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Time and Temperature Dependent Stress-Strain Behavior of Unidirectional Carbon Fiber/Polyimide Composites Under On-axis and Off-axis Tensile Loading 单向碳纤维/聚酰亚胺复合材料在轴向和离轴拉伸载荷下的应力-应变行为
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/25961
Ryuunosuke Minegishi, T. Ogasawara, T. Aoki, Y. Kubota, Y. Ishida
Phenylethynyl terminated polyimide “TriA-X” developed in Japan Aerospace Exploration Agency (JAXA) exhibits excellent mechanical properties with high glass transition temperature (> 350 °C), therefore it is suitable as matrix resin of high temperature composites. However, the time and temperature dependent mechanical properties have not been investigated. This study examined the mechanical behavior of unidirectional (UD) carbon fiber (CF)/ TriA-X polyimide composites by off-axis monotonic tensile tests and off-axis tensile creep tests. As results, it was revealed that one parameter plasticity model by Sun and Chen was effective to represent the nonlinear stress-strain behavior of UD-CF/ TriA-X composites. Furthermore, linear viscoelastic behavior was observed from the off-axis tensile creep tests of UD-CF/ TriA-X composites. On the other hand, residual strain was observed in creep recovery curves after unloading, which suggested that the creep and creep recovery behaviors of UDCF/ TriA-X composites are not affected only by viscoelastic and plastic deformation, but also by viscoplastic deformation.
日本宇宙航空研究开发机构(JAXA)开发的苯基乙基端部聚酰亚胺“TriA-X”具有优异的机械性能,具有较高的玻璃化转变温度(> 350℃),因此适合作为高温复合材料的基体树脂。然而,对其随时间和温度变化的力学性能尚未进行研究。本研究通过离轴单调拉伸试验和离轴拉伸蠕变试验研究了单向(UD)碳纤维/ TriA-X聚酰亚胺复合材料的力学行为。结果表明,Sun和Chen的单参数塑性模型可以有效地表征UD-CF/ TriA-X复合材料的非线性应力-应变行为。此外,从UD-CF/ TriA-X复合材料的离轴拉伸蠕变试验中观察到线性粘弹性行为。另一方面,在卸载后的蠕变恢复曲线中观察到残余应变,表明UDCF/ TriA-X复合材料的蠕变和蠕变恢复行为不仅受到粘弹和塑性变形的影响,还受到粘塑性变形的影响。
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引用次数: 0
Fabrication of Cellulose Nanofiber/Glass Fiber-reinforced Composites and Their Bending Behavior Evaluation 纤维素纳米纤维/玻璃纤维增强复合材料的制备及其弯曲性能评价
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26061
Y. Xie, H. Kurita, Risa Honda, K. Katabira, F. Narita
It is required a joint technic with excellent mechanical properties to fabricate glass fiber reinforced plastic (GFRP) components. However, it is well-known that the mechanical jointing often causes the fracture of fiber reinforced plastics. It seems that the adhesive bonding is suitable to joint GFRPs, and it is necessary to develop an adhesive with outstanding mechanical properties. Recently, cellulose nanofibers (CNFs) have been obtained from plants by mechanical and chemical methods and it has been reported that CNFs have remarkable mechanical properties. In this study, we inserted epoxy resin with CNFs between GFRP and investigated its bending behavior, to estimate the capability of epoxy resin with CNFs as an adhesive for GFRPs. The flexural behavior and modulus of GFRP was similar regardless of the inserted part of epoxy resin with CNFs layer in GFRP. The flexural strength of GFRP was drastically increased (up to 600 MPa) by the insert of epoxy resin with CNFs of 5 or 10 wt.%, although that of GFRP was decreased by the insert of epoxy resin with CNFs of 25 wt.%. Therefore, it seems that the epoxy resin with CNFs is available as an adhesive for GFRP. However, it is required the observation of CNFs dispersion in epoxy resin to understand the strengthening mechanism of epoxy resin with CNFs.
