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An Interactive Fluid–Solid Approach for Numerical Modeling of Composite Metal Foam Behavior under Compression 复合材料金属泡沫压缩行为流固耦合数值模拟方法
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202470070
Aman Kaushik, Afsaneh Rabiei

Composite Metal Foam Behavior

In article number 2401267, Afsaneh Rabiei and Aman Kaushik present a numerical approach to study the performance of composite metal foam (CMF) under compression using smooth particle hydrodynamics modeling of entrapped air inside the porosities of CMF. The numerical and experimental results agree well, opening room to further the fluid–solid interaction study of entrapped air inside the porosities of CMF to effectively predict its performance under a variety of loading scenarios.

在文章2401267中,Afsaneh Rabiei和Aman Kaushik提出了一种数值方法来研究复合金属泡沫(CMF)在压缩条件下的性能,该方法采用光滑颗粒流体动力学模型来模拟CMF孔隙内的夹闭空气。数值结果与实验结果吻合较好,为进一步开展CMF孔隙内夹持空气的流固相互作用研究,有效预测CMF在各种加载工况下的性能开辟了空间。
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引用次数: 0
Manufacturing of Continuous Core–Shell Hydrated Salt Fibers for Room Temperature Thermal Energy Storage 室温储热用连续芯壳水合盐纤维的研制
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-18 DOI: 10.1002/adem.202470068
Michael D. Toomey, Nihal Kanbargi, Logan T. Kearney, Holly Hinton, Sumit Gupta, Reyad Sawafta, Amit K. Naskar, Jaswinder Sharma

Room Temperature Thermal Energy Storage

In article number 2400012, Michael D. Toomey, Jaswinder Sharma, and co-workers demonstrate the first example of wet-spun PCM fibers comprised of a polymer sheath and a salt hydrate core for thermal energy storage applications. Fibers produced using this scalable production method achieve enthalpies of melting of ca. 130 J/g, melting onset at 29°C, and supercooling of 4.8°C while retaining 96.5% of its phase change capacity after 1000 cycles.

在2400012号文章中,Michael D. Toomey、Jaswinder Sharma及其同事展示了湿纺PCM纤维的第一个例子,该纤维由聚合物护套和盐水合物芯组成,用于热能储存应用。使用这种可扩展的生产方法生产的纤维的熔化焓约为130 J/g,熔化开始于29°C,过冷度为4.8°C,在1000次循环后保持96.5%的相变能力。
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引用次数: 0
Synthesis of Spherical Hexagonal Boron Nitride via Precursor Morphology Control 通过前驱体形态控制合成球形六方氮化硼
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-04 DOI: 10.1002/adem.202470064
Minho Nam, Gyeongho Yun, Suhyeon Cho, Rian Kim, Seog-Young Yoon, Seunghyup Lee

Spherical Hexagonal Boron Nitride

In article number 2401027, Seog-Young Yoon, Seunghyup Lee, and co-workers propose a synthetic strategy for submicron-scale spherical hexagonal boron nitride (s-BN) particles using a droplet-based morphology control method. s-BN exhibits superior fluidity, allowing for homogeneous dispersion and alignment within the polymer matrix. s-BN can be applied to thermal management by overcoming the limitations of conventional shapes while preserving its original advantages.

在文章编号2401027中,Seog-Young Yoon, Seunghyup Lee及其同事提出了一种利用基于液滴的形貌控制方法合成亚微米尺度球形六方氮化硼(s-BN)颗粒的策略。s-BN表现出优越的流动性,允许均匀分散和排列在聚合物基体内。s-BN可以应用于热管理,克服传统形状的限制,同时保持其原有的优势。
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引用次数: 0
Microreactor-Assisted Soft Lithography for Rapid and Inexpensive Patterning of Nanostructured ZnO/CuO Heterojunctions 微反应器辅助软光刻快速和廉价的纳米结构ZnO/CuO异质结图像化
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-04 DOI: 10.1002/adem.202470065
Zhongwei Gao, V. Vinay K. Doddapaneni, Changqing Pan, Rajiv Malhotra, Chih-hung Chang

Microreactor-Assisted Soft Lithography

In article number 2401112, Chih-hung Chang and co-workers demonstrate a novel microreactor-assisted soft lithography process to deposit nanostructures with multiscale 3D geometric shapes and fabricate p-n heterojunction with n-type ZnO and p-type CuO. Factors determining the printing process are studied based on COMSOL simulation and experimental results. This novel process enables the scalable fabrication of complicated functional nanostructures on the desired regions using low-cost and facile solution-based methods.

