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Fracture load of colored and non-colored high translucent zirconia three-unit fixed dental prosthesis frameworks. 彩色和非彩色高半透明氧化锆三单元固定义齿框架的断裂载荷。
Pub Date : 2018-04-04 eCollection Date: 2018-01-01 DOI: 10.1080/23337931.2018.1459626
Deyar Jallal Hadi Mahmood, Michael Braian, Abdul-Salam Khan, Armin Shabaz, Christel Larsson

Aim: The use of colored translucent zirconia may enable restorations of a more natural tooth-like appearance than previous opaque white zirconia. The shift from non-colored to colored zirconia may however entail a risk of reduced strength. The aim of the present study was to compare fracture load and fracture mode of fixed dental prostheses frameworks made of colored translucent zirconia to that of non-colored controls. Methods: A total of forty three-unit FDP frameworks were manufactured from two different high translucent zirconia materials (Zenostar, Wieland Dental, and DD cubeX2, Dental Direkt). Each group contained two subgroups, one colored and one non-colored. Coloring was performed before final sintering using two different infiltration techniques. All FDPs underwent an artificial aging process in the form of heat treatment, thermocycling and preloading whereafter the specimens were subjected to load until fracture. Fracture load and mode was registered. Results: For one of the zirconia materials, Zenostar, the non-colored frameworks showed significantly higher fracture loads (p < .0001) compared to its colored counterpart. No significant difference (p > .05) was found between colored and non-colored frameworks in the other zirconia material, DD cubeX2. All FDPs fractured through the connector. Some fractures ran through the mesial and some through the distal side of the connector but there were no significant differences in fracture mode between groups. Conclusion: Coloring before sintering of high-translucent zirconia may decrease the fracture load of FDP frameworks for certain materials and techniques. Fracture mode however, does not appear to be affected.

目的:使用彩色半透明的氧化锆可以使修复比以前不透明的白色氧化锆更自然的牙齿样外观。然而,从有色氧化锆到有色氧化锆的转变可能会带来强度降低的风险。本研究的目的是比较有色半透明氧化锆固定义齿框架与非有色对照的断裂载荷和断裂模式。方法:采用两种不同的高半透明氧化锆材料(Zenostar, Wieland Dental和DD cubeX2, Dental direckt)制作共43个单元的FDP框架。每个组包含两个子组,一个有色组和一个非有色组。在最终烧结前使用两种不同的渗透技术进行着色。所有FDPs都经历了热处理、热循环和预加载等人工老化过程,然后试样承受载荷直至断裂。记录断裂载荷和断裂模式。结果:对于一种氧化锆材料Zenostar,在另一种氧化锆材料DD cubeX2中,有色框架与有色框架之间的断裂载荷显著高于有色框架(p p > 0.05)。所有fdp通过连接器断裂。有些骨折穿过接头的中端,有些穿过接头的远端,但两组之间的骨折方式无显著差异。结论:高半透明氧化锆烧结前着色可以降低某些材料和工艺的FDP框架的断裂载荷。然而,骨折模式似乎不受影响。
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引用次数: 5
Effect of low-shrinkage monomers on the physicochemical properties of experimental composite resin. 低收缩单体对实验性复合树脂理化性能的影响。
Pub Date : 2018-02-28 eCollection Date: 2018-01-01 DOI: 10.1080/23337931.2018.1444488
Jingwei He, Sufyan Garoushi, Pekka K Vallittu, Lippo Lassila

This study was conducted to determine whether novel experimental low-shrinkage dimethacrylate co-monomers could provide low polymerization shrinkage composites without sacrifice to degree of conversion, and mechanical properties of the composites. Experimental composites were prepared by mixing 28.6 wt% of bisphenol-A-glycidyl dimethacrylate based resin matrix (bis-GMA) with various weight-fractions of co-monomers; tricyclo decanedimethanol dacrylate (SR833s) and isobornyl acrylate (IBOA) to 71.4 wt% of particulate-fillers. A composite based on bis-GMA/TEGDMA (triethylene glycol dimethacrylate) was used as a control. Fracture toughness and flexural strength were determined for each experimental material following international standards. Degree of monomer-conversion (DC%) was determined by FTIR spectrometry. The volumetric shrinkage in percent was calculated as a buoyancy change in distilled water by means of the Archimedes' principle. Polymerization shrinkage-strain and -stress of the specimens were measured using the strain-gage technique and tensilometer, respectively with respect to time. Statistical analysis revealed that control group had the highest double-bond conversion (p < .05) among the experimental resins tested. All of the experimental composite resins had comparable flexural strength, modulus, and fracture toughness (p > .05). Volumetric shrinkage and shrinkage stress decreased with increasing IBOA concentration. Replacing TEGDMA with SR833s and IBOA can decrease the volumetric shrinkage, shrinkage strain, and shrinkage stress of composite resins without affecting the mechanical properties. However, the degree of conversion was also decreased.