玻璃纤维增强塑料(GFRP)构件的制造需要一种具有优异力学性能的连接技术。然而,众所周知,机械连接往往会导致纤维增强塑料的断裂。认为胶粘剂粘接适用于接缝gfrp,有必要开发一种具有优异力学性能的胶粘剂。近年来,人们通过机械和化学方法从植物中制备了纤维素纳米纤维,并报道了纤维素纳米纤维具有优异的力学性能。在这项研究中,我们将环氧树脂与CNFs插入GFRP之间,并研究其弯曲行为,以评估环氧树脂与CNFs作为GFRP的粘合剂的能力。在GFRP中加入CNFs层的环氧树脂后,GFRP的抗弯性能和模量基本相同。GFRP的抗弯强度在添加5%或10% CNFs的环氧树脂后得到显著提高(可达600 MPa),而添加25% CNFs的环氧树脂会降低GFRP的抗弯强度。因此,CNFs环氧树脂作为GFRP的粘结剂是可行的。但要了解CNFs对环氧树脂的强化机理,还需要观察CNFs在环氧树脂中的分散情况。
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引用次数: 0
Experimental Investigation Into the Failure of CFRP T-joints Under Ice Impact and Quasi-static Loadings 冰冲击和准静态荷载作用下CFRP t形接头破坏试验研究
Pub Date : 2018-11-07 DOI: 10.12783/asc33/26154
Huawen Zhang, Huifang Liu, Zhenqiang Zhao, Yulong Li, Chao Zhang
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引用次数: 1
Coupled Thermo-mechanical Micromechanics Modeling of the Influence of Thermally Grown Oxide Layer in an Environmental Barrier Coating System 环境屏障涂层中热生长氧化层影响的热-机耦合细观力学建模
Pub Date : 2018-11-07 DOI: 10.12783/asc33/26027
T. Ricks, S. Arnold, B. Harder
Environmental Barrier Coatings (EBCs) have emerged as a promising means of protecting silicon based ceramic matrix composite (CMC) components for high temperature applications (e.g., aircraft engines). EBCs are often used to protect an underlying material (substrate) such as silicon carbide from extreme thermal/chemical environments. In a typical CMC/EBC system, an EBC may or may not be adhered to an underlying substrate with a bond coat (e.g., silicon). Irrespective, systems that utilize EBCs are susceptible to a number of failure modes including oxidation/delamination, recession, chemical attack and dissolution, thermomechanical degradation, erosion, and foreign object damage. Current work at NASA Glenn Research Center is aimed at addressing these failure modes in EBC systems and developing robust analysis tools to aid in the design process. The Higher-Order Theory for Functionally Graded Materials (HOTFGM), a precursor to the High- Fidelity Generalized Method of Cells micromechanics approach, was developed to investigate the coupled thermo-mechanical behavior of functionally graded composites and will be used herein to assess the development and growth of a lowstiffness thermally grown oxide (TGO) layer in EBC/CMC systems without a silicon bond coat. To accomplish this a sensitivity study is conducted to examine the influence of uniformly and nonuniformly grown oxide layer on the associated driving forces leading to mechanical failure (spallation) of EBC layer when subjected to isothermal loading.
环境屏障涂层(EBCs)已成为保护高温应用(例如飞机发动机)中硅基陶瓷基复合材料(CMC)组件的一种有前途的手段。EBCs通常用于保护底层材料(衬底),如碳化硅,免受极端热/化学环境的影响。在典型的CMC/EBC系统中,EBC可以或可以不粘附在具有粘结涂层(例如硅)的底层衬底上。尽管如此,使用ebc的系统容易受到多种失效模式的影响,包括氧化/分层、衰退、化学侵蚀和溶解、热机械降解、侵蚀和异物损坏。NASA格伦研究中心目前的工作旨在解决EBC系统中的这些失效模式,并开发强大的分析工具来帮助设计过程。功能梯度材料的高阶理论(HOTFGM)是高保真细胞微力学方法的先驱,用于研究功能梯度复合材料的耦合热-力学行为,并将在本文中用于评估EBC/CMC系统中无硅键涂层的低刚度热生长氧化物(TGO)层的发育和生长。为了实现这一目标,进行了一项敏感性研究,以检验均匀和非均匀生长的氧化层对等温加载时导致EBC层机械失效(剥落)的相关驱动力的影响。
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引用次数: 1
Deployable Structures Constructed from Composite Origami 由复合折纸构造的可展开结构
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/25907
James O’Neil, A. A. Deleo, H. Yasuda, M. Salviato, Jinkyu Yang
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引用次数: 5
Finite Element Based Buckling Cross-Sectional Optimization for Composite Arrows 基于有限元的复合材料箭头屈曲截面优化
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26163
A. Srinivas, D. Dancila
In archery, dynamic buckling during the launch phase compromises the target accuracy of arrows. For both dynamic and quasi-static arrow buckling, the critical load depends upon the area moment of inertia of the cross-section which should be increased at constant arrow weight, by redistributing the material as far away from the principal point of the cross-section as possible, and while keeping the material thick enough to prevent local buckling. In this paper we present an effort to optimize the cross-sectional shape of a composite arrow shaft, using a finite element based, quasi static buckling analysis keeping the length and area of the cross-section constant. The composite column considered is assumed pinned at both ends and is assumed made with fibers oriented along the length of the column. Four cross-sectional shapes, tubular circular, tubular equilateral triangular, star shaped and star with beads are analyzed in this study. The composite column is modeled in ABAQUS, and the buckling load is determined by using the “Linear Perturbation, Buckle” analysis. The transition from global to local buckling characterized by a decrease in bucking load and change in the buckled shape of the column is determined for each cross-sectional shape. The point of transition marks the maximum load that can be sustained for that cross-sectional shape. The maximum load for all the cross-sections is determined and compared. The tubular circular cross-section composite column is found to provide the highest buckling load followed by the star with bead cross-section, star shaped cross-section and tubular equilateral triangular cross-section composite column in the respective order. Thus, of the shapes considered, the tubular circular cross-section is the optimum shape for the cross-section of the arrow shaft.
