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Arc plasma ablation of quartz crystals 电弧等离子体烧蚀石英晶体
Q3 ORTHOPEDICS Pub Date : 2021-03-03 DOI: 10.1088/2516-1067/abf911
C. Corbella, S. Portal, M. Keidar
Spherical quartz stones of around 1 cm in diameter have been exposed to anodic arc discharges in a helium atmosphere at 300 Torr. The arc current flowing between the graphite electrodes was set either in continuous DC mode (30–150 A) or in pulsed mode at 2 Hz (220 A peak). The ablation rate in each sample was systematically measured after several seconds of arc plasma treatment. Optical emission spectroscopy (OES) diagnostics and 2D fluid simulations of the arc discharge have shed light on the heat flux transport and the heating mechanisms of the quartz crystals. A linear correlation is found between the absorbed power density and the resulting rate of penetration, which yields a maximal value of 15 cm h−1 for approximately 150 W cm−2. The linear fit on the slope provides a specific energy of 40 kJ cm−3. The incident energy flux onto the sample surface promoted a phase transition from crystalline to glassy silica, as characterized via Raman spectroscopy. This study points out the strong potential of arc plasma technology for geothermal drilling applications.
直径约1cm的球形石英石已在300托的氦气气氛中暴露于阳极电弧放电。石墨电极之间流动的电弧电流设置为连续直流模式(30–150 A)或2 Hz的脉冲模式(峰值220 A)。在电弧等离子体处理几秒钟后,系统地测量每个样品中的消融速率。电弧放电的光学发射光谱(OES)诊断和2D流体模拟揭示了石英晶体的热通量传输和加热机制。在吸收的功率密度和由此产生的穿透率之间存在线性相关性,对于大约150 W cm−2,穿透率的最大值为15 cm h−1。斜坡上的线性拟合提供了40 kJ cm−3的比能量。入射到样品表面的能量通量促进了从晶体二氧化硅到玻璃态二氧化硅的相变,如通过拉曼光谱所表征的。该研究指出了电弧等离子体技术在地热钻探应用中的强大潜力。
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引用次数: 1
Polydisperse inter-electrode plasma of Pd nanoclusters as a random cavity for x-ray spontaneous emission bursts Pd纳米团簇的多分散电极间等离子体作为x射线自发发射暴的随机腔
Q3 ORTHOPEDICS Pub Date : 2021-03-01 DOI: 10.1088/2516-1067/abe293
I. Smetanin, Y. Kurilenkov, A. Oginov, V. Tarakanov, I. Samoylov
It is demonstrated experimentally that polydisperse Pd plasma of low energy (∼1 J) nanosecond vacuum discharge operating in a virtual cathode regime becomes an effective stochastic cavity in hard x-ray domain. A diffusion model of stochastic propagation of spontaneous x-ray radiation in the volume of randomly located reflecting clusters is developed also. The model provides qualitative explanation of both the experimentally observed effects of high-intensity bursts and partial ‘trapping’ of x-ray radiation. The x-ray burst emerges when photons are stored inside the plasma volume followed by instant release at the end of the discharge while the trapping regime corresponds to the slow developing x-ray diffusion with the characteristic time larger than the discharge duration. The results obtained are compared qualitatively with well-known concept of Letokhov’s random laser.
