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Effect of In Situ Bonding on Microstructure and Compression Performance of Aluminum Foam-Filled Tubes 原位键合对泡沫铝填充管微观结构和压缩性能的影响
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202502041
Jicheng Fan, Zhanhao Feng, Peng Huang, Yutian Li, Xixi Su, Qiang Gao, Guoyin Zu

This study develops a novel melt foaming technique for fabricating aluminum foam-filled tubes (FFTs) with in situ bonding. Through a high-temperature foaming process within a dynamically rotating mold, the foam and tube of FFT are cofabricated. The microstructure of FFT is observed, and the compression performance of FFT is also explored. The results demonstrate that the plateau stress of FFT is 25.50 MPa. The energy absorption and specific energy absorption of FFT are 12.75 MJ m3 and 15.0 kJ kg−1, respectively. Due to the in situ bonding, the energy absorption of FFT is increased by 87.2%. The stress remains stable in the axial compression process, and no macroscopic fracture occurs in FFT. Finite element models based on specimens are reconstructed by X-ray tomography. The tensile test is applied to the tube of FFT to obtain the parameters of the finite element simulation. The results of the finite element simulation also show that the composite structure of FFT deforms cooperatively in axial compression. The purpose of this study is to provide a high-efficiency strategy for achieving a composite structure aluminum foam with superior energy absorption and overcoming bonding failure during the deformation process.

本文研究了一种新型的熔体发泡原位键合法制备泡沫铝填充管的方法。通过在动态旋转模具内的高温发泡工艺,将FFT的泡沫与管材合成。观察了FFT的微观结构,探讨了FFT的压缩性能。结果表明,FFT的平台应力为25.50 MPa。FFT的吸能和比能分别为12.75 MJ m−3和15.0 kJ kg−1。由于原位键合,FFT的吸能提高了87.2%。在轴向压缩过程中应力保持稳定,在FFT过程中不发生宏观断裂。基于试样的有限元模型通过x射线断层扫描重建。对FFT管进行拉伸试验,获得有限元模拟参数。有限元模拟结果还表明,FFT复合材料结构在轴向压缩下具有协同变形。本研究的目的是提供一种高效的策略,以实现复合结构泡沫铝具有良好的能量吸收和克服变形过程中的粘结破坏。
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引用次数: 0
Numerical and Experimental Investigation of Failure Mechanisms in Additively Manufactured Multimaterial Triply Periodic Minimal Surface Polymer Cellular Materials 增材制造多材料三周期最小表面聚合物蜂窝材料失效机理的数值与实验研究
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202502387
Fatih Huzeyfe Öztürk, Abdurrahim Temiz, Fatih Pehlivan

Triply periodic minimal surface (TPMS) lattices are an emerging class of cellular materials with excellent potential for lightweight structural and energy-absorbing applications. In this study, gyroid (G), diamond (D), and primitive (P) architectures were fabricated via fused filament fabrication (FFF) using three material configurations: (i) single-phase polylactic acid (PLA) or polyethylene terephthalate glycol (PETG); (ii) layered PLA-PETG composite structures (50/50), in which the lower half was printed with PLA and the upper half with PETG; and (iii) layered composites with PLA shells and PETG cores. Quasi-static compression tests were combined with finite element simulations to elucidate stress distribution, deformation mechanisms, and collapse progression. The results demonstrate that homogeneous blends delay crack initiation and enhance specific energy absorption through progressive collapse, while layered composites improve stability by redirecting stresses via the PLA shell. Finite element analysis successfully captured shear banding, layer-wise buckling, and localized fracture, confirming the predictive capability of the simulations. The findings highlight the strong interplay between lattice geometry and material configuration in tailoring mechanical performance and provide guidelines for the design of multifunctional polymer-based cellular composites produced by additive manufacturing.

三周期最小表面(TPMS)晶格是一类新兴的细胞材料,在轻量化结构和吸能应用方面具有良好的潜力。在本研究中,通过熔融长丝制造(FFF),使用三种材料结构(i)单相聚乳酸(PLA)或聚对苯二甲酸乙二醇酯(PETG)制备了陀螺(G),金刚石(D)和原始(P)结构;(ii)层状PLA-PETG复合结构(50/50),下半部分打印PLA,上半部分打印PETG;(iii) PLA外壳和PETG芯层状复合材料。准静态压缩试验与有限元模拟相结合,阐明了应力分布、变形机制和坍塌过程。结果表明,均质共混材料通过逐渐坍塌延缓裂纹萌生,提高比能吸收,而层状复合材料通过PLA外壳重定向应力,提高稳定性。有限元分析成功捕获了剪切带、分层屈曲和局部断裂,证实了模拟的预测能力。研究结果强调了晶格几何形状和材料结构之间在定制机械性能方面的强烈相互作用,并为增材制造生产的多功能聚合物基蜂窝复合材料的设计提供了指导。
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引用次数: 0
Experimental Study on Low-Velocity Impact Damage of Aluminum Honeycomb-Basalt Fiber Composite Sandwich Panels 铝蜂窝-玄武岩复合夹层板低速冲击损伤试验研究
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202502274
Yaoyao Zhao, Yajun Zhao