在文章编号2401112中,张志宏和他的同事展示了一种新的微反应器辅助软光刻工艺,可以沉积具有多尺度三维几何形状的纳米结构,并用n型ZnO和p型CuO制备p-n异质结。基于COMSOL仿真和实验结果,研究了影响打印过程的因素。这种新颖的工艺可以使用低成本和简单的基于溶液的方法在所需区域上可扩展地制造复杂的功能纳米结构。
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引用次数: 0
High-Throughput Production of Gelatin-Based Touch-Spun Nanofiber for Biomedical Applications 高通量生产用于生物医学应用的明胶基触纺纳米纤维
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-04 DOI: 10.1002/adem.202470067
Md Farhad Ismail, Rong Wu, Maedeh Khodamoradi, Islam Hassan, P. Ravi Selvaganapathy

Touch-Spun Nanofibers

In article number 2401022, P. Ravi Selvaganapathy and co-workers present gelatin-zein composite nanofibers formed at high throughput through collectorless touch spinning

在文章编号2401022中,P. Ravi Selvaganapathy及其同事介绍了通过无收集器接触纺丝制备的高通量明胶-玉米蛋白复合纳米纤维
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引用次数: 0
Combining Micro and Macro Relative Density: An Experimental and Computational Study on Hierarchical Porous 3D-Printed Polylactic Acid Structures 结合微观和宏观相对密度:分层多孔 3D 印刷聚乳酸结构的实验和计算研究
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-23 DOI: 10.1002/adem.202402012
Savvas Koltsakidis, Konstantinos Tsongas, Dimitrios Tzetzis

Polymer foams and cellular solids have gained significant interest due to their enhanced properties. This study introduces a novel approach by employing foamed fused filament fabrication printing of cellular solids. A composite polylactic acid filament containing chemical blowing agents is used to create structures with varying micro relative density, which is examined through scanning electron microscopy and tensile testing, with comparisons made to a Mori Tanaka analytical model and representative volume elements investigation. Two different types of cellular solid structures, specifically body-centered cubic and Gyroid triple periodic minimal surface structures, have been created with different thicknesses and printed at various temperatures. This is done to attain a range of micro- and macroporosity, leading to samples with equal total relative densities. Compression tests, coupled with finite element analysis, provide insights into the influence of each type of porosity. The fabricated specimens exhibit compressive strengths ranging from 1.07 to 79.14 MPa and elastic moduli ranging from 0.064 to 3.35 GPa. The findings suggest that porous structures relying on macroporosity exhibit higher compressive strength, while those relying on microporosity demonstrate more appealing energy absorption properties, particularly under stresses approaching the plateau region.

聚合物泡沫和蜂窝状固体由于其增强的性能而获得了极大的兴趣。本研究介绍了一种利用泡沫熔丝制造多孔固体材料的新方法。使用含有化学发泡剂的复合聚乳酸长丝来创建具有不同微相对密度的结构,通过扫描电子显微镜和拉伸测试进行了检查,并与Mori Tanaka分析模型和代表性体积元素进行了比较。两种不同类型的细胞固体结构,特别是体心立方和陀螺三周期最小表面结构,已经创建了不同厚度和不同温度下的打印。这样做是为了获得一定范围的微观和宏观孔隙度,从而使样品具有相等的总相对密度。压缩试验与有限元分析相结合,可以深入了解每种孔隙度的影响。试样的抗压强度为1.07 ~ 79.14 MPa,弹性模量为0.064 ~ 3.35 GPa。研究结果表明,依赖于大孔隙度的多孔结构具有更高的抗压强度,而依赖于微孔隙度的多孔结构具有更吸引人的能量吸收特性,特别是在接近高原地区的应力下。
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引用次数: 0
Thermally Induced Enhancement of Photoresponse in Radio Frequency-Sputtered CdS Thin-Film Photodetectors 热诱导增强射频溅射CdS薄膜光电探测器的光响应
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-23 DOI: 10.1002/adem.202401942
Athulkrishna Manilal, Shantikumar Nair, Laxman Raju Thoutam

