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Influence of Nano-encapsulation on Chemical Composition, Antioxidant Activity and Thermal Stability of Rosemary Essential Oil 纳米包封对迷迭香精油化学成分、抗氧化活性和热稳定性的影响
Pub Date : 2017-04-15 DOI: 10.3923/AJFT.2017.170.177
A. Hussein, M. Kamil, S. Lotfy, K. Mahmoud, F. Mehaya, A. Mohammad
Background: Herbs have been used for several purposes i.e., flavorings, beverages, repellents, fragrances, cosmetics and for their medicinal properties. Now a days, the interest in herbs has considerably increased, particularly as a natural source of flavor and antioxidants for the food and pharmaceutical industries. The quality and acceptability of food are related to flavor stability. It is well known that, manufacturing and storage processes, package materials and ingredient of foods often reduce aroma compound intensity. In order to minimize aroma degradation or loss during processing and storage, it is beneficial to encapsulate volatile ingredients prior to use in foods or beverages. Objective: This study aimed to investigate the effect of using different carrier materials on chemical composition, thermal stability and antioxidant activity of nano-encapsulated rosemary essential oil. Methodology: About 100 g of rosemary was subjected to hydro-distillation using Clevenger apparatus for 4 h to isolate its essential oil. Essential oil sample was analysis by GC-FID and GC-MS. The nano-encapsulation was procedure by homogenization technique in all samples. Encapsulation Efficiency (EE), Transmission Electron Microscopy (TEM), DPPH scavenging activity and total phenolic content of encapsulated essential oil samples were evaluated. Thermal stability assessment was done by Differential Scanning Calorimetric (DSC). Results: The results revealed that the highest release of total phenol (3349.4 μg GAE mLG1) and DPPH scavenging activity of rosemary EO were found in case of using chitosan as carrier material for nano-encapsulation process compared to CMC or sodium alginate. Also, the nano-encapsulation process improved thermal stability of rosemary EO. The TEM of nano-encapsulated of rosemary EO in CMC showed the lowest nano-particle size (10-20 nm) compared with chitosan or sodium alginate. After the GC-MS analysis of the volatile compounds of rosemary EO revealed that 1,8-cineole (30.88%), camphor (22.71%), "-terpineol (15.01%), "-pinene (8.78%) and camphene (4.31%) were the major compounds in rosemary EO. The results showed an increasing content of oxygenated monoterpenes, sesquiterpenes, sesquiterpene oxide and ester in nano-encapsulated rosemary EO samples. An opposite behavior was observed in content of monoterpens. Conclusion: In this study, the major components of rosemary EO were 1,8-cineole (30.88%), camphor (22.71%), "-terpineol (15.01%), "-pinene (8.78%) and camphene (4.31%). The type of wall materials has influence on the particles size and encapsulation efficiency and antioxidant activity of rosemary EO. The results indicated that nano-capsulation process increased the thermal stability of rosemary EO and could be useful as antioxidant for various thermal processing applications in industry.
