同负载(0.5、1.0和2.0 wt.%)和分散质量(剪切混合和喇叭超声的3种不同组合)的氧化石墨烯(C:O比1:1)和还原氧化石墨烯(C:O比5:1)的环氧纳米复合材料并对其进行了表征。利用透射光学显微镜(TOM)和扫描电子显微镜(SEM)对每种色散技术的色散水平进行定性评估。采用闪蒸扩散率分析和差示扫描量热法(DSC)分别测量每个样品的热扩散率和比热容,并以此计算导热系数。然后,导热系数与复合材料的分散和填料(GO或rGO)的水平相关。利用纳米压痕来评估纳米复合材料在分散、负载和填料类型方面的力学性能。
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引用次数: 0
NASA’s 2040 Vision Roadmap Study: A Framework for Integrated Computational Materials Engineering (ICME) NASA 2040年愿景路线图研究:综合计算材料工程(ICME)框架
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/25911
S. Arnold
Over the last few decades, advances in high-performance computing, new materials characterization methods, and, more recently, an emphasis on integrated computational materials engineering (ICME) and additive manufacturing have been a catalyst for multiscale modeling and simulation-based design of materials and structures in the aerospace industry. While these advances have driven significant progress in the development of aerospace components and systems, that progress has been limited by persistent technology and infrastructure challenges that must be overcome to realize the full potential of integrated materials and systems design and simulation modeling throughout the supply chain. As a result, NASA’s Transformational Tools and Technology (TTT) Project sponsored an industry led study to define the potential 25-year future state required for integrated multiscale modeling of materials and systems (e.g., load-bearing structures) to accelerate the pace and reduce the expense of innovation in future aerospace and aeronautical systems. Herein the overall findings of this 2040 Vision study will be briefly reviewed, with an emphasis toward those applicable to ICME of composites. These findings for example include the 2040 vision state; the required interdependent core technical work areas defined as Key Elements (KE); associated critical gaps and actions to close those gaps; and major recommendations.
在过去的几十年里,高性能计算、新材料表征方法的进步,以及最近对集成计算材料工程(ICME)和增材制造的重视,已经成为航空航天工业中基于多尺度建模和仿真的材料和结构设计的催化剂。虽然这些进步推动了航空航天部件和系统的发展取得了重大进展,但这种进展受到持续存在的技术和基础设施挑战的限制,这些挑战必须克服,才能在整个供应链中实现集成材料和系统设计以及仿真建模的全部潜力。因此,NASA的转型工具和技术(TTT)项目赞助了一项行业主导的研究,以确定材料和系统(例如承重结构)集成多尺度建模所需的潜在25年未来状态,以加快未来航空航天系统的创新步伐并减少成本。本文将简要回顾2040 Vision研究的总体结果,重点是适用于复合材料的ICME。例如,这些发现包括2040年愿景状态;定义为关键要素的所需相互依赖的核心技术工作领域;相关的关键差距和消除这些差距的行动;以及主要的建议。
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引用次数: 0
期刊
American Society for Composites 2018
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