实验证明,在虚拟阴极区工作的低能(~1J)纳秒真空放电的多分散Pd等离子体在硬x射线域中成为一个有效的随机腔。还建立了自发x射线辐射在随机反射团簇中随机传播的扩散模型。该模型对实验观察到的高强度爆发和x射线辐射的部分“捕获”效应提供了定性解释。当光子被存储在等离子体体积内,然后在放电结束时立即释放时,x射线爆发出现,而捕获状态对应于缓慢发展的x射线扩散,其特征时间大于放电持续时间。将所得结果与众所周知的Letokhov随机激光概念进行了定性比较。
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引用次数: 2
Effects of pulse rise time and repetition frequency on nanosecond pulsed plasma ignition for combustion 脉冲上升时间和重复频率对纳秒脉冲等离子体点火燃烧的影响
Q3 ORTHOPEDICS Pub Date : 2021-03-01 DOI: 10.1088/2516-1067/ab880a
David Alderman, Christopher Tremble, D. Singleton, J. Sanders, C. Jiang
Transient plasma ignition (TPI) employs highly non-equilibrium plasmas driven by nanosecond high-voltage pulses for combustion ignition. The effects of rise time and pulse repetition frequency (PRF) on combustion ignition are evaluated when transient plasmas, powered by 10-ns, kilovolt pulses, are employed to initiate combustion of lean, stoichiometric, or rich methane-dry air mixtures at atmospheric pressure. It was found that the plasmas driven by high voltage pulses with a faster rise time and PRF between 6–10 kHz enhanced combustion with higher peak pressure and/or shorter ignition delay. A mode transition in the plasma, corresponding to the combustion initiation, was observed based on voltage and current waveforms of four consecutive pulsed plasmas driven by a pulse burst at kilohertz PRFs. Although benefits in combustion ignition from a shorter rise time and optimal PRF were observed for all three equivalence mixture ratios, the highest peak pressure and shortest ignition delay were associated with the stoichiometric mixtures. In addition, the gas temperature of the transient plasma was measured by determining the rotational temperature of the 2nd positive system of nitrogen to be ∼1000 K for the first pulse and increased up to 2000 K after the application of the 4th pulse in a four-pulse burst TPI.
瞬态等离子体点火技术是利用纳秒级高压脉冲驱动高度非平衡等离子体进行燃烧点火。当瞬态等离子体在大气压下由10ns,千伏脉冲驱动,启动稀薄、化学计量或富含甲烷-干空气混合物的燃烧时,评估了上升时间和脉冲重复频率(PRF)对燃烧着火的影响。结果表明,在上升时间较快、PRF在6 ~ 10 kHz之间的高压脉冲驱动等离子体时,燃烧峰值压力增大,点火延迟缩短。基于脉冲脉冲爆发驱动的四个连续脉冲等离子体的电压和电流波形,观察到等离子体中的模式转变,对应于燃烧的开始。虽然在所有三种等效混合比例下,较短的上升时间和最佳的PRF都有利于燃烧点火,但最高的峰值压力和最短的点火延迟与化学计量混合物有关。此外,瞬态等离子体的气体温度通过测定第一个脉冲时氮的第二个正极系统的旋转温度为~ 1000 K,在四脉冲爆发TPI中应用第四个脉冲后增加到2000 K来测量。
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引用次数: 7
Studies and optimization of hybrid X-pinches 混合X形夹的研究与优化
Q3 ORTHOPEDICS Pub Date : 2021-02-17 DOI: 10.1088/2516-1067/abe71e
A. Elshafiey, J. Musk, S. Pikuz, T. Shelkovenko, D. Hammer
Studies were carried out on the hybrid X-pinch (HXP) configuration for several wire materials using a 40 ns risetime, 300-kA pulsed-power generator with the goal of optimizing the HXP x-ray burst parameters for different applications. The gap distance between the conical electrodes of the hybrid X-pinch was varied from 0.5 to 5 mm for Al, Ag, Ti, and Mo using different wire diameters to maintain a consistent mass per unit length from one material to the next. It was found that 0.5–1 mm gap spacing was optimal to obtain a single x-ray burst, while the number of x-ray bursts increased with gap spacing for all materials at a rate of 1–2/mm. Time consistency studies of the first x-ray burst were carried out for Ti wire by changing the gap distance and wire diameter while observing the time of occurrence of the x-ray bursts. It was found that a 40 μm Ti wire load with a 3 mm electrode gap spacing had the highest probability to have the first x-ray burst reproducibly within a 2 ns time window. Time-resolved and time-integrated diagnostics provided information about the source size, time of occurrence, intensity, and the number of the x-ray bursts.
