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Study on the Precipitation Behavior of SiC/7075Al Composite Material Controlled by Pulse Current-Assisted Treatment
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-09 DOI: 10.1002/adem.202401912
Xian Wang, Wei Zhao, Jie Yan, Wenxian Wang

In order to further improve the comprehensive mechanical properties of as-rolled SiC/7075Al composites, the microstructure and mechanical properties of the composites are modified by pulse current-assisted treatment (PCAT). The results show that the pulse current acts on the interior of the material in a unique way, reducing the nucleation barrier of the precipitated phase. Two nano-scale precipitated phases of MgZn2 (η′) and Mg2Si (β′) are formed inside the composite. The fine precipitates play a significant role in the strengthening of dislocation and dispersion of the material, which makes the material obtain excellent strength and plasticity. The mechanical properties analysis reveals that the yield strength (YS), ultimate tensile strength (UTS), and elongation of the samples subjected to PCAT are 223.6, 434.5 MPa, and 20.6%, respectively. Compared to the as-rolled samples, the YS exhibits an enhancement of 4.7%, the UTS increases significantly by 25.6%, and the elongation improves remarkably by 108%. PCAT enhances the strength and plasticity of SiC/7075Al composites, breaking the competition between strength and plasticity.

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引用次数: 0
Development of Magnetically Actuated Pillars with NiTi–Polydimethylsiloxane Integration for Advanced Mobility in Soft Robotics
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-09 DOI: 10.1002/adem.202402468
Cristian Padilha Fontoura, Cesar Aguzzoli

The use of responsive pillar arrays and cilia-like structures is linked with many groundbreaking applications, including microfluidic devices, biomedical applications, and soft robotics. To be effective, cilia or pillar arrays must exhibit flexible and controllable motion tailored to their specific applications. In this context, in this work, developing a compliant structure, which combines longitudinal stiffness controlled by a shape-memory alloy and magnetically actuated pillars, is aimed at. Polydimethylsiloxane is used as the matrix material, while nickel–titanium (NiTi) alloy provides stiffening to the base, and the pillars are enriched with iron via magnetron sputtering. The structures are generated through cast molding, employing pillar array-forming templates obtained by additive manufacturing. Various physicochemical and mechanical analyses are conducted to assess the composite's properties, including tensile testing, pullout test, and magnetometry. Overall, tailored dexterity and actuation are achieved by controlling temperature and magnetic field application. This advancement not only demonstrates the feasibility of creating responsive pillars at a relatively low cost—in comparison to commercial iron nanoparticles—and environmentally friendly techniques but also opens avenues for their integration into sophisticated devices requiring precise and adaptable movements. Future research should focus on optimizing the actuation efficiency and exploring broader applications in bioengineering and robotics.

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引用次数: 0
Improving Surface Properties of AlSi10Mg Fabricated by Cold Spray: Mechanical Milling is a Tool for Fabrication of Composite ZrN/AlSi10Mg Particles
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-09 DOI: 10.1002/adem.202401862
Veronika S. Suvorova, Dmitrii S. Suvorov, Fedor Yu. Bochkanov, Victoriya U. Mnatsakanyan, Artur Chkirya, Samat K. Mukanov, Stanislav V. Chernyshikhin, Andrey A. Nepapushev, Dmitry O. Moskovskikh

In this study, the possibility of employing ZrN/AlSi10Mg composite powders with 10, 20, and 30 wt% ZrN and a low-pressure cold spraying (CS) unit to enhance the surface properties of AlSi10Mg obtained through laser powder bed fusion (LPBF) is investigated for the first time. A high-energy ball mill is used to produce composite powders from AlSi10Mg and ZrN powders. ZrN/AlSi10Mg powders are sprayed onto the surface of LPBFed AlSi10Mg at a pressure of 0.7 MPa and a temperature of 400 °C. It is demonstrated that the utilization of composite powders facilitates a uniform distribution of ceramic particles in the coating and reduces the share of their losses during the CS process to 2%. It is found that the microhardness and elastic modulus of composite coatings increase with increasing mass fractions of ZrN, while the wear rate (WR) decreases. A change in the wear mechanism from adhesive to abrasive is observed. It is possible to increase the microhardness and elastic modulus of the LPBFed AlSi10Mg surface with a coating containing 30 wt% ZrN by 43% (193 ± 5 HV0.1) and 62% (105 ± 9 GPa), respectively, and reduce the WR by 25% (8.26 ± 0.09) × 10−4 mm3 m−1.