To meet the urgent need for lightweight impact-resistant structures in new energy vehicles battery protection, an aluminum-honeycomb/basalt-fiber composite panel is proposed as a novel protective underbody, offering lightweight design, high specific strength and energy absorption. Drop-weight impact testing was conducted to characterize the dynamic mechanical response, and high-speed three-dimensional digital image correlation (3D-DIC) was used to quantify the influence of the thickness of the aluminum facesheet, basalt fiber ply count, core density of the aluminum honeycomb, and impact energy on the impact resistance. The peak impact force increased by factors of 3.60, 3.98, and 4.85 relative to the aluminum baseline. The dominant failure modes were penetration, tearing, and buckling. The ultimate load-carrying capacity of the panels with aluminum honeycomb core increases by factors of 4.54, 5.62, and 6.71 relative to aluminum. Local indentation and honeycomb crushing are the prevailing deformation modes, and no perforations occur. The aluminum honeycomb significantly enhances the panel stiffness and impact resistance. With increasing impact energy, the delaminationand tearing is delayed by crack bridging in the basalt fiber plies and interlaminar constraint, while progressive core crushing combined with face-sheet plasticity established multiple energy-dissipation pathways.

针对新能源汽车电池防护对轻量化抗冲击结构的迫切需求,提出了一种设计轻量化、比强度高、吸能性好的铝蜂窝/玄武岩纤维复合板作为新型防护底板。采用落锤冲击试验表征动态力学响应,采用高速三维数字图像相关技术(3D-DIC)量化铝面板厚度、玄武岩纤维层数、铝蜂窝芯密度和冲击能对抗冲击性能的影响。峰值冲击力相对于铝基准分别增加了3.60、3.98和4.85倍。主要的破坏模式是穿透、撕裂和屈曲。铝蜂窝芯板的极限承载能力相对于铝提高了4.54、5.62和6.71倍。局部压痕和蜂窝状破碎是主要的变形模式,不发生穿孔。铝蜂窝显著提高面板刚度和抗冲击性。随着冲击能量的增加,玄武岩纤维层内的裂缝桥接和层间约束延缓了岩心的分层和撕裂,而岩心的递进破碎结合面片塑性则建立了多种能量耗散途径。
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引用次数: 0
Tribological Behavior of Ceramic Ball/Nitride Coating Pairs: A Comparative Study Integrating Time-Series Analysis, Interface Morphology Characterization, and Numerical Simulation 陶瓷球/氮化物涂层对摩擦学行为:结合时间序列分析、界面形貌表征和数值模拟的比较研究
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202502019
Xin Zhang, Meiling Xie, Liuchen Wu

This study investigates the friction and wear mechanisms of CrN, AlCrN, TiN, and AlTiN coatings deposited on SUS316L stainless steel. The experiments are conducted under 50% humidity and a 5 N normal load, combining tribological tests with numerical simulation. The results show that the TiN coating paired with an Al2O3 ball exhibits the lowest wear rate of 8.9 × 10−4 mm3 (N·m)−1. In contrast, the AlCrN coating with ZrO2 ball achieves the lowest coefficient of friction of 0.318. The dominant wear mechanism is determined by the coating material. Specifically, TiN shows slight adhesive and fatigue wear, AlTiN experiences abrasive wear, and AlCrN exhibits fatigue wear. Furthermore, oxidative wear occurs in all coatings, with the highest degree in AlTiN and the lowest in CrN and AlCrN. Numerical simulations corroborate these findings, indicating that the stress distribution patterns vary with different ball-coating pairs and that the coating material is the primary factor influencing the stress distribution.

