Pub Date : 2025-11-24DOI: 10.1007/s10064-025-04607-2
Chenxi Ding, Xu Guo, Xiao Guo, Jiye Xu
With the continuous increase in mining depth, the effects of groundwater and in-situ stress on rock mass strength have become key controlling factors in mining engineering. Through blasting experiments integrating CT (Computed Tomography), SEM (Scanning Electron Microscroscope), 3D reconstruction and fractal analysis, this study investigates water content effects and in-situ stress impacts on sandstone damage mechanisms. Comparative analysis of oven-dried (0%), natural (3.89%) and saturated (7.81%) specimens reveals non-monotonic damage evolution: decreasing from dry to natural states then increasing to saturation. The blasting damage in natural sandstone is significantly reduced under in-situ stress compared to the unstressed condition. Fracture morphology analysis demonstrates two competing water effects: weakening mechanisms (lubrication and cementation hydrolysis) dominate at high water content, while strengthening effects (Stefan adhesion and meniscus forces) peak then decline during intermediate water.
随着开采深度的不断增加,地下水和地应力对岩体强度的影响已成为采矿工程的关键控制因素。通过结合CT (Computed Tomography)、SEM (Scanning Electron microscopy)、三维重建和分形分析的爆破实验,研究了含水率和地应力对砂岩损伤机制的影响。通过对干燥状态(0%)、自然状态(3.89%)和饱和状态(7.81%)试样的对比分析,发现了非单调的损伤演化规律:从干燥状态到自然状态,再到饱和状态,损伤逐渐减小。天然砂岩在地应力作用下的爆破损伤比无应力条件下明显减小。裂缝形态分析显示了两种相互竞争的水效应:在高含水量时,弱化机制(润滑和胶结水解)占主导地位,而在中等含水量时,强化机制(Stefan附着力和半月板力)达到峰值,然后下降。
{"title":"Experimental study on the effects of water content and in-situ stress on blasting damage characteristics and fracture modes of sandstone","authors":"Chenxi Ding, Xu Guo, Xiao Guo, Jiye Xu","doi":"10.1007/s10064-025-04607-2","DOIUrl":"10.1007/s10064-025-04607-2","url":null,"abstract":"<div><p>With the continuous increase in mining depth, the effects of groundwater and in-situ stress on rock mass strength have become key controlling factors in mining engineering. Through blasting experiments integrating CT (Computed Tomography), SEM (Scanning Electron Microscroscope), 3D reconstruction and fractal analysis, this study investigates water content effects and in-situ stress impacts on sandstone damage mechanisms. Comparative analysis of oven-dried (0%), natural (3.89%) and saturated (7.81%) specimens reveals non-monotonic damage evolution: decreasing from dry to natural states then increasing to saturation. The blasting damage in natural sandstone is significantly reduced under in-situ stress compared to the unstressed condition. Fracture morphology analysis demonstrates two competing water effects: weakening mechanisms (lubrication and cementation hydrolysis) dominate at high water content, while strengthening effects (Stefan adhesion and meniscus forces) peak then decline during intermediate water.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145612632","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Evaluating rock properties under different thermal treatments has gained substantial attention in the last few decades concerning its implication in various sub-surface rock engineering applications. Although basaltic rock masses are frequently subjected to high temperatures, the impact of thermal damage, especially under rapid cooling with liquid nitrogen, has received relatively little attention over the years. This study investigates these effects by analyzing changes in effective porosity, ultrasonic wave velocities, Brazilian tensile strength index (BTS), and microstructure following thermal treatment, where specimens were heated at 100–800 °C, followed by immediate cooling with atmospheric air for one cycle (AC-1), liquid nitrogen (LN2) for one cycle (LN2C-1) and five cycles (LN2C-5). Broadly, AC-1 and LN2C-1 show decreased porosity, minimal change in ultrasonic velocities, and higher BTS values at ≤ 200 °C, while LN2C-5 shows similar behavior at ≤ 100 °C. This could be attributed to dehydration and thermal expansion, which lead to pore closure and the formation of a more compact structure. Between 200 and 600 °C in AC-1 and LN2C-1 and 100 °C–600 °C in LN2C-5, effective porosity and damage coefficients gradually increase, while BTS decreases. From 600 to 800 °C, rock properties change more rapidly, primarily due to the formation and propagation of thermal microcracks that weaken the grain bonding. These trends were supported by microstructural analysis. Given the frequent exploration of basaltic terrains for geothermal energy, thermal energy storage, and other underground rock engineering projects, the findings of this study will help optimize drilling parameters and build the sustainable design of rock structures.
