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Understanding a new wrinkling behavior of annular grooved panel during flexible free incremental sheet forming 了解柔性自由增量板材成型过程中环形槽板的新起皱行为
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-23 DOI: 10.1016/j.jmatprotec.2024.118608
Zhidong Chang , Mei Yang , Yongbing Li , Jun Chen
Wrinkling behavior of sheet metal by inappropriate process parameters and the resultant variation of thickness and microstructure during incremental sheet forming (ISF) have significant impact on forming stability and geometric profile. The wrinkling-related mechanism is yet to be well understood, which make it difficult to effectively control wrinkling defects during ISF. In the present work, the wrinkling behavior and related mechanism of a typical annular grooved panel are investigated during a novel flexible free ISF process. Experiments demonstrate that during this ISF process, the sheet material sequentially undergoes 4 deformation modes: contacting state under plane strain condition, contracting state with only elastic deflection, thickening state under uniaxial compression condition, and wrinkling state where the circumferential compressive stress exceeds the critical wrinkling stress. The evolution of these deformation modes is dominantly caused by the increasing of edge contraction and circumferential stress, which are induced by the bending moment from the forming tool and auxiliary sheets. Based on the mechanism, an analytical model is developed to predict the wrinkling behavior, by which the corresponded sheet thickness, bending moment, circumferential compressive stress and critical wrinkling stress during the wrinkling process could be comprehensively calculated. Experimental results validate that the analytical model can accurately predict the wrinkling behavior under different process parameters, material properties and auxiliary sheet materials. Through microstructural characterization, numerical simulation and analytical modeling, the influence of process parameter and material property on wrinkling behavior is systematically investigated, along with the variation of sheet thickness and microstructure under different wrinkling modes. This work enhance a deep understanding of wrinkling behavior during ISF process, thereby providing effective methods for process optimization and quality improvement.
在增量板材成形(ISF)过程中,不适当的工艺参数会导致板材起皱,由此产生的厚度和微观结构变化会对成形稳定性和几何轮廓产生重大影响。与起皱相关的机理尚待深入了解,因此很难在 ISF 过程中有效控制起皱缺陷。在本研究中,我们研究了一种新型柔性自由 ISF 工艺中典型环形沟槽面板的起皱行为和相关机理。实验证明,在 ISF 过程中,板材会依次经历 4 种变形模式:平面应变条件下的接触状态、仅有弹性挠度的收缩状态、单轴压缩条件下的增厚状态以及周向压应力超过临界起皱应力的起皱状态。这些变形模式的演变主要是由成型工具和辅助板材的弯矩引起的边缘收缩和周向应力增加造成的。根据这一机理,建立了预测起皱行为的分析模型,从而可以全面计算起皱过程中相应的板材厚度、弯矩、周向压应力和临界起皱应力。实验结果验证了该分析模型能准确预测不同工艺参数、材料特性和辅助板材材料下的起皱行为。通过微观结构表征、数值模拟和分析模型,系统地研究了工艺参数和材料特性对起皱行为的影响,以及不同起皱模式下板材厚度和微观结构的变化。这项研究加深了对 ISF 工艺中起皱行为的理解,从而为工艺优化和质量改进提供了有效方法。
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引用次数: 0
A 3D simulation of grain structure evolution during powder bed fusion additive manufacturing and subsequent laser rescanning process 粉末床熔融增材制造和后续激光重新扫描过程中晶粒结构演变的三维模拟
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-20 DOI: 10.1016/j.jmatprotec.2024.118603
Kai Kang , Lang Yuan , André B. Phillion

Laser rescanning is often used as a post-process treatment during Laser Powder Bed Fusion (LPBF) processes to improve product quality. Taking AlSi10Mg material as a case, this study presents a 3D mesoscopic Cellular Automaton (CA) model coupled with Finite Element Analysis (FEA) to simulate grain structure evolution during the Laser Powder Bed Fusion process and its subsequent laser rescanning treatments incorporating non-equilibrium effects under rapid solidification conditions. A key focus of our investigation centers on exploring the potential origins of grain refinement during the laser rescanning process, and the subsequent impact on the resultant grain structure. Our model introduces two key innovations: (i) a diffusion-based grain growth function that tracks composition redistribution during solidification, enhancing the accuracy of grain structure prediction, and (ii) a novel fusion boundary nucleation model that accounts for local composition variations, providing deeper insights into grain refinement mechanisms. By incorporating epitaxial growth, bulk nucleation and fusion boundary nucleation models, we have observed a mixed grain structure in the melt pool, mirroring experimental findings in other studies, delineated into three zones: fine grains at the melt pool boundary (Zone I), long columnar grains (Zone II), and fine equiaxed grains (Zone III). Two factors contributing to grain refinement in our model are presented: (i) Columnar to equiaxed transition (CET) and elevated cooling rate within the rescan melt pool; (ii) Extending volume of fine grains near the rescan melt pool boundary due to fusion boundary nucleation. As a result, laser rescanning treatments, notably, yielded a refined grain structure with approximately 20% reduction in grain dimensions and a pronounced texture under current process parameters. The implications of these findings hold potential for optimized Laser Powder Bed Fusion processes and grain refinement control in future applications.