本文研究了在SUS316L不锈钢表面沉积CrN、AlCrN、TiN和AlTiN涂层的摩擦磨损机理。试验在50%湿度和5n法向载荷条件下进行,采用摩擦学试验和数值模拟相结合的方法。结果表明,与Al2O3球配对的TiN涂层的磨损率最低,为8.9 × 10−4 mm3 (N·m)−1;而ZrO2球的AlCrN涂层的摩擦系数最低,为0.318。主要的磨损机理是由涂层材料决定的。其中,TiN表现出轻微的粘着磨损和疲劳磨损,AlTiN表现出磨粒磨损,AlCrN表现出疲劳磨损。此外,所有涂层都发生氧化磨损,AlTiN涂层的氧化磨损程度最高,CrN和AlCrN涂层的氧化磨损程度最低。数值模拟结果证实了上述发现,表明不同球包对的应力分布规律不同,涂层材料是影响应力分布的主要因素。
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引用次数: 0
Dynamic Precipitation during High-Pressure Torsion of a Magnesium–Manganese Alloy 镁锰合金高压扭转过程中的动态析出
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202500424
Julian M. Rosalie, Anton Hohenwarter

An ultrafine-grained magnesium alloy has been produced through room temperature high-pressure torsion (HPT) of solutionized Mg–1.35 wt% Mn. Dynamic precipitation of nanometer-scale Mn particles occurs during deformation. These particles populate the grain boundaries, acting as pinning sites which allow the alloy to develop a grain size of 140 nm after 0.5 rotations. Further, HPT deformation results in a gradual increase in grain size with no increase in precipitate size. Despite the extensive deformation applied, the alloy does not develop a bimodal grain structure and retains a grain size of 230 nm after 10 complete rotations, demonstrating the stability and effectiveness of these pinning particles.

采用Mg-1.35 wt% Mn固溶室温高压扭转法制备了超细晶镁合金。纳米级Mn颗粒在变形过程中发生动态析出。这些颗粒填充在晶界上,充当固定位置,使合金在0.5旋转后形成140 nm的晶粒尺寸。HPT变形导致晶粒尺寸逐渐增大,而析出相尺寸没有增加。尽管施加了广泛的变形,但合金没有形成双峰晶粒结构,并且在10次完整旋转后仍保持230 nm的晶粒尺寸,证明了这些钉住颗粒的稳定性和有效性。
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引用次数: 0
Geometric Optimization and Mechanical Performance Enhancement of Auxetic Structures for High-Impact Applications Through Fused Deposition Modeling 基于熔融沉积建模的高冲击辅助结构几何优化与力学性能增强
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2026-01-03 DOI: 10.1002/adem.202500265
Malik Hassan, Manjusri Misra, Alexander Bardelcik, Stefano Gregori, Amar K. Mohanty

This study investigates the mechanical performance of three auxetic structures: re-entrant, re-entrant-star hybrid, and S-shape, to identify the most effective design for high-impact applications. Among these, the re-entrant-star hybrid structure demonstrates superior specific energy absorption (SEA), achieving 0.92 ± 0.12 J g−1, attributed to its combination of re-entrant and star-shaped elements, which enhances both energy dissipation and structural integrity. In contrast, the re-entrant and S-shaped structures recorded SEAs of 0.80 ± 0.02 and 0.19 ± 0.05 J g−1, respectively. The hybrid structure also exhibits the highest crush force efficiency (CFE) and equivalent plateau stress (EPS), highlighting its ability to maintain consistent load-bearing capacity and to sustain stress during compression. Flexural and impact tests further validate the hybrid structure's performance, with notable improvements in bending strength and impact resistance. To further enhance its performance, finite element analysis (FEA) simulations are conducted to optimize geometric parameters, specifically strut thickness and inclination angle, to maximize mechanical performance. Postoptimization, the SEA of the re-entrant-star structure increases by 449%, EPS by 3400%, and in-plane flexural modulus by 514%. These results demonstrate the effectiveness of optimizing geometric parameters to maximize the mechanical performance of auxetic structures for applications requiring high-energy absorption.

本研究考察了三种增减结构的力学性能:再入式、再入式星形混合结构和s形结构,以确定高冲击应用中最有效的设计。其中,重入-星杂化结构具有较好的比能吸收(SEA),达到0.92±0.12 J g−1,这主要归功于重入-星杂化结构与星形元件的结合,增强了能量耗散和结构完整性。而再入和s形结构的sea分别为0.80±0.02和0.19±0.05 J g−1。混合结构还表现出最高的挤压力效率(CFE)和等效平台应力(EPS),突出了其在压缩过程中保持一致的承载能力和承受应力的能力。弯曲和冲击试验进一步验证了混合结构的性能,在弯曲强度和抗冲击性方面有显著改善。为了进一步提高其性能,进行了有限元分析(FEA)仿真,以优化几何参数,特别是支撑厚度和倾角,以最大限度地提高力学性能。优化后,再入星形结构的SEA提高了449%,EPS提高了3400%,面内弯曲模量提高了514%。这些结果证明了优化几何参数以最大限度地提高需要高能吸收的减振结构的力学性能的有效性。
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引用次数: 0
Chemo-Mechanical Response and Thickness Effect of Silicon Anode Films during Lithiation 硅阳极薄膜在锂化过程中的化学-机械响应和厚度效应
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-12-29 DOI: 10.1002/adem.202502857
Xinyu Li, Pengfei Wan, Lihong Liang

