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Effect of osmotic dehydration and gamma irradiation on quality characteristics of dried vegetable slices 渗透脱水和伽马辐照对干蔬菜片质量特性的影响
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-08 DOI: 10.1007/s11694-024-02869-0
Naglaa A. A. Hassan, Esraa A. M. Mousa, Khalid R. A. Elbassiony, Maha I.K. Ali

Osmotic drying is commonly utilized to create innovative products, as it can improve the sensory and nutritional qualities of the final products. The present study aims to investigate the effect of different osmotic solutions, including soaking in 1% citric acid, 10% NaCl, and a combination of 1% citric acid and 10% NaCl, as well as different doses of gamma irradiation (1 and 3 kGy), on the quality properties of dehydrated vegetable slices. The chemical composition, mineral content, Color measurement, texture profile, vitamin C levels, and sensory attributes were evaluated for dried vegetable slices. The findings showed that treating vegetable slices with a combination of 1% citric acid and 10% NaCl increased ash (3.43–4.34%), hardness, and total phenolic content (38.37–117.04 mg GAE/100 g). It was the most preferred by the panelists in sensory evaluation scores in comparison to the other treatments. Moreover, there were no significant differences in terms of chemical composition, mineral content, and texture profile analysis between irradiation doses of 1 and 3 kGy. Furthermore, samples irradiated at 1 kGy had significantly higher scores in sensory evaluation compared to both irradiated and unirradiated samples. The current study recommends treating vegetable slices with a combination of 1% citric acid and 10% NaCl before drying to enhance most of the quality attributes of the dried vegetable slices.

渗透性干燥通常被用来制作创新产品,因为它可以改善最终产品的感官和营养质量。本研究旨在探讨不同渗透溶液(包括在 1%柠檬酸、10%氯化钠和 1%柠檬酸与 10%氯化钠的混合溶液中浸泡)以及不同剂量的伽马射线照射(1 kGy 和 3 kGy)对脱水蔬菜片质量特性的影响。对脱水蔬菜片的化学成分、矿物质含量、色度测量、质地、维生素 C 含量和感官特性进行了评估。研究结果表明,用 1%柠檬酸和 10%氯化钠的组合处理蔬菜片可增加灰分(3.43%-4.34%)、硬度和总酚含量(38.37-117.04 毫克 GAE/100 克)。与其他处理相比,它在感官评价得分方面最受专家小组成员的青睐。此外,辐照剂量为 1 kGy 和 3 kGy 的样品在化学成分、矿物质含量和质地分析方面没有明显差异。此外,与辐照过和未辐照过的样品相比,辐照剂量为 1 kGy 的样品在感官评价中得分明显更高。目前的研究建议在烘干前用 1%柠檬酸和 10%氯化钠混合液处理蔬菜片,以提高干蔬菜片的大部分质量属性。
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引用次数: 0
Effect of physical field-assisted freezing on the quality attributes of frozen baked sweet potato and its optimization 物理现场辅助冷冻对冷冻烤红薯质量属性的影响及其优化
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-08 DOI: 10.1007/s11694-024-02902-2
Yi Zhang, Ruixue Yue, Hong Zhu, Wenting Zhang, Chen Ma, Shaoying Deng, Jian Sun

Freezing plays a crucial role in ensuring the safety of foods over long storage periods. However, ice crystals within the cells can cause irreversible damages to tissue structures during the freezing process, resulting a significant problem on the quality. The present study aimed to investigate the effects of physical field-assisted freezing on the quality attributes of frozen baked sweet potato and identify the optimum operational parameters of quick-frozen process. Combination of magnetic field and ultrasound suggested the best results, with a 58.33% reduction in freezing time, 59.63% reduction in thawing loss, compared to IF. The hardness and the signal values of Sweetness and W2W of CF were 58.90%, 20.03%, and 27.07% higher than those of IF, which showed that CF have better maintenance of sample quality. Low field-nuclear magnetic resonance results showed that CF caused a decrease in the proportion of free water and an increase in the proportion of immobile water, and the water status are more similar to FB. Microscopic observations confirmed that the CF had the smallest and the most evenly distribution of ice crystals. Optimization of frozen baked sweet potato via response surface methodology, which revealed that the optimal conditions included a magnetic field intensity of 30 mT, an ultrasonic intensity of 320 W, and an ultrasonic time of 10 s. Therefore, treatment of combination with magnetic field and ultrasound is a promising novel method to improve the quality of frozen foods.

