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Surface Texturing on Polycrystalline Diamond Compact Cutter by Nanosecond Laser Processing
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-23 DOI: 10.1002/adem.202402204
Yanbo Ding, Qiankun Li, Ruizhi Jia, Lei Chen, Baochang Liu

In this article, a method for preparing surface texture of polycrystalline diamond compact (PDC) cutter based on nanosecond laser direct is reported. The relationship between the structure of the surface texture with the laser power, scanning speed, and processing cycle of the nanosecond laser is systematically investigated. By changing the laser power, scanning speed, and the number of processing cycle, different nanosecond laser energies are obtained for processing PDC cutter, and the nanosecond laser parameters are precisely changed to achieve the purpose of laser modification and ablation. By controlling the parameters of nanosecond laser processing, micrometer-scale surface texture on PDC cutter are realized. The surface morphology of the resulting preparation is analyzed. This study provids an experimental basis for the utilization of laser surface texturing technology to improve the performance of PDC cutter, and promotes the further research and development of drilling and machining tools.

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引用次数: 0
Recent Progress in Particulate Reinforced Copper-Based Composites: Fabrication, Microstructure, Mechanical, and Tribological Properties—A Review
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-20 DOI: 10.1002/adem.202401748
Chandra Shekhar, Mohmmad Farooq Wani, Rakesh Sehgal, Sheikh Shahid Saleem, Umida Ziyamukhamedova, Nodirjon Tursunov

In recent years, there has been a significant increase in research studies that include the fabrication and characterization of metal matrix composites (MMCs) with unique features. This comprehensive review delves into the evolution and current status of copper MMCs (Cu-MMCs) across various industrial sectors. Cu-MMCs have garnered attention due to their remarkable properties, which include excellent thermal and electrical conductivity, corrosion resistance, and wear resistance. This study explores the fabrication processes, and intricate connections between microstructure and properties of Cu-MMCs, which encompass ceramic and solid lubricants (SLs) reinforcements. The various types of reinforcement and fabrication methods are examined and highlighted advancements in designing compositions and optimizing microstructures during fabrication. Additionally, this study evaluates the friction and wear characteristics of self-lubricating hybrid composites, providing insights into effective lubrication ranges and overall tribological behavior patterns. This review highlights that Cu-MMCs demonstrate superior mechanical strength, wear resistance, and self-lubricating properties due to ceramics and SLs reinforcements. The mechanisms underlying this behavior involve the formation of a protective transfer layer during sliding and effective lubrication provided by SLs, which reduces direct contact and facilitates smoother interactions between the mating surfaces. The review culminates in an outlook on the prospects of Cu-MMCs, emphasizing the advantages conferred by their utilization.

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引用次数: 0
Porosity Reduction and Strength Increase of SS316&Cu Produced through Cold Spray Additive Manufacturing
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-20 DOI: 10.1002/adem.202402181
Michael Pagan, Styler Goring, HuChun Yi, Aaron P. Stebner

Cold spray additive manufacturing (CSAM) is an attractive solid-state bonding technique due to its rapid manufacturing rate and the ability to avoid deleterious effects found in solidification-based additive manufacturing. Unfortunately, CSAM of steel components has been difficult to date to the high strength of the steel particles which resists deformation and creates interparticle porosity. Herein, it is found adding softer Cu powder particles to steel (SS316) powder and utilizing a heat treatment can decrease the porosity of the as-sprayed structure while increasing the mechanical properties. The mixture results in an increased sprayability of the structure, as the Cu particles preferentially fill the pores, increasing the density. The microstructural evolution of the SS316 and Cu particles at the particle interfaces and interiors is investigated and reveals that the materials undergo a heterogeneous deformation route which facilitates the densification of the CSAM structure. Through annealing these components, the tensile strength increases and the density increases further. Both materials undergo microstructural recovery along with selected interdiffusion of elements which improves the metallurgical bonding. It is demonstrated that the heterogeneous deposition and microstructural evolution between the dissimilar materials can improve the overall component properties.