{"title":"Improving Surface Properties of AlSi10Mg Fabricated by Cold Spray: Mechanical Milling is a Tool for Fabrication of Composite ZrN/AlSi10Mg Particles","authors":"Veronika S. Suvorova,&nbsp;Dmitrii S. Suvorov,&nbsp;Fedor Yu. Bochkanov,&nbsp;Victoriya U. Mnatsakanyan,&nbsp;Artur Chkirya,&nbsp;Samat K. Mukanov,&nbsp;Stanislav V. Chernyshikhin,&nbsp;Andrey A. Nepapushev,&nbsp;Dmitry O. Moskovskikh","doi":"10.1002/adem.202401862","DOIUrl":"https://doi.org/10.1002/adem.202401862","url":null,"abstract":"<p>\u0000In this study, the possibility of employing ZrN/AlSi10Mg composite powders with 10, 20, and 30 wt% ZrN and a low-pressure cold spraying (CS) unit to enhance the surface properties of AlSi10Mg obtained through laser powder bed fusion (LPBF) is investigated for the first time. A high-energy ball mill is used to produce composite powders from AlSi10Mg and ZrN powders. ZrN/AlSi10Mg powders are sprayed onto the surface of LPBFed AlSi10Mg at a pressure of 0.7 MPa and a temperature of 400 °C. It is demonstrated that the utilization of composite powders facilitates a uniform distribution of ceramic particles in the coating and reduces the share of their losses during the CS process to 2%. It is found that the microhardness and elastic modulus of composite coatings increase with increasing mass fractions of ZrN, while the wear rate (WR) decreases. A change in the wear mechanism from adhesive to abrasive is observed. It is possible to increase the microhardness and elastic modulus of the LPBFed AlSi10Mg surface with a coating containing 30 wt% ZrN by 43% (193 ± 5 HV<sub>0.1</sub>) and 62% (105 ± 9 GPa), respectively, and reduce the WR by 25% (8.26 ± 0.09) × 10<sup>−4</sup> mm<sup>3</sup> m<sup>−1</sup>.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 4","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-01-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143431158","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Broadband Sound Absorption in a Composite of Localized Aluminum Foam and Microperforated Plates
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-08 DOI: 10.1002/adem.202402205
Jin Chen, Sihan Li, Gexuan Ning, Lisi Liang, Lixing Zhang, Zhongyi Cui, Zeming Wang, Zhuyue Zhang

A composite structure (L-LDMPP) consisting of localized aluminum foam, a localized microperforated plate (MPP), and a double-layer MPP is proposed to enhance sound absorption. A simulation model using COMSOL is developed to predict the sound absorption coefficient and investigate the acoustic benefits of localized aluminum foam and localized MPP. A comparative analysis is performed to evaluate the sound absorption performance of four configurations: L-SMPP (localized aluminum foam with a single-layer MPP), L-DMPP (localized aluminum foam with a double-layer MPP), L-LSMPP (localized aluminum foam with a localized MPP and a single-layer MPP), and L-LDMPP (localized aluminum foam with a localized MPP and a double-layer MPP). The model's accuracy is validated against experimental data. Results show that localized aluminum foam, localized MPP, and double-layer MPP optimize acoustic impedance matching. The sound absorption characteristics of L-LDMPP are divided into two domains: the resonance acoustic domain, influenced by the double-layer MPP structure behind the localized aluminum foam, and the coupled acoustic domain, influenced by both the localized aluminum foam and localized MPP.

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引用次数: 0
Overview of Ruthenium Thin Films Annealed by Microsecond Scanning UV Pulsed Laser: Structural, Electrical, and Failure Modes Analysis
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-07 DOI: 10.1002/adem.202402656
Richard Daubriac, Leonardo Cancellara, Zeinab Chehadi, Lu Lu, Louis Thuries, Mohamed Ali Khaled, Fabien Roze, Nicolas Jourdan, Zsolt Tokei, Armel Descamps-Mandine, Teresa Hungria, Pier-Francesco Fazzini, Toshiyuki Tabata, Karim Huet

Ruthenium (Ru) has been identified as a durable and relevant substitute to copper (Cu) to answer the access resistance lowering of the back-end-of-line (BEOL) metal levels, which is a high-priority concern for future devices. Herein, the nonequilibrium and local properties of pulsed scanning laser annealing (SLA) technique are used to enhance the structural and electrical properties of thin polycrystalline Ru layers (<30 nm). For the best annealing conditions, transmission electron microscopy observations show a substantial grain size enlargement, with large grains (≈80 nm) occupying the whole layer height. It goes with a 53% resistivity reduction, measured by 4-point probe, confirming the strong grain boundary scattering reduction. A Mayadas–Shatzkes model incorporating temperature-dependent resistivity measurements allows the extraction of promising reflectivity and specularity coefficients of around 0.58 and 0.98, respectively. Beyond the best conditions, failure modes for devices integration are observed, such as surface wrinkling and local buckling. Given the studied system, a semiquantitative analysis of these phenomena is given and simulations based on the finite element method are used to find further optimal annealing conditions. This study confirms the potential of Ru as a promising BEOL material, but also SLA as a convincing technique for future 3D architectures.