本研究旨在确定新型实验低收缩二甲基丙烯酸酯共单体能否在不牺牲转化率和复合材料力学性能的情况下提供低聚合收缩复合材料。将28.6 wt%的双酚- a -缩水甘油酯二甲基丙烯酸酯基树脂基质(bis-GMA)与不同重量分数的共聚物混合制备实验复合材料;三环癸二甲醇丙烯酸酯(SR833s)和丙烯酸异鸟酯(IBOA)为71.4 wt%的颗粒填料。以双gma /TEGDMA(三甘醇二甲基丙烯酸酯)为基础的复合材料作为对照。每种实验材料的断裂韧性和抗弯强度均按照国际标准进行测定。用红外光谱法测定了单体转化率(DC%)。用阿基米德原理计算蒸馏水的浮力变化来计算体积收缩率。采用应变片技术和拉力仪分别测量了试样的聚合收缩应变和收缩应力随时间的变化。统计分析显示,对照组的双键转化率最高(p p > 0.05)。体积收缩率和收缩应力随IBOA浓度的增加而减小。用SR833s和IBOA替代TEGDMA可以降低复合树脂的体积收缩率、收缩应变和收缩应力,而不影响复合树脂的力学性能。然而,转化程度也有所下降。
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引用次数: 27
In vitro analysis of the marginal adaptation and discrepancy of stainless steel crowns. 不锈钢冠的体外边缘适应与差异分析。
Pub Date : 2018-02-28 eCollection Date: 2018-01-01 DOI: 10.1080/23337931.2018.1444995
Riaan Mulder, Rasha Medhat, Nadia Mohamed

Aim: The purpose of the study was to assess the marginal adaptation and discrepancy of SSC's. Differences in adaptation and discrepancy between the four surfaces (mesial, lingual, distal, and buccal) were evaluated. Methods: The placement of stainless steel crowns were completed on a phantom head in accordance with the clinical technique. The ideal tooth preparation was made and this 'master tooth' duplicated to achieve a sample size of 15. The stainless steel crowns were placed, trimmed, and cemented as per the clinical technique. The cemented stainless crowns were analyzed under 100× stereomicroscope magnification. The marginal adaptation and discrepancy of each specimen was measured every 2 µm. Results: All the specimens showed marginal adaptation and discrepancy. The lingual margin had a significantly better adaptation (p < .0001) over the other surfaces. The buccal surface was the only surface that had an appropriate supra-CEJ level with a significance of p < .0001. Conclusion: The marginal discrepancies occur during the trimming procedure and assessment of the gingival approximation of the SSC margin. The inspection of stainless steel crown adaptation and discrepancy is an essential clinical step.

目的:研究SSC的边缘适应和差异。评估了四个面(中、舌、远端和颊)的适应差异和差异。方法:按照临床技术,在假体头上完成不锈钢冠的放置。制作了理想的牙齿准备,并复制了这颗“主牙”,以达到15个样本量。按照临床技术放置、修剪和粘接不锈钢冠。在100倍立体显微镜下对胶结后的不锈钢冠进行分析。每2µm测量每个标本的边际适应和差异。结果:所有标本均表现出一定程度的适应性和差异性。结论:侧切缘的边缘差异发生在侧切缘的修整过程和龈缘近似的评估过程中。不锈钢冠的适应和差异检查是临床必不可少的步骤。
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引用次数: 11
Repair bond strength of nanohybrid composite resins with a universal adhesive. 纳米复合树脂与通用胶粘剂的修复粘合强度。
Pub Date : 2017-12-12 eCollection Date: 2018-01-01 DOI: 10.1080/23337931.2017.1412262
Pinar Altinci, Murat Mutluay, Arzu Tezvergil-Mutluay

Objective: To investigate the repair bond strength of fresh and aged nanohybrid and hybrid composite resins using a universal adhesive (UA). Materials and methods: Fresh and aged substrates were prepared using two nanohybrid (Venus Pearl, Heraus Kulzer; Filtek Supreme XTE, 3 M ESPE) and one hybrid (Z100, 3 M ESPE) composite resin, and randomly assigned to different surface treatments: (1) no treatment (control), (2) surface roughening with 320-grit (SR), (3) SR + UA (iBOND, Heraus Kulzer), (4) SR + Silane (Signum, Ceramic Bond I, Heraeus Kulzer) + UA, (5) SR + Sandblasting (CoJet, 3 M ESPE) + Silane + UA. After surface treatment, fresh composite resin was added to the substrates at 2 mm layer increments to a height of 5 mm, and light cured. Restored specimens were water-stored for 24 h and sectioned to obtain 1.0 × 1.0 mm beams (n = 12), and were either water-stored for 24 h at 37 °C, or water-stored for 24 h, and then thermocycled for 6000 cycles before microtensile bond strength (µTBS) testing. Data were analyzed with ANOVA and Tukey's HSD tests (p = .05). Results: Combined treatment of SR, sandblasting, silane and UA provided repair bond strength values comparable to the cohesive strength of each tested resin material (p < .05). Thermocycling significantly reduced the cohesive strength of the composite resins upto 65% (p < .05). Repair bond strengths of UA-treated groups were more stable under thermocycling. Conclusions: Universal adhesive application is a reliable method for composite repair. Sandblasting and silane application slightly increases the repair strength for all substrate types.