在激光粉末床融合(LPBF)过程中,激光重扫描通常被用作一种后处理方法,以提高产品质量。本研究以 AlSi10Mg 材料为例,提出了一种结合有限元分析(FEA)的三维介观细胞自动机(CA)模型,用于模拟激光粉末床熔融过程中的晶粒结构演变,以及在快速凝固条件下结合非平衡效应的后续激光重新扫描处理。我们研究的一个重点是探索激光重新扫描过程中晶粒细化的潜在起源,以及随后对所产生的晶粒结构的影响。我们的模型引入了两项关键创新:(i) 基于扩散的晶粒生长函数,可跟踪凝固过程中的成分再分布,从而提高晶粒结构预测的准确性;(ii) 新型熔融边界成核模型,可考虑局部成分变化,从而更深入地了解晶粒细化机制。通过结合外延生长、体成核和熔融边界成核模型,我们观察到熔池中的混合晶粒结构,这与其他研究的实验结果一致,并将其划分为三个区域:熔池边界的细晶粒(I 区)、长柱状晶粒(II 区)和细等轴晶粒(III 区)。在我们的模型中,有两个因素导致了晶粒细化:(i) 重扫描熔池内柱状到等轴状的转变(CET)和冷却速率升高;(ii) 由于熔融边界成核,重扫描熔池边界附近的细晶粒体积不断扩大。因此,在当前的工艺参数下,激光重扫描处理明显产生了细化的晶粒结构,晶粒尺寸减少了约 20%,纹理明显。这些发现为优化激光粉末床融合工艺和未来应用中的晶粒细化控制提供了可能。
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引用次数: 0
Achieving high-thermal-conductivity brazed joint between carbon-based composites and Mo-Cu alloys by increasing the heat transfer area 通过增加传热面积实现碳基复合材料和钼铜合金之间的高导热钎焊连接
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-19 DOI: 10.1016/j.jmatprotec.2024.118606
Pengpeng Xue , Xiaoqing Si , Ji Zhou , Chun Li , Junlei Qi , Jian Cao
Carbon-fiber-reinforced carbon matrix (Cf/C)-Mo30Cu brazed joints play an important role in the cooling systems of thermonuclear reactors. However, the limited contact area of heterogeneous interfaces severely limits the heat transfer efficiency. To overcome this drawback, we prepare three-dimensional porous interfaces by pre-oxidizing the Cf/C composite. Results show that circular gaps are formed between the carbon fibers and the pyrolyzed carbon after pre-oxidization at 600 °C in air. Fster braze penetration in the Cf/C composite is achieved, and the heat-transfer area across the interface is dramatically increased. The room-temperature thermal conductivity of the joints reaches a maximum value of 146 W·m−1·K−1 at a pre-oxidation time of 2 min; this value is 30 % higher than that obtained without treatment. The enhancement in thermal conductivity is mainly attributed to the increased contact area at the interface between the brazing seam and the Cf/C matrix, which provides more channels for heat transfer. This method of significantly improving the thermal conductivity is an important guide for the thermal management of thermonuclear reactors.