使用40ns上升时间、300kA脉冲发生器对几种线材的混合X夹点(HXP)配置进行了研究,目的是优化不同应用的HXP X射线爆发参数。对于Al、Ag、Ti和Mo,混合X箍缩的锥形电极之间的间隙距离在0.5到5mm之间变化,使用不同的线直径来保持从一种材料到下一种材料的单位长度的一致质量。研究发现,0.5–1 mm的间隙间距对于获得单个x射线爆发是最佳的,而对于所有材料,x射线爆发的数量随着间隙间距的增加而以1–2/mm的速率增加。通过改变间隙距离和金属丝直径,同时观察x射线爆发的发生时间,对钛丝的第一次x射线爆发进行了时间一致性研究。研究发现,电极间隙间距为3mm的40μm钛丝负载在2ns时间窗口内再现第一次x射线爆发的概率最高。时间分辨和时间集成诊断提供了有关源大小、发生时间、强度和x射线爆发次数的信息。
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引用次数: 1
Arbitrary amplitude ion acoustic double layer in plasma with k-distributed electrons and negative ions 具有k分布电子和负离子的等离子体中任意振幅离子声双层
Q3 ORTHOPEDICS Pub Date : 2021-01-21 DOI: 10.1088/2516-1067/abd958
K. Kumar, M. K. Mishra
In this paper we have discussed the consequence of superthermal electrons and negative ion concentration on the arbitrary amplitude ion-acoustic double layers (IA-DLs) for plasma comprising the hot negative and positive ions with kappa distribution electrons. The energy equation is deduced for ion acoustic waves using Pseudo potential technique. We have investigated different parametric regimes for the existence of rarefactive and compressive ion acoustic DLs. The existence of double layers in term of minimum and maximum Mach number has calculated numerically. The effect of spectral index k on the amplitude of DLs and depth of Sagdeev potential has been discussed in detail. From numerical analysis, it is found that the compressive DLs exist at low values of α and rarefactive double layer exist at higher values of α. On the other hand, the effect of ionic temperature ratio (σ 1 and σ 2) plays significant role for the formation of double layer. Our analytical work also shows that the system supports coexistence of compressive and rarefactive DLs. It is also observed that the mass ratio μ affect the basic properties of DLs. We expect that the present results may be used to explain the ion-acoustic double layer in space plasma, where two ionic species and superthermal electrons are observed NO52.35g.
本文讨论了过热电子和负离子浓度对具有kappa分布电子的热负离子和正离子组成的等离子体任意振幅离子声双层(ia - dl)的影响。利用伪势技术推导了离子声波的能量方程。我们研究了不同的参数制度,为存在的稀薄和压缩离子声dl。从最小马赫数和最大马赫数两方面计算了双层的存在性。详细讨论了谱指数k对Sagdeev电位振幅和深度的影响。数值分析发现,低α值下存在压缩双相层,高α值下存在稀薄双相层。另一方面,离子温度比(σ 1和σ 2)对双层的形成起着重要的作用。我们的分析工作还表明,该系统支持压缩和屈光光共存。质量比μ对DLs的基本性质也有影响。我们期望本结果可以用来解释空间等离子体中离子-声双层,其中两个离子种和超热电子被观察到NO52.35g。
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引用次数: 2
On the frequency spectra of the electrostatic upper hybrid wave and linear Landau damping in a weakly magnetized relativistic electron plasma 弱磁化相对论性电子等离子体中静电上杂波和线性朗道阻尼的频谱
Q3 ORTHOPEDICS Pub Date : 2021-01-20 DOI: 10.1088/2516-1067/abd530
S. Noureen, G. Abbas, M. Sarfraz, L. James
On the basis of Vlasov-Kinetic model and using Maxwell-Juttner distribution function, dispersion relation of electrostatic wave in a collisionless homogeneous relativistic electron plasma is derived. The analysis of the oscillation spectra is carried out in a weak magnetic field limit ω−kvth ≥ Ω. Approximate analytic expression for the weakly damped mode is obtained in the subluminal limiting range. It is shown that the relativistic weakly damped mode can be estimated analytically in the range where the wave phase velocity v φ becomes greater than relativistic thermal velocity of the electron but less than speed of light. Results in the non-relativistic and the ultrarelativistic cases are also discussed.
