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Transient Liquid Phase Bonding of ZGH451 Superalloy Fabricated by Directed Energy Deposition 定向能沉积法制造的 ZGH451 超耐热合金的瞬态液相结合
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-14 DOI: 10.1002/adem.202401433
Xingyu Hou, Xindong Qin, Yuan Sun, Shiyang Wang, Hongyu Zhang, Hongwei Zhang, Chuanyong Cui, Zhuqing Wang, Shiwei Liu, Jinguo Li, Yizhou Zhou

ZGH451, a directionally solidified Ni-based superalloy designed for additive manufacturing, has garnered significant attention in the realm of next-generation turbine blades. Welding the ZGH451 superalloy is crucial for promoting its practical application. In this study, transient liquid phase (TLP) bonding is applied to weld ZGH451 superalloy produced through directed energy deposition. A Ni-based interlayer alloy powder is developed and prepared via thermodynamic calculation, with the interlayer subsequently characterized using differential thermal analysis. TLP bonding is conducted at 1200 °C for 4 h. The influence of the preset gap on the joint microstructure and mechanical properties is examined. The microstructure of the TLP bonding joints comprises athermally solidified zones (ASZ), isothermally solidified zones, and diffusion-affected zones. The ASZ width significantly increases with the growing preset gap. A preset gap not exceeding 100 μm enables complete isothermal solidification of the joints. Particularly, joints with a preset gap ranging from 0 to 30 μm demonstrate optimal reliability, exhibiting a tensile strength of up to 1375 MPa at room temperature, which is 12% higher than the room temperature strength of the base metal (BM), and a tensile strength of 983 MPa at 760 °C, surpassing 86% of the BM's strength at the same temperature.

ZGH451 是一种为增材制造而设计的定向凝固镍基超级合金,在下一代涡轮叶片领域备受关注。焊接 ZGH451 超级合金对于促进其实际应用至关重要。本研究采用瞬态液相 (TLP) 焊接技术,对通过定向能沉积技术生产的 ZGH451 超级合金进行焊接。通过热力学计算开发和制备了镍基夹层合金粉末,随后利用差热分析对夹层进行了表征。研究了预设间隙对接头微观结构和机械性能的影响。TLP 粘合接头的微观结构包括热凝固区 (ASZ)、等温凝固区和扩散影响区。ASZ 宽度随着预设间隙的增大而明显增加。预设间隙不超过 100 μm 时,接头可完全等温凝固。尤其是预设间隙在 0 至 30 μm 之间的接合点具有最佳的可靠性,在室温下的抗拉强度高达 1375 兆帕,比基体金属(BM)的室温强度高出 12%,在 760 °C 时的抗拉强度为 983 兆帕,超过基体金属在相同温度下强度的 86%。
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引用次数: 0
Strategy and Advancement in Hybrid Hydrogel and Their Applications: Recent Progress and Trends 混合水凝胶及其应用的战略与进展:最新进展与趋势
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-13 DOI: 10.1002/adem.202400944
Arpita Choudhary, Anirudh Sharma, Abhinav Singh, Sung Soo Han, Ankur Sood

Advancements in polymers have made significant contribution in diverse application-oriented fields. The multidisciplinary application of polymers generates a range of strategies, which is applicable in a wide range of biomedicines. Polymeric compounds such as hydrogels have been explored globally as a potent biomaterial that can furnish essential attributes due to their three-dimensional (3D) soft and highly hydrophilic polymeric network. These hydrogels have been used extensively in various applications due to their biocompatible, biodegradable, and biosorption nature. However, they have some limitations, owing to their soft nature, low mechanical properties, and unsatisfactory degradation profile. Therefore, there is a need to develop novel, stronger, and more durable hybrid hydrogels with enhanced biocompatible and multifunctional properties. The current review gives a broad spectrum of hybrid hydrogels with its importance and significance. Further, the review highlights the strategies of generation of hybrid hydrogels reinforced with nanomaterials, biomaterials, and nanobiocomposites along with their advantages and disadvantages. The review also features various applications of these hybrid hydrogels in the field of biomedicines, photocatalysis, agriculture, and food industry over the last 5 years. This review will give a comprehensive overview to researchers working in the field of hybrid hydrogels development.