{"title":"Effect of heating-liquid nitrogen cooling cycles on the physical properties and tensile strength of basalt","authors":"Bikash Kumar Ram, Rajeswar Das, Deepak Amban Mishra, Ranjan Pramanik, Himangshu Kakati, Rajat Jain","doi":"10.1007/s10064-025-04678-1","DOIUrl":"10.1007/s10064-025-04678-1","url":null,"abstract":"<div><p>Evaluating rock properties under different thermal treatments has gained substantial attention in the last few decades concerning its implication in various sub-surface rock engineering applications. Although basaltic rock masses are frequently subjected to high temperatures, the impact of thermal damage, especially under rapid cooling with liquid nitrogen, has received relatively little attention over the years. This study investigates these effects by analyzing changes in effective porosity, ultrasonic wave velocities, Brazilian tensile strength index (BTS), and microstructure following thermal treatment, where specimens were heated at 100–800 °C, followed by immediate cooling with atmospheric air for one cycle (AC-1), liquid nitrogen (LN<sub>2</sub>) for one cycle (LN<sub>2</sub>C-1) and five cycles (LN<sub>2</sub>C-5). Broadly, AC-1 and LN<sub>2</sub>C-1 show decreased porosity, minimal change in ultrasonic velocities, and higher BTS values at ≤ 200 °C, while LN<sub>2</sub>C-5 shows similar behavior at ≤ 100 °C. This could be attributed to dehydration and thermal expansion, which lead to pore closure and the formation of a more compact structure. Between 200 and 600 °C in AC-1 and LN<sub>2</sub>C-1 and 100 °C–600 °C in LN<sub>2</sub>C-5, effective porosity and damage coefficients gradually increase, while BTS decreases. From 600 to 800 °C, rock properties change more rapidly, primarily due to the formation and propagation of thermal microcracks that weaken the grain bonding. These trends were supported by microstructural analysis. Given the frequent exploration of basaltic terrains for geothermal energy, thermal energy storage, and other underground rock engineering projects, the findings of this study will help optimize drilling parameters and build the sustainable design of rock structures.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145612519","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Salt crystallization, one of the key deterioration mechanisms, can cause significant damage to heritage structures over time. This study investigates the effects of salt crystallization on the physical, mechanical, and microstructural properties of two granite types with distinct pore characteristics. A comprehensive experimental campaign, including mercury intrusion porosimetry, capillary absorption, ultrasonic pulse velocity, uniaxial compressive tests, and digital image correlation, was conducted to evaluate the progression of salt-induced damage. Results from MIP, capillary absorption, and UPV primarily reflected the initial formation and growth of sodium chloride crystals within the pore network, highlighting their utility in capturing early-stage processes. Uniaxial compressive tests provided clear evidence of damage, revealing significant reductions in compressive strength and elastic modulus. The interplay between pore characteristics, crystallization pressures, and mechanical degradation revealed distinct damage behaviors in the two granite types. Granite with a capillary-active pore network showed greater susceptibility to salt crystallization, with a 55% reduction in compressive strength and a 14% increase in open porosity. DIC analysis complemented these findings, capturing early strain concentration and crack propagation patterns in salt-contaminated samples. The findings provide valuable insights into the salt-induced deterioration mechanisms of granite, emphasizing the importance of integrating multiple assessment methods for reliable damage evaluation strategies.
