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A new Approach for Qualitative Proficiency Testing Assessment Based on Homogeneity Proportion Tests 基于同质性比例测验的定性能力测试评价新方法
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-27 DOI: 10.1007/s12647-025-00835-9
Luiz Henrique da Conceição Leal, Werickson Fortunato de Carvalho Rocha

In qualitative proficiency testing schemes, the participants’ results are categorical classifications of test items. In this case, the goal is to assess the percentage of test items correctly classified as the provider’s expected result. The ISO 13528 international standard does not provide a detailed description of statistical methods for categorical data analysis. This work proposes a novel approach to assessing laboratories’ performance in qualitative proficiency testing based on homogeneity proportion tests. Overall and pairwise homogeneity proportion tests identify atypical percentage among the participating laboratories. In this approach, the outlying percentage is unacceptable. This methodology was compared with three agreement measures: Cohen’s Kappa, Krippendorff’s alpha, and Gwet’s gamma. Preliminary results indicate that the number of test items sent to each participant may influence the performance evaluation of the participants.

在定性能力测试方案中,参与者的结果是对测试项目的分类。在这种情况下,目标是评估被正确分类为提供者预期结果的测试项的百分比。ISO 13528国际标准没有提供分类数据分析的统计方法的详细描述。本文提出了一种基于同质性比例测试的实验室定性能力评估方法。总体和两两同质性比例测试确定参与实验室的非典型百分比。在这种方法中,外围百分比是不可接受的。该方法与三种一致性度量进行了比较:Cohen的Kappa, Krippendorff的alpha和Gwet的gamma。初步结果表明,发送给每个参与者的测试项目数量可能会影响参与者的绩效评估。
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引用次数: 0
Research on Material Outgassing Measurement System with an In-Situ Calibration 基于原位校准的材料放气测量系统研究
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-24 DOI: 10.1007/s12647-025-00828-8
Yan Luo, Wenyu Lin, Kuibo Wang, Xiaobin Wu, Xudi Wang

To ensure the accuracy of output data, it is essential to calibrate the material outgassing test device regularly. This study first established a set of micro-flow intake systems based on the new standard leak element and then researched an in-situ calibration method for the outgassing system. High-purity nitrogen, argon, and helium were introduced through the micro-flow intake system to the outgassing system to calibrate the vacuum gauge, Quadrupole Mass Spectrometer (QMS), and outgassing amount online. The calibration pressure for the gauge ranged from 10–4 to 10–2 Pa, while that for QMS was between 10–4 and 10–3 Pa. The calibration range of outgassing amount varied among 10–6 Pa m3/s, 10–5 Pa m3/s and 10–4 Pa m3/s. The results showed good linearity and repeatability in calibrations of gauge and outgassing amounts. Additionally, sensitivities, pressure and outgassing correction factors were obtained for each gas type. It was found that the correction factor of pressure is consistent with that of outgassing; moreover, sensitivities of separation gauge and QMS depended on gas type, leading to different correction factors and sensitivities for each gas. Using this in-situ calibrated outgassing system enabled measurement of electron-induced outgassing characteristics of polymethyl methacrylate. The results demonstrate the operability and traceability of the material outgassing test system with in-situ calibration used in the study.

为了保证输出数据的准确性,必须定期对放气试验装置进行校准。本研究首先建立了一套基于新标准泄漏元件的微流进气系统,然后研究了放气系统的原位标定方法。通过微流进气系统将高纯氮气、氩气和氦气引入放气系统,在线校准真空计、四极杆质谱仪(QMS)和放气量。量规的校准压力范围为10-4 ~ 10-2 Pa, QMS的校准压力范围为10-4 ~ 10-3 Pa。放气量标定范围为10-6 Pa m3/s、10-5 Pa m3/s和10-4 Pa m3/s。结果表明,在量规和放气量的校准中具有良好的线性和重复性。此外,还获得了每种气体类型的灵敏度、压力和放气校正系数。结果表明,压力校正系数与放气校正系数基本一致;此外,分离规和质量管理体系的灵敏度取决于气体类型,导致每种气体的校正因子和灵敏度不同。使用这种原位校准放气系统,可以测量聚甲基丙烯酸甲酯的电子诱导放气特性。实验结果表明,采用原位标定的材料放气测试系统具有良好的可操作性和可追溯性。
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引用次数: 0
Research on Metrological Detection Device for Ultrasonic Sensor for Evaporation Measurement 超声波蒸发测量传感器计量检测装置的研究
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-23 DOI: 10.1007/s12647-025-00824-y
Taocheng Zhou, Mingming Wei, Xingwang Chen, Yang Zeng, Debing Zheng