Silicon anodes are considered to be the most promising new generation materials of Li-ion batteries. However, silicon anode undergoes significant volume expansion during charging, inducing cracking and deteriorating battery capacity and life span. Therefore, investigating the failure behavior and mechanism of silicon film anodes is crucial for ensuring the safety of batteries. In this article, a finite element model of high-capacity silicon anode film bonded copper current collector is established based on mechanical and chemical coupling effect combined with a thermal-analogy method. Volume expansion, Li-ion concentration distribution, and stress evolution of the silicon electrode thin film during the charge process are analyzed. A series of thickness silicon film-current collector models are further established, and the thickness effect of silicon film on state of lithiation at critical interface cracking is studied. The results show that stress changes resulting from Li-ion concentration variations can induce the risk of interface cracking. As the silicon film thickness decreases, its critical fracture strain and critical state of lithiation are higher, resisting interface peeling better and having better chemical and mechanical properties. This research provides a guideline for the dimensional design of silicon thin film electrode.

硅阳极被认为是最有前途的新一代锂离子电池材料。然而,硅阳极在充电过程中会发生明显的体积膨胀,导致电池开裂,降低电池容量和寿命。因此,研究硅膜阳极的失效行为和失效机理对保证电池的安全使用至关重要。本文基于力学和化学耦合效应,结合热类比法,建立了大容量硅阳极膜结合铜集流器的有限元模型。分析了硅电极薄膜在充电过程中的体积膨胀、锂离子浓度分布和应力演化。进一步建立了一系列厚度硅膜集流模型,研究了硅膜厚度对临界界面开裂时锂化状态的影响。结果表明,锂离子浓度变化引起的应力变化会诱发界面开裂风险。随着硅膜厚度的减小,其临界断裂应变和锂化临界状态越高,抗界面剥离性能越好,化学力学性能也越好。该研究为硅薄膜电极的尺寸设计提供了指导。
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引用次数: 0
Tribological Behavior of Zr-Based Bulk Metallic Glass Against WC Balls under Normal Load 正常载荷下zr基大块金属玻璃与WC球的摩擦学行为
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-12-29 DOI: 10.1002/adem.202501053
Su Zhao, Xuhui Chen, Zhihui Yang, Liping Tong, Lianyi Xu

This article explores the tribological behaviors of Zr46.5Cu45Al7Ti1.5 bulk metallic glass (BMG) during linear reciprocating sliding against WC ball under different loads. The time-dependent coefficient of friction indicates the presence of a significant “Running-in” stage during wear tests, with the duration of this stage extending as the normal load increases. The structural characteristics of the samples are examined using X-ray diffraction, which confirmed their noncrystalline nature. The wear surfaces and debris of the BMG and WC ball are analyzed using scanning electron microscopy coupled with energy-dispersive spectroscopy. The results demonstrate that the predominant wear mechanisms at low loads are abrasive and adhesive wear, accompanied by minimal oxidative wear. Under high loads, adhesive and oxidative wear dominate. A high wear rate is associated with adhesive wear, whereas a low wear rate is linked to oxidative wear.

研究了Zr46.5Cu45Al7Ti1.5大块金属玻璃(BMG)在不同载荷下与WC球直线往复滑动时的摩擦学行为。随时间变化的摩擦系数表明,在磨损试验中存在一个显著的“磨合”阶段,该阶段的持续时间随着正常载荷的增加而延长。用x射线衍射检查了样品的结构特征,证实了它们的非晶性质。采用扫描电子显微镜结合能谱仪对BMG和WC球的磨损面和磨屑进行了分析。结果表明,在低负荷下,主要的磨损机制是磨粒磨损和粘着磨损,并伴有最小的氧化磨损。在高负荷下,粘着磨损和氧化磨损占主导地位。高磨损率与黏着磨损有关,而低磨损率与氧化磨损有关。
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引用次数: 0
Rheocasting versus Die Casting: An Insight into the Low-Cycle Fatigue Behavior of AlSi7Mg0.6 流变铸造与压铸:AlSi7Mg0.6低周疲劳性能的研究
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-12-29 DOI: 10.1002/adem.202502276
Julia Richter, Thomas Wegener, Andreas Schilling, Martin Fehlbier, Thomas Niendorf