冷喷增材制造(CSAM)是一种极具吸引力的固态粘接技术,因为它不仅制造速度快,而且能够避免基于凝固的增材制造所产生的有害影响。遗憾的是,迄今为止,钢部件的 CSAM 一直难以实现,原因是钢颗粒的高强度会阻碍变形并产生颗粒间孔隙。本文发现,在钢(SS316)粉末中加入较软的铜粉末颗粒并进行热处理,可以降低喷涂结构的孔隙率,同时提高机械性能。这种混合物可提高结构的可喷涂性,因为铜颗粒会优先填充孔隙,从而增加密度。对 SS316 和铜粒子在粒子界面和内部的微观结构演变进行了研究,结果表明,这些材料经历了异质变形过程,从而促进了 CSAM 结构的致密化。通过退火,这些成分的抗拉强度增加,密度进一步提高。这两种材料都经历了微观结构的恢复以及元素的选择性相互扩散,从而改善了冶金结合。这表明,异种材料之间的异质沉积和微观结构演变可以改善部件的整体性能。
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引用次数: 0
An Experimental and Computational Framework to Investigate the Microstructural Effects on the Mechanical Properties of Pearlitic Steels
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-20 DOI: 10.1002/adem.202402441
Ravi Kiran Bollineni, Reza Mirzaeifar, Mehdi Ahmadian, Ling Li

Fully pearlitic steels are essential in many demanding structural applications due to their exceptional mechanical properties. These superior mechanical properties are attributed to the microstructural features of pearlite. However, investigating these steels via entirely experimental approaches is both time-consuming and costly, and only limited computational frameworks consider mesoscale plastic deformation of ferrite and cementite phases. This study introduces a comprehensive framework, integrating experimental and computational approaches, to scrutinize the impact of microstructural features on the mechanical behavior of pearlitic steels. Assigning specific plastic deformation and damage mechanics material models to the phases in the pearlite microstructure, along with calibrated parameters, enables a detailed investigation of the relationship between microstructure and mechanical behavior. Consistent with previous findings, the results show that a higher cementite volume fraction improves strength but diminishes failure strain, while increased interlamellar spacing correlates with reductions in both strength and fracture strain. Varying from random ferrite orientations to the [110] texture increases strength and reduces failure strain. These results validate the computational approach and reinforce the relationships between microstructural attributes and mechanical properties in pearlitic steels. Additionally, the study provides the basis for further computational material design that can enable tailored microstructures to achieve desired mechanical properties.

全珠光体钢因其卓越的机械性能,在许多要求苛刻的结构应用中至关重要。这些优异的机械性能归功于珠光体的微观结构特征。然而,完全通过实验方法研究这些钢既费时又费钱,而且只有有限的计算框架考虑了铁素体和雪明碳酸盐相的中尺度塑性变形。本研究引入了一个综合框架,整合了实验和计算方法,以仔细研究微观结构特征对珠光体钢机械行为的影响。将特定的塑性变形和损伤力学材料模型与校准参数一起分配给珠光体微结构中的各相,可以详细研究微结构与力学行为之间的关系。与之前的研究结果一致,研究结果表明,较高的雪明碳柱体积分数会提高强度,但会降低破坏应变,而增加层间间距则会降低强度和破坏应变。从随机铁素体取向到[110]纹理的变化可提高强度并降低破坏应变。这些结果验证了计算方法,并加强了珠光体钢中微观结构属性与机械性能之间的关系。此外,该研究还为进一步的计算材料设计提供了基础,从而可以定制微结构以实现所需的机械性能。
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引用次数: 0
3D-Printed Pyramidal Honeycomb Structures Plated with Silver and Infused with Fe3O4–Epoxy Composite for Microwave Absorption Applications
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-20 DOI: 10.1002/adem.202402030
Ubaid ur Rehman, Ahmed Bilal, Junaid Faizan, Asif Warsi, Amna Ramzan, Khaqan Shati, Muhammad Nadeem

As the electronic industry continues to progress, there is a parallel increase in demand of materials for advanced electromagnetic interference (EMI) shielding. A hybrid approach is introduced by combining 3D geometrical structure with the integration of radar-absorbing materials (RAMs) to develop absorptive materials. Present study involves the fabrication of polylactic acid-based pyramidal honeycomb structures using 3D printing technology, followed by electroless silver plating and infusion with Fe3O4/epoxy composite. These developed structures/materials test comprehensive within frequency range of 8.2–12.4 GHz (X-band) using free space, and waveguide methods, focusing on both electromagnetic properties of RAM and EMI shielding performance of structures. Experimental results showcase exceptional potential of fabricated structures, demonstrating efficient EMI shielding up-to −55 dB, equivalent to 99.999% attenuation of EM waves. Particularly noteworthy is the dominant role of absorption as a primary shielding mechanism, as evidenced by more than 99% (−20 dB) absorption across the entire tested frequency spectrum.