碳纤维增强碳基(Cf/C)-Mo30Cu 钎焊接头在热核反应堆冷却系统中发挥着重要作用。然而,异质界面有限的接触面积严重限制了传热效率。为了克服这一缺点,我们通过对 Cf/C 复合材料进行预氧化制备了三维多孔界面。结果表明,在 600 °C 的空气中进行预氧化后,碳纤维和热解碳之间形成了圆形间隙。在 Cf/C 复合材料中实现了 Fster 铜焊渗透,并显著增加了界面上的传热面积。在预氧化时间为 2 分钟时,接头的室温热导率达到最大值 146 W-m-1-K-1;该值比未经处理的热导率高出 30%。导热率的提高主要归因于钎缝与 Cf/C 基体之间的界面接触面积增大,从而提供了更多的传热通道。这种大幅提高热导率的方法对热核反应堆的热管理具有重要指导意义。
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引用次数: 0
The energy synergistic mechanism of coaxial heterogeneous-wavelength hybrid laser beam and its effect on welding molten pool dynamics for aluminum alloy 同轴异质波长混合激光束的能量协同机制及其对铝合金焊接熔池动力学的影响
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-18 DOI: 10.1016/j.jmatprotec.2024.118605
Yanqiu Zhao, Xiaohong Zhan, Longfei Ma, Hengchang Bu, Yue Li, Chao Ma
The coaxial heterogeneous-wavelength hybrid laser beam (HW-HLB) heat source featuring a “Gauss + Flat top” energy distribution, which integrates the 1080 nm and 915 nm laser beam, was employed in this paper to achieve excellent stability in the welding of aluminum alloy. The interaction mechanism between aluminum alloy and laser beams with different wavelengths was taken as a point cut to explore the synergistic enhancement mechanism of coaxial HW-HLB . A thermal-fluid coupling model for HW-HLB welding, considering the synergistic effect of dual lasers, was established according to the welding experiment results. The influence of fiber laser power (PF) and diode laser power (PD) on the molten pool flow behavior during welding process was investigated. The dynamic of the molten pool and the maintenance mechanism of the keyhole were elucidated through in-situ monitoring experiments and thermal-flow simulations. The results indicated that, in contrast to the single fiber laser beam (FLB), the power density of HW-HLB presents a significant increase, which results in the “avalanche-like” augmentation of the plasma plume, as well as deeper depth of the keyhole. The energy synergistic enhancement effect of coaxial HW-HLB with PF=2800 W and PD=2500 W performs stronger and thorough changes in the morphology and flow behavior of the molten pool. The introduction of 915 nm laser beam improves the multi-reflection behavior in the inner keyhole. The findings of our research provide a theoretical framework for improving the stability of the laser weld molten pool and the quality of welds in aluminum alloys through the implementation of HW-HLB.