With respect to process and resource efficiency, semisolid casting processes, such as rheocasting, represent promising technologies for processing lightweight materials in the automotive industry. The reduced temperature of the melt during the casting process allows longer service life for the molds and less production rejects in industrial applications. However, up to now process–microstructure–property correlations have not been investigated in detail. Most studies focusing on these processes are producing simple geometries without a reduction in the cross section. Moreover, mechanical properties are only tested in the quasistatic regime. The present study investigates specimens taken from application-oriented parts. These specimens are examined comprehensively, i.e., from microstructure to the fatigue properties, and are compared to high pressure die cast counterparts. Based on the main findings, the following conclusion can be drawn: Although some differences can be found with respect to the microstructure appearance, under quasistatic loading the results are similar for the die cast and rheocast material (with a yield strength of 125 MPa and ultimate tensile strength of 240 MPa); however, with respect to fatigue properties in the low-cycle fatigue regime, the rheocast material shows reduced scatter: Thus, rheocasting is found to be the method of choice when improved fatigue properties are required.

在工艺和资源效率方面,半固态铸造工艺,如流变铸造,代表了在汽车工业中加工轻质材料的有前途的技术。在铸造过程中,熔体温度的降低可以延长模具的使用寿命,减少工业应用中的生产废品。然而,到目前为止,尚未对工艺-显微组织-性能的相关性进行详细的研究。大多数研究集中在这些过程产生简单的几何形状没有减少的横截面。此外,力学性能仅在准静态状态下进行测试。本研究调查了取自应用部件的样品。这些试样进行了全面的检查,即从微观结构到疲劳性能,并与高压压铸相比较。根据主要研究结果,可以得出以下结论:压铸和流变材料在准静态加载下的组织形貌虽然存在一定差异,但结果基本一致(屈服强度为125 MPa,极限抗拉强度为240 MPa);然而,相对于低周疲劳状态下的疲劳性能,流变铸造材料显示出更少的散射:因此,当需要改善疲劳性能时,流变铸造是一种选择方法。
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引用次数: 0
Understanding the Effect of Resistance Temperature Detector Temperature Controllers on Microstructural Alignment in Magnetic Freeze Casting 电阻式测温仪对磁冻铸造组织取向影响的研究
IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-12-29 DOI: 10.1002/adem.202500790
Maddie A. Schmitz, Steven E. Naleway

Magnetic freeze-casting is an up-and-coming method used to fabricate porous structures that are light in weight, yet relatively high in strength for biomedical and aerospace applications. A method has recently been discovered using magnetic fields to create effectively 100% microstructural alignment in freeze-cast scaffolds, resulting in impressive mechanical properties. Unfortunately, these results are limited to materials that are ferrimagnetic in nature. Previously, the magnetic field strength and the magnetic susceptibility of the particles used were thought to be the primary limiting factors to achieving 100% microstructural alignment. Recent work suggests there may be other factors at play that are preventing the microstructure from aligning. This work investigates these factors and identifies the voltage generated by the resistance temperature detector temperature controller, which is often employed in freeze-casting to control the freezing rate, as a significant factor. The voltage generated by the temperature controller affects the ability to align the microstructure of freeze-cast scaffolds using magnetic fields and therefore should be considered when trying to align microstructures.

磁性冷冻铸造是一种很有前途的方法,用于制造重量轻但强度相对较高的多孔结构,用于生物医学和航空航天应用。最近发现了一种方法,利用磁场在冷冻铸造支架中有效地产生100%的微观结构对齐,从而产生令人印象深刻的机械性能。不幸的是,这些结果仅限于铁磁性材料。以前,磁场强度和所用颗粒的磁化率被认为是实现100%微观结构对齐的主要限制因素。最近的研究表明,可能还有其他因素在阻止微观结构对齐。本文对这些因素进行了研究,并确定了电阻温度检测器温度控制器产生的电压是一个重要因素,该温度控制器通常用于冷冻铸造以控制冻结速率。温度控制器产生的电压会影响利用磁场对冻铸支架的微观结构进行排列的能力,因此在试图对微观结构进行排列时应予以考虑。
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引用次数: 0
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Advanced Engineering Materials
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