冷冻在确保食品长期储存的安全性方面发挥着至关重要的作用。然而,在冷冻过程中,细胞内的冰晶会对组织结构造成不可逆的破坏,从而导致严重的质量问题。本研究旨在探讨物理场辅助冷冻对冷冻烤红薯质量属性的影响,并确定速冻过程的最佳操作参数。与中频相比,磁场和超声波的组合效果最佳,冷冻时间缩短了 58.33%,解冻损失减少了 59.63%。CF 的硬度、甜度和 W2W 信号值分别比 IF 高 58.90%、20.03% 和 27.07%,这表明 CF 能更好地保持样品质量。低场核磁共振结果表明,CF 使游离水比例下降,固定水比例上升,水状态与 FB 更为相似。显微观察证实,CF 的冰晶最小且分布最均匀。通过响应面方法对冷冻烤红薯进行优化,发现最佳条件包括磁场强度 30 mT、超声波强度 320 W 和超声波时间 10 s。
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引用次数: 0
Sustainable use of coffee roasting by-products: development of high value-added gummy candies 咖啡烘焙副产品的可持续利用:开发高附加值软糖
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-08 DOI: 10.1007/s11694-024-02898-9
Miriam Arianna Boninsegna, Iolanda Cilea, Amalia Piscopo, Alessandra De Bruno, Marco Poiana

The sustainable utilization of production wastes in the agri-food sector is an increasing challenge. This work aims to evaluate the applicability of coffee silverskin, the main by-product of coffee roasting, in the formulation of gummy candies. Firstly, the experimental plan envisaged the extraction and characterization of bioactive compounds from coffee silverskin. The influence of different concentrations of coffee silverskin extract (1%, 2%, and 4%) was then evaluated on chemical, physical, microbiological, structural, and sensory gummy candies characteristics for 120 storage days. Candies formulated without coffee silverskin extract were used as control. The results up to 120 days of storage revealed the higher quality of gummy candies enriched with 1%, 2% and 4% coffee silverskin extract not only for their bioactive content, ranging from 147.9 to 161.1 mg GAE Kg -1 of phenolic compounds, but also for their antioxidant activity, with values at the end of storage of 15.06, 30.25, 31.50 and 28.20 µmol TE g-1 respectively in control and gummy candies enriched with 1%, 2% and 4% coffee silverskin extract. Moreover, all the candies enriched with silverskin coffee extract showed better physical and sensory characteristics compared to the control taste. The results show that the proposed use of silver coffee skin improves and preserves the quality of gummy candies and then be employed as an ingredient to improve the quality of confectionery products.

农业食品行业对生产废弃物的可持续利用是一项日益严峻的挑战。这项工作旨在评估咖啡烘焙的主要副产品--咖啡银皮在软糖配方中的适用性。首先,实验计划设想从咖啡银皮中提取生物活性化合物并确定其特征。然后评估了不同浓度的咖啡银皮提取物(1%、2% 和 4%)在 120 天储存期内对软糖的化学、物理、微生物、结构和感官特性的影响。不含咖啡银皮提取物的糖果作为对照。贮藏 120 天的结果表明,富含 1%、2% 和 4% 咖啡银皮提取物的软糖质量更高,不仅生物活性含量更高(酚类化合物的 GAE 为 147.9 至 161.1 毫克 GAE Kg -1 不等),而且抗氧化活性更高(贮藏结束时,对照组和富含 1%、2% 和 4% 咖啡银皮提取物的软糖的抗氧化活性值分别为 15.06、30.25、31.50 和 28.20 µmol TE g-1)。此外,与对照组相比,所有添加了银皮咖啡提取物的糖果都具有更好的物理和感官特性。结果表明,建议使用的咖啡银皮可改善和保持软糖的质量,并可用作提高糖果产品质量的配料。
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引用次数: 0
Measurement and comparison of quality characteristics, bioactivity of marmalades produced with wild Rosa and Berberis fruit species 测量和比较用野生蔷薇和小檗果实制作的橘子酱的质量特性和生物活性
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-08 DOI: 10.1007/s11694-024-02899-8
Mehmet Ali Salık