聚合物技术的进步为各种应用领域做出了重大贡献。聚合物的多学科应用产生了一系列策略,适用于广泛的生物医学领域。水凝胶等高分子化合物作为一种有效的生物材料,因其三维(3D)柔软且高度亲水的高分子网络而具有重要的特性,已在全球范围内得到探索。这些水凝胶具有生物相容性、生物可降解性和生物吸附性,因此被广泛应用于各种领域。然而,由于其柔软的性质、较低的机械性能和不理想的降解特性,它们也有一些局限性。因此,有必要开发具有更强生物相容性和多功能特性的新型、更坚固、更耐用的混合水凝胶。本综述广泛介绍了混合水凝胶的重要性和意义。此外,综述还重点介绍了用纳米材料、生物材料和纳米生物复合材料增强的混合水凝胶的生成策略及其优缺点。综述还介绍了过去五年中这些混合水凝胶在生物医学、光催化、农业和食品工业领域的各种应用。本综述将为从事杂化水凝胶开发的研究人员提供一个全面的概览。
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引用次数: 0
Improvement of Arc Erosion Resistance of Ag–SnO2 Contact Materials by Reducing Molten Pool Size 通过减小熔池尺寸提高 Ag-SnO2 触头材料的抗电弧侵蚀能力
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-13 DOI: 10.1002/adem.202400688
Pengyu Chen, Yaping Wang

The splash of molten Ag under arc erosion is the major reason for the failure of Ag-based contact materials. Changing the size of the molten pool may manipulate the splash process and suppress the arc erosion. Herein, the size effect by fabricating a SnO2 network with pores smaller than the typical Ag molten pool is investigated. Silver is subsequently infiltrated into the SnO2 network to form Ag–SnO2 interpenetrating contact materials. It is found that the SnO2 network with small pore sizes separates the Ag matrix into smaller regions, reducing the melting volume. Compared with the particle-dispersed one, the interpenetrating composite decreases ≈90% mass loss and temperature rise, as well as provides superior microstructure stability. This finding demonstrates a promising way to improve the arc erosion resistance of contact materials by tailoring the size of molten pool, benefiting long-lifetime contact materials for smart grid applications.

电弧侵蚀下的熔融银飞溅是银基触头材料失效的主要原因。改变熔池的尺寸可以控制飞溅过程,抑制电弧侵蚀。本文研究了通过制造孔隙小于典型银熔池的二氧化锡网络的尺寸效应。随后将银渗入二氧化锡网络,形成银-二氧化锡互穿接触材料。研究发现,具有小孔径的二氧化锡网络可将银基体分隔成更小的区域,从而减小熔化体积。与颗粒分散的材料相比,互穿复合材料的质量损失和温升降低了≈90%,并且具有优异的微观结构稳定性。这一发现为通过调整熔池尺寸来提高触头材料的抗电弧侵蚀能力提供了一种可行的方法,有利于智能电网应用中触头材料的长寿命化。
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引用次数: 0
Experimental and Numerical Investigations of Tensile Properties of SiC Particle-Reinforced Composites 碳化硅粒子增强复合材料拉伸性能的实验和数值研究
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-13 DOI: 10.1002/adem.202401455
Datao Li, Yingrong Gao, Xiahui Wei, Binhua Wang