本文采用能量分布为 "高斯+平顶 "的同轴异质波长混合激光束(HW-HLB)热源,将1080 nm和915 nm激光束集成在一起,实现了铝合金焊接的优异稳定性。以铝合金与不同波长激光束之间的相互作用机理为切入点,探讨了同轴 HW-HLB 的协同增强机理。根据焊接实验结果,建立了考虑双激光协同效应的 HW-HLB 焊接热流耦合模型。研究了光纤激光器功率(PF)和二极管激光器功率(PD)对焊接过程中熔池流动行为的影响。通过原位监测实验和热流模拟,阐明了熔池的动态和锁孔的维持机制。结果表明,与单光纤激光束(FLB)相比,HW-HLB 的功率密度显著增加,从而导致等离子体羽流的 "雪崩式 "增长,并加深了键孔的深度。PF=2800 W 和 PD=2500 W 的同轴 HW-HLB 的能量协同增强效应使熔池的形态和流动行为发生了更强烈、更彻底的变化。915 nm 激光束的引入改善了内锁孔的多重反射行为。我们的研究结果为通过实施 HW-HLB 提高激光焊接熔池的稳定性和铝合金的焊接质量提供了理论框架。
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引用次数: 0
Research on the bonding performance and mechanism of hot-rolled Ti/steel clad plates based on surface state 基于表面状态的热轧钛/钢复合板结合性能及机理研究
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-18 DOI: 10.1016/j.jmatprotec.2024.118604
Jinlong Bai , Chang Liu , Yue Wu , Zhongkai Ren , Tao Wang , Qingxue Huang

The interfacial bonding strength of Ti/steel clad plates is a crucial factor that affects their application. However, the effect of the surface state, which is a significant determinant, is often neglected. In this study, various surface treatment processes were employed to create different surface states based on the hot-rolling of double-layer steel billets, and the effects and mechanisms of these surface states on the bonding performance of hot-rolled Ti/steel clad plates were systematically examined. The results showed that the Ti/steel clad plates pretreated with a louver wheel exhibited the highest bonding performance, with the average bonding strength peaking at 328.67 MPa and stabilising at approximately 300 MPa. This strength was approximately 50 % greater than that achieved with wire brush treatment and significantly surpassed the results obtained with sanding belts and diamond grinding discs. The analysis of the surface properties and microstructural characteristics revealed that various surface treatments led to different levels of work hardening and lattice distortion at the surface, and the interface bonding strength depended on the degree of matching between these factors. Proper surface hardening can promote the transformation of lattice distortion energy into a diffusion-driving force of elements on both sides of the interface during rolling, enabling sufficient diffusion of elements on both sides of the interface and obtaining good interface bonding performance. A phenomenological prediction mechanism-based model was established to quantify the relationship between the surface state and the bonding strength. This study elucidats the mechanism by which the surface state of materials influences the interfacial bonding performance of hot-rolled Ti/steel clad plates. These findings have significant implications for enhancing the interfacial properties of these composite plates and for selecting suitable pre-rolling surface treatment processes.

钛/钢复合板的界面结合强度是影响其应用的关键因素。然而,作为重要决定因素的表面状态的影响往往被忽视。本研究在热轧双层钢坯的基础上,采用多种表面处理工艺形成不同的表面状态,并系统研究了这些表面状态对热轧钛/钢复合板结合性能的影响和机理。结果表明,使用百叶轮预处理的钛/钢复合板具有最高的粘结性能,平均粘结强度达到峰值 328.67 兆帕,并稳定在约 300 兆帕。这一强度比钢丝刷处理的强度高出约 50%,大大超过了砂带和金刚石磨盘处理的结果。对表面特性和微观结构特征的分析表明,各种表面处理会导致不同程度的加工硬化和表面晶格畸变,而界面结合强度取决于这些因素之间的匹配程度。适当的表面硬化可以促进晶格畸变能量在轧制过程中转化为界面两侧元素的扩散驱动力,使界面两侧元素充分扩散,从而获得良好的界面结合性能。研究建立了一个基于现象预测机制的模型,以量化表面状态与结合强度之间的关系。该研究阐明了材料表面状态影响热轧钛/钢复合板界面结合性能的机理。这些发现对提高这些复合板的界面性能和选择合适的轧制前表面处理工艺具有重要意义。
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引用次数: 0
A new technique for electrochemical self-discharge machining of macro-sized hole in the glass using an integrated tool electrode 使用集成工具电极在玻璃上加工大尺寸孔的电化学自放电加工新技术
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-18 DOI: 10.1016/j.jmatprotec.2024.118607
Zhixiang Zou , Kangcheung Chan , Yukui Wang , Ting Huang , Taiman Yue , Zhongning Guo , Jiangwen Liu