In this study, the physicochemical, color, bioactive and sensory properties of marmalades wild red rosehip (Rosa canina L.), black rosehip (Rosa pimpinellifolia L.), red barberry (Berberis vulgaris L.) and purple barberry (Berberis crataegina DC.) fruits were investigated. The differences among the samples in terms of pH, titration acidity, dry matter, ash, protein, reducing sugar contents, sucrose, total sugars, calories, L*, a*, b*, , C*, BI and ∆E were found to be statistically significant (p < 0.01). Marmalade samples have a characteristic color and taste. The highest protein content was detected in the marmalade samples produced from barberry fruits (2.44–3.28%). The total phenolic content (TPC), total flavonoid content (TFC), total monomeric anthocyanin (TMA) content and total antioxidant capacity (DPPH•, CUPRAC and FRAP) of the marmalades ranged from 12.07 to 28.95 mg GAE/g, 12.01–38.51 mg QE/g, 7.43-331.97 mg Cyn-3-glu/100 g, 7.36–17.85 mg TE/g, 33.56–85.40 mg TE/g and 9.96–25.87 mg TE/g, respectively (p < 0.01). Among the fruit species examined, the marmalade samples prepared from black rosehip and purple barberry were richer in bioactive compounds and exhibited high antioxidant capacity. All samples scored between 6.0 and 8.2 for sensory parameters (p < 0.01). The order of general acceptability of the marmalades was red rosehip > black rosehip > red barberry > purple barberry. Overall, the results highlighted the potential of using these wild fruits as a potentially rich source of bioactive compounds for marmalade manufacturing.

Graphical abstract

本研究调查了野生红玫瑰果(Rosa canina L.)、黑玫瑰果(Rosa pimpinellifolia L.)、红小檗(Berberis vulgaris L.)和紫小檗(Berberis crataegina DC.)果实果酱的理化、颜色、生物活性和感官特性。结果发现,各样品在 pH 值、滴定酸度、干物质、灰分、蛋白质、还原糖含量、蔗糖、总糖、热量、L*、a*、b*、H°、C*、BI 和 ∆E 方面的差异均有统计学意义(p < 0.01)。橘子酱样品具有独特的颜色和味道。巴旦木果实制成的橘子酱样品蛋白质含量最高(2.44%-3.28%)。橘子酱的总酚含量(TPC)、总黄酮含量(TFC)、总单体花青素含量(TMA)和总抗氧化能力(DPPH-、CUPRAC 和 FRAP)在 12.07 至 28.95 毫克 GAE 之间。分别为 12.07 至 28.95 毫克 GAE/克、12.01-38.51 毫克 QE/克、7.43-331.97 毫克 Cyn-3-glu/100克、7.36-17.85 毫克 TE/克、33.56-85.40 毫克 TE/克和 9.96-25.87 毫克 TE/克(p < 0.01)。在检测的水果种类中,黑玫瑰果和紫刺莓制备的橘子酱样品含有更丰富的生物活性化合物,并表现出较高的抗氧化能力。所有样品的感官参数得分都在 6.0 和 8.2 之间(p < 0.01)。橘子酱的总体可接受性依次为红玫瑰果酱、黑玫瑰果酱、红刺莓酱和紫刺莓酱。总之,研究结果凸显了利用这些野生水果作为生物活性化合物的潜在丰富来源来制造橘子酱的潜力。 图文摘要
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引用次数: 0
A bilayer emulsion containing encapsulated catfish oil, stabilized with whey protein isolates and fish gelatin for development of PUFA rich mayonnaise 一种双层乳液,含有包裹的鲶鱼油,并用乳清蛋白分离物和鱼类明胶进行稳定,用于开发富含 PUFA 的蛋黄酱
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-07 DOI: 10.1007/s11694-024-02872-5
Jaydeep Dave, Vikas Kumar, Passakorn Kingwascharapong, Ali Muhammed Moula Ali, Sri Charan Bindu Bavisetty