目的:用通用粘合剂(UA)研究新鲜和老化纳米杂化树脂和杂化复合树脂的修复粘结强度。材料与方法:采用两种纳米杂化材料(Venus Pearl, Heraus Kulzer;Filtek Supreme XTE, 3 M ESPE)和一种混合(Z100, 3 M ESPE)复合树脂,随机分配到不同的表面处理:(1)不处理(对照),(2)表面粗化320粒(SR), (3) SR + UA (iBOND, Heraeus Kulzer), (4) SR +硅烷(Signum, Ceramic Bond I, Heraeus Kulzer) + UA, (5) SR +喷砂(CoJet, 3 M ESPE) +硅烷+ UA。表面处理后,将新鲜的复合树脂以2 mm层增量添加到基材中,至5 mm高度,光固化。修复后的标本水保存24 h,切片得到1.0 × 1.0 mm梁(n = 12),在37°C下水保存24 h,或水保存24 h,然后热循环6000次,然后进行微拉伸粘结强度(µTBS)测试。数据分析采用方差分析和Tukey’s HSD检验(p = 0.05)。结果:SR、喷砂、硅烷和UA联合处理可提供与各被试树脂材料的内聚强度相当的修复结合强度值(p p)。结论:通用粘合剂应用是一种可靠的复合修复方法。喷砂和硅烷的应用稍微增加了所有基材类型的修复强度。
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引用次数: 51
Triethylene glycol dimethacrylate: adjuvant properties and effect on cytokine production. 三甘醇二甲基丙烯酸酯:佐剂性质及对细胞因子产生的影响。
Pub Date : 2017-12-05 eCollection Date: 2018-01-01 DOI: 10.1080/23337931.2017.1409075
Sara Alizadehgharib, Anna-Karin Östberg, Ulf Dahlgren

Objective: Leakage of monomers from dental fillings due to incomplete curing is very common. The objective of the present study was to examine the cytokine profile in cells exposed to triethyleneglycol dimethacrylate (TEGDMA) and the adjuvant properties of TEGDMA. Materials and methods: Human peripheral blood mononuclear cells were exposed to TEGDMA (500 and 1000 μM) for 24 h in vitro. Bio-Plex Pro™ assays were used for analysis and detection of cytokines. In vivo, BALB/c mice were immunized subcutaneously in the base of the tail with TEGDMA in combination with ovalbumin (OVA). Results: The cytokine levels of IL-8, IL-18, GRO-α and MCP-1 were significantly increased for both concentrations. IL-1β, IL-6 and TNF-α was only significantly increased in cultures exposed to 500 μM TEGDMA. The concentration of TNF-α was significantly decreased in cultures exposed to 1000 μM TEGDMA. Animals immunized with OVA co-administrated with TEGDMA had a significantly higher IgE and IgG anti-OVA antibody levels in blood than animals immunized with OVA only. Conclusions: TEGDMA affects production of proinflammatory cytokines IL-1β, IL-6, IL-8, IL-18 and TNF-α. This inflammatogenic capacity renders TEGDMAs adjuvant properties, which may interfere with the homeostasis between the immune system and the indigenous microflora in the oral cavity.