在vlasov -动力学模型的基础上,利用Maxwell-Juttner分布函数,推导了无碰撞均匀相对论电子等离子体中静电波的色散关系。振荡谱分析是在弱磁场极限ω−kvth≥Ω下进行的。得到了弱阻尼模态在亚光速极限范围内的近似解析表达式。结果表明,在波相速度v φ大于电子的相对论热速度但小于光速的范围内,可以解析地估计出相对论弱阻尼模式。讨论了非相对论性和超相对论性情况下的结果。
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引用次数: 1
Comment on ‘Mapping the electric field vector of guided ionization waves at atmospheric pressure’, (2020) Plasma Res. Express 2 025014 关于“大气压力下引导电离波的电场矢量映射”的评论,(2020),等离子体学报,2:25014
Q3 ORTHOPEDICS Pub Date : 2021-01-01 DOI: 10.1088/2516-1067/ac18b9
S. Dozias, J. Pouvesle, É. Robert
Recently, Iséni reported measurements and analysis of electric field (EF) strengths adjacent to, and in propagating ionization waves (IWs) for non-thermal atmospheric pressure He plasma jets [1]. This paper [1] is almost the full copy of the 2017 ArXiv :1709.03109v1 [2] for which the authors already published a comment [3]. In this comment, we confirm first that the reported results are wrong due to an improperly aligned electric field probe, and second, that even these wrong measurements are themselves inconsistent.
最近,issamini报道了在非热压大气压He等离子体喷射[1]中邻近和传播电离波(IWs)的电场强度的测量和分析。这篇论文[1]几乎是2017 ArXiv:1709.03109v1[2]的完整副本,作者已经发表了评论[3]。在这篇评论中,我们首先确认报告的结果是错误的,因为一个不正确的电场探头对准,其次,即使这些错误的测量本身也是不一致的。
{"title":"Comment on ‘Mapping the electric field vector of guided ionization waves at atmospheric pressure’, (2020) Plasma Res. Express 2 025014","authors":"S. Dozias, J. Pouvesle, É. Robert","doi":"10.1088/2516-1067/ac18b9","DOIUrl":"https://doi.org/10.1088/2516-1067/ac18b9","url":null,"abstract":"Recently, Iséni reported measurements and analysis of electric field (EF) strengths adjacent to, and in propagating ionization waves (IWs) for non-thermal atmospheric pressure He plasma jets [1]. This paper [1] is almost the full copy of the 2017 ArXiv :1709.03109v1 [2] for which the authors already published a comment [3]. In this comment, we confirm first that the reported results are wrong due to an improperly aligned electric field probe, and second, that even these wrong measurements are themselves inconsistent.","PeriodicalId":36295,"journal":{"name":"Plasma Research Express","volume":"3 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"61181174","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 16
Low jitter parabolic profile low density plasma channel in 3D printed gas filled capillary 3D打印充气毛细管中的低抖动抛物型低密度等离子体通道
Q3 ORTHOPEDICS Pub Date : 2021-01-01 DOI: 10.1088/2516-1067/ac0d4b
Y. Raz, E. Behar, Y. Ferber, A. Biagioni, M. Galletti, Maria Pia Anania, R. Pompili, Costa Gemma, A. Zigler
A parabolic profile plasma channel formed by an electric discharge inside a gas filled capillary are currently used to achieve optimal conditions for laser guiding and electron acceleration. Acceleration of high quality externally injected electron beam by laser induced wake field requires precise synchronization between several systems. In our experiment the measured jitter in plasma ignition was on the scale of 1 ns, providing possibility for the synchronization with high intensity laser and other auxiliary systems (e.g injectors). We confirmed the existence of a parabolic density plasma profile inside the capillary using an 84 MHz oscillator laser and found its duration to be approximately 300 ns.