In this study, experiments and finite element modeling (FEM) are performed to study the tensile mechanical properties of SiC particle-reinforced 6061 Al-matrix composites (SiCp/6061Al) at various volume fractions (VFs) of SiCp. The Young's modulus, yield strength, and tensile strength of SiCp/6061Al display an overall upward trend with the increment of the VF of SiCp. The fracture analysis results demonstrate that the fracture of SiCp/6061Al is a hybrid of matrix fracture, reinforcement fracture, and interface debonding. An algorithm is developed to construct the mesostructure of particle-reinforced composites, based on the random sequential absorption algorithm. The VFs of the particles of the representative volume element (RVE) model constructed using the novel algorithm are as high as 42%. The tensile mechanical properties of SiCp/6061Al are predicted by replacing the irregular particle reinforcements in SiCp/6061Al with spherical particles in the RVE model. Comparisons reveal that the stress–strain curves obtained via experiment and FEM are highly consistent in the elastic-plastic stage, which verifies the effectiveness and rationality of the novel algorithm.

本研究通过实验和有限元建模(FEM)研究了不同 SiCp 体积分数(VFs)下 SiC 粒子增强 6061 Al 基复合材料(SiCp/6061Al)的拉伸力学性能。随着 SiCp 体积分数的增加,SiCp/6061Al 的杨氏模量、屈服强度和拉伸强度总体呈上升趋势。断裂分析结果表明,SiCp/6061Al 的断裂是基体断裂、加固断裂和界面脱粘的混合断裂。基于随机顺序吸收算法,开发了一种构建颗粒增强复合材料介观结构的算法。使用新算法构建的代表体积元素(RVE)模型的颗粒VF值高达42%。通过在 RVE 模型中用球形颗粒取代 SiCp/6061Al 中的不规则颗粒增强材料,预测了 SiCp/6061Al 的拉伸机械性能。对比结果表明,在弹塑性阶段,实验和有限元模型得到的应力应变曲线高度一致,这验证了新算法的有效性和合理性。
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引用次数: 0
Dynamic Constitutive Model of Tungsten-Whisker-Reinforced Aluminum/Polytetrafluoroethylene Composite Material and Quantitative Determination of Impact Reaction Release Energy in Vacuum Environment 钨须增强铝/聚四氟乙烯复合材料的动态结构模型及真空环境下冲击反应释放能的定量测定
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-10 DOI: 10.1002/adem.202400817
Enling Tang, Zhiwei Deng, Ruizhi Wang, Yafei Han, Chuang Chen, Mengzhou Chang, Kai Guo, Liping He

To meet the strength requirements of aluminum/polytetrafluoroethylene (Al/PTFE) in practical applications, tungsten (W) whisker is added into the traditional formula Al/PTFE (26.5%/73.5%) to improve the dynamic compressive strength of the reactive material. Mechanical properties of reactive material specimens prepared by sintering are tested. In the results, it is shown that the dynamic compressive strength of Al/PTFE-reactive material reinforced by tungsten whisker with volume fraction of 13.1% can reach 141 MPa at strain rate of 1800 s−1. The constitutive model of dynamic compression for tungsten-whisker-enhanced Al/PTFE-reactive material is constructed, and the results are basically consistent with the experimental results. The quantitative impact energy release of reactive material specimens under vacuum environment are performed by using the two-stage light gas gun loading system, and the quantitative impact release energies of Al/PTFE-reactive material reinforced by tungsten whisker under different whisker percentage content and diameter are obtained.

为了满足铝/聚四氟乙烯(Al/PTFE)在实际应用中的强度要求,在传统配方 Al/PTFE (26.5%/73.5%)中加入了钨(W)晶须,以提高反应材料的动态抗压强度。对烧结制备的反应材料试样进行了力学性能测试。结果表明,体积分数为 13.1% 的钨晶须增强 Al/PTFE 反应材料在应变速率为 1800 s-1 时的动态压缩强度可达 141 MPa。构建了钨晶须增强 Al/PTFE 反应材料的动态压缩构效模型,结果与实验结果基本一致。利用两级光气枪加载系统对真空环境下的反应材料试样进行了定量冲击能量释放,得到了不同晶须百分比含量和直径下钨晶须增强 Al/PTFE 反应材料的定量冲击释放能量。
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引用次数: 0
Effect of Process Parameters on Yttria-Stabilized Zirconia Particles In-Flight Behavior and Melting State in Atmospheric Plasma Spraying 工艺参数对大气等离子喷涂中钇稳氧化锆粒子飞行行为和熔融状态的影响
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-10 DOI: 10.1002/adem.202400550
Zijian Jia, Wenrui Wang, Wu Qi, Jiaming Zhang, Kaiqiang Song