This work focuses on understanding the defect-related electronic transport in cadmium sulfide (CdS) thin films, and finds thermal treatment as an efficient tool to tailor its intrinsic defect charge carrier concentration for optimum visible-light photodetection performance. The radio frequency (RF)-sputtered CdS thin-films show a substantial decrease in measured dark-current by three orders of magnitude (μA to nA) with an increase in substrate deposition temperature (Ts) from room-temperature (RT) to a maximum of 400 °C. With increase in Ts, the current conduction behavior changes from Ohmic (at RT) to Schottky-behavior (Ts ≥ 100–400 °C). The decrease in dark-current and the crossover from Ohmic to Schottky electronic transport behavior, pointed to a decrease in defect-density charge carrier concentration, with increased Ts. Additionally, post-deposition thermal annealing of CdS thin films also is found to result in a similar decrease in dark-current (μA to nA). The photo-to-dark-current ratio of CdS thin-film visible-light photodetectors increased by two-orders of magnitude, and its dynamic response time decreased by an order of magnitude via. thermal engineering. The thermal-annealing treatment possibly reduced the defect-related trap-sites, which enables a reliable and faster photo-switching response for CdS thin-film-based visible-light photodetectors.

本研究的重点是了解硫化镉(cd)薄膜中与缺陷相关的电子输运,并发现热处理是一种有效的工具,可以调整其固有缺陷电荷载流子浓度,以获得最佳的可见光光电探测性能。随着衬底沉积温度(Ts)从室温(RT)升高到最高400℃,射频溅射CdS薄膜的暗电流测量值(μA ~ nA)显著降低了3个数量级。随着Ts的增加,电流传导行为从欧姆(RT)转变为肖特基行为(Ts≥100-400℃)。暗电流的减小和从欧姆到肖特基电子输运行为的交叉表明,缺陷密度载流子浓度随着Ts的增加而降低。此外,沉积后CdS薄膜的热退火也发现了类似的暗电流(μA到nA)的降低。CdS薄膜可见光探测器的光暗电流比提高了两个数量级,动态响应时间降低了一个数量级。热工程。热退火处理可能会减少缺陷相关的陷阱位点,从而为基于CdS薄膜的可见光光电探测器提供可靠和更快的光开关响应。
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引用次数: 0
Effect of an Electrical Field Applied to the Metal Capping Layer on the Electrical Properties of SiZnSnO Thin-Film Transistors for Touch Sensor Application 施加在金属盖层上的电场对用于触摸传感器的SiZnSnO薄膜晶体管电性能的影响
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-23 DOI: 10.1002/adem.202401555
Sunjin Lee, Sang Yeol Lee

Thin-film transistors (TFTs) have been studied for their high mobility and stability to facilitate the development of TFT-based touch sensors and electronic devices. A metal capping (MC) layer on the back channel of Si–Zn–Sn–O(SZTO) TFTs has been proposed to improve the electrical properties. MC, when adopted on the channel layer, has low resistance, leading to an improvement in the mobility of the TFT. The mobility of Ti/Al MC TFT has improved from 20.7 to 37.9 cm2 V−1 s compared to the pristine TFTs. Applying a potential voltage to the MC layer sensitively modulates the IV characteristics of the TFT. The present study applies a voltage of 60 mV, similar to that of the human body, to MC-TFTs to explore their possibilities as human touch sensors. The sensitivity and the energy bandgap modulation are also discussed.

薄膜晶体管(TFTs)由于其高迁移性和稳定性而受到广泛的研究,从而促进了基于薄膜晶体管的触摸传感器和电子器件的发展。提出了在Si-Zn-Sn-O (SZTO) TFTs的后通道上添加金属封盖层(MC)以改善其电学性能。当在通道层上采用MC时,具有低电阻,导致TFT的迁移率提高。与原始TFT相比,Ti/Al MC TFT的迁移率从20.7 cm2 V−1 s提高到37.9 cm2 V−1 s。对MC层施加电位电压可灵敏地调制TFT的I-V特性。目前的研究对mc - tft施加了与人体相似的60毫伏电压,以探索其作为人体触摸传感器的可能性。讨论了灵敏度和能量带隙调制。
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引用次数: 0
Thermo-mechanical Study on Auxetic Shape Memory Periodic Open Cellular Structures—Part II: Mechanical and Shape Memory Properties 增塑型形状记忆周期开孔结构的热力学研究——第二部分:力学和形状记忆性能
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-22 DOI: 10.1002/adem.202401310
Alexander Fink, Dominik Rudolf, Benjamin Wahlmann, Hannsjörg Freund, Carolin Körner