Owing to stray electrochemical discharge effects, it is still a significant challenge to obtain high machining quality and efficiency in conventional electrochemical discharge machining (ECDM) of macro-sized holes (>1 mm) in glass. Thus, in this study, an electrochemical self-discharge machining (EC-SDM) technique using an integrated tool electrode is proposed. In the new design, the tool anode and cathode are configured coaxially in an integral manner. The simulation and high-speed camera observation results indicated that the electrochemical discharges were more concentrated at the tool electrode end when using the EC-SDM. Thus, the stray electrochemical discharge capacity decreased significantly. With the formation of a dense oxidized layer on the anode electrode surface, the EC-SDM technique is frequently interrupted by DC pulse; however, the discharge is continuous under bipolar pulse conditions. Furthermore, the EC-SDM technique can utilize the advantage of the hydrogen-oxygen gas mixture generated at the integrated electrode end for combustion close to the workpiece surface, thus increasing machining efficiency. When compared with the conventional ECDM, the machining efficiency increased by 6.09 times, and the entrance heat affected zone (HAZ) reduced by 54.05 %. A macro-sized hole (entrance diameter of 1303 μm) with depth of 1520 μm, minimal thermal and mechanical damage was successfully obtained in the glass substrate by using the EC-SDM technique. The results illustrate that employing the novel EC-SDM technique is a straightforward way to reduce stray electrochemical discharge and improve the machining performance of macro-sized glass holes. The potential of the EC-SDM technique for MEMS applications was also highlighted.

由于杂散电化学放电效应,在传统的电化学放电加工(ECDM)中,要获得玻璃上大尺寸孔(1 毫米)的高加工质量和效率仍是一项重大挑战。因此,本研究提出了一种使用集成工具电极的电化学自放电加工(EC-SDM)技术。在新设计中,工具阳极和阴极以整体方式同轴配置。模拟和高速摄像观察结果表明,使用 EC-SDM 时,电化学放电更集中在刀具电极端。因此,杂散电化学放电能力明显下降。由于阳极电极表面形成了致密的氧化层,EC-SDM 技术经常会被直流脉冲中断;但在双极脉冲条件下,放电是连续的。此外,EC-SDM 技术还能利用集成电极端部产生的氢氧混合气体的优势,在靠近工件表面的地方进行燃烧,从而提高加工效率。与传统的 ECDM 相比,加工效率提高了 6.09 倍,入口热影响区(HAZ)减少了 54.05%。利用 EC-SDM 技术,成功地在玻璃基板上加工出了深度为 1520 μm、热损伤和机械损伤最小的大尺寸孔(入口直径为 1303 μm)。结果表明,采用新颖的 EC-SDM 技术是减少杂散电化学放电和提高大尺寸玻璃孔加工性能的直接方法。此外,EC-SDM 技术在微机电系统应用方面的潜力也得到了强调。
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引用次数: 0
A new severe plastic deformation technique of combined extrusion and torsion to prepare bulk ultrafine grained copper 用挤压和扭转相结合的新型严重塑性变形技术制备大块超细晶粒铜
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-17 DOI: 10.1016/j.jmatprotec.2024.118600
Qingzhong Mao , Yusheng Li , Yanfang Liu , Jiansheng Li , Wei Jiang , Zhongchen Zhou , Yonghao Zhao , Yuntian Zhu

Reducing grain size is a well-established method for strengthening metals. In this study, a novel severe plastic deformation technique—combined extrusion and torsion (CET) with composite strain—was developed to fabricate bulk ultrafine grained metals. A single pass of CET treatment (with a rotation velocity of 1 r/s and extrusion speed of 3 mm/s) refined coarse-grained copper from 54 μm to 450 nm at room temperature, resulting a significant increase in hardness from 0.55 GPa to 1.3 GPa. The CET technique addresses the limitations of conventional extrusion-processed copper (without torsion), which suffers from gradient microstructure and hardness distribution. It provides enhanced strain accumulation under the same extrusion ratio conditions. The more homogeneous microstructures and properties of CET-processed copper rods are attributed to the reduced strain gradient due to torsion. Additionally, targeted finite element analysis indicated that the CET technology requires 37 % less extrusion load and offers at least 30 % more strain compared to conventional extrusion methods. Compared with other severe plastic deformation methods, such as equal channel angular pressing and high-pressure torsion, which involve simpler deformation processes, the CET technique shows considerable promise for large-scale manufacturing of ultrafine-grained metals.