The preparation of coatings by atmospheric plasma spraying gives rise to complex physical processes, which present challenges to the study of plasma jet characteristics and particle in-flight behavior. Herein, a 3D numerical model that integrates multiple physical phenomena, including electromagnetism and thermal and gas dynamics, to simulate the heating, acceleration, and melting of particles under the thermal–mechanical effect, is developed. Meanwhile, yttria-stabilized zirconia (YSZ) coatings are prepared under varying process parameters. The DPV-2000 system is employed for the diagnosis of particle velocity, surface temperature, and diameter. Following comparison, the simulation exhibits errors of 4.5% and 14.8% for the maximum temperature and velocity, respectively. An increase in current intensity from 500 to 600 A results in a rise in the proportion of particles exhibiting temperatures above the melting point (2963 K), from 75.1 to 93.4%, accompanied by an increase in average velocity of ≈16.6%. As the spraying distance increases from 60 to 100 mm, the proportion of particles melting decreases from 93.5 to 66.3%, and the average velocity decreases by ≈9.2%. This work will provide a theoretical foundation for the optimization of process parameters to adjust particle behavior and melting state, thus achieving an optimal spraying effect.

通过大气等离子喷涂制备涂层会产生复杂的物理过程,这给等离子射流特性和粒子飞行行为的研究带来了挑战。本文开发了一种三维数值模型,该模型综合了电磁学、热动力学和气体动力学等多种物理现象,模拟了粒子在热机械效应下的加热、加速和熔化过程。同时,在不同的工艺参数下制备钇稳定氧化锆(YSZ)涂层。采用 DPV-2000 系统对颗粒速度、表面温度和直径进行诊断。经过比较,模拟显示的最高温度和速度误差分别为 4.5% 和 14.8%。电流强度从 500 安培增加到 600 安培后,温度高于熔点(2963 K)的颗粒比例从 75.1% 增加到 93.4%,同时平均速度增加了 ≈16.6%。当喷射距离从 60 毫米增加到 100 毫米时,熔化颗粒的比例从 93.5% 下降到 66.3%,平均速度下降了 ≈9.2%。这项工作将为优化工艺参数,调整颗粒行为和熔化状态,从而达到最佳喷涂效果提供理论依据。
{"title":"Effect of Process Parameters on Yttria-Stabilized Zirconia Particles In-Flight Behavior and Melting State in Atmospheric Plasma Spraying","authors":"Zijian Jia,&nbsp;Wenrui Wang,&nbsp;Wu Qi,&nbsp;Jiaming Zhang,&nbsp;Kaiqiang Song","doi":"10.1002/adem.202400550","DOIUrl":"https://doi.org/10.1002/adem.202400550","url":null,"abstract":"<p>The preparation of coatings by atmospheric plasma spraying gives rise to complex physical processes, which present challenges to the study of plasma jet characteristics and particle in-flight behavior. Herein, a 3D numerical model that integrates multiple physical phenomena, including electromagnetism and thermal and gas dynamics, to simulate the heating, acceleration, and melting of particles under the thermal–mechanical effect, is developed. Meanwhile, yttria-stabilized zirconia (YSZ) coatings are prepared under varying process parameters. The DPV-2000 system is employed for the diagnosis of particle velocity, surface temperature, and diameter. Following comparison, the simulation exhibits errors of 4.5% and 14.8% for the maximum temperature and velocity, respectively. An increase in current intensity from 500 to 600 A results in a rise in the proportion of particles exhibiting temperatures above the melting point (2963 K), from 75.1 to 93.4%, accompanied by an increase in average velocity of ≈16.6%. As the spraying distance increases from 60 to 100 mm, the proportion of particles melting decreases from 93.5 to 66.3%, and the average velocity decreases by ≈9.2%. This work will provide a theoretical foundation for the optimization of process parameters to adjust particle behavior and melting state, thus achieving an optimal spraying effect.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"26 21","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142641838","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Light- and Heat-Responsive Superhydrophobic Surfaces with Shape Memory Capacity Prepared by 4D Printing 通过 4D 印刷制备具有形状记忆能力的光热响应型超疏水表面
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-10 DOI: 10.1002/adem.202401415
Xiang Li, Yanlong Zhan, Wen Li, Zhihong Huang, Alidad Amirfazli