目的:口腔填充物因不完全固化导致单体渗漏的现象十分普遍。本研究的目的是检查细胞暴露于三乙二醇二甲基丙烯酸酯(TEGDMA)的细胞因子谱和TEGDMA的辅助特性。材料与方法:将人外周血单个核细胞体外暴露于500 μM和1000 μM的TEGDMA中24 h。Bio-Plex Pro™法用于分析和检测细胞因子。在体内,用TEGDMA联合卵清蛋白(OVA)在BALB/c小鼠尾部皮下免疫。结果:两种浓度下细胞因子IL-8、IL-18、GRO-α、MCP-1水平均显著升高。IL-1β、IL-6和TNF-α仅在500 μM TEGDMA中显著升高。在1000 μM TEGDMA下,TNF-α浓度显著降低。TEGDMA与OVA联合免疫动物血清中抗OVA的IgE和IgG抗体水平显著高于单独免疫动物。结论:TEGDMA影响促炎细胞因子IL-1β、IL-6、IL-8、IL-18和TNF-α的产生。这种致炎能力使tegdma具有佐剂特性,这可能会干扰免疫系统和口腔内本地微生物群之间的稳态。
{"title":"Triethylene glycol dimethacrylate: adjuvant properties and effect on cytokine production.","authors":"Sara Alizadehgharib,&nbsp;Anna-Karin Östberg,&nbsp;Ulf Dahlgren","doi":"10.1080/23337931.2017.1409075","DOIUrl":"https://doi.org/10.1080/23337931.2017.1409075","url":null,"abstract":"<p><p><b>Objective:</b> Leakage of monomers from dental fillings due to incomplete curing is very common. The objective of the present study was to examine the cytokine profile in cells exposed to triethyleneglycol dimethacrylate (TEGDMA) and the adjuvant properties of TEGDMA. <b>Materials and methods:</b> Human peripheral blood mononuclear cells were exposed to TEGDMA (500 and 1000 μM) for 24 h <i>in vitro</i>. Bio-Plex Pro™ assays were used for analysis and detection of cytokines. <i>In vivo,</i> BALB/c mice were immunized subcutaneously in the base of the tail with TEGDMA in combination with ovalbumin (OVA). <b>Results:</b> The cytokine levels of IL-8, IL-18, GRO-α and MCP-1 were significantly increased for both concentrations. IL-1β, IL-6 and TNF-α was only significantly increased in cultures exposed to 500 μM TEGDMA. The concentration of TNF-α was significantly decreased in cultures exposed to 1000 μM TEGDMA. Animals immunized with OVA co-administrated with TEGDMA had a significantly higher IgE and IgG anti-OVA antibody levels in blood than animals immunized with OVA only. <b>Conclusions:</b> TEGDMA affects production of proinflammatory cytokines IL-1β, IL-6, IL-8, IL-18 and TNF-α. This inflammatogenic capacity renders TEGDMAs adjuvant properties, which may interfere with the homeostasis between the immune system and the indigenous microflora in the oral cavity.</p>","PeriodicalId":6997,"journal":{"name":"Acta Biomaterialia Odontologica Scandinavica","volume":"4 1","pages":"1-9"},"PeriodicalIF":0.0,"publicationDate":"2017-12-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/23337931.2017.1409075","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"35244937","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Release of titanium after insertion of dental implants with different surface characteristics - an ex vivo animal study. 植入不同表面特征的牙种植体后钛的释放-一项离体动物研究。
Pub Date : 2017-11-14 eCollection Date: 2017-01-01 DOI: 10.1080/23337931.2017.1399270
Mattias Pettersson, Jean Pettersson, Margareta Molin Thorén, Anders Johansson

In the present study, amount of titanium (Ti) released into the surrounding bone during placement of implants with different surface structure was investigated. Quantification of Ti released during insertion from three different implants was performed in this ex vivo study. Jaw bone from pigs was used as model for installation of the implants and Inductively Coupled Plasma Atomic Emission Spectroscopy (ICP-AES) was used for analysis of the released Ti. Implant surface were examined with scanning electron microscopy (SEM), before and after the placement into the bone. Ti was abraded to the surrounding bone upon insertion of a dental implant and the surface roughness of the implant increased the amount of Ti found. Diameter and total area of the implant were of less importance for the Ti released to the bone. No visible damages to the implant surfaces could be identified in SEM after placement.

在本研究中,研究了不同表面结构种植体放置过程中钛(Ti)释放到周围骨中的量。在这项离体研究中,对三种不同植入物在植入过程中释放的钛进行了定量分析。采用猪颚骨作为植入体的模型,电感耦合等离子体原子发射光谱(ICP-AES)对释放的Ti进行分析。在植入骨之前和之后,用扫描电镜检查种植体表面。在植入牙种植体时,钛被磨损到周围的骨头上,种植体表面的粗糙度增加了钛的含量。种植体的直径和总面积对钛释放到骨的影响较小。植入后扫描电镜未发现明显的种植体表面损伤。
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引用次数: 26
Fracture strength of veneered translucent zirconium dioxide crowns with different porcelain thicknesses. 不同瓷厚贴面半透明二氧化锆冠的断裂强度。
Pub Date : 2017-11-14 eCollection Date: 2017-01-01 DOI: 10.1080/23337931.2017.1403288
Fahad Bakitian, Przemek Seweryniak, Evaggelia Papia, Christel Larsson, Per Vult von Steyern