This study explores the potential of periodic open cellular structures (POCS) that combine the auxetic and the shape memory effect (SME) with the aim of enhancing heat transfer in catalytic tubular reactors. On the one hand, these structures exhibit a negative Poisson's ratio, contracting perpendicular to the load axis under compression, driven by the rotation of nodes generating complex stress fields. On the other hand, the shape memory alloy (SMA) Nitinol (NiTi) with a reversible strain of up to 8% produced via electron beam powder bed fusion (PBF-EB) shows extraordinary material properties with a high degree of freedom in structure design. The study conducts finite element method simulations and experiments to design POCS with tailored properties. Compression tests on less expensive Ti-6Al-4V POCS compared to NiTi POCS validate the simulative parameter study applied to fabricate novel auxetic hexagonal reentrant structures from NiTi with a unique stacking order and curved struts. The aim of this part of the study is to offer a pathway to design a NiTi auxetic POCS based on validated simulations. Further, it explains the interactions between geometrical parameters and mechanical properties of cellular reentrant NiTi structures. An optimized auxetic NiTi POCS achieved a Poisson's ratio of −1.

本研究探讨了周期开孔结构(POCS)的潜力,该结构结合了辅助和形状记忆效应(SME),旨在增强催化管式反应器的传热。一方面,这些结构在产生复杂应力场的节点旋转的驱动下,呈现负泊松比,在压缩下垂直于荷载轴收缩。另一方面,通过电子束粉末床熔合(PBF-EB)制备的可逆应变高达8%的形状记忆合金(SMA) Nitinol (NiTi)在结构设计上具有很高的自由度,表现出非凡的材料性能。本研究通过有限元模拟和实验来设计具有定制性能的POCS。在较便宜的Ti-6Al-4V POCS和NiTi POCS上进行的压缩试验验证了模拟参数研究应用于由NiTi制造具有独特堆叠顺序和弯曲支撑的新型auxetic六角形可重入结构。这部分研究的目的是提供一种基于验证仿真的NiTi辅助POCS设计途径。此外,它解释了几何参数和细胞可重入NiTi结构的力学性能之间的相互作用。优化后的增塑型NiTi POCS的泊松比为−1。
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引用次数: 0
Correction to “Fatigue Crack Characteristics in Gradient Predeformed Pearlitic Steel under Multiaxial Loading” 对 "多轴载荷下梯度预变形珠光体钢的疲劳裂纹特征 "的更正
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-21 DOI: 10.1002/adem.202402410
D. Gren, J. Ahlström, M. Ekh

Adv. Eng. Mater. 2024, 26, 2400950, https://doi.org/10.1002/adem.202400950

In Figure A3 the top left subfigure should be replaced as it is a duplicate of the center top subfigure. In the below figure, the top left subfigure of Figure A3 is replaced.

We would also like to make an adjustment to the text in section 3.4 Crack Path to better match the new image. In the first paragraph under section 3.4 Crack Path, the text should read:

The difference in crack path between the undeformed material PD0 and PD1 is small. Both show an inclined crack growth, but the crack propagates at a slightly shallower angle for PD1. However, as the degree of predeformation increases to PD3, a marked difference is observed. The crack now propagates closer to the direction of the microstructure alignment resulting from the predeformation, leading to a transverse fracture. For both duplicate PD3 test bars and one of the PD1 test bars, the final fatigue crack length prior to fracture is much shorter compared to the other cases. This indicates that at certain combinations of predeformation, crack geometry, and loading, the effective critical stress intensity is reached at shorter crack lengths.

Adv.Mater.2024, 26, 2400950, https://doi.org/10.1002/adem.202400950In 图 A3 左上方的子图应替换掉,因为它与中间上方的子图重复。在下图中,图 A3 的左上角子图已被替换。我们还希望对第 3.4 节 "裂纹路径 "中的文字进行调整,以便与新图片更加匹配。在第 3.4 节 "裂纹路径 "的第一段中,文字应为:未变形材料 PD0 和 PD1 的裂纹路径差异很小。两者都显示出倾斜的裂纹生长,但 PD1 的裂纹扩展角度稍小。然而,当预变形程度增加到 PD3 时,就会发现明显的不同。现在,裂纹的扩展方向更接近预变形产生的微观结构排列方向,从而导致横向断裂。对于两个 PD3 试验棒和一个 PD1 试验棒,断裂前的最终疲劳裂纹长度与其他情况相比要短得多。这表明,在预变形、裂纹几何形状和加载的特定组合下,有效临界应力强度在较短的裂纹长度上就能达到。
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引用次数: 0
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