减小晶粒尺寸是强化金属的一种行之有效的方法。在这项研究中,开发了一种新型的严重塑性变形技术--复合应变的组合挤压和扭转(CET)--用于制造大块超细晶粒金属。在室温下,单次 CET 处理(旋转速度为 1 r/s,挤压速度为 3 mm/s)可将粗晶粒铜从 54 μm 细化至 450 nm,使硬度从 0.55 GPa 显著提高至 1.3 GPa。CET 技术解决了传统挤压加工铜(无扭转)微观结构和硬度分布不均的局限性。在相同的挤压比率条件下,它能增强应变积累。由于扭转导致的应变梯度减小,CET 加工铜杆的微观结构和性能更加均匀。此外,有针对性的有限元分析表明,与传统挤压方法相比,CET 技术所需的挤压负荷减少了 37%,应变增加了至少 30%。与其他涉及较简单变形过程的严重塑性变形方法(如等通道角压和高压扭转)相比,CET 技术为大规模制造超细晶粒金属带来了巨大的前景。
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引用次数: 0
Anisotropic formability and deformation mechanism of near-α titanium alloy sheet under continuous nonlinear strain paths at high temperature 高温连续非线性应变路径下近α钛合金薄板的各向异性成形性和变形机理
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-14 DOI: 10.1016/j.jmatprotec.2024.118602
Ronglei Fan, Yong Wu, Hongliang Yin, Junjie Zhang, Minghe Chen

In the present study, the anisotropic formability and underlying deformation mechanism of near-α TA32 titanium alloy sheet under continuous nonlinear strain paths (CNSPs) at high temperature were investigated in depth. To achieve this goal, a new experimental method combining hot gas bulging with step-combined dies was proposed, and the hot CNSPs of metal sheets can be flexibly and conveniently realized by changing the number and shape of step-combined dies. Based on this method, the anisotropic deformation behavior and forming limits of TA32 sheet under fifteen CNSPs were tested at 800 ℃ with a strain rate of 0.001 s−1. Then, two advanced constitutive models with different scales were embedded into the classical Marciniak-Kuczyński (M-K) theory to predict the forming limits of TA32 sheet under different strain paths: the macro-scale viscoplastic model coupled with Hill48 yield criterion and non-associated flow rule (NAFR) as well as the meso-scale three-dimensional crystal plasticity finite element (CPFE) model coupled with cellular automata (CA). The results demonstrate that the CPFE-CA-MK coupled model exhibits higher accuracy in predicting the forming limits of TA32 sheet under linear and continuous nonlinear strain paths. Especially for the tension-tension strain paths, the CPFE-CA-MK coupled model improves accuracy by at least 3.1 % compared to macro-scale models. Due to the material anisotropy, the initial inclination angle of the groove in the CPFE-CA-MK model is closely related to the strain path and significantly affects the prediction accuracy. Based on the CPFE simulation, the effects of anisotropy and strain path change on the dislocation slip mode of different texture components was analyzed in depth, which provides a theoretical guidance for the optimization of hot forming process of TA32 titanium alloy complex components.