Objective: To evaluate fracture strength of veneered translucent zirconium dioxide crowns designed with different porcelain layer thicknesses. Materials and Methods: Sixty crowns, divided into six groups of 10, were used in this study. Groups were divided according to different thicknesses of porcelain veneer on translucent zirconium dioxide cores of equal thickness (0.5 mm). Porcelain thicknesses were 2.5, 2.0, 1.0, 0.8, 0.5 and 0.3 mm. Crowns were artificially aged before loaded to fracture. Determination of fracture mode was performed using light microscope. Results: Group 1.0 mm showed significantly (p ≤ .05) highest fracture loads (mean 1540 N) in comparison with groups 2.5, 2.0 and 0.3 mm (mean 851, 910 and 1202 N). There was no significant difference (p>.05) in fracture loads among groups 1.0, 0.8 and 0.5 mm (mean 1540, 1313 and 1286 N). There were significantly (p ≤ .05) more complete fractures in group 0.3 mm compared to all other groups which presented mainly cohesive fractures. Conclusions: Translucent zirconium dioxide crowns can be veneered with minimal thickness layer of 0.5 mm porcelain without showing significantly reduced fracture strength compared to traditionally veneered (1.0-2.0 mm) crowns. Fracture strength of micro-veneered crowns with a layer of porcelain (0.3 mm) is lower than that of traditionally veneered crowns but still within range of what may be considered clinically sufficient. Porcelain layers of 2.0 mm or thicker should be used where expected loads are low only.

目的:评价不同瓷层厚度的半透明二氧化锆冠的断裂强度。材料与方法:60个冠体,分为6组,每组10个。根据等厚度(0.5 mm)的半透明二氧化锆芯上瓷贴面厚度的不同进行分组。瓷厚分别为2.5、2.0、1.0、0.8、0.5、0.3 mm。冠在加载断裂前人工老化。光镜下测定断裂模式。结果:1.0 mm组骨折载荷最高(平均1540 N),显著高于2.5、2.0、0.3 mm组(平均851、910、1202 N) (p≤0.05),1.0、0.8、0.5 mm组(平均1540、1313、1286 N)骨折载荷差异无统计学意义(p> 0.05), 0.3 mm组骨折完整程度显著高于其他以内聚性骨折为主的组(p≤0.05)。结论:与传统贴面(1.0-2.0 mm)冠相比,半透明二氧化锆冠可以用0.5 mm的瓷薄层贴面,而不会明显降低断裂强度。带有瓷层(0.3 mm)的微贴面冠的断裂强度低于传统贴面冠,但仍在临床认为足够的范围内。只有在预期载荷较低的地方才应使用2.0毫米或更厚的瓷层。
{"title":"Fracture strength of veneered translucent zirconium dioxide crowns with different porcelain thicknesses.","authors":"Fahad Bakitian,&nbsp;Przemek Seweryniak,&nbsp;Evaggelia Papia,&nbsp;Christel Larsson,&nbsp;Per Vult von Steyern","doi":"10.1080/23337931.2017.1403288","DOIUrl":"https://doi.org/10.1080/23337931.2017.1403288","url":null,"abstract":"<p><p><b>Objective:</b> To evaluate fracture strength of veneered translucent zirconium dioxide crowns designed with different porcelain layer thicknesses. <b>Materials and Methods:</b> Sixty crowns, divided into six groups of 10, were used in this study. Groups were divided according to different thicknesses of porcelain veneer on translucent zirconium dioxide cores of equal thickness (0.5 mm). Porcelain thicknesses were 2.5, 2.0, 1.0, 0.8, 0.5 and 0.3 mm. Crowns were artificially aged before loaded to fracture. Determination of fracture mode was performed using light microscope. <b>Results:</b> Group 1.0 mm showed significantly (<i>p</i> ≤ .05) highest fracture loads (mean 1540 N) in comparison with groups 2.5, 2.0 and 0.3 mm (mean 851, 910 and 1202 N). There was no significant difference (<i>p</i>>.05) in fracture loads among groups 1.0, 0.8 and 0.5 mm (mean 1540, 1313 and 1286 N). There were significantly (<i>p</i> ≤ .05) more complete fractures in group 0.3 mm compared to all other groups which presented mainly cohesive fractures. <b>Conclusions:</b> Translucent zirconium dioxide crowns can be veneered with minimal thickness layer of 0.5 mm porcelain without showing significantly reduced fracture strength compared to traditionally veneered (1.0-2.0 mm) crowns. Fracture strength of micro-veneered crowns with a layer of porcelain (0.3 mm) is lower than that of traditionally veneered crowns but still within range of what may be considered clinically sufficient. Porcelain layers of 2.0 mm or thicker should be used where expected loads are low only.</p>","PeriodicalId":6997,"journal":{"name":"Acta Biomaterialia Odontologica Scandinavica","volume":"3 1","pages":"74-83"},"PeriodicalIF":0.0,"publicationDate":"2017-11-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/23337931.2017.1403288","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"35658165","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 11
Dimensional stability of two impression materials after a 6-month storage period. 两种压印材料储存6个月后的尺寸稳定性。
Pub Date : 2017-11-14 eCollection Date: 2017-01-01 DOI: 10.1080/23337931.2017.1401933
Francisco Martins, Patrícia Branco, José Reis, Ignacio Barbero Navarro, Paulo Maurício

