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Low Loss Chip-to-Chip Couplers for High-Density Co-Packaged Optics
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-02-18 DOI: 10.1002/adem.202570012
Drew Weninger, Samuel Serna, Luigi Ranno, Lionel Kimerling, Anuradha Agarwal

Co-Packaged Optics

In article number 2402095, Drew Weninger, Samuel Serna, and co-workers present a co-packaged optics system with an electrical chip (black, center) surrounded by 8 silicon photonic chips. Chips are bonded using an automated pick-and-place tool, shown placing the final chip into position. The automation is enabled by a novel optical chip-to-chip coupler (green callout).

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引用次数: 0
Reactive Multilayers, Their Design and Their Applications: Bonding, Debonding, Repair, Recycle
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-02-04 DOI: 10.1002/adem.202402295
Anne Jung, Christoph Pauly, Peter Schaaf
<p>While the redox-reaction-based thermite mixtures for exothermic reactions are well-known since a long time, systematic research on non-thermite reactive materials dates back to the 1960s in the USSR when Merzhanov and Borovinskaya did groundbreaking work on powder-based transition metal/carbon mixtures. Since then, the class of ingredients has widened to include metal/metal mixtures and with the progress in physical vapor deposition, precise nanoscale layering of the reactant has become possible. These reactive multilayer systems (RMS), comprising up to several hundred repetitions of individual layers, reach total film thicknesses of up to several tens of micrometers. The characteristic of these films is their capability of undergoing self-propagating exothermic reactions at up to ≈100 m/s and 2000 °C and more. Thermodynamics, reaction kinetics as well as thermal and chemical diffusion set the boundary conditions defining the reaction properties, thus providing means for reaction design.</p><p>The application of such self-propagating reactions is of great technological interest, e.g. for the joining of electronic components in electronics, the debonding of parts or even a repair of failure parts. However, the self-propagating reaction after multilayer ignition is hard to control in real technical systems. While the influence of the most prominent parameter, the bilayer thickness, has been studied extensively for various material combinations, many open questions exist regarding the effect of factors like surfaces, materials properties, roughness, morphology, thermo-mechanical stress, structuring or combined systems.</p><p>This special issue contains the latest research on such reactive multilayer systems based on Ni/Al and Ru/Al, the current understanding and their applications. The articles investigate the impact of the morphological characteristics and physical properties of the joining partners on the microstructural features of the fabricated RMS, as well as the role of thermophysical properties of the system and the kinetics of the reaction. The vision is the design of a “suitable” microjoining process with fitting electrical and thermal properties of a high-quality mechanical joining <b>Figure</b> 1.</p><p>Means to manipulate and tailor the reaction are explored for both improving the understanding of fundamental mechanisms as well as for application on a system level. Different approaches for multilayer modification by substrate patterning are investigated, i.e. photolithography, deep etching and direct laser interference patterning. The resulting structure shows more or less strong deviations from the well-known planar multilayer structure when depositing on flat substrates, like curved layers, pores and discontinuities, which unfold their effect on the scale of up to a few bilayers. Their effects on the self-propagating reactions are discussed with respect to thermal and chemical diffusivity and interface mixing. These modifications o
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引用次数: 0
Tailoring the Reaction Path: External Crack Initiation in Reactive Al/Ni Multilayers
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-02-04 DOI: 10.1002/adem.202570009
Sebastian Matthes, Marcus Glaser, Emina Vardo, Yesenia Haydee Sauni Camposano, Konrad Jaekel, Jean Pierre Bergmann, Peter Schaaf

Reactive Al/Ni Multilayers

The image depicts a reactive multilayer system (RMS) envisioned for future chip-bonding applications. Individual layers of aluminum (Al) and nickel (Ni) are activated by a brief energy pulse, initiating a diffusion-driven reaction that reaches peak temperatures up to 1500 °C. In the course of this self-sustaining high-temperature synthesis, the two face-centered cubic metals transform into a body-centered cubic AlNi B2 phase. Further details can be found in article number 2302271 by Sebastian Matthes and co-workers.