In order to enhance the quality of evaporation data, research has been conducted on the metrology of ultrasonic evaporation sensors. By analyzing the principles underlying ultrasonic sensors and their metrological characteristics, this study focuses on the development of metrological detection devices for ultrasonic evaporation sensors. The hardware design incorporates an enhanced voltage measurement circuit along with touch display components, utilizing low-temperature drift high-precision resistors to ensure a stable resistance environment. The software employs the C# programming language to facilitate the acquisition, transmission, processing, and display of data, and incorporates the digital multimeter data monitoring channel. A comparison test was conducted between the experimental points (0, 60 and 98.1 mm), the measurement results of the metrological testing device, and the standard method (galvanometry) of the maximum difference of 0.0006 mm. The Guide to the Expression of Uncertainty in Measurement (GUM) method was utilized to evaluate the results. The uncertainty associated with the current measurement technique and the measurement outcomes of this device were assessed using the GUM method, yielding U = 0.058 mm (with a coverage factor k = 2) and U = 0.029 mm (with a coverage factor k = 2), respectively. The study demonstrated that the device operated correctly, with measurement data showing high agreement with the flow measurement method. The uncertainty of the device was approximately half that of the flow measurement method, resulting in higher quality measurement data.

为了提高蒸发数据的质量,对超声蒸发传感器的计量进行了研究。本文在分析超声蒸发传感器原理及其计量特性的基础上,重点研究了超声蒸发传感器计量检测装置的研制。硬件设计结合了增强型电压测量电路以及触摸显示组件,利用低温漂移高精度电阻确保稳定的电阻环境。软件采用c#编程语言,便于数据的采集、传输、处理和显示,并结合数字万用表数据监控通道。将实验点(0、60、98.1 mm)、计量测试装置的测量结果与最大差值为0.0006 mm的标准方法(振镜法)进行对比试验。采用测量不确定度表达指南(GUM)方法对结果进行评价。使用GUM方法评估与当前测量技术相关的不确定度和该装置的测量结果,分别产生U = 0.058 mm(覆盖因子k = 2)和U = 0.029 mm(覆盖因子k = 2)。研究表明,该装置运行正确,测量数据与流量测量方法高度吻合。该装置的不确定度约为流量测量方法的一半,从而获得更高质量的测量数据。
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引用次数: 0
Measurement and Evaluation of Sound Absorption Characteristics of Auditorium and Office Seats for Prioritizing Efficacious Acoustics in Auditoriums, Halls and Meeting Rooms 礼堂和办公室座椅吸声特性的测量与评价,以优先考虑礼堂、大厅和会议室的有效声学
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-09 DOI: 10.1007/s12647-025-00829-7
C. Gautam, N. Garg, A. Devi, S. Bhatia

The study intends to measure the sound absorption characteristics of auditoriums and office seats, aiming to comprehend and compare their acoustic performance. Paper explores specific design factors affecting sound absorption characteristics, including material composition, arrangement, and overall seat configuration. Compact seating is favoured over traditional layouts, emphasizing the importance of minimizing high-frequency noise. The study focuses on the acoustic implications of compact seat arrangements, examining factors such as the seat dip effect, high-frequency reduction strategies, spacing and density, rectangular arrangements, P/A (perimeter/area) ratio, and airgap. The comprehensive exploration of these parameters aims to provide insights into designing spaces with optimized acoustic qualities, particularly in environments with compact seating arrangements. The P/A method is recommended for predicting auditoriums and office seats absorption. It involves extrapolating from measurements in a reverberation chamber with varying P/A values, to estimate absorption in larger samples with lower P/A ratios found in typical closed spaces. The findings contribute in formulating the guidelines for architects and designers, enabling the design of spaces that emphasize optimal acoustics for various purposes, from large-scale auditoriums to professional office environments. The study also reports the measurement uncertainty in evaluation of sound absorption coefficient of auditorium and office seats in the reverberation chamber.