Objective: Oral rehabilitation success is enhanced by an accurate and reproducible final impression. The purpose of this study is to evaluate the dimensional changes of a polyether and addition silicone subjected to disinfection and/or sterilization after a long storage period. Material and methods: Ninety samples were obtained from polyether ImpregumTM PentaTM (3M ESPETM, Seefeld, Germany) and 90 of addition silicone ImprintTM 4 PentaTM Putty (3M ESPETM, Seefeld, Germany) according to ISO 4823:2000. The samples of each material were split to form three groups with 30 samples each: a control group, a hypochlorite group (disinfection) and an autoclave group (sterilization). Samples were stored in the Portuguese Institute for Quality for six months at 23 °C. Samples were measured by laser interferometry, according to the Michelson technique before calculating dimensional stability according ISO 4823:2000. A statistical analysis via a three-way mixed ANOVA was performed. Results: Significant shrinkage of ImpregumTM PentaTM was 0.77 ± 0.17% in the control group, 0.42 ± 0.19% in the hypochlorite group and 0.52 ± 0.28% in the autoclave group. For ImprintTM 4 PentaTM Putty, the control group had a shrinkage of 0.42 ± 0.12%, the hypochlorite group 0.36 ± 0.09% and the autoclave group 0.59 ± 0.13%. Conclusions: The long-term storage of samples subjected to disinfection with 5.25% hypochlorite or autoclave sterilization can be used in a clinical setting as the dimensional changes are below the maximum permitted by the ISO 4823:2000, since there are no clinically significant changes in the dimension of the samples during the storage period.

目的:准确、可重复的最终印模可提高口腔康复成功率。本研究的目的是评价聚醚和添加有机硅经过长期储存消毒和/或灭菌后的尺寸变化。材料和方法:根据ISO 4823:2000,从聚醚ImpregumTM PentaTM (3M ESPETM, Seefeld, Germany)和90个添加硅酮ImprintTM 4 PentaTM腻子(3M ESPETM, Seefeld, Germany)中获得样品。每种材料的样品被分成三组,每组30个样品:对照组,次氯酸盐组(消毒)和高压灭菌组(灭菌)。样品在葡萄牙质量研究所保存6个月,温度23°C。在根据ISO 4823:2000计算尺寸稳定性之前,根据迈克尔逊技术,用激光干涉测量法测量样品。通过三向混合方差分析进行统计分析。结果:ImpregumTM PentaTM的收缩率在对照组为0.77±0.17%,次氯酸盐组为0.42±0.19%,高压釜组为0.52±0.28%。对于imprinttm4pentatm腻子,对照组收缩率为0.42±0.12%,次氯酸盐组为0.36±0.09%,高压灭菌组为0.59±0.13%。结论:经5.25%次氯酸盐或高压灭菌器消毒后的样品长期存放,由于样品在存放期间尺寸变化小于ISO 4823:2000允许的最大尺寸变化,因此可用于临床。
{"title":"Dimensional stability of two impression materials after a 6-month storage period.","authors":"Francisco Martins,&nbsp;Patrícia Branco,&nbsp;José Reis,&nbsp;Ignacio Barbero Navarro,&nbsp;Paulo Maurício","doi":"10.1080/23337931.2017.1401933","DOIUrl":"https://doi.org/10.1080/23337931.2017.1401933","url":null,"abstract":"<p><p><b>Objective:</b> Oral rehabilitation success is enhanced by an accurate and reproducible final impression. The purpose of this study is to evaluate the dimensional changes of a polyether and addition silicone subjected to disinfection and/or sterilization after a long storage period. <b>Material and methods:</b> Ninety samples were obtained from polyether Impregum<sup>TM</sup> Penta<sup>TM</sup> (3M ESPE<sup>TM</sup>, Seefeld, Germany) and 90 of addition silicone Imprint<sup>TM</sup> 4 Penta<sup>TM</sup> Putty (3M ESPE<sup>TM</sup>, Seefeld, Germany) according to ISO 4823:2000. The samples of each material were split to form three groups with 30 samples each: a control group, a hypochlorite group (disinfection) and an autoclave group (sterilization). Samples were stored in the Portuguese Institute for Quality for six months at 23 °C. Samples were measured by laser interferometry, according to the Michelson technique before calculating dimensional stability according ISO 4823:2000. A statistical analysis via a three-way mixed ANOVA was performed. <b>Results:</b> Significant shrinkage of Impregum<sup>TM</sup> Penta<sup>TM</sup> was 0.77 ± 0.17% in the control group, 0.42 ± 0.19% in the hypochlorite group and 0.52 ± 0.28% in the autoclave group. For Imprint<sup>TM</sup> 4 Penta<sup>TM</sup> Putty, the control group had a shrinkage of 0.42 ± 0.12%, the hypochlorite group 0.36 ± 0.09% and the autoclave group 0.59 ± 0.13%. <b>Conclusions:</b> The long-term storage of samples subjected to disinfection with 5.25% hypochlorite or autoclave sterilization can be used in a clinical setting as the dimensional changes are below the maximum permitted by the ISO 4823:2000, since there are no clinically significant changes in the dimension of the samples during the storage period.</p>","PeriodicalId":6997,"journal":{"name":"Acta Biomaterialia Odontologica Scandinavica","volume":"3 1","pages":"84-91"},"PeriodicalIF":0.0,"publicationDate":"2017-11-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/23337931.2017.1401933","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"35658167","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 8
Cobalt-chromium alloys in fixed prosthodontics in Sweden. 钴铬合金在瑞典固定修复中的应用。
Pub Date : 2017-08-11 eCollection Date: 2017-01-01 DOI: 10.1080/23337931.2017.1360776
Maria Kassapidou, Victoria Franke Stenport, Lars Hjalmarsson, Carina B Johansson