This study investigated the impact of sequential deposition of whey protein isolate (WPI) and fish gelatin (FG) on primary o/w emulsions containing 5% catfish oil at concentrations of 0.1–0.75%. Initially, the emulsions were stabilized using 0.5% FG and WPI. The study also examined the influence of sequentially depositing WPI and FG within the emulsions on various parameters, such as stability, particle size, viscosity, electronegativity, and oxidative stability of bilayer fish oil emulsions. It was observed that the particle size increased significantly when FG was deposited onto the primary WPI emulsion, from 0.57 to 1.61 μm. Furthermore, this process increased the apparent viscosity of the emulsion while reducing its droplet charge from − 24.93 to -12.17 mV. Conversely, depositing WPI onto the primary FG emulsion led to a reduction in the particle size and a slight increase in both electronegativity and viscosity. Concerning oxidative stability, a bilayer emulsion consisting of 0.5% WPI and 0.75% FG showed the lowest levels (hexanal concentration: 0.32 ppm) of oxidation after 21 days of storage. The mayonnaise fortified with a 20% bilayer emulsion consisting of 0.5% WPI and 0.75% FG exhibited rheological and microstructural properties comparable to those of commercial mayonnaise. Moreover, the fortification of mayonnaise with emulsified fish oil enhanced the fatty acid profile by increasing Polyunsaturated fatty acids (PUFA) and reducing Saturated fatty acids (SFA).

本研究调查了连续沉积乳清蛋白分离物(WPI)和鱼明胶(FG)对浓度为 0.1-0.75% 的含 5%鲶鱼油的初级水包油型乳液的影响。乳液最初使用 0.5% 的 FG 和 WPI 进行稳定。研究还考察了在乳液中依次沉积 WPI 和 FG 对双层鱼油乳液的稳定性、粒度、粘度、电负性和氧化稳定性等各种参数的影响。研究发现,在初级 WPI 乳液中沉积 FG 后,粒径明显增大,从 0.57 μm 增大到 1.61 μm。此外,这一过程还增加了乳液的表观粘度,同时将其液滴电荷从 - 24.93 mV 降至 -12.17 mV。相反,在原生 FG 乳液上沉积 WPI 会导致粒径减小,电负性和粘度略有增加。在氧化稳定性方面,由 0.5% WPI 和 0.75% FG 组成的双层乳液在储存 21 天后氧化程度最低(己醛浓度:0.32 ppm)。添加了由 0.5% WPI 和 0.75% FG 组成的 20% 双层乳液的蛋黄酱,其流变学和微观结构特性与商用蛋黄酱相当。此外,在蛋黄酱中添加乳化鱼油还能增加多不饱和脂肪酸(PUFA),减少饱和脂肪酸(SFA),从而改善蛋黄酱的脂肪酸组成。
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引用次数: 0
Optimization of ultrasonication-assisted enzymatic extraction of Kangra orthodox black tea for the development of low-calorie ready-to-drink tea 为开发低热量即饮茶优化超声波辅助酶解康拉正宗红茶提取工艺
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-05 DOI: 10.1007/s11694-024-02891-2
Chahat Thakur, Manisha Kaushal, Devina Vaidya, Anil Kumar Verma, Anil Gupta