在射箭运动中,箭在发射阶段的动态屈曲会影响箭的瞄准精度。对于动态和准静态箭头屈曲,临界载荷取决于截面的面积惯性矩,在箭头重量不变的情况下,应通过将材料重新分配到尽可能远离截面主点的地方,同时保持材料足够厚以防止局部屈曲来增加截面的惯性矩。本文采用基于有限元的准静态屈曲分析方法,在保持截面长度和面积不变的情况下,对复合材料箭头轴的截面形状进行了优化设计。假定所考虑的复合柱在两端固定,并假定纤维沿柱的长度取向。本文分析了管状圆形、管状等边三角形、星形和星形带珠四种截面形状。在ABAQUS中对复合柱进行建模,采用“线性摄动,屈曲”分析确定了复合柱的屈曲载荷。确定了从整体屈曲到局部屈曲的过渡,其特征是屈曲载荷的减少和柱的屈曲形状的变化。过渡点标志着该截面形状所能承受的最大载荷。确定并比较所有截面的最大荷载。管状圆截面复合柱的屈曲载荷最大,其次是星形头截面、星形截面和管状等边三角形截面复合柱。因此,在考虑的形状中,管状圆形截面是箭头轴截面的最佳形状。
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引用次数: 0
In-situ Damage Precursor Detection in Fiber Reinforced Composites Using Mechanochemical Materials 基于力学化学材料的纤维增强复合材料损伤前兆原位检测
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26140
B. Koo, Jack Miller, Ryan Gunckel, A. Chattopadhyay, Lenore L. Dai
Optical responses of mechanophore (stress-responsive materials) in fiber reinforced polymer composites under mechanical loads were characterized. A new experimental system was developed to capture in situ mechanophore activation by recording ultraviolet (UV) excited fluorescence during uniaxial load tests. Anthracene- based mechanophore, dimeric 9-anthracene carboxylic acid (Di-AC) was synthesized and incorporated into an epoxy-based thermoset successfully. This Di-AC embedded epoxy mixture was applied to glass fiber fabric to fabricate mechanophore embedded glass fiber reinforced polymer (GFRP) composites through hand-layup process. Quasistatic and cyclic loads were performed to investigate the effect of different types of loads on mechanophore activation. The results indicated that mechanophore activation occurred at the beginning of the test during the quasistatic loading test and continued linearly before yield. Microcracks were formed in the matrix prior to yield, and UV intensity of the mechanophore exhibited nonlinear response. During fatigue tests, the intensity of fluorescence increased after a certain number of cycles. Microcracks were initiated around the middle stage of the fatigue test, the intensity also showed a nonlinear response. The potential of anthracene-based mechanophore for early damage detection in GFRP under complex loading was observed.
研究了应力响应材料在机械载荷作用下的光响应特性。开发了一种新的实验系统,通过记录单轴负载测试中紫外线激发的荧光来捕捉机械团的原位激活。合成了蒽基机械基团二聚体9-蒽羧酸(Di-AC),并成功地将其掺入环氧基热固性材料中。将该Di-AC包埋环氧树脂混合物应用于玻璃纤维织物中,通过手工铺层法制备机械团包埋玻璃纤维增强聚合物(GFRP)复合材料。采用准静态和循环载荷研究了不同类型载荷对机械团活化的影响。结果表明,机械团激活发生在准静态加载试验开始时,并在屈服前呈线性持续。微裂纹在屈服前在基体中形成,机械团的UV强度表现出非线性响应。在疲劳试验中,经过一定循环次数后,荧光强度增加。疲劳试验中期前后出现微裂纹,强度也呈现非线性响应。观察了蒽基力学团在复合荷载作用下对玻璃钢早期损伤检测的潜力。
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引用次数: 0
An Efficient Multiscale Virtual Testing Platform for Composite Via Component-wise Models 基于组件模型的高效复合材料多尺度虚拟测试平台
Pub Date : 2018-11-07 DOI: 10.12783/asc33/25959
I. Kaleel, M. Nagaraj, M. Petrolo, E. Carrera, A. Waas
The aim of the current work is to develop a multiscale framework based on higherorder 1D finite elements developed using the Carrera Unified Formulation (CUF). The multiscale framework consists of a macroscale model to describe the global structure, and a CUF micromechanical model described using the Component-Wise approach. Such an approach allows for the explicit modelling of the fiber and matrix at the microscale, resulting in a high-fidelity finite element model at both scales. The use of refined CUF elements result in a computationally efficient analysis, due to a reduction in the degrees of freedom at both scales, as well as the reduction in total computational time when compared to standard 3D finite element analysis. The parallel implementation of the multiscale framework results in additional savings in computational time.