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引用次数: 0
Impact of Sample Preparation Approach on Transmission Electron Microscopy Investigation of Sputtered AlNi Multilayers Used for Reactive Soldering
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-02-04 DOI: 10.1002/adem.202570011
Juan Jesús Jiménez, Konrad Jaekel, Christoph Pauly, Christian Schäfer, Heike Bartsch, Frank Mücklich, Francisco Miguel Morales

Sputtered AlNi Multilayers

In article number 2302215, Juan Jesús Jiménez and co-workers show that preparation methods have crucial influence on transmission electron microscopy results when investigating the intermixing between Al and Ni in reactive multilayers. The comparison of three lamella preparation methods shows that Xe-based FIB leads to low contamination, although Ga-FIB is a good alternative. This outcome presents an important aspect for the investigation of self-sustaining reactions on nanostructures and rough surfaces.

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引用次数: 0
Low-Velocity Impact Behavior of 3D-Printed Sandwich Panels with Integrated Composite Face Sheets 集成复合材料面板的 3D 打印夹芯板的低速冲击性能
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-23 DOI: 10.1002/adem.202401923
Sajad Karami, Mojtaba Haghighi-Yazdi, Majid Safarabadi

Composite panels are made of a core and skins that are typically bonded with adhesive. Traditional adhesive bonding is time-consuming and requires precision, often leading to debonding under varied loading conditions. Additionally, thermal expansion differences between the core, skin, and adhesive cause residual stresses, compromising performance. This research develops a cost-effective method for creating integrated sandwich panels, addressing the effectiveness of such unification under low-velocity impact loading. Using a standard dual-nozzle fused deposition modeling 3D printer with minimal modifications, continuous fibers embedded in a thermoplastic polymer for the skin and a thermoplastic polymer for the core are simultaneously deposited, ensuring material consistency between the core and matrix of the skins, leading to an integrated panel. Integrated samples are compared to pure (fiberless) and adhesive-bonded samples under an 18 J low-velocity impact test. The integrated samples show significant improvements, with maximum impactor acceleration (279.7 m s−2) and force per unit mass (83 283 N kg−1), surpassing adhesive-bonded and pure samples by 35 and 110%, respectively. Additionally, integrated samples show significantly less damage, with dent diameters (9.77 mm) and dent depths (1.52 mm) considerably lower. These findings highlight the benefits of this approach in enhancing impact resistance, reducing damage, and improving energy absorption in composite sandwich structures.

{"title":"Low-Velocity Impact Behavior of 3D-Printed Sandwich Panels with Integrated Composite Face Sheets","authors":"Sajad Karami,&nbsp;Mojtaba Haghighi-Yazdi,&nbsp;Majid Safarabadi","doi":"10.1002/adem.202401923","DOIUrl":"https://doi.org/10.1002/adem.202401923","url":null,"abstract":"<p>Composite panels are made of a core and skins that are typically bonded with adhesive. Traditional adhesive bonding is time-consuming and requires precision, often leading to debonding under varied loading conditions. Additionally, thermal expansion differences between the core, skin, and adhesive cause residual stresses, compromising performance. This research develops a cost-effective method for creating integrated sandwich panels, addressing the effectiveness of such unification under low-velocity impact loading. Using a standard dual-nozzle fused deposition modeling 3D printer with minimal modifications, continuous fibers embedded in a thermoplastic polymer for the skin and a thermoplastic polymer for the core are simultaneously deposited, ensuring material consistency between the core and matrix of the skins, leading to an integrated panel. Integrated samples are compared to pure (fiberless) and adhesive-bonded samples under an 18 J low-velocity impact test. The integrated samples show significant improvements, with maximum impactor acceleration (279.7 m s<sup>−2</sup>) and force per unit mass (83 283 N kg<sup>−1</sup>), surpassing adhesive-bonded and pure samples by 35 and 110%, respectively. Additionally, integrated samples show significantly less damage, with dent diameters (9.77 mm) and dent depths (1.52 mm) considerably lower. These findings highlight the benefits of this approach in enhancing impact resistance, reducing damage, and improving energy absorption in composite sandwich structures.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 4","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143431429","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Hybrid Preceramic Aerogels for Oil and Solvent Cleanup
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-22 DOI: 10.1002/adem.202402182
Oyku Icin, Cekdar Vakifahmetoglu