The quest for healthier beverage options has led to the development of low-calorie alternatives to conventional sugary drinks. This study focused on the use of ultrasonication-enzymatic extraction to produce a low-calorie ready-to-drink Kangra orthodox black tea with the natural sweetener Stevia rebaudiana. By employing sonication time (9 to 45 min) and temperature (35 to 55 °C) as independent variables, statistical analysis revealed significant effects of these parameters on key quality indicators. In the ultrasonicated-assisted enzymatic extraction, the optimal conditions were 27.58 min at 45.06 °C with 0.0095% Tannase, to maximize the water extract content, total phenolic content, antioxidant capacity, caffeine, tannins content, colour, theaflavins, thearubigins, total colour, brightness, a*, b* colour value and overall acceptability and to minimize the pH, tea cream, and colour value L* of the ultrasonicated-assisted enzymatic extraction of Kangra orthodox black tea. The predicted water extract was 47.69%, the total phenolic content was 233.77 µg GAE/100 mL, the antioxidant capacity was 78.50 mM TE/mL, caffeine was 35.30 µg CAE/100 mL, tannins were 167.14 µg TAE/100 mL, theaflavins were 0.88%, thearubigins were 8.49%, the total colour percentage was 9.22%, the brightness was 14.98%, a* was 5.02, b* was 8.88, the overall acceptability was 8.14, the pH was 5.61, tea cream was 0.36 g/100 mL, and the L* colour value was 23.66 under optimum ultrasonication-assisted enzymatic extraction conditions. To improve the overall palatability of the Kangra Orthodox ready-to-drink tea, sugar (7–11° Brix) was utilized to balance the taste. The optimal sugar concentration for ready-to-drink Kangra orthodox tea based on a sensory score of 10° Brix was the highest. The substitution of sucrose with stevia up to 60% led to an equi-sweet taste eliminating any characteristic bitter aftertaste, in addition to a substantial decline in energy value from 31.44 to 15.72 kcal/100 g. A low-calorie Kangra Orthodox ready-to-drink tea beverage was developed that contained a high level of functional compounds at a reduced energy level. This tea offers a healthy alternative to traditional sweetened beverages and is potentially appealing to a broad market of health-conscious consumers.

对健康饮料的追求促使人们开发低热量饮料来替代传统的含糖饮料。本研究的重点是利用超声波酶解萃取技术生产添加了天然甜味剂甜叶菊的低热量即饮康拉正宗红茶。通过采用超声时间(9 至 45 分钟)和温度(35 至 55 °C)作为自变量,统计分析显示这些参数对关键质量指标有显著影响。在超声辅助酶提取中,最佳条件是在 45.06 °C、27.58 分钟和 0.0095%的单宁酶,使康格拉正山小种红茶的水提取物含量、总酚含量、抗氧化能力、咖啡碱、单宁含量、色泽、茶黄素、茶红素、总色泽、亮度、a*、b*色值和总体可接受性最大化,pH值、茶膏和色值L*最小化。预测的水提取率为 47.69%,总酚含量为 233.77 µg GAE/100 mL,抗氧化能力为 78.50 mM TE/mL,咖啡因为 35.30 µg CAE/100 mL,单宁酸为 167.14 µg TAE/100 mL,茶黄素为 0.88%,茶红素为 8.在最佳超声波辅助酶解提取条件下,总色度为 9.22%,白度为 14.98%,a*为 5.02,b*为 8.88,总体可接受性为 8.14,pH 为 5.61,茶膏为 0.36 克/100 毫升,L*色值为 23.66。为了提高 Kangra Orthodox 即饮茶的整体口感,使用了糖(7-11° Brix)来平衡口感。根据 10° Brix 的感官评分,Kangra 正宗即饮茶的最佳糖浓度最高。用甜菊糖替代蔗糖(最高达 60%)后,口感等同于甜味,没有任何特有的苦涩回味,能量值也从 31.44 千卡/100 克大幅降至 15.72 千卡/100 克。这种茶为传统的甜饮料提供了一种健康的替代品,对具有健康意识的广大消费者具有潜在的吸引力。
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引用次数: 0
Innovative fluorescent aptasensor for sensitive tropomyosin detection in shrimp products using DNA-templated silver nanoclusters and catalytic hairpin assembly 利用 DNA 示踪银纳米簇和催化发夹组装创新型荧光诱导传感器灵敏检测虾产品中的肌球蛋白
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-05 DOI: 10.1007/s11694-024-02871-6
Jun-Hu Cheng, Xinxue Zhang, Ji Ma, Da-Wen Sun