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引用次数: 0
High-Temperature Oxidation Behavior and Grinding Performance of CoCrFeMnNi High-Entropy Alloy
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-20 DOI: 10.1002/adem.202401927
Jiangyu Zhang, Yueqiu Liu, Yanling Chen, Shizhao Liu

Herein, the mechanical properties, oxidation behavior, and processing performance of the CoCrFeNiMn high-entropy alloy are investigated using multiple characterization methods. The alloy exhibits a yield stress of 462 MPa, an ultimate tensile strength of 1037 MPa, and a fracture strain of 31.8% at room temperature. Oxidation tests reveal that the oxide layer consists of an outermost oxide layer and a Cr2O3 layer at both 1000 and 1200 °C. The Cr2O3 layer formed at 1000 °C is dense and continuous, whereas it transitions from continuous to discontinuous as the temperature increases to 1200 °C. Localized peeling of the oxide layer is observed at 1200 °C due to the diminished protective effect of the Cr2O3 layer and the increased stress in the oxide layer caused by the formation of multiple complex oxides. Grinding experiments indicate that both the grinding force and surface roughness increase as the load increases. Additionally, energy-dispersive X-ray spectroscopy results show that the oxygen content of particles at a 120 N is higher than at 60 and 90 N, suggesting an elevated grinding temperature at 120 N, which leads to the formation of bonded convex particles.

本文采用多种表征方法研究了 CoCrFeNiMn 高熵合金的机械性能、氧化行为和加工性能。该合金在室温下的屈服应力为 462 兆帕,极限拉伸强度为 1037 兆帕,断裂应变为 31.8%。氧化测试表明,在 1000 和 1200 °C 温度下,氧化层由最外层氧化层和 Cr2O3 层组成。在 1000 ℃ 时形成的 Cr2O3 层致密且连续,而当温度升高到 1200 ℃ 时,则从连续过渡到不连续。在 1200 ℃ 时,由于 Cr2O3 层的保护作用减弱以及多种复合氧化物的形成导致氧化层应力增加,氧化层出现局部剥落。磨削实验表明,随着载荷的增加,磨削力和表面粗糙度都会增加。此外,能量色散 X 射线光谱分析结果表明,120 N 时颗粒中的氧含量高于 60 N 和 90 N 时的氧含量,这表明 120 N 时磨削温度升高,导致形成粘结凸粒。
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引用次数: 0
Enhanced Oxidation Resistance of Pt-Containing Inconel 718 Alloy through Facilitated Formation of Protective Chromia
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202402008
Jianshu Zheng, Boning Zhang, Guowei Wang, Lan Liu, Chao Shen, Zhuorui Song, Lei Zheng

This study investigates the influence of Pt addition on the oxidation behavior of a Cr2O3-forming superalloy. Inconel 718 (IN718) alloys with varying Pt content were prepared and subjected to isothermal oxidation tests. The results demonstrate that Pt significantly enhances the oxidation resistance of IN718, as evidenced by reduced weight gain, thinner oxide layers, and smaller oxide particles. Pt addition also increases the activation energy for both initial interface oxidation and ion diffusion during long-term oxidation. Furthermore, Pt promotes the formation of a Cr2O3 layer while suppressing the formation of other undesirable oxides, resulting in a more cohesive and stable oxide layer. The improved oxidation resistance is attributed to two key factors: during the initial oxidation stage, Pt, as a noble element, reduces the activity of the primary oxide-forming element Cr to oxidative environments, thereby lowering its susceptibility to initial oxidation at the metal–oxidant interface. During long-term oxidation, Pt preferentially substitutes for Ni in major phases such as γ-Ni(Cr,Fe) and γ′-Ni3(Al,Ti), locally increasing the Cr composition. This promotes Cr oxidation, effectively suppressing the oxidation of Ni or Fe. These findings suggest that Pt addition is a promising approach for enhancing oxidation resistance in alloy design.

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引用次数: 0
Near-Infrared Reflectance, Thermal Shielding, and Corrosion Resistance of Neodymium-Modified Zinc Aluminate Spinel-Based Zinc Phosphate Coatings
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202401351
Subodhana Praballian Aswathy, Asha S. Kumar, Viswanathan S. Saji, Sheik Muhammadhu Aboobakar Shibli

Given the increasing demand for energy-efficient and durable coatings, particularly in outdoor environments, this study investigates the development of lavender-shaded neodymium (Nd)-modified zinc aluminate pigment for thermal energy-saving applications. The results evidence the potential of incorporating this Nd-modified ZnAl2O4 pigment in zinc phosphate (ZP) coating to tune the morphology, microstructure, near-infrared (NIR) reflectance, thermal shielding, and corrosion resistance capability. The study provides a detailed elucidation of the mechanism of pigment particles’ incorporation into ZP coating, revealing enhanced nucleation and crystal size refinement, leading to denser coating with improved NIR reflectance and corrosion resistance, with aesthetic requirements potentially suitable for outdoor environments. Quantitative analysis reveals a maximum NIR reflectance of 93%, thermal shielding capacity with a temperature difference of 15.4 °C, and a more than threefold reduction in corrosion current density. The study underscores the potential of these coatings for energy-saving applications and outdoor use, highlighting their stability and effectiveness in various environmental conditions.