当前工作的目的是开发一个基于使用Carrera统一公式(CUF)开发的高阶一维有限元的多尺度框架。多尺度框架由描述全局结构的宏观模型和使用组件智能方法描述的CUF微观力学模型组成。这种方法允许在微观尺度上对纤维和基体进行明确的建模,从而在两个尺度上产生高保真的有限元模型。与标准3D有限元分析相比,由于降低了两个尺度的自由度,以及减少了总计算时间,因此使用精炼的CUF单元可以实现计算效率高的分析。多尺度框架的并行实现可以节省额外的计算时间。
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引用次数: 1
A Dielectric Resonant Cavity Method for Monitoring of Damage Progression in Moisture-Contaminated Composites 一种监测湿污染复合材料损伤进展的介电谐振腔方法
Pub Date : 2018-11-07 DOI: 10.12783/asc33/25963
O. Idolor, Rishabh D Guha, L. Grace
A method for monitoring of damage progression due to combined mechanical and hygroscopic loading in polymer composite materials is presented. Polymer-based materials have a tendency to absorb moisture from their operating environment. Dielectric properties of these materials are significantly affected by the total amount of absorbed moisture and the degree of its interaction with the host polymer. Bound water molecules which are restricted in their ability to rotate with an applied electromagnetic field contribute less to the bulk relative permittivity. 'Free' water molecules rotate without impediment and are therefore associated with a higher relative permittivity. The bulk relative permittivity as a function of total water content of a contaminated composite is a unique function of the internal physical and chemical characteristics of the specimen. Holding chemical contributions constant, physical characteristics dominate. Thus, relative permittivity provides insight into the physical state of composite, including amount of free space from processing-induced voids or, critically, the presence of physical damage such as cracks and voids across multiple length scales. Here, we demonstrate a method for leveraging this phenomenon to provide insight into the initiation and accumulation of physical damage in moisturecontaminated composites. This is accomplished using a split-post dielectric resonant technique operating in the low GHz frequency range, where dipolar contributions to relative permittivity dominate. Further, continuous and non-contact monitoring of relative permittivity is achieved by integrating a resonant cavity with a fatigue loading frame. Preliminary experimental assessment of this test method is supportive of its potential in damage tracking. Water-contaminated 12-ply bismaleimide (BMI) / quartz laminate specimens were tested in impact and flexural fatigue, while a 4-ply glass/epoxy laminate was tested in tensile fatigue while changes in relative permittivity were recorded. The results show a distinct rise in relative permittivity consistent with the expected magnitude and progression of damage in all cases.
提出了一种监测高分子复合材料在机械和吸湿双重载荷作用下损伤进展的方法。聚合物基材料有从其操作环境中吸收水分的倾向。这些材料的介电性能受到吸收水分总量及其与基体聚合物相互作用程度的显著影响。受外加电磁场旋转能力限制的结合水分子对体相对介电常数的贡献较小。“自由”水分子旋转时没有阻碍,因此具有较高的相对介电常数。体积相对介电常数作为受污染复合材料总含水量的函数是试样内部物理和化学特性的独特函数。保持化学贡献不变,物理特性占主导地位。因此,相对介电常数可以深入了解复合材料的物理状态,包括加工引起的空隙的自由空间量,或者更重要的是,在多个长度尺度上存在物理损伤,如裂缝和空隙。在这里,我们展示了一种利用这种现象的方法,以深入了解湿污染复合材料中物理损伤的开始和积累。这是通过在低GHz频率范围内工作的分柱介电谐振技术实现的,在该频率范围内,偶极子对相对介电常数的贡献占主导地位。此外,通过将谐振腔与疲劳加载框架集成,实现了相对介电常数的连续和非接触监测。对该测试方法的初步实验评估支持了其在损伤跟踪方面的潜力。对受水污染的12层双马来酰亚胺(BMI) /石英层压板试样进行了冲击和弯曲疲劳测试,对4层玻璃/环氧层压板试样进行了拉伸疲劳测试,并记录了相对介电常数的变化。结果表明,在所有情况下,相对介电常数明显上升,与预期的损伤幅度和进展一致。
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引用次数: 8
Defects Characterization, Damage Mapping, and Property Evaluation of Composites 复合材料的缺陷表征、损伤映射和性能评估
Pub Date : 2018-11-07 DOI: 10.12783/ASC33/26144
J. Lua, A. Sadeghirad, Xiaodong Cui, A. Karuppiah, C. Saathoff, W. Seneviratne
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引用次数: 1
期刊
American Society for Composites 2018
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