Tropomyosin (TM), the major allergen in shellfish, is a common protein cause of allergenic diseases, hence a sensitive, efficient method for TM detection is urgently needed to protect allergy sufferers in food products. In this work, a novel fluorescent aptasensor for TM-sensitive detection based on DNA-templated silver nanoclusters (AgNCs) and catalytic hairpin assembly (CHA) was designed. With the rapid separation and enrichment of magnetic beads, the detection of TM was converted to the detection of cDNA (complementary DNA). Then the cDNA was utilized as the initiator to successfully trigger the CHA amplification technique, which ultimately formed double-stranded to induce high fluorescence signals by AgNCs. Specifically, the cDNA could trigger repeated cycles, which enabled signal amplification and enhanced aptasensor performance with an excellent linear relationship in a wide linear range from 0.1 to 50 μg/mL (R2 = 0.9967) and a desirable low detection limit of 0.0179 μg/mL. It is worth noting that the method was successfully validated with high specificity and stability for detecting processed shrimp products, implying great potential in the field of allergen assay.

贝类中的主要过敏原肌球蛋白(TM)是导致过敏性疾病的常见蛋白质,因此迫切需要一种灵敏、高效的 TM 检测方法来保护食品过敏患者。在这项研究中,我们设计了一种基于DNA模板银纳米簇(AgNCs)和催化发夹组装(CHA)的新型荧光诱导传感器,用于TM的灵敏检测。通过磁珠的快速分离和富集,TM 的检测被转换为 cDNA(互补 DNA)的检测。然后利用 cDNA 作为启动子,成功触发 CHA 扩增技术,最终形成双链,诱导 AgNCs 发出高荧光信号。具体来说,cDNA 可触发重复循环,从而实现信号放大,提高了灵敏度,在 0.1 至 50 μg/mL 的宽线性范围内具有极佳的线性关系(R2 = 0.9967),检出限低至 0.0179 μg/mL。值得注意的是,该方法成功地验证了其在检测加工虾产品方面的高特异性和稳定性,这意味着该方法在过敏原检测领域具有巨大的潜力。
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引用次数: 0
Analysis of volatile compounds of ginger (Zingiber officinale) during far-infrared combined with hot-air drying by GC-MS and MOS e-nose 利用 GC-MS 和 MOS 电子鼻分析生姜(Zingiber officinale)在远红外结合热风干燥过程中的挥发性化合物
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-04 DOI: 10.1007/s11694-024-02843-w
Yongsheng Pei, Changzhi Wang, Lin Fan, Guizhong Tian, Shiyuan Miao, Xiangyi Meng, Zhenfeng Li, Wanxiu Xu

In this study, ginger slices were dehydrated through a combination of far-infrared radiation and hot-air drying (FIR-HAD). The changes in volatile composition were subsequently identified using gas chromatography-mass spectrometry (GC-MS) and metal oxide semiconductor electronic nose (MOS e-nose). The GC-MS analysis revealed that terpenes comprised over 75% of volatile compounds in all examined samples, with zingiberene, β-sesquiphellandrene, and (E, E)-α-farnesene being the dominant constituents. Fresh ginger contained a higher relative proportion compared to dried samples. After FIR-HAD treatment, the terpene levels decreased by 11.9%, 8.9%, 13.7%, and 18.2% at 50 °C, 60 °C, 70 °C, and 80 °C, respectively. Among the various drying conditions, ginger subjected to FIR-HAD at 60 °C displayed the highest concentrations of volatile compounds and exhibited flavor characteristics closest to those of fresh samples. The flavor profiles were further evaluated using MOS e-nose analysis. The terpene compounds demonstrated a strong correlation with the response values of W1W and W2W sensors according to partial least squares regression models. In addition, the concentrations of 6-gingerol, 8-gingerol, and 10-gingerol in ginger exposed to FIR-HAD at 60 °C were also higher compared to other drying conditions. This indicated that the FIR-HAD at 60 °C is more suitable for producing dried ginger with remaining flavor attributes. These findings offer theoretical insights into the changes in volatile compounds of ginger slices during the FIR-HAD procedure. They also highlight the potential for improving drying efficiency through aroma online control techniques in future research.