目前,利用充气毛细管内的放电形成抛物型等离子体通道是实现激光引导和电子加速的最佳条件。激光诱导尾流场加速高质量外部注入电子束需要多个系统之间的精确同步。在我们的实验中,测量到的等离子体点火抖动在1 ns的范围内,为与高强度激光和其他辅助系统(如注入器)同步提供了可能。利用84 MHz振荡激光器,我们证实了毛细管内部存在抛物线密度等离子体分布,并发现其持续时间约为300 ns。
{"title":"Low jitter parabolic profile low density plasma channel in 3D printed gas filled capillary","authors":"Y. Raz, E. Behar, Y. Ferber, A. Biagioni, M. Galletti, Maria Pia Anania, R. Pompili, Costa Gemma, A. Zigler","doi":"10.1088/2516-1067/ac0d4b","DOIUrl":"https://doi.org/10.1088/2516-1067/ac0d4b","url":null,"abstract":"A parabolic profile plasma channel formed by an electric discharge inside a gas filled capillary are currently used to achieve optimal conditions for laser guiding and electron acceleration. Acceleration of high quality externally injected electron beam by laser induced wake field requires precise synchronization between several systems. In our experiment the measured jitter in plasma ignition was on the scale of 1 ns, providing possibility for the synchronization with high intensity laser and other auxiliary systems (e.g injectors). We confirmed the existence of a parabolic density plasma profile inside the capillary using an 84 MHz oscillator laser and found its duration to be approximately 300 ns.","PeriodicalId":36295,"journal":{"name":"Plasma Research Express","volume":"3 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"61181117","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Single and double null equilibria in the SMART Tokamak SMART托卡马克的单零平衡和双零平衡
Q3 ORTHOPEDICS Pub Date : 2021-01-01 DOI: 10.1088/2516-1067/ac2a0e
S. J. Doyle, A. Mancini, M. Agredano-Torres, J. L. García-Sánchez, J. Segado-Fernandez, J. Ayllon-Guerola, M. Garcia-Muñoz, E. Viezzer, J. Garcia-Lopez, Y. Hwang, K. Chung
The SMall Aspect Ratio Tokamak (SMART) device is a novel, compact (R geo = 0.42 m, a = 0.22 m, A ≥ 1.70) spherical tokamak, currently under development at the University of Seville. The SMART device is being developed over 3 phases, with target on-axis toroidal magnetic fields between 0.1 ≤ B ϕ ≤ 1.0 T, and target plasma currents of between 35 ≤ I p ≤ 400 kA; with phases 2 and 3 enabling access to a wide range of elongations (κ ≤ 2.30) and triangularities ( − 0.50 ≤ δ ≤ 0.50). SMART employs four internal divertor coils with two internal and two external poloidal field coils, enabling operation in lower-single, upper-single and double-null configurations. This work examines phase 3 of the SMART device, presenting a prospective L-mode discharge scenario without external heating, before examining five highly-shaped equilibria, including: two double null triangular configurations, two single null triangular configurations and a baseline double null configuration. All equilibria are obtained via an axisymmetric Grad-Shafranov force balance solver (Fiesta), in combination with a circuit equation rigid current displacement model (RZIp) to obtain time-resolved vessel and plasma currents.