钌(Ru)已被确定为铜(Cu)的一种耐用且相关的替代品,可用于降低线路后端(BEOL)金属层的接入电阻,这是未来设备的一个高度优先考虑的问题。本文利用脉冲扫描激光退火(SLA)技术的非平衡和局部特性来提高多晶Ru薄层(30 nm)的结构和电学特性。在最佳退火条件下,透射电子显微镜观察显示晶粒尺寸大幅增大,大晶粒(≈80 nm)占据了整个层高。同时,通过四点探针测量,电阻率降低了 53%,证实了晶界散射的强烈减弱。采用 Mayadas-Shatzkes 模型,并结合随温度变化的电阻率测量值,可以得出反射率和镜面反射系数分别为 0.58 和 0.98 左右。在最佳条件之外,还可观察到器件集成的失效模式,如表面起皱和局部弯曲。针对所研究的系统,我们对这些现象进行了半定量分析,并基于有限元法进行了模拟,以进一步找到最佳退火条件。这项研究证实了 Ru 作为一种有前途的 BEOL 材料的潜力,同时也证实了 SLA 是一种令人信服的未来 3D 架构技术。
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引用次数: 0
Shape Morphing of Re-Entrant Honeycomb Metamaterials for Linear Auxetic Behaviors
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-06 DOI: 10.1002/adem.202570001
Hong-Gap Choi, Soonjae Pyo, Jae-Won Choi, Keun Park

Re-Entrant Honeycomb Metamaterials

The cover image illustrates a re-entrant honeycomb metamaterial with graded shape morphing, fabricated via additive manufacturing. The shape morphing is achieved by adaptively changing the geometric parameters of sigmoid-based morphing functions to enable linear auxetic behaviors. Six cell designs with different morphing parameters, highlighted in the cover image, are analyzed to achieve linear auxetics with minimal deviations in the negative Poisson’s ratio. The experimental results reveal a 70% reduction in the relative variation of Poisson’s ratio, while maintaining a high magnitude. Further details can be found in article 2400889 by Keun Park and co-workers.

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引用次数: 0
Conductive Graphene–Polyethylene Terephthalate Composite Yarns with Synergistic Multiwalled Carbon Nanotube Additives by Melt-Spinning
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-06 DOI: 10.1002/adem.202570004
Yuzhu Jin, Yue Kang, Shuyan Hu, Yaping Lu, Zengcai Zhao, Dihua Wu, Weitao Su, Yuan Li, Qiaolan Fan, Yangxin Zhou

Conductive Yarns

In article number 2401629, Qiaolan Fan, Yangxin Zhou, and co-workers fabricate conductive graphene-PET (polyethylene terephthalate) composite yarns through the integration of synergistic multi-wall carbon nanotube (MWCNT) additives, utilizing industrially established melt-spinning process. These yarns are endowed with conductivity, facilitated by conductive pathways established through interfacial contacts between graphene and MWCNTs.

{"title":"Conductive Graphene–Polyethylene Terephthalate Composite Yarns with Synergistic Multiwalled Carbon Nanotube Additives by Melt-Spinning","authors":"Yuzhu Jin,&nbsp;Yue Kang,&nbsp;Shuyan Hu,&nbsp;Yaping Lu,&nbsp;Zengcai Zhao,&nbsp;Dihua Wu,&nbsp;Weitao Su,&nbsp;Yuan Li,&nbsp;Qiaolan Fan,&nbsp;Yangxin Zhou","doi":"10.1002/adem.202570004","DOIUrl":"https://doi.org/10.1002/adem.202570004","url":null,"abstract":"<p><b>Conductive Yarns</b>\u0000 </p><p>In article number 2401629, Qiaolan Fan, Yangxin Zhou, and co-workers fabricate conductive graphene-PET (polyethylene terephthalate) composite yarns through the integration of synergistic multi-wall carbon nanotube (MWCNT) additives, utilizing industrially established melt-spinning process. These yarns are endowed with conductivity, facilitated by conductive pathways established through interfacial contacts between graphene and MWCNTs.\u0000\u0000 <figure>\u0000 <div><picture>\u0000 <source></source></picture><p></p>\u0000 </div>\u0000 </figure></p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 1","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-01-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/adem.202570004","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143112722","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Multiplexing Integration Meta-Absorber in an Ultrathin Planar Board
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-06 DOI: 10.1002/adem.202570002
Tong Cai, Xiangyang Meng, Hailin Huang, Dan Liu, Xingshuo Cui, Cunqian Feng, Guimei Zheng, Chunsheng Guan, Wenye Ji