本研究旨在测量礼堂和办公座椅的吸声特性,了解和比较它们的声学性能。本文探讨了影响吸声特性的具体设计因素,包括材料成分、排列方式和座椅整体配置。紧凑的座位比传统布局更受青睐,强调了最小化高频噪音的重要性。该研究的重点是紧凑型座椅布局的声学影响,考察了座椅倾斜效应、高频降低策略、间距和密度、矩形布局、P/A(周长/面积)比和气隙等因素。对这些参数的全面探索旨在为优化声学质量的空间设计提供见解,特别是在紧凑座位安排的环境中。建议采用P/A法预测礼堂和办公室座位的吸收量。它涉及从具有不同P/ a值的混响室的测量中推断,以估计在典型封闭空间中具有较低P/ a比的较大样品的吸收。研究结果有助于为建筑师和设计师制定指导方针,使空间设计能够强调各种用途的最佳声学,从大型礼堂到专业办公环境。本文还报道了混响室内礼堂和办公座椅吸声系数评定的测量不确定度。
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引用次数: 0
Interlaboratory Comparison of Vacuum Pressure Gauge Calibration Across Public Institution Branches 公共事业单位真空压力表检定的实验室间比较
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-09 DOI: 10.1007/s12647-025-00831-z
Can Ekici

This study evaluates the results of an interlaboratory comparison between two Turkish Standards Institution (TSE) calibration laboratories in the field of vacuum pressure gauge calibration. The goal was to assess measurement consistency and harmonization between the TSE Gebze and TSE Bursa calibration laboratories. The comparison focused on pressure measurements at various points, and the En values calculated for these measurements were all below 1, indicating that the results from both laboratories were closely aligned. This confirms that both laboratories employed accurate and consistent measurement techniques, reinforcing the reliability of their calibration processes. The results demonstrate the crucial role of interlaboratory comparisons in ensuring high-quality measurements, validating the technical competence of the laboratories, and supporting the harmonization of metrological practices.

本研究评估了两个土耳其标准机构(TSE)校准实验室在真空压力表校准领域的实验室间比较的结果。目的是评估TSE Gebze和TSE Bursa校准实验室之间的测量一致性和协调性。对比集中在各点的压力测量,这些测量计算的En值都小于1,说明两个实验室的结果非常接近。这证实了两个实验室采用了准确和一致的测量技术,加强了其校准过程的可靠性。结果表明,实验室间比较在确保高质量测量、验证实验室技术能力和支持计量实践的协调方面发挥了至关重要的作用。
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引用次数: 0
An Accurate Fault Identification, Measurement and Protection in Radial Power System Network Using a New Hybrid Bell Algorithm 基于新型混合贝尔算法的径向电网故障准确识别、测量和保护
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-06-07 DOI: 10.1007/s12647-025-00827-9
Abhinav Saxena, Md. Abul Kalam, Gyanesh Singh, Yogendra Arya