{"title":"Salt-induced deterioration in granites with different pore structures: destructive and non-destructive assessment","authors":"Amin Nazerigivi, Bahman Ghiassi, Amélia Dionísio, Graça Vasconcelos","doi":"10.1007/s10064-025-04655-8","DOIUrl":"10.1007/s10064-025-04655-8","url":null,"abstract":"<div><p>Salt crystallization, one of the key deterioration mechanisms, can cause significant damage to heritage structures over time. This study investigates the effects of salt crystallization on the physical, mechanical, and microstructural properties of two granite types with distinct pore characteristics. A comprehensive experimental campaign, including mercury intrusion porosimetry, capillary absorption, ultrasonic pulse velocity, uniaxial compressive tests, and digital image correlation, was conducted to evaluate the progression of salt-induced damage. Results from MIP, capillary absorption, and UPV primarily reflected the initial formation and growth of sodium chloride crystals within the pore network, highlighting their utility in capturing early-stage processes. Uniaxial compressive tests provided clear evidence of damage, revealing significant reductions in compressive strength and elastic modulus. The interplay between pore characteristics, crystallization pressures, and mechanical degradation revealed distinct damage behaviors in the two granite types. Granite with a capillary-active pore network showed greater susceptibility to salt crystallization, with a 55% reduction in compressive strength and a 14% increase in open porosity. DIC analysis complemented these findings, capturing early strain concentration and crack propagation patterns in salt-contaminated samples. The findings provide valuable insights into the salt-induced deterioration mechanisms of granite, emphasizing the importance of integrating multiple assessment methods for reliable damage evaluation strategies.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145561662","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The state of water and its transformation exert strong controls on the properties of soils, which has long been concerned in soil science and engineering practice. Under various environmental conditions, the water in soils may undergo dynamic migration and phase changes, for which conventional methods usually lack sufficient resolution or provide inaccurate results. To resolve these issues, the low-field nuclear magnetic resonance (NMR) technology capable of directly detecting hydrogen nuclei in water, has been introduced in the field of petroleum and geotechnical engineering with successes. Even though low-field NMR has shown its great potentials in identifying and quantifying fluids of different constituents in geotechnical porous media, this technique has not been fully explored in investigating the state of water in clayey soils, and very limited works have been made to summarize the existing progresses. In this work, we conduct a systematical review on the application of low-field NMR in investigating the state of water in clayey soils. We first summarize practical strategies for optimizing acquisition parameters and measurement sequences. Next, we review the application of low-field NMR techniques in quantifying the content, detecting the migration, and tracking phase transition processes of water in clayey soils, with particular emphasis on how T1 and T2 relaxation times enable differentiation of adsorbed, capillary, and bulk water. We then discuss the advantages and limitations of current experimental methods. This paper finally provides recommendations for advancing the use of low-field NMR technology in clayey soils.
{"title":"A review of the low-field NMR technique for analyzing the state of water in clayey soils","authors":"Yingyao Qin, Liang Wang, Xiaolong Ma, Yong Wan, Rui Xu, Houzhen Wei","doi":"10.1007/s10064-025-04651-y","DOIUrl":"10.1007/s10064-025-04651-y","url":null,"abstract":"<div><p>The state of water and its transformation exert strong controls on the properties of soils, which has long been concerned in soil science and engineering practice. Under various environmental conditions, the water in soils may undergo dynamic migration and phase changes, for which conventional methods usually lack sufficient resolution or provide inaccurate results. To resolve these issues, the low-field nuclear magnetic resonance (NMR) technology capable of directly detecting hydrogen nuclei in water, has been introduced in the field of petroleum and geotechnical engineering with successes. Even though low-field NMR has shown its great potentials in identifying and quantifying fluids of different constituents in geotechnical porous media, this technique has not been fully explored in investigating the state of water in clayey soils, and very limited works have been made to summarize the existing progresses. In this work, we conduct a systematical review on the application of low-field NMR in investigating the state of water in clayey soils. We first summarize practical strategies for optimizing acquisition parameters and measurement sequences. Next, we review the application of low-field NMR techniques in quantifying the content, detecting the migration, and tracking phase transition processes of water in clayey soils, with particular emphasis on how <i>T</i><sub>1</sub> and <i>T</i><sub>2</sub> relaxation times enable differentiation of adsorbed, capillary, and bulk water. We then discuss the advantages and limitations of current experimental methods. This paper finally provides recommendations for advancing the use of low-field NMR technology in clayey soils.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145561757","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Characterizing rock hardness and abrasivity is essential for drill-bit design. However, intact cores are often unobtainable in complex formations and in extraterrestrial settings, precluding conventional laboratory determination of these indices. In this context, we develop models that relate hardness and abrasivity to mineral composition and microstructural parameters, and examine how these factors connect to mechanical behavior. The dataset comprises 64 rock samples with quartz and feldspar contents and grain sizes, together with hardness and abrasivity. The key advance is a fully automated workflow for microstructural quantification. Gray-level co-occurrence matrix (GLCM) texture features are extracted from thin-section images and then interpreted qualitatively to tie these statistics to grain size, surface condition, cleavage development, and fabric, thereby improving interpretability. Before feature extraction, histogram equalization enhances image texture. Correlation analysis reveals strong cross-orientation redundancy among texture metrics and significant correlations among quartz and feldspar contents and grain sizes, which supports feature reduction. For hardness prediction, support vector regression with a Gaussian kernel performs best. Quartz content is the dominant control, and adding physically meaningful texture measures such as contrast and energy significantly improves accuracy, and highlights the nonlinear microstructural effects. For abrasivity, a linear kernel is more suitable, reflecting a stronger linear dependence on mineral composition; quartz grain size is the primary control, followed by quartz and feldspar contents. Texture features add little to abrasivity prediction. Together, these results unite interpretable automated texture metrics with mineralogical information, clarify the differing controls on hardness and abrasivity, and offer guidance for bit design and engineering applications.