小宽高比托卡马克(SMART)装置是一种新颖、紧凑(R geo = 0.42 m, a = 0.22 m, a≥1.70)的球形托卡马克,目前正在塞维利亚大学开发中。SMART器件分3个阶段开发,目标轴向环面磁场在0.1≤B φ≤1.0 T,目标等离子体电流在35≤I p≤400 kA;相位2和3可以获得大范围的伸长(κ≤2.30)和三角形(- 0.50≤δ≤0.50)。SMART采用四个内部分流器线圈,两个内部和两个外部极向磁场线圈,可在低单、高单和双零配置下运行。本研究考察了SMART装置的第三阶段,在考察五种高形状平衡(包括两个双零三角形配置、两个单零三角形配置和一个基线双零配置)之前,提出了一个没有外部加热的l模式放电场景。所有平衡都是通过轴对称的grada - shafranov力平衡求解器(Fiesta)获得的,结合电路方程刚性电流位移模型(RZIp)获得时间分辨的容器和等离子体电流。
{"title":"Single and double null equilibria in the SMART Tokamak","authors":"S. J. Doyle, A. Mancini, M. Agredano-Torres, J. L. García-Sánchez, J. Segado-Fernandez, J. Ayllon-Guerola, M. Garcia-Muñoz, E. Viezzer, J. Garcia-Lopez, Y. Hwang, K. Chung","doi":"10.1088/2516-1067/ac2a0e","DOIUrl":"https://doi.org/10.1088/2516-1067/ac2a0e","url":null,"abstract":"The SMall Aspect Ratio Tokamak (SMART) device is a novel, compact (R geo = 0.42 m, a = 0.22 m, A ≥ 1.70) spherical tokamak, currently under development at the University of Seville. The SMART device is being developed over 3 phases, with target on-axis toroidal magnetic fields between 0.1 ≤ B ϕ ≤ 1.0 T, and target plasma currents of between 35 ≤ I p ≤ 400 kA; with phases 2 and 3 enabling access to a wide range of elongations (κ ≤ 2.30) and triangularities ( − 0.50 ≤ δ ≤ 0.50). SMART employs four internal divertor coils with two internal and two external poloidal field coils, enabling operation in lower-single, upper-single and double-null configurations. This work examines phase 3 of the SMART device, presenting a prospective L-mode discharge scenario without external heating, before examining five highly-shaped equilibria, including: two double null triangular configurations, two single null triangular configurations and a baseline double null configuration. All equilibria are obtained via an axisymmetric Grad-Shafranov force balance solver (Fiesta), in combination with a circuit equation rigid current displacement model (RZIp) to obtain time-resolved vessel and plasma currents.","PeriodicalId":36295,"journal":{"name":"Plasma Research Express","volume":"375 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"61181635","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Modifications of an electrolytic aluminum oxide film under the treatment with microdischarges during plasma electrolytic oxidation, a self-organized dielectric barrier discharge (DBD) and a DBD-like plasma jet 等离子体电解氧化、自组织介质阻挡放电(DBD)和类DBD等离子体射流处理下电解铝氧化膜的改性
Q3 ORTHOPEDICS Pub Date : 2021-01-01 DOI: 10.1088/2516-1067/ac2e0f
Vera Bracht, F. Kogelheide, Sven Gröger, P. Hermanns, Simon Böddeker, N. Bibinov, P. Awakowicz
A key to the understanding of mechanisms during plasma electrolytic oxidation (PEO) is the interaction between microdischarges and an amorphous oxide film. The PEO microdischarges, which are randomly distributed on the surface of a treated lightweight metal substrate (Al, Ti, Mg), cause material extraction and support the formation of hard and dense crystalline oxide films. Characterization of these microdischarges is a complicated task under PEO conditions, because of the stochastically temporal and spatial behavior as well as the small dimension of the microdischarges. Microdischarges at atmospheric pressure conditions can leave similar erosion traces on metallic films (Al, Ti) as PEO microdischarges on oxide films, and possibly can support a better understanding of the plasma-solid-interactions as well as microdischarge characteristics during PEO. A porous aluminum oxide film is deposited on aluminum substrates by pre-anodizing at a voltage of 250 V and is treated afterwards with a relative short (duration of 1 min) PEO process at a voltage of about 500 V or filamentary dielectric barrier discharges, namely a self-organized Dielectric Barrier Discharge (DBD) and a DBD-like plasma jet operated both with a He/N2 (95%/5%) gas flow. The gas temperature at DBD plasma conditions, measured using the rotational distribution in the emission spectra of molecular nitrogen, is low and amounts to about 400 K. Erosion traces on the surface of the oxide film caused by PEO and plasma spots of both atmospheric pressure discharges are studied by scanning electron microscopy and energy dispersed x-ray spectroscopy. Form and dimensions of erosion traces and established modifications of the material composition generated by the treatment with these DBD microdischarges under atmospheric pressure conditions are similar to those ones generated by the PEO process. Hence, a similar mechanism of these processes is supposed. For stronger evidences of the assumed PEO mechanism additional experimental studies are needed.