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引用次数: 0
Effect of Four Process Parameters on Flexural Strength and Porosity of Metakaolin Ceramics Fabricated by Material Extrusion: Optimization and Predictive Models via Orthogonal Experiments
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202401197
Ming Wu, Fuchu Liu, Yuxiao Lin, Miao Wang, Yi Wang, Shilin Zhou, Hao Liu, Guangchao Han

A high-strength metakaolin-based porous ceramics are fabricated using slurry-based material extrusion via optimizing four key process parameters, including nozzle internal diameter, height to diameter ratio, filling rate, and printing speed. The orthogonal experiments are used to adjust flexural strength and porosity, and the optimal process parameters are obtained by comprehensive scoring and range analysis methods. The predictive models of strength-parameters, porosity-parameters, and strength-porosity are established and validated. The results show that the optimal process parameters for high-strength and high-porosity ceramics are 0.51 mm nozzle internal diameter, 70% height to diameter ratio, 100% filling rate, and 15 mm s−1 printing speed. The correctness and predictability of three predictive models are proved by two methods, which are the mutual validation and comparison between theoretical and actual values. And the error rates between theoretical and actual results are less than 7%. This work provides guidance for the rapid fabrication of ceramics with adjustable strength and porosity by material extrusion, and the established predictive models can pave the way for its wider application in the practice.

{"title":"Effect of Four Process Parameters on Flexural Strength and Porosity of Metakaolin Ceramics Fabricated by Material Extrusion: Optimization and Predictive Models via Orthogonal Experiments","authors":"Ming Wu,&nbsp;Fuchu Liu,&nbsp;Yuxiao Lin,&nbsp;Miao Wang,&nbsp;Yi Wang,&nbsp;Shilin Zhou,&nbsp;Hao Liu,&nbsp;Guangchao Han","doi":"10.1002/adem.202401197","DOIUrl":"https://doi.org/10.1002/adem.202401197","url":null,"abstract":"<p>A high-strength metakaolin-based porous ceramics are fabricated using slurry-based material extrusion via optimizing four key process parameters, including nozzle internal diameter, height to diameter ratio, filling rate, and printing speed. The orthogonal experiments are used to adjust flexural strength and porosity, and the optimal process parameters are obtained by comprehensive scoring and range analysis methods. The predictive models of strength-parameters, porosity-parameters, and strength-porosity are established and validated. The results show that the optimal process parameters for high-strength and high-porosity ceramics are 0.51 mm nozzle internal diameter, 70% height to diameter ratio, 100% filling rate, and 15 mm s<sup>−1</sup> printing speed. The correctness and predictability of three predictive models are proved by two methods, which are the mutual validation and comparison between theoretical and actual values. And the error rates between theoretical and actual results are less than 7%. This work provides guidance for the rapid fabrication of ceramics with adjustable strength and porosity by material extrusion, and the established predictive models can pave the way for its wider application in the practice.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 2","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-12-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143116019","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
An Interactive Fluid–Solid Approach for Numerical Modeling of Composite Metal Foam Behavior under Compression 复合材料金属泡沫压缩行为流固耦合数值模拟方法
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202470070
Aman Kaushik, Afsaneh Rabiei

Composite Metal Foam Behavior

In article number 2401267, Afsaneh Rabiei and Aman Kaushik present a numerical approach to study the performance of composite metal foam (CMF) under compression using smooth particle hydrodynamics modeling of entrapped air inside the porosities of CMF. The numerical and experimental results agree well, opening room to further the fluid–solid interaction study of entrapped air inside the porosities of CMF to effectively predict its performance under a variety of loading scenarios.

在文章2401267中,Afsaneh Rabiei和Aman Kaushik提出了一种数值方法来研究复合金属泡沫(CMF)在压缩条件下的性能,该方法采用光滑颗粒流体动力学模型来模拟CMF孔隙内的夹闭空气。数值结果与实验结果吻合较好,为进一步开展CMF孔隙内夹持空气的流固相互作用研究,有效预测CMF在各种加载工况下的性能开辟了空间。
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引用次数: 0
期刊
Advanced Engineering Materials
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