本研究深入探讨了高温连续非线性应变路径(CNSPs)下近α TA32 钛合金薄板的各向异性成形性及其基本变形机理。为实现这一目标,提出了热气鼓胀与阶梯组合模相结合的新实验方法,并通过改变阶梯组合模的数量和形状,灵活方便地实现了金属板的热CNSP。在此基础上,在 800 ℃、应变速率为 0.001 s-1 的条件下测试了 15 种 CNSP 条件下 TA32 薄板的各向异性变形行为和成形极限。然后,在经典的马西尼亚克-库钦斯基(M-K)理论中嵌入了两种不同尺度的先进组成模型,以预测不同应变路径下 TA32 片材的成型极限:宏观尺度粘塑性模型与 Hill48 屈服准则和非关联流动规则(NAFR)耦合,以及中观尺度三维晶体塑性有限元(CPFE)模型与细胞自动机(CA)耦合。结果表明,CPFE-CA-MK 耦合模型在预测 TA32 板材在线性和连续非线性应变路径下的成形极限方面表现出更高的精度。特别是在拉伸-张力应变路径下,CPFE-CA-MK 耦合模型比宏观尺度模型的精度至少提高了 3.1%。由于材料的各向异性,CPFE-CA-MK 模型中凹槽的初始倾角与应变路径密切相关,并对预测精度产生显著影响。基于 CPFE 模拟,深入分析了各向异性和应变路径变化对不同质构构件位错滑移模式的影响,为 TA32 钛合金复杂构件热成形工艺优化提供了理论指导。
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引用次数: 0
In situ preparations of bi-continuous interpenetrating porous composites with high energy absorption 原位制备具有高能量吸收能力的双连续互穿多孔复合材料
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-13 DOI: 10.1016/j.jmatprotec.2024.118601
Endian Liu , Yu Bai , Jiawen Li , Mingming Su , Huanyue Zhang , Hai Hao

In this paper, porous composites with bi-continuous interpenetrating aluminum foam (AF) and lattice structure were prepared via different sequences. The effect of the preparation sequence on the mechanical properties was analyzed. The results showed that the composites prepared by disordered-ordered and ordered-disordered sequences had higher mechanical properties than the sum of their single components. Porous composite prepared by the disordered-ordered sequence had a discontinuous interface while the one prepared by the ordered-disordered sequence presented a continuous bonding interface and a bubble-free layer. The energy absorption of the porous composite structure prepared by the disordered-ordered sequence was enhanced by the factors of 0.89 and 1.12 over the sum of their single components, while the ordered-disordered was enhanced by the factor of 1.9 and 3.81, which was attributed to the metallurgical bonding, 3D mechanical constraints and the fraction of bubble-free layer that formed between the interfaces. The continuous interface contributed the excellent mechanical properties of the composites due to its higher failure strength before detaching. The presence of the bubble-free layer increased the interfacial contact area, which can effectively absorb energy and exhibit significant deformation resistance. The porous composite exhibited excellent comprehensive performance, which provided a new idea for the structurally and functionally integrated design of porous composites.

本文通过不同的顺序制备了具有双连续互穿泡沫铝(AF)和晶格结构的多孔复合材料。分析了制备顺序对力学性能的影响。结果表明,无序-有序和有序-无序序列制备的复合材料的力学性能高于其单一成分的总和。无序-有序序列制备的多孔复合材料具有不连续的界面,而有序-无序序列制备的复合材料则具有连续的粘合界面和无气泡层。无序-有序序列制备的多孔复合材料结构的能量吸收能力比其单组分之和分别提高了 0.89 和 1.12 倍,而有序-无序序列则提高了 1.9 和 3.81 倍,这归因于冶金结合、三维机械约束以及界面之间形成的无气泡层。连续界面在脱落前具有较高的破坏强度,因此复合材料具有优异的机械性能。无泡层的存在增加了界面接触面积,可有效吸收能量并表现出显著的抗变形能力。多孔复合材料表现出优异的综合性能,为多孔复合材料的结构和功能一体化设计提供了新思路。
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引用次数: 0
Achieving excellent bond strength and tensile strength synergy of ultrafine-grained Al/Cu bimetallic sheets developed by an innovative hybrid manufacturing process 通过创新混合制造工艺开发的超细晶粒铝/铜双金属片实现出色的粘接强度和拉伸强度协同效应
IF 6.7 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL Pub Date : 2024-09-12 DOI: 10.1016/j.jmatprotec.2024.118596
B. Prathyusha , A. Dhal , S.K. Panigrahi