Aim: The aim of this study was to compile the usage of Co-Cr alloys in fixed prosthodontics (FP) among dental laboratories in Sweden. Methods: From March to October 2015, questionnaires were sent to 542 registered dental laboratories in Sweden. The questionnaires were divided in two parts, one for fixed dental-supported prosthodontics (FDP) and one for fixed implant-supported prosthodontics (FIP). Reminders were sent three times. Results: In total of 542 dental laboratories, 55% answered the questionnaires. Most dental laboratories use Co-Cr in FP, 134 (74%) in FDP and 89(66%) in FIP. The laboratories used Co-Cr alloys of various compositions in the prostheses, 35 for FDP and 30 for FIP. The most commonly used Co-Cr alloys for tooth-supported FDPs were (a) Wirobond® 280, (b) Cara SLM and (c) Wirobond® C. For implant-supported frameworks the frequently used alloys were: (a) Cara SLM, (b) Cara Milled and (c) Wirobond® 280. Except for the difference in composition of these alloys, they were also manufactured with various techniques. In tooth-supported prostheses the dominating technique was the cast technique while newer techniques as laser-sintering and milling were more commonly reported for implant-supported constructions. A fourth technique; the 'pre-state' milling was reported in FDP. Conclusion: More than 30 different Co-Cr alloys were reported as being used in FP. Thus, there is a need for studies exploring the mechanical and physical behavior and the biological response to the most commonly used Co-Cr alloys.