Meta-Absorbers

In article number 2401738, Tong Cai, Chunsheng Guan, Wenye Ji, and co-workers propose a multiplexing integration meta-absorber in a one-layer planar board by harnessing the coupling of four resonant modes, achieving an ultra-thin thickness and an ultrawide absorption band. Our work presents a feasible absorption strategy that is closer to practical applications and may pave a way for the development of ultra-thin meta-devices.

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引用次数: 0
Investigating the Effect of Volumetric Energy Density on Tensile Characteristics of As-Built and Heat-Treated AlSi10Mg Alloy Fabricated by Laser Powder Bed Fusion
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-24 DOI: 10.1002/adem.202401924
Vijaykumar S. Jatti, A. Saiyathibrahim, R. Murali Krishnan, Ashwini V. Jatti, G. Suganya Priyadharshini, Dhanesh G. Mohan

Pore emergence during the laser powder bed fusion (LPBF) technique significantly impairs mechanical characteristics. Therefore, the elimination of pores is a pressing issue to ensure the quality and productivity of manufactured components. The objective of this study is to evaluate how certain parameters, such as laser power, layer thickness, exposure time, hatch distance, and volumetric energy density, affect the microstructure and tensile properties of AlSi10Mg specimens generated by LPBF in both their original state and after undergoing a solution heat treatment. The volumetric energy density (VED) is often used to optimize process parameters in the LPBF approach since it thoroughly evaluates all four main factors. This article specifically examines the impact of VED on the microstructural features and tensile characteristics of printed parts. The high VED of 78.13 J mm−3 decreases the occurrence of porosity and defects, hence enhancing the tensile characteristics of the specimens produced. Regarding specimens that have undergone solution heat treatment, the recommendation is to decrease the laser power to 350 W, which results in a VED of 60.76 J mm−3 and outstanding tensile characteristics. These findings provide fresh perspectives to achieve improved tensile properties of AlSi10Mg parts using LPBF processing settings.

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引用次数: 0
Smart Hydrogen-Producing Nanoparticles with the Potential for Arthritic Microenvironment Regulation
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-12-23 DOI: 10.1002/adem.202401465
Pingping Zhang, Yutong Hou, Dezhi Lu, Qixing Li, Chaoyi Zhang, Liang Zhou, Tao Li, Tao Wu

The joint microenvironment contributes significantly to arthritis by shaping the synovial sheath and inducing cartilage damage. Hydrogen has antioxidant and anti-inflammatory potential and shows promise in the treatment of arthritis, particularly in selectively reducing free radical levels while preserving normal cell redox reactions. However, the short retention time of hydrogen and its low solubility in body fluids pose challenges for its use to achieve an optimal therapeutic effect. Smart biomaterials respond to alterations in physiological parameters and external stimuli, enabling precise targeting and continuous local treatment, thus maintaining local H2 concentration at the treatment site. In this review, the recent advances in hydrogen-producing nanomaterials for the treatment of arthritis are presented and the challenges and prospects for their clinical application are evaluated.

{"title":"Smart Hydrogen-Producing Nanoparticles with the Potential for Arthritic Microenvironment Regulation","authors":"Pingping Zhang,&nbsp;Yutong Hou,&nbsp;Dezhi Lu,&nbsp;Qixing Li,&nbsp;Chaoyi Zhang,&nbsp;Liang Zhou,&nbsp;Tao Li,&nbsp;Tao Wu","doi":"10.1002/adem.202401465","DOIUrl":"https://doi.org/10.1002/adem.202401465","url":null,"abstract":"<p>The joint microenvironment contributes significantly to arthritis by shaping the synovial sheath and inducing cartilage damage. Hydrogen has antioxidant and anti-inflammatory potential and shows promise in the treatment of arthritis, particularly in selectively reducing free radical levels while preserving normal cell redox reactions. However, the short retention time of hydrogen and its low solubility in body fluids pose challenges for its use to achieve an optimal therapeutic effect. Smart biomaterials respond to alterations in physiological parameters and external stimuli, enabling precise targeting and continuous local treatment, thus maintaining local H<sub>2</sub> concentration at the treatment site. In this review, the recent advances in hydrogen-producing nanomaterials for the treatment of arthritis are presented and the challenges and prospects for their clinical application are evaluated.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 4","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-12-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143431825","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Advanced Engineering Materials
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