This article presents the operation and control of various faults in the radial power system network, which includes the faults identification, measurement, categorization, and protection. The continuous presence of faults may damage the components of the network. It makes the power system engineers think to identify and trip the faults. The existing methods are able to identify faults with huge complex mathematics, more data occupation, poor accuracy, poor sensitivity, and inappropriate power quality problems like higher total harmonic distortion (THD). The existing methods also take more time to trip the fault. In order to overthrow the existing methods, an optimal hybrid bell algorithm (HBA) is proposed that is simple, consumes less data, and is easily applicable, which shows the novelty of the proposed research. The architecture of the HBA is a combined operation and control of the standard normal distribution and Poisson distribution methods for fault analysis. The performance parameters like accuracy, sensitivity, and THD are used for estimation of SLG (single line to ground), LL (line to line), LLG (line to line to ground), and LLL (line to line to line) faults in the network. The validity of the method is tested on the IEEE standard 9-bus and 39-bus systems. The performance realization for fault identification and termination in a radial network has been assessed with invasive weed optimization (IWO), fuzzy logic controller (FLC), artificial neural networks (ANN), and other existing methods. It is observed that performance parameters like improved accuracy (0.41%), improved sensitivity (0.49%), and least THD (9%) have been obtained with the proposed method in comparison with IWO, FLC, ANN, and other existing methods for fault identification and classification. The HBA also shows its dominance for protection against various faults, with the least time taken (0.55 s) for fault termination and the least change in current (51%) with a simple mathematical approach. Such better results with the proposed method show its novelty. The critical situations like high impedance fault and voltage zero crossing have also been analyzed, in which the proposed approach shows its dominance over other methods. Further, the stability of the proposed method is validated with Routh-Hurwitz criteria.

本文介绍了径向电网中各种故障的运行和控制,包括故障识别、故障测量、故障分类和故障保护。故障的持续存在可能会对网络的组成部分造成损坏。这引起了电力系统工程师对故障的识别和跳闸的思考。现有的故障识别方法存在数学量大、数据占用多、精度差、灵敏度差、总谐波失真(THD)高等不合适的电能质量问题。现有的方法也需要更多的时间来触发故障。为了推翻现有方法,提出了一种简单、数据消耗少、易于应用的最优混合贝尔算法(HBA),显示了本文研究的新颖性。HBA的体系结构是标准正态分布和泊松分布方法的组合操作和控制,用于故障分析。准确度、灵敏度、THD等性能参数用于估计网络中的SLG(单线对地)、LL(线对线)、LLG(线对地)和LLL(线对线)故障。在IEEE标准9总线和39总线系统上测试了该方法的有效性。采用入侵杂草优化(IWO)、模糊逻辑控制器(FLC)、人工神经网络(ANN)等现有方法对径向网络故障识别和终止的性能实现进行了评估。与IWO、FLC、ANN等现有故障识别分类方法相比,该方法获得了精度提高(0.41%)、灵敏度提高(0.49%)、THD最小(9%)等性能参数。HBA在各种故障保护方面也显示出其优势,通过简单的数学方法,HBA的故障终止时间最短(0.55 s),电流变化最小(51%)。该方法取得了较好的结果,显示了其新颖性。对高阻抗故障和电压过零等关键情况进行了分析,表明了该方法的优越性。通过Routh-Hurwitz准则验证了该方法的稳定性。
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引用次数: 0
Evaluation of calibration efficacy for negative temperature coefficient thermistors in marine thermal environments 海洋热环境中负温度系数热敏电阻的校准效果评价
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-05-25 DOI: 10.1007/s12647-025-00826-w
Mengyang Liu, Yue Yin, Qindan Liu, Lijun Zhang, Hua Zhang, Jiangyong Hu

In response to the national strategy for maritime power enhancement, there is a critical need for deep-sea temperature sensors with short response times and high sensitivity. This study aims to support the increasing domestic substitution trend for CTD measuring instruments used in marine surveys. By integrating high-precision marine temperature measurement requirements, we have employed a technique that involves the use of a temperature equalization block for instantaneous comparison, fixed calibration temperature points, and varying the degree of polynomial fitting. A fitting program was developed using MATLAB to compare the performance of the Hoge equation with different degrees of fitting within the marine temperature range. The study also assessed the uncertainty of fitting residuals and analyzed the long-term stability of NTC thermistor thermometers, clarifying the methods for verifying long-term stability. The results indicate that the performance of the Hoge equation with 3rd, 4th, and 5th order for NTC thermistor thermometers meet the high-precision measurement requirements of the marine temperature range. A method for verifying the long-term stability of NTC thermistor thermometers at the water triple point was adopted, and the calibration efficacy meet the requirements for the domestic substitution of temperature sensors in CTD measuring instruments and the precision demands of deep-sea temperature measurement. High-precision measurement equipment, a stable calibration environment, appropriate calibration methods, and proper data processing are essential for achieving high-precision calibration efficacy. The findings of this study contribute to defining standards for the selection of temperature sensors in marine survey CTD measuring instruments and deep-sea temperature sensors, providing a reference for the metrological calibration and long-term stability verification of NTC thermistor thermometers °C.