在这项研究中,生姜片通过远红外辐射和热风干燥(FIR-HAD)相结合的方法进行脱水。随后使用气相色谱-质谱联用仪(GC-MS)和金属氧化物半导体电子鼻(MOS e-nose)对挥发性成分的变化进行了鉴定。气相色谱-质谱分析表明,在所有检测样品中,萜烯类化合物占挥发性化合物的 75% 以上,其中最主要的成分是辛夷烯、β-鞘氨醇和(E,E)-α-法呢烯。与干燥样品相比,新鲜生姜中的相对比例更高。经过 FIR-HAD 处理后,萜烯含量在 50 ℃、60 ℃、70 ℃ 和 80 ℃ 下分别降低了 11.9%、8.9%、13.7% 和 18.2%。在不同的干燥条件下,60 °C的FIR-HAD条件下生姜的挥发性化合物浓度最高,风味特征最接近新鲜样品。使用 MOS 电子鼻分析法对风味特征进行了进一步评估。根据偏最小二乘法回归模型,萜烯化合物与 W1W 和 W2W 传感器的响应值有很强的相关性。此外,与其他干燥条件相比,在 60 °C的FIR-HAD条件下,生姜中6-姜酚、8-姜酚和10-姜酚的浓度也更高。这表明,60 °C下的FIR-HAD更适于生产具有其余风味特性的干姜。这些发现从理论上揭示了 FIR-HAD 过程中生姜片挥发性化合物的变化。它们还强调了在未来研究中通过香气在线控制技术提高干燥效率的潜力。
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引用次数: 0
Optimization of lycopene extraction from tomato processing by-products with essential oils and effect of extract on oxidative stability of refined olive oil 用精油优化番茄加工副产品中番茄红素的提取,以及提取物对精炼橄榄油氧化稳定性的影响
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-03 DOI: 10.1007/s11694-024-02888-x
Hajar El Basett, Hassan Hajjaj

Lycopene, a lipophilic antioxidant, was extracted from a Moroccan industrial tomato peels by-product using essential oils (EOs) as eco-friendly solvents. Peppermint essential oil (PEO), rosemary essential oil (REO), verbena essential oil (VEO), and thyme essential oil (TEO) were used as solvents. The highest extraction yield was obtained with REO. Response surface methodology (RSM) combined with a Box-Behnken design was used to maximize the extraction yield of lycopene. Optimal conditions were determined as follows: a solvent-to-material ratio of 35:1 (mL/g), a time of 60 min and a temperature of 60 °C. As a plant-based antioxidant, the lycopene extract was added to refined olive oil (ROO) to evaluate its oxidative stability during 5 months of storage at 40 °C. ROO enriched with lycopene extract at a concentration of 1 mg/g showed the lowest degree of oxidation, as evidenced by the lowest values of peroxide value, p-anisidine value, total oxidation value, free acidity, and specific extinction coefficients K232 and K270, compared to ROO containing 0.5 mg/g of lycopene extract and ROO containing 0.2 mg/g of BHA + BHT. The results of this study demonstrate that EOs are effective solvents for producing a value-added lycopene extract that can be an effective alternative to synthetic antioxidants. The study also highlights the synergistic effect of lycopene extract on ROO oxidation stability, shelf life and nutritional value.