This study presents the first synthesis and characterization of monolithic hybrid preceramic aerogels using distinct drying techniques: ambient pressure (ambigels) and CO2 supercritical drying. Polymeric ambi/aerogels, derived from polyhydromethlysiloxane (PHMS) and divinylbenzene (DVB), are processed at 200 °C, while hybrid ceramic-polymer (ceramer) is produced through pyrolysis at 600 °C. Despite variations in drying methods, polymer and ceramer ambi/aerogels exhibit comparable microstructural characteristics, bulk density, pore size and volume, and specific surface area (542–841 m2 g−1). Polymeric and ceramer ambigel with 90 vol% total porosity yield a compressive strength, reaching 2.5 MPa, demonstrating a low thermal conductivity of 0.046 W m−1 K−1. Sorption tests are conducted using oil and organic solvents in aqueous media to benefit their high hydrophobicity (112° < θ < 142°). Aerogels exhibit high sorption capacities: 13.17 g g−1 for sesame oil, 11.74 g g−1 for toluene, and 9.19 g g−1 for n-hexane. The sorption rate for the oil is nearly 10 times slower than that for toluene and n-hexane. Regarding regeneration and reusability, polymer and ceramer aerogels show consistent sorption properties cycles tested for n-hexane and toluene.

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引用次数: 0
Precision Macroporous Monoliths Made Using High-Throughput Microfluidic Emulsification
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-21 DOI: 10.1002/adem.202570006
Iacopo Mattich, Alessandro Ofner, André R. Studart

Precision Macroporous Monoliths

In article number 2401363, André R. Studart, Iacopo Mattich, and Alessandro Ofner fabricate centimeter-scale macroporous materials with precisely controlled pore sizes from monodisperse droplets made by high-throughput microfluidics. Macroporosity is created by gravity-induced self-assembly of droplets, followed by polymerization of the continuous phase. Because it combines scalability, pore size control, and tunable chemistry, this microfluidic platform offers a powerful self-assembly approach to produce macroporous materials for catalysis, electrochemistry and separation processes.

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引用次数: 0
Monodomain Liquid-Crystal Elastomer Lattices for Broad Strain-Rate Mechanical Damping
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-21 DOI: 10.1002/adem.202570008
Adam Bischoff, Carter Bawcutt, Maksim Sorkin, Joel Yazzie, Caitlyn C. Cook, Samuel C. Leguizamon, Adam W. Cook, Devin J. Roach

Liquid-Crystal Elastomer Lattices

In article number 2401796, Devin J. Roach and co-workers use direct ink write 3D printing to fabricate aligned, monodomain liquid-crystal elastomer (LCE) lattice structures for broad strain-rate mechanical damping. It is shown that these structures can dissipate strain energy in quasi-static environments, comparable to traditional elastomeric lattices, and provide improved damping under high strain-rate drop testing due to LCE soft elasticity. Art by the team of INMYWORK Studio (https://inmywork.com).

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引用次数: 0
Phase Transformation-Assisted Sintering for the Fabrication of a Bulk Nanocrystalline Fe–5 at.% Zr Alloy
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-21 DOI: 10.1002/adem.202402064
Yubin Cong, Jie Wan, Guibin Shan, Yuzeng Chen

The powder metallurgy route of high-energy ball milling followed by sintering is a common method used to fabricate nanocrystalline (NC) metals. However, the poor thermal stability of NC metals limits the use of high temperatures during sintering, which can result in insufficient densification. In order to achieve a higher relative density at low sintering temperatures, phase transformation-induced volume expansion during sintering is taken advantage of. To prove this hypothesis, NC Fe–5 at.% Zr alloy is sintered at a temperature above A3 (1073 K), which is then decreased below A1 (873 K) to introduce volume expansion caused by phase transformation from austenite to ferrite. For comparison, it is also sintered at a constant temperature above A3 (1073 K). Results show that the proposed strategy can not only enhance the relative density of as-sintered NC Fe–5 at.% Zr alloy, but also ensure a relatively smaller grain size. This study is beneficial for the fabrication of high-performance NC metals.

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引用次数: 0
Breaking the Cardiovascular Flow Barrier for Dielectric Elastomer Actuator-Based Pumping: Design and Characterization
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-21 DOI: 10.1002/adem.202570005
Amine Benouhiba, Armando Walter, Silje Ekroll Jahren, Francesco Clavica, Dominik Obrist, Yoan Civet, Yves Perriard

Dielectric Elastomer Actuators

In article number 2401306, Amine Benouhiba and co-workers present a high-performance tubular dielectric elastomer pump optimized for heart assist applications. Operating at pressures of 15, 70, and 120 mmHg, it achieves a flow rate of 6.5 L min–1 and a pressure head of 27.5 mmHg, underscoring its potential to enhance fluid circulation and support cardiovascular function in medical applications.

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引用次数: 0
期刊
Advanced Engineering Materials
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