为响应国家海洋力量增强战略,迫切需要响应时间短、灵敏度高的深海温度传感器。这项研究的目的是支持国内在海洋调查中使用的CTD测量仪器越来越多的替代趋势。通过整合高精度海洋温度测量要求,我们采用了一种技术,该技术涉及使用温度均衡块进行瞬时比较,固定校准温度点,并改变多项式拟合的程度。利用MATLAB编写拟合程序,比较不同拟合程度下Hoge方程在海洋温度范围内的拟合性能。研究还评估了拟合残差的不确定性,分析了NTC热敏电阻温度计的长期稳定性,明确了验证长期稳定性的方法。结果表明,NTC热敏电阻温度计的三阶、四阶和五阶Hoge方程的性能满足海洋温度范围的高精度测量要求。采用了一种验证NTC热敏电阻温度计在水三相点长期稳定性的方法,校准效果满足CTD测量仪器中温度传感器的国内化替代要求和深海温度测量的精度要求。高精度的测量设备、稳定的校准环境、合适的校准方法和正确的数据处理是实现高精度校准效果的关键。研究结果有助于确定海洋测量CTD测量仪器和深海温度传感器中温度传感器的选择标准,为NTC热敏电阻温度计°C的计量校准和长期稳定性验证提供参考。
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引用次数: 0
An Integrated Analysis of Digitalization in Metrology: Insights from Researchers and Industry Professionals on Enablers and Barriers 计量数字化的综合分析:来自研究人员和行业专业人士对推动因素和障碍的见解
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-05-24 DOI: 10.1007/s12647-025-00821-1
Neeraj Bhanot

Metrology plays a crucial role in ensuring equitable trade and economic stability through reliable measurement traceability. As industries advance, the systematic digitalization of calibration processes becomes increasingly vital. This study proposes a comprehensive framework for digitalizing the metrology domain, focusing on strengthening enablers and mitigating barriers based on the responses of researchers and industry professionals. The study first compared the group’s perceptions using independent t-tests, then identified key enablers and barriers using Grey Relational Analysis, and finally, established causal relationships between the factors by utilizing Structural Equation Modeling to facilitate the digitalization of metrology. For causal relations, the initial model was developed by leveraging a locally developed Large Language Model (FLAN-T5-LARGE) on the available research literature, followed by rigorous evaluation based on fitness statistics. However, to construct a more robust model and compare results with the large language model, multiple combinations of enablers and barriers were systematically evaluated in view of approx. 72 quadrillion scenarios for each group based on fitness statistics. The results indicate that while both groups recognize the importance of digitalization in metrology, researchers prioritize metrological performance and addressing technical limitations, whereas industry professionals emphasize efficiency and cost-effectiveness for successful implementation. The LLM-based model showed a slight performance gap compared to the systematic approach, validating its utility. These insights provide a robust foundation for bridging perception gaps and fostering digital metrology adoption.