以精油(EO)为环保溶剂,从摩洛哥工业番茄皮副产品中提取了亲脂性抗氧化剂番茄红素。溶剂包括薄荷精油(PEO)、迷迭香精油(REO)、马鞭草精油(VEO)和百里香精油(TEO)。REO 的萃取率最高。为了最大限度地提高番茄红素的萃取率,采用了响应面法(RSM)与箱型贝肯设计相结合的方法。最佳条件确定如下:溶剂与材料的比例为 35:1(毫升/克),时间为 60 分钟,温度为 60 °C。作为一种植物抗氧化剂,番茄红素提取物被添加到精炼橄榄油(ROO)中,以评估其在 40 °C 下储存 5 个月期间的氧化稳定性。与含有 0.5 毫克/克番茄红素提取物的 ROO 和含有 0.2 毫克/克 BHA + BHT 的 ROO 相比,富含 1 毫克/克番茄红素提取物的 ROO 的氧化程度最低,过氧化值、对甲氧基苯胺值、总氧化值、游离酸度以及特定消光系数 K232 和 K270 的值都最低。这项研究结果表明,环氧乙烷是生产高附加值番茄红素提取物的有效溶剂,可以有效替代合成抗氧化剂。该研究还强调了番茄红素提取物对 ROO 氧化稳定性、保质期和营养价值的协同作用。
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引用次数: 0
Adhesion of Escherichia coli O157:H7 during freezing-induced sublethal injury and recovery on stainless steel and lettuce 大肠埃希氏菌 O157:H7 在冷冻引起的亚致死性损伤和恢复过程中在不锈钢和莴苣上的附着情况
IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-10-03 DOI: 10.1007/s11694-024-02868-1
Yujun Zhai, Ru Zhang, Siyuan Zhou, Hui Shi

Freezing as an effective approach for food storage is commonly used in food industry. Notably, Escherichia coli O157:H7 can survive in a sublethally injured state after freezing and recover under suitable conditions, which is a great threat. This research was to investigate changes and mechanism in adhesion of sublethally injured E. coli O157:H7 during freezing and recovery. Adhesion on stainless steel or lettuce surface showed an increase after 16 h-freezing with sublethal ratio of more than 99%. Adhesion recovered to untreated level in recovery on lettuce while didn’t recover on stainless steel. Motility decreased as freezing time increasing, reached minimum after 12 h-freezing and didn’t repair to untreated level after recovery. Extracellular polymeric substances production and carbohydrate to protein ratio both reached minimum after 4 h-freezing and then increased in freezing-induced sublethally injured state. No significant change of LPS structural feature or gene expression was observed during injury and recovery. Besides, the expressions of flagella, pili and EPS related genes were all down-regulated during freezing while were up-regulated in recovery. The results revealed adhesion behavior of freezing-induced sublethally injured E. coli O157:H7, which provided theoretical basis to bacterial prevention.

冷冻作为一种有效的食品储存方法,在食品工业中被普遍使用。值得注意的是,O157:H7 型大肠杆菌在冷冻后可在亚肺损伤状态下存活,并在适当条件下恢复,这对食品安全构成了极大威胁。本研究旨在探究在冷冻和恢复过程中,亚低温损伤大肠杆菌 O157:H7 的粘附变化和机制。经过 16 小时冷冻后,大肠杆菌在不锈钢或莴苣表面的附着力增加,亚致死率超过 99%。莴苣表面的附着力在恢复过程中恢复到未处理的水平,而不锈钢表面的附着力则没有恢复。运动能力随着冷冻时间的延长而下降,在冷冻 12 小时后达到最低水平,恢复后也没有恢复到未处理水平。细胞外高分子物质的产生和碳水化合物与蛋白质的比例均在冷冻 4 小时后达到最低值,然后在冷冻诱导的亚低温损伤状态下增加。在损伤和恢复过程中,未观察到 LPS 结构特征和基因表达的明显变化。此外,鞭毛、纤毛和 EPS 相关基因的表达均在冷冻过程中下调,而在恢复过程中上调。研究结果揭示了冷冻诱导的亚低温损伤大肠杆菌O157:H7的粘附行为,为细菌预防提供了理论依据。
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引用次数: 0
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Journal of Food Measurement and Characterization
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