{"title":"Predictive modeling of rock hardness and abrasivity based on mineral composition and texture parameters","authors":"Zhenkun Wu, Hui Gao, Junping Li, Yule Hu, Songcheng Tan, Qian Li, Longchen Duan","doi":"10.1007/s10064-025-04650-z","DOIUrl":"10.1007/s10064-025-04650-z","url":null,"abstract":"<div><p>Characterizing rock hardness and abrasivity is essential for drill-bit design. However, intact cores are often unobtainable in complex formations and in extraterrestrial settings, precluding conventional laboratory determination of these indices. In this context, we develop models that relate hardness and abrasivity to mineral composition and microstructural parameters, and examine how these factors connect to mechanical behavior. The dataset comprises 64 rock samples with quartz and feldspar contents and grain sizes, together with hardness and abrasivity. The key advance is a fully automated workflow for microstructural quantification. Gray-level co-occurrence matrix (GLCM) texture features are extracted from thin-section images and then interpreted qualitatively to tie these statistics to grain size, surface condition, cleavage development, and fabric, thereby improving interpretability. Before feature extraction, histogram equalization enhances image texture. Correlation analysis reveals strong cross-orientation redundancy among texture metrics and significant correlations among quartz and feldspar contents and grain sizes, which supports feature reduction. For hardness prediction, support vector regression with a Gaussian kernel performs best. Quartz content is the dominant control, and adding physically meaningful texture measures such as contrast and energy significantly improves accuracy, and highlights the nonlinear microstructural effects. For abrasivity, a linear kernel is more suitable, reflecting a stronger linear dependence on mineral composition; quartz grain size is the primary control, followed by quartz and feldspar contents. Texture features add little to abrasivity prediction. Together, these results unite interpretable automated texture metrics with mineralogical information, clarify the differing controls on hardness and abrasivity, and offer guidance for bit design and engineering applications.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145561547","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Rigid and flexible boundary limits are two main types of boundary conditions used in subgrade construction, and they have significant effects on the deformation and settlement of foundation soil. In this paper, cube-triaxial compression tests were conducted on compacted loess under different compaction degrees using both rigid and flexible boundary conditions, and the resulting deformation differences of the compacted loess were studied. Additionally, the effects of lateral deformation of compacted loess under triaxial compression using these two boundary conditions on compaction degree, void ratio, and vertical strain and volume strain were analyzed. The relationship between vertical strain and volume strain was proposed, and the relationship between vertical strain and lateral strain was derived. The research results indicate that the deformation coordination ability of flexible constraints is greater than that of rigid constraints. These findings provide important theoretical reference and engineering application value for settlement calculation and maintenance of subgrade filling in loess areas.
{"title":"Study on the stress–strain behavior of loess by cube-triaxial compression with rigid and flexible boundary limits","authors":"Zhe Li, Yufeng Guo, Zhenguo Zhu, Shixin Lv, Lulu Liu, Jingjing Xia","doi":"10.1007/s10064-025-04567-7","DOIUrl":"10.1007/s10064-025-04567-7","url":null,"abstract":"<div><p>Rigid and flexible boundary limits are two main types of boundary conditions used in subgrade construction, and they have significant effects on the deformation and settlement of foundation soil. In this paper, cube-triaxial compression tests were conducted on compacted loess under different compaction degrees using both rigid and flexible boundary conditions, and the resulting deformation differences of the compacted loess were studied. Additionally, the effects of lateral deformation of compacted loess under triaxial compression using these two boundary conditions on compaction degree, void ratio, and vertical strain and volume strain were analyzed. The relationship between vertical strain and volume strain was proposed, and the relationship between vertical strain and lateral strain was derived. The research results indicate that the deformation coordination ability of flexible constraints is greater than that of rigid constraints. These findings provide important theoretical reference and engineering application value for settlement calculation and maintenance of subgrade filling in loess areas.</p></div>","PeriodicalId":500,"journal":{"name":"Bulletin of Engineering Geology and the Environment","volume":"84 12","pages":""},"PeriodicalIF":4.2,"publicationDate":"2025-11-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145561028","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}