计量通过可靠的计量溯源,在确保公平贸易和经济稳定方面发挥着至关重要的作用。随着工业的发展,校准过程的系统化数字化变得越来越重要。本研究提出了一个全面的计量领域数字化框架,重点是根据研究人员和行业专业人士的反应,加强推动因素和减少障碍。该研究首先使用独立t检验比较了小组的看法,然后使用灰色关联分析确定了关键的推动因素和障碍,最后利用结构方程模型建立了因素之间的因果关系,以促进计量的数字化。对于因果关系,初始模型是利用本地开发的大型语言模型(FLAN-T5-LARGE)在现有研究文献的基础上开发的,然后根据适应度统计进行严格的评估。然而,为了构建一个更稳健的模型,并将结果与大型语言模型进行比较,我们系统地评估了促成因素和障碍的多种组合。根据健身统计,每个群体有72千万亿次的场景。结果表明,虽然两组都认识到数字化在计量中的重要性,但研究人员优先考虑计量性能和解决技术限制,而行业专业人士则强调成功实施的效率和成本效益。与系统方法相比,基于llm的模型显示出轻微的性能差距,验证了其实用性。这些见解为弥合认知差距和促进数字计量的采用提供了坚实的基础。
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引用次数: 0
Assessment of Metrological Characterization of 30,000 kg Weighing Balance Using a Novel Step-Up Method Expandable up to 50,000 kg 使用一种可扩展至50,000公斤的新型升压法评估30,000公斤称重秤的计量特性
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-05-23 DOI: 10.1007/s12647-025-00822-0
Goutam Mandal, Sanjoy Mandal, Anil Kumar

It is important to assess the metrological characterization of heavy-capacity weighing balances before using them, particularly when determining the volume of heavy-capacity volumetric tanks using the gravimetric method. In order to support industry with the best uncertainties in the corresponding range and enhance product quality, metrological properties of a heavy-capacity weighing balance of 30,000 kg were assessed using standard weights traceable to the National Standard of Mass. Only 7,000 kg weights of standard denominations that could be traced to the national standard were available; thus, a novel step-up method, which can be expanded to 50,000 kg, was employed in this characterization procedure. We have outlined a thorough procedure in this work that satisfies the requirements of the OIML R 76-1: 2006 standard as being economical and affordable.

在使用大容量称重秤之前,评估其计量特性是很重要的,特别是在使用重量法确定大容量容积罐的体积时。为了支持在相应范围内具有最佳不确定度的行业并提高产品质量,使用可追溯到国家质量标准的标准重量评估了30,000 kg重容量称重天平的计量特性。只有7000公斤可追溯至国家标准的标准面额砝码;因此,在此表征过程中采用了一种新的升压方法,可以扩展到50,000 kg。我们在这项工作中概述了一个完整的程序,满足OIML R 76-1: 2006标准的要求,即经济实惠。
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引用次数: 0
A New Technique for Volumetric Soil Moisture Evaluation Using Geostationary Satellite 基于地球同步卫星的体积土壤水分评价新技术
IF 1.3 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2025-05-21 DOI: 10.1007/s12647-025-00825-x
C. D. Raisy, Sharda Vashisth, Amitava Sen Gupta

GNSS-Interferometric Reflectometry technique normally uses Medium Earth Orbiting (MEO) satellites as they appear to travel slowly across the sky relative to a stationary observer on ground. In this work, we propose a novel method of GNSS-IR using a geostationary satellite by steadily changing the antenna height at small known steps, thereby producing the required interference pattern. The phase of this interference pattern is a function of the volumetric soil moisture. Our simulation results show a 6.5° phase change corresponding to a 10% change in volumetric soil moisture (VSM). The method has been verified experimentally using receptions from a NavIC geostationary satellite. Running the experiment over an extended period of a few months established the linear relationship between the phase of the interference pattern and the volumetric soil moisture, having a slope of 7.1° per 10% change in VSM.

gnss干涉反射测量技术通常使用中地球轨道卫星(MEO),因为相对于地面上静止的观测者,它们在天空中运行得很慢。在这项工作中,我们提出了一种使用地球静止卫星的GNSS-IR新方法,通过以已知的小步骤稳定地改变天线高度,从而产生所需的干扰图。这种干涉图样的相位是土壤体积湿度的函数。我们的模拟结果表明,6.5°的相位变化对应于10%的体积土壤湿度(VSM)变化。该方法已通过一颗中国海军地球同步卫星的接收实验得到验证。在几个月的延长时间内进行实验,建立了干涉图案的相位与体积土壤湿度之间的线性关系,VSM每变化10%,斜率为7.1°。
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引用次数: 0
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