In the present work, two new parameters that influence the bond strength and tensile strength of Al/Cu bimetallic sheets are explored using an innovative hybrid manufacturing process. The innovative hybrid manufacturing process includes engineering of four different microstructures, 1. Ultrafine grained (UFG); 2. Bimodal grained (BM); 3. Fine grained (FG) and 4. Coarse grained (CG) in parent Cu and Al via integration of cryogenic based thermo-mechanical treatment followed by an unique tailored criss-cross surface pattern generation and high deformation roll bonding to develop high performance Al/Cu engineered sheets with four microstructural combinations: UFG‐Al + UFG-Cu, UFG‐Al + BM-Cu, UFG‐Al + FG-Cu and CG‐Al + CG-Cu. The criss-cross pattern aids in initiation of crack at the junctions and fissure formations at cross paths during the roll bonding process. This kind of pattern develops mechanical bond in the form of nugget bunches, which result in enhancement of bond strength in all the microstructural combinations of Al/Cu bimetallic sheets. The ascending order of increase in bond strength-tensile strength synergy of all four engineered microstructural combinations is: CG‐Al + CG-Cu, UFG‐Al + FG-Cu, UFG‐Al + BM-Cu and UFG‐Al + UFG-Cu. The UFG‐Al + UFG-Cu combination has achieved an extraordinary bond strength of 18 N/mm, which is almost 1.6 times the bond strength of its conventional coarse grained counterpart CG‐Al + CG-Cu combination (10 N/mm). Similarly, the UFG‐Al + UFG-Cu combination showed excellent tensile strength of 323 MPa which is around 25 % higher than that of CG‐Al + CG-Cu combination (258 MPa). The engineered UFG microstructure in Al and Cu samples promote the dynamic recrystallization and partial diffusion kinetics at the interface region and established the mechanical and metallurgical bonding between Al/Cu bimetallic sheets during roll bonding process. The adopted surface pattern and the engineered microstructure have enhanced the bond strength and tensile strength of Al/Cu bimetallic sheets both at macro and micro levels. The underlying scientific knowhow for obtaining excellent bond strength-mechanical property synergy in the engineered Al/Cu bimetallic sheets are established.

在本研究中,我们采用一种创新的混合制造工艺,探索了影响铝/铜双金属片结合强度和拉伸强度的两个新参数。创新的混合制造工艺包括四种不同微结构的工程设计:1.超细晶粒 (UFG);2.双峰晶粒 (BM);3.细晶粒 (FG) 和 4.粗晶粒 (CG)。通过整合基于低温的热机械处理方法,在铜和铝母体中形成粗晶粒 (CG),然后生成独特的定制十字交叉表面图案,并进行高变形轧制粘接,从而开发出具有四种微观结构组合的高性能铝/铜工程板材:UFG-Al + UFG-Cu、UFG-Al + BM-Cu、UFG-Al + FG-Cu 和 CG-Al + CG-Cu。在轧制粘合过程中,十字形图案有助于在交界处产生裂纹,并在交叉路径上形成裂缝。这种纹路形成的机械粘合是以金块串的形式出现的,从而提高了铝/铜双金属片所有微观结构组合的粘合强度。所有四种工程微结构组合的结合强度-拉伸强度协同增效作用的递增顺序为CG-Al + CG-Cu、UFG-Al + FG-Cu、UFG-Al + BM-Cu 和 UFG-Al + UFG-Cu。UFG-Al + UFG-Cu 组合达到了 18 牛顿/毫米的超常粘结强度,几乎是传统粗粒材料 CG-Al + CG-Cu 组合(10 牛顿/毫米)粘结强度的 1.6 倍。同样,UFG-Al + UFG-Cu 组合显示出 323 兆帕的优异抗拉强度,比 CG-Al + CG-Cu 组合(258 兆帕)高出约 25%。铝和铜样品中的工程 UFG 微结构促进了界面区域的动态再结晶和部分扩散动力学,并在轧制粘合过程中建立了铝/铜双金属片之间的机械和冶金结合。所采用的表面图案和工程微结构从宏观和微观层面提高了铝/铜双金属片的结合强度和拉伸强度。建立了在工程铝/铜双金属片中获得出色的粘接强度-机械性能协同作用的基本科学知识。
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引用次数: 0
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Journal of Materials Processing Technology
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