背景:草药已被用于多种用途,即调味料、饮料、驱虫剂、香料、化妆品及其药用特性。如今,人们对草药的兴趣大大增加,尤其是作为食品和制药行业的天然香料和抗氧化剂的来源。食品的质量和可接受性与风味稳定性有关。众所周知,食品的生产和储存过程、包装材料和配料往往会降低香气复合强度。为了在加工和储存过程中尽量减少香气的降解或损失,在食品或饮料中使用之前将挥发性成分封装是有益的。目的:研究不同载体材料对纳米迷迭香精油化学成分、热稳定性及抗氧化活性的影响。方法:取约100 g迷迭香,用Clevenger蒸馏仪蒸馏水4 h,分离其精油。精油样品采用气相色谱- fid和气相色谱-质谱分析。所有样品均采用均质技术进行纳米包封。对精油样品的包封效率(EE)、透射电镜(TEM)、DPPH清除活性和总酚含量进行了评价。热稳定性评价采用差示扫描量热法(DSC)。结果:壳聚糖对迷迭香精油的总酚释放量(3349.4 μg GAE mLG1)和清除DPPH的活性均高于CMC和海藻酸钠。纳米包封工艺也提高了迷迭香精油的热稳定性。CMC包封的迷迭香精油的透射电镜显示,其纳米粒径最小(10 ~ 20 nm),高于壳聚糖和海藻酸钠。经GC-MS分析,迷迭香精油的挥发性成分主要为1,8-桉叶脑(30.88%)、樟脑(22.71%)、-松油醇(15.01%)、-蒎烯(8.78%)和樟烯(4.31%)。结果表明,迷迭香EO纳米包封样品中氧合单萜、倍半萜、倍半萜氧化物和酯的含量均有所增加。在单翅草的含量中观察到相反的行为。结论:迷迭香精油的主要成分为1,8-桉叶脑(30.88%)、樟脑(22.71%)、-松油醇(15.01%)、-蒎烯(8.78%)和樟烯(4.31%)。壁材类型对迷迭香精油的粒径、包封效率和抗氧化活性均有影响。结果表明,纳米胶囊化工艺提高了迷迭香精油的热稳定性,可作为抗氧化剂用于工业上的各种热加工。
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引用次数: 22
Optimum Extraction of Phenolic Compounds from Flaxseed Meal 亚麻籽粕中酚类化合物的最佳提取工艺研究
Pub Date : 2017-04-15 DOI: 10.3923/AJFT.2017.152.169
E. Akl, S. Mohamed, A. Hashem, F. Taha
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引用次数: 6
Retrospective Analysis of Moringa Leaf as a Substitute to Ethylene Gas in Hastening Ripening of Banana Fruit 辣木叶替代乙烯气体加速香蕉果实成熟的回顾性分析
Pub Date : 2017-04-15 DOI: 10.3923/AJFT.2017.186.192
Betewulign Eshetu Ademe, A. A. Tanga
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引用次数: 3
Effect of Pre-gelatinization on Physicochemical and Functional Properties of Gayam (Inocarfus fagifer Forst.) Flour 预糊化对加亚木理化及功能特性的影响面粉
Pub Date : 2017-04-15 DOI: 10.3923/AJFT.2017.178.185
Agus Wijanarka, Toto Sudargo, E. Harmayani, Y. Marsono
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引用次数: 8
A Rapid Method for the Determination of the Total Conjugated Linoleic Acid (CLA) Encapsulated in β-casein Nanoparticles β-酪蛋白纳米颗粒包封总共轭亚油酸的快速测定方法
Pub Date : 2017-02-15 DOI: 10.3923/AJFT.2017.140.143
M. El-Salam, Moustapha Hassan, A. El-Fattah, M. M. El-Sayed, F. Assem, M. El-Aaser
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引用次数: 2
Physicochemical, Molecular and Functional Characteristics of Hyaluronic Acid as a Functional Food 功能食品透明质酸的理化、分子及功能特性
Pub Date : 2017-02-15 DOI: 10.3923/AJFT.2017.72.85
S. Sohaimy, G. Hamad, Tarek H. Taha, E. Hafez
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引用次数: 17
Establishment of a Sterilization Regime for Sugarcane Molasses Used in Baker's Yeast Production Baker酵母生产中甘蔗糖蜜灭菌制度的建立
Pub Date : 2017-02-15 DOI: 10.3923/ajft.2017.106.115
Salah H. Salem, Y. Heikal, M. Naguib, H. El-Sheikh
Background and Objective: Geobacillus stearothermophilus is a major contaminant of sugarcane molasses which withstand the traditional primary heat treatment of crude molasses and compete with baker’s yeast in sugar fermentation. Present work aims to study the thermal death kinetics of G. stearothermophilus and to establish a heat treatment regime for the molasses used in baker’s yeast production. Methodology: Thermal inactivation studies were carried out on spores of G. stearothermophilus strain-isolated from Egyptian sugarcane molasses and populated on TSB as well as diluted molasses (10E Brix) adjusted to pH 4.7. Thermal death kinetics were calculated using TDT-tubes at temperatures ranging from 90-130EC. The thermal death experiments were done after 1 h from primary preheating the spore suspensions at 80EC for 10 min to eliminate the vegetative cells and induce heat shock for the spores. Results: Survival curves of spores are linear following first-order kinetic pattern for spore heated at temperatures >115EC. Obtained decimal reduction time (D-values) were 23.71, 8.07, 4.68, 0.834, 0.473 and 0.174 min for spore suspensions heated in molasses media at 100, 110, 115, 120, 125 and 130EC, respectively. Spore suspensions heated in TSB media showed higher D-values. The temperature range (Z-value) required to reduce the D-value by 1/10 was in the range of 14.05EC. The obtained D and Z-values were used to establish a continuous sterilization regime for molasses to achieve a reduction of G. stearothermophilus spores of 7 logarithmic cycles to insure molasses sterility. The proposed sterilization system is based on steam injection, holding the molasses in a sterilization tube for the necessary time and flashing to reduce the molasses temperature. Calculated sterilization time was 73.08, 32.11 and 14.11 sec for sterilization temperatures 130, 135 and 140EC, respectively. The corresponding length of necessary holding tube was 89.16, 39.17 and 17.21 m, respectively. Conclusion: The pump power required to force the flow of molasses through sterilization system was in the range of 1.37-1.7 HP and the steam pressure needed for sterilization was 4-5 bar. The steam requirement is of 1 kg steam for each 10 kg molasses.