The precise manipulation of microdroplets on solid surfaces is crucial for the practical application and future development of microfluidic control technology. Traditionally, methods to achieve precise control over microdroplets often involve complex fabrication processes. Herein, the control of surface wettability is achieved based on the light- and heat-responsive shape memory effect of the microstructure. An innovative superhydrophobic shape-memory material with a simplified and efficient manufacturing process is proposed to precisely control microdroplets through surface wettability switching. Firstly, microplates with shape-memory effects are manufactured using 4D printing technology and polylactic acid as the base material. Then, a mixture of carbon black and epoxy resin is sprayed onto the surface for superhydrophobic modification, resulting in a contact angle of up to 165°. The addition of carbon black endows the surface with excellent photothermal conversion effects. Anisotropy and photothermal response studies are incorporated. Through periodic heating, pressing, and deformation, the microplate array exhibits controllable wettability switching. Based on the shape-memory effect of polylactic acid, the superhydrophobic surface has adjustable adhesion and is successfully applied to microfluidic platforms and microdroplet size screening. This innovative material and process offer significant potential for advancing the field of microfluidic control technology.

在固体表面精确控制微滴对于微流体控制技术的实际应用和未来发展至关重要。传统上,实现微滴精确控制的方法往往涉及复杂的制造工艺。在这里,基于微结构的光热响应形状记忆效应实现了对表面润湿性的控制。我们提出了一种创新的超疏水形状记忆材料,其制造工艺简单高效,可通过表面润湿性切换来精确控制微滴。首先,使用 4D 打印技术和聚乳酸作为基础材料,制造出具有形状记忆效应的微板。然后,在表面喷涂碳黑和环氧树脂的混合物,进行超疏水改性,使接触角达到 165°。碳黑的加入使表面具有出色的光热转换效果。研究还包括各向异性和光热反应研究。通过周期性加热、加压和变形,微孔板阵列表现出可控的润湿性切换。基于聚乳酸的形状记忆效应,超疏水表面具有可调节的粘附性,并成功应用于微流控平台和微滴尺寸筛选。这种创新材料和工艺为推动微流体控制技术领域的发展提供了巨大潜力。
{"title":"Light- and Heat-Responsive Superhydrophobic Surfaces with Shape Memory Capacity Prepared by 4D Printing","authors":"Xiang Li,&nbsp;Yanlong Zhan,&nbsp;Wen Li,&nbsp;Zhihong Huang,&nbsp;Alidad Amirfazli","doi":"10.1002/adem.202401415","DOIUrl":"https://doi.org/10.1002/adem.202401415","url":null,"abstract":"<p>The precise manipulation of microdroplets on solid surfaces is crucial for the practical application and future development of microfluidic control technology. Traditionally, methods to achieve precise control over microdroplets often involve complex fabrication processes. Herein, the control of surface wettability is achieved based on the light- and heat-responsive shape memory effect of the microstructure. An innovative superhydrophobic shape-memory material with a simplified and efficient manufacturing process is proposed to precisely control microdroplets through surface wettability switching. Firstly, microplates with shape-memory effects are manufactured using 4D printing technology and polylactic acid as the base material. Then, a mixture of carbon black and epoxy resin is sprayed onto the surface for superhydrophobic modification, resulting in a contact angle of up to 165°. The addition of carbon black endows the surface with excellent photothermal conversion effects. Anisotropy and photothermal response studies are incorporated. Through periodic heating, pressing, and deformation, the microplate array exhibits controllable wettability switching. Based on the shape-memory effect of polylactic acid, the superhydrophobic surface has adjustable adhesion and is successfully applied to microfluidic platforms and microdroplet size screening. This innovative material and process offer significant potential for advancing the field of microfluidic control technology.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"26 22","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142674120","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Achieving Well-Balanced Strength and Ductility in Warm-Rolled Fe–30.5Mn–8Al–1.0C Lightweight Austenitic Steels via Aging Treatment 通过时效处理实现热轧 Fe-30.5Mn-8Al-1.0C 轻质奥氏体钢的强度和延展性平衡
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-10 DOI: 10.1002/adem.202401797
Feng Zhang, Peng Chen, Pengfei Wang, Xiaowu Li