了解等离子体电解氧化(PEO)机制的关键是微放电与非晶氧化膜之间的相互作用。PEO微放电随机分布在处理过的轻质金属基底(Al, Ti, Mg)表面,导致材料萃取并支持形成坚硬致密的结晶氧化膜。由于微放电在时间和空间上的随机性以及微放电的小尺寸,在PEO条件下表征这些微放电是一项复杂的任务。大气压条件下的微放电可以在金属膜(Al, Ti)上留下与PEO在氧化膜上微放电相似的侵蚀痕迹,并且可能有助于更好地理解等离子体-固体相互作用以及PEO过程中的微放电特性。在250 V的电压下,通过预阳极氧化在铝基板上沉积多孔氧化铝膜,然后在500 V电压下进行相对较短(持续时间为1 min)的PEO工艺或丝状介质阻挡放电,即自组织介质阻挡放电(DBD)和类似DBD的等离子体射流,同时以He/N2(95%/5%)气体流动。利用分子氮发射光谱中的旋转分布测量,DBD等离子体条件下的气体温度较低,约为400k。利用扫描电子显微镜和能量分散x射线能谱研究了两种大气压放电的PEO和等离子体斑对氧化膜表面的侵蚀痕迹。在常压条件下,这些DBD微排放处理产生的侵蚀痕迹的形式和尺寸以及材料成分的既定变化与PEO工艺产生的类似。因此,假设这些过程具有类似的机制。为了更有力地证明假设的PEO机制,还需要进一步的实验研究。
{"title":"Modifications of an electrolytic aluminum oxide film under the treatment with microdischarges during plasma electrolytic oxidation, a self-organized dielectric barrier discharge (DBD) and a DBD-like plasma jet","authors":"Vera Bracht, F. Kogelheide, Sven Gröger, P. Hermanns, Simon Böddeker, N. Bibinov, P. Awakowicz","doi":"10.1088/2516-1067/ac2e0f","DOIUrl":"https://doi.org/10.1088/2516-1067/ac2e0f","url":null,"abstract":"A key to the understanding of mechanisms during plasma electrolytic oxidation (PEO) is the interaction between microdischarges and an amorphous oxide film. The PEO microdischarges, which are randomly distributed on the surface of a treated lightweight metal substrate (Al, Ti, Mg), cause material extraction and support the formation of hard and dense crystalline oxide films. Characterization of these microdischarges is a complicated task under PEO conditions, because of the stochastically temporal and spatial behavior as well as the small dimension of the microdischarges. Microdischarges at atmospheric pressure conditions can leave similar erosion traces on metallic films (Al, Ti) as PEO microdischarges on oxide films, and possibly can support a better understanding of the plasma-solid-interactions as well as microdischarge characteristics during PEO. A porous aluminum oxide film is deposited on aluminum substrates by pre-anodizing at a voltage of 250 V and is treated afterwards with a relative short (duration of 1 min) PEO process at a voltage of about 500 V or filamentary dielectric barrier discharges, namely a self-organized Dielectric Barrier Discharge (DBD) and a DBD-like plasma jet operated both with a He/N2 (95%/5%) gas flow. The gas temperature at DBD plasma conditions, measured using the rotational distribution in the emission spectra of molecular nitrogen, is low and amounts to about 400 K. Erosion traces on the surface of the oxide film caused by PEO and plasma spots of both atmospheric pressure discharges are studied by scanning electron microscopy and energy dispersed x-ray spectroscopy. Form and dimensions of erosion traces and established modifications of the material composition generated by the treatment with these DBD microdischarges under atmospheric pressure conditions are similar to those ones generated by the PEO process. Hence, a similar mechanism of these processes is supposed. For stronger evidences of the assumed PEO mechanism additional experimental studies are needed.","PeriodicalId":36295,"journal":{"name":"Plasma Research Express","volume":"3 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"61181814","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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Plasma Research Express
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