目的:本研究的目的是汇编Co-Cr合金在瑞典牙科实验室固定修复(FP)中的使用情况。方法:2015年3月至10月,向瑞典542家注册牙科实验室发放问卷。问卷分为两部分,固定牙体支持修复(FDP)和固定种植体支持修复(FIP)。提醒发送了三次。结果:共有542家口腔实验室,55%的人回答了问卷。大多数牙科实验室在FP中使用钴铬,在FDP中使用134(74%),在FIP中使用89(66%)。实验室在假体中使用不同成分的Co-Cr合金,35用于FDP, 30用于FIP。牙支撑fdp最常用的Co-Cr合金是(a) Wirobond®280,(b) Cara SLM和(c) Wirobond®c。对于种植支撑框架,最常用的合金是:(a) Cara SLM, (b) Cara milling和(c) Wirobond®280。除了这些合金的成分不同外,它们的制造工艺也各不相同。在牙齿支持的修复体中,主要的技术是铸造技术,而较新的技术如激光烧结和铣削更常被报道用于种植体支持的结构。第四种技巧;FDP报告了“预状态”铣削。结论:有30多种不同的Co-Cr合金被报道用于FP。因此,有必要对最常用的Co-Cr合金的力学和物理行为以及生物反应进行研究。
{"title":"Cobalt-chromium alloys in fixed prosthodontics in Sweden.","authors":"Maria Kassapidou,&nbsp;Victoria Franke Stenport,&nbsp;Lars Hjalmarsson,&nbsp;Carina B Johansson","doi":"10.1080/23337931.2017.1360776","DOIUrl":"https://doi.org/10.1080/23337931.2017.1360776","url":null,"abstract":"<p><p><b>Aim:</b> The aim of this study was to compile the usage of Co-Cr alloys in fixed prosthodontics (FP) among dental laboratories in Sweden. <b>Methods:</b> From March to October 2015, questionnaires were sent to 542 registered dental laboratories in Sweden. The questionnaires were divided in two parts, one for fixed dental-supported prosthodontics (FDP) and one for fixed implant-supported prosthodontics (FIP). Reminders were sent three times. <b>Results:</b> In total of 542 dental laboratories, 55% answered the questionnaires. Most dental laboratories use Co-Cr in FP, 134 (74%) in FDP and 89(66%) in FIP. The laboratories used Co-Cr alloys of various compositions in the prostheses, 35 for FDP and 30 for FIP. The most commonly used Co-Cr alloys for tooth-supported FDPs were (a) Wirobond<sup>®</sup> 280, (b) Cara SLM and (c) Wirobond<sup>®</sup> C. For implant-supported frameworks the frequently used alloys were: (a) Cara SLM, (b) Cara Milled and (c) Wirobond<sup>®</sup> 280. Except for the difference in composition of these alloys, they were also manufactured with various techniques. In tooth-supported prostheses the dominating technique was the cast technique while newer techniques as laser-sintering and milling were more commonly reported for implant-supported constructions. A fourth technique; the 'pre-state' milling was reported in FDP. <b>Conclusion:</b> More than 30 different Co-Cr alloys were reported as being used in FP. Thus, there is a need for studies exploring the mechanical and physical behavior and the biological response to the most commonly used Co-Cr alloys.</p>","PeriodicalId":6997,"journal":{"name":"Acta Biomaterialia Odontologica Scandinavica","volume":"3 1","pages":"53-62"},"PeriodicalIF":0.0,"publicationDate":"2017-08-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/23337931.2017.1360776","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"35658230","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 32
Water sorption and solubility of polyamide denture base materials. 聚酰胺义齿基托材料的吸水性和溶解度。
Pub Date : 2017-05-13 eCollection Date: 2017-01-01 DOI: 10.1080/23337931.2017.1326009
Long G Nguyen, Hilde M Kopperud, Marit Øilo

Purpose: Some patients experience adverse reactions to poly(methyl methacrylate)-based (PMMA) dentures. Polyamide (PA) as an alternative to PMMA has, however, not been well documented with regard to water sorption and water solubility. The aim of this in vitro study was to measure water sorption and water solubility of two PA materials compared with PMMA, and to evaluate the major components released from the PA materials and the effect on hardness of the materials. Methods: Ten discs (40.0 mm diameter, 2.0 mm thick) of each material (PA: Valplast and Breflex; PMMA: SR Ivocap HIP) were prepared according to manufacturers' recommendations. The specimens were tested for water sorption and water solubility, according to a modification of ISO 20795-1:2008. Released substances were analysed by gas chromatography/mass spectrometry (GC/MS). Results: There were statistically significant differences among the materials regarding water sorption, water solubility and time to water saturation. Breflex had the highest water sorption (30.4 μg/mm3), followed by PMMA-material (25.8 μg/mm3) and Valplast (13.6 μg/mm3). Both PA materials had statistically significant lower water solubility than the PMMA. Both PA had a net increase in weight. Analysis by GC/MS identified release of the compound 12-aminododecanolactam from the material Valplast. No release was found from the Breflex material. Conclusions: The PA denture materials show differences in water sorption and solubility, but within the limits of the standard requirements. The PA showed a net increase in weight after long-term water sorption. The clinical implications of the findings are not elucidated.

目的:一些患者对聚甲基丙烯酸甲酯(PMMA)基假牙有不良反应。然而,聚酰胺(PA)作为PMMA的替代品,在吸水性和水溶性方面还没有得到很好的证明。本体外实验的目的是测定两种PA材料与PMMA相比的吸水性和水溶性,并评价PA材料释放的主要成分及其对材料硬度的影响。方法:每种材料10个(直径40.0 mm,厚2.0 mm) (PA: Valplast和Breflex;PMMA: SR Ivocap HIP)是根据制造商的建议制备的。根据ISO 20795-1:2008的修改,测试了样品的吸水性和水溶性。采用气相色谱/质谱(GC/MS)分析释放物质。结果:两种材料在吸水性、水溶性、达到水饱和时间方面差异有统计学意义。Breflex的吸水率最高(30.4 μg/mm3),其次是PMMA-material (25.8 μg/mm3)和Valplast (13.6 μg/mm3)。两种PA材料的水溶性均显著低于PMMA。两种PA的体重都有净增加。GC/MS分析鉴定了Valplast材料中化合物12-氨基十二醇内酰胺的释放。没有发现Breflex材料的释放。结论:PA义齿材料的吸水性和溶解度存在差异,但均在标准要求范围内。PA在长期吸水后表现出净重量增加。这些发现的临床意义尚未阐明。
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引用次数: 19
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Acta Biomaterialia Odontologica Scandinavica
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