In this study, it is attempted to achieve a balanced enhancement of strength and ductility in warm-rolled Fe–30.5Mn–8Al–1.0C (wt%) lightweight austenitic steel through aging treatment. Samples are warm rolled at 350 °C with different reductions of 25%, 45%, and 65%, followed by aging at 600 °C for 10 min. In the results, it is indicated that the 65% reduction sample exhibits an exceptional performance with well-balanced ultimate tensile strength (1610.3 ± 1.2 MPa) and total elongation (16.2% ± 0.6%). Such an excellent strength–ductility match is primarily attributed to deformation twinning, shear band refinement, and κ-carbide precipitation strengthening, which collectively contribute to an improved work-hardening capacity. In this study, the efficacy of combined warm-rolling and aging treatments in optimizing the mechanical properties of Fe–Mn–Al–C steel is highlighted.

本研究试图通过时效处理,均衡提高热轧Fe-30.5Mn-8Al-1.0C(重量百分比)轻质奥氏体钢的强度和延展性。试样在 350 ℃ 温轧制,减薄率分别为 25%、45% 和 65%,然后在 600 ℃ 时效 10 分钟。结果表明,减薄率为 65% 的试样具有优异的性能,极限抗拉强度(1610.3 ± 1.2 兆帕)和总伸长率(16.2% ± 0.6%)非常均衡。这种出色的强度-电导率匹配主要归功于变形孪晶、剪切带细化和κ-碳化物沉淀强化,它们共同提高了加工硬化能力。本研究强调了联合热轧和时效处理在优化 Fe-Mn-Al-C 钢机械性能方面的功效。
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引用次数: 0
Superplastic Deformation Behavior of 2 mm Ti60 Rolled Sheet in Air Environment 2 mm Ti60 轧制板材在空气环境中的超塑性变形行为
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-05 DOI: 10.1002/adem.202401667
Shulin Dong, Shiwen Qu, Zhiyong Chen, Yingdong Qu, Ruirun Chen, Guanglong Li, Wei Zhang, Shibing Liu

The superplastic deformation behavior of 2 mm Ti60 sheet is studied, and the constitutive equation of superplastic deformation is established. The results show that when the strain rate is 5.00 × 10−3 s−1 and the temperature is 950 °C, the maximum superplastic elongation reaches 400%. Through the analysis of the true strain–true stress curve, it is found that the average apparent activation energy (Q) is 490.783 kJ mol−1 and the average strain rate sensitivity (m) is 0.49. Dynamic spheroidization (DG) promotes the transformation of lath α phase to equiaxed α phase. Dynamic recrystallization (DRX) promotes the generation of high-angle grain boundaries (θ > 15°). After deformation, the strength of R-type textures changes significantly. From the grip to the tip, the strength of R-type texture gradually weakens, which is mainly caused by the rotation of grains during deformation. The deformation mechanism of Ti60 sheet is dominated by grain boundary sliding, and is coordinated by grain growth, DG, DRX, dislocation motion, and grain rotation.