背景与目的:嗜热硬脂地杆菌是甘蔗糖蜜的主要污染物,它经受住了粗糖蜜的传统初级热处理,在糖发酵过程中与面包酵母竞争。目前的工作旨在研究嗜热硬脂菌的热死亡动力学,并建立用于面包酵母生产的糖蜜的热处理制度。方法:对从埃及甘蔗糖蜜中分离出来的嗜热硬脂嗜热菌G. stearothermophilus菌株孢子进行热失活研究,该菌株在TSB和调至pH 4.7的稀释糖蜜(10E Brix)上繁殖。使用tdt管在90-130℃的温度范围内计算热死亡动力学。热死亡实验是将孢子悬浮液在80℃下初加热10 min, 1 h后进行,以消除营养细胞,诱导孢子热休克。结果:当温度>115℃时,孢子的存活曲线符合一级动力学模式。在100、110、115、120、125和130EC温度下,孢子悬浮液的十进制还原时间(d值)分别为23.71、8.07、4.68、0.834、0.473和0.174 min。在TSB培养基中加热的孢子悬浮液显示出较高的d值。将d值降低1/10所需的温度范围(z值)在14.05EC范围内。获得的D和z值用于建立糖蜜的连续灭菌制度,以实现7个对数周期的G.硬脂嗜热菌孢子的减少,以确保糖蜜的无菌性。所提出的灭菌系统是基于蒸汽注入,将糖蜜在灭菌管中保持必要的时间并闪烁以降低糖蜜温度。在130℃、135℃和140℃条件下,计算出的灭菌时间分别为73.08、32.11和14.11秒。所需保温管长度分别为89.16 m、39.17 m和17.21 m。结论:强制糖蜜通过灭菌系统所需的泵功率为1.37 ~ 1.7 HP,灭菌所需的蒸汽压力为4 ~ 5 bar。每10kg糖蜜需要1kg蒸汽。
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引用次数: 0
Enhancing the Nutritive Values of Ice Milk Based on Dry Leaves and Oil of Moringa oleifera 以辣木干叶和辣木油为原料提高冰奶的营养价值
Pub Date : 2017-02-15 DOI: 10.3923/AJFT.2017.86.95
H. Salama, S. El‐Sayed, A. Abdalla
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引用次数: 7
Chemical Composition and Genetics of Indonesian Maize Hybrids 印度尼西亚玉米杂交种的化学成分和遗传
Pub Date : 2017-02-15 DOI: 10.3923/AJFT.2017.116.123
H. Marta, E. Suryadi, D. Ruswandi
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引用次数: 10
Treatment of Jojoba and Jatropha Seeds Hulls Wastes and Production of New Value Added Products 荷荷巴和麻疯树种子壳废弃物的处理及新附加值产品的生产
Pub Date : 2017-02-15 DOI: 10.3923/AJFT.2017.96.105
S. Wagdy, F. Taha, S. Omar
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引用次数: 3
期刊
American Journal of Food Technology
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