研究了 2 mm Ti60 薄板的超塑性变形行为,并建立了超塑性变形的构成方程。结果表明,当应变速率为 5.00 × 10-3 s-1 和温度为 950 ℃ 时,最大超塑性伸长率达到 400%。通过分析真实应变-真实应力曲线,发现平均表观活化能(Q)为 490.783 kJ mol-1,平均应变速率灵敏度(m)为 0.49。动态球化(DG)促进板条α相向等轴α相转变。动态再结晶(DRX)促进了高角度晶界(θ >15°)的产生。变形后,R 型纹理的强度发生了显著变化。从握持处到尖端,R 型纹理的强度逐渐减弱,这主要是由变形过程中晶粒的旋转引起的。Ti60 薄片的变形机制以晶界滑动为主,并与晶粒生长、DG、DRX、位错运动和晶粒旋转相协调。
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引用次数: 0
Effect of Laser Powder Bed Fusion Parameters on the Evolution of Melt Pool, Densification, Microstructure, and Hardness in 420 Stainless Steel Parts 激光粉末床熔融参数对 420 不锈钢零件熔池、致密化、微观结构和硬度演变的影响
IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-05 DOI: 10.1002/adem.202301745
Ângela Cunha, Michael Gasik, Filipe Samuel Silva, Bruno Trindade, Flávio Bartolomeu, Óscar Carvalho

Laser powder bed fusion (LPBF) involves depositing, melting, and solidifying metal powder particles layer by layer to create 3D components. In this study, a deep fundamental understanding on how process parameters—laser power, scan speed, and hatch spacing—affect the melt pool, densification, microstructure, hardness, and thermal behavior of 420 stainless steel (420SS) parts produced by such technology is provided. The conducted investigation considers five levels of laser power and hatch spacing, and four scan speeds. Optimal single tracks, based on geometry and profile, are achieved with laser powers between 40 and 80 W and a scan speed of 10 mm s−1. In the multitrack analysis, it is indicated that a dense, smooth surface is obtained with a hatch spacing of 250 μm, corresponding to an overlapping rate of ≈30%. The 420SS samples show high densification (≈99%) and low surface roughness (≈3.62 μm). The microstructure consisted of martensite laths and retained austenite. The hardness and thermal conductivity of the samples are measured at 540 HV and 15.3 W m−1 K−1, respectively. In this study, the understanding of the process–structure–property relationships in LPBF of 420SS is expanded.

激光粉末床熔融技术(LPBF)涉及金属粉末颗粒的逐层沉积、熔化和凝固,以制造三维部件。在本研究中,我们从根本上深入了解了激光功率、扫描速度和舱口间距等工艺参数如何影响用这种技术生产的 420 不锈钢(420SS)部件的熔池、致密化、微观结构、硬度和热行为。研究考虑了五种激光功率、舱口间距和四种扫描速度。在激光功率为 40 至 80 W、扫描速度为 10 mm s-1 的情况下,根据几何形状和轮廓实现了最佳单轨。多轨分析表明,当舱口间距为 250 μm 时,可获得致密光滑的表面,重叠率≈30%。420SS 样品的致密化程度高(≈99%),表面粗糙度低(≈3.62 μm)。显微结构由马氏体板条和残余奥氏体组成。样品的硬度和热导率分别是在 540 HV 和 15.3 W m-1 K-1 下测得的。这项研究加深了人们对 420SS LPBF 的工艺-结构-性能关系的理解。
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引用次数: 0
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Advanced Engineering Materials
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