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Particle Distribution Measurement of Highly Concentrated Emulsions Based on Ultrasonic Extended Coupled Phase Model 基于超声波扩展耦合相模型的高浓度乳液颗粒分布测量
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-08 DOI: 10.1134/S1061830923601344
Huaishu Hou, Yuxiang An, Han Yun, Chenhuai Tang

This paper introduces a method for measuring solute particle size in solution. The working principle of this method is to characterize the particle size by using the ultrasonic extended coupled phase model combined with the acoustic attenuation coefficient of the solution. In the ultrasonic detection of highly concentrated emulsion particles, the inter-particle interaction, namely the structural loss, becomes the main factor affecting the ultrasonic attenuation. In this study, micron-sized emulsions with 10, 15, and 20% concentration were experimentally detected by the extended coupled-phase model, and the inverse calculation of the particle size distribution was carried out using a differential evolutionary algorithm. The detection results showed an average error of 4.266% compared with those of laser particle sizer. The results show that ultrasonic detection based on the extended coupled phase model combined with differential evolution inversion algorithm can achieve accurate measurement of particle size distribution of emulsions with high concentration.

摘要 本文介绍了一种测量溶液中溶质粒度的方法。该方法的工作原理是利用超声扩展耦合相模型结合溶液的声衰减系数来表征粒度。在对高浓度乳液颗粒进行超声检测时,颗粒间的相互作用(即结构损失)成为影响超声衰减的主要因素。本研究利用扩展耦合相模型对浓度分别为 10%、15% 和 20% 的微米级乳液进行了实验检测,并利用微分进化算法对粒度分布进行了反演计算。与激光粒度仪相比,检测结果的平均误差为 4.266%。结果表明,基于扩展耦合相模型的超声波检测结合微分进化反演算法可以实现对高浓度乳液粒度分布的精确测量。
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引用次数: 0
Determination of Position and Size of Non-Flaws at Albedo Flaw Detection 在反照率缺陷检测中确定非缺陷的位置和大小
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-08 DOI: 10.1134/S1061830924601636
E. E. Zhuravskiy, D. S. Belkin, B. I. Kapranov, S. V. Chakhlov

In this article the methods of determining the position and size of non-flaws in albedo flaw detection are considered. Analytical and numerical solutions of the problem of determining the location of non-flaws on the basis of known parameters of the collimation system are shown. The dependence of the location of the flaw on the parameters of the collimation system is shown. It is proposed to determine not the true size of the flaw, but its equivalent area, similar to ultrasonic flaw detection.

摘要 本文探讨了反照探伤中确定非缺陷位置和尺寸的方法。文章给出了在准直系统已知参数基础上确定非缺陷位置问题的分析和数值解决方案。显示了缺陷位置对准直系统参数的依赖性。建议确定的不是缺陷的真实大小,而是其等效面积,类似于超声波探伤。
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引用次数: 0
Identification and Classification of Buckwheat Grain by Microfocus Radiography and Hyperspectral Imaging Methods 用微聚焦射线照相法和高光谱成像法对荞麦粒进行识别和分类
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-08 DOI: 10.1134/S1061830924601697
Yu. T. Platov, S. L. Beletskii, D. A. Metlenkin, R. A. Platova, A. L. Vereshchagin, V. A. Marin

Classification of buckwheat grains is important because the absence of defective grains is a guarantee of yield and quality. Buckwheat grains were randomly selected from a batch with grains that varied in quality. The identification and classification of buckwheat grains according to the degree of fulfillment was carried out by a combination of microfocus X-ray and hyperspectral image analysis and multivariate analysis techniques. Using microfocus radiography, buckwheat grains were categorized into groups according to the degree of fulfillment. Hyperspectral image of buckwheat grains in the range of 935–1720 nm was acquired using a Specim FX17 camera. Using the polygon selection function, the averaged spectra were obtained and a data matrix of grain samples was generated. The bands of the spectrum contributing most to the grading of the grain samples by the degree of fulfillment were identified using the principal component analysis. The classification model of grading buckwheat grain into groups by the degree of fulfillment was constructed by partial least squares discriminant analysis method. The results showed that hyperspectral image is a potential tool for rapid and accurate identification of buckwheat grains, which can be used in large-scale grain classification and grain quality determination.

摘要 荞麦谷粒的分类非常重要,因为没有缺陷谷粒是产量和质量的保证。荞麦谷粒是从一批质量参差不齐的谷粒中随机挑选出来的。采用微焦 X 射线和高光谱图像分析以及多元分析技术,根据荞麦粒的合格程度对其进行鉴定和分类。利用微焦射线照相术,根据荞麦颗粒的饱满程度将其分为不同的组别。使用 Specim FX17 相机获取了荞麦粒在 935-1720 纳米范围内的高光谱图像。使用多边形选择功能获得了平均光谱,并生成了谷物样本的数据矩阵。利用主成分分析法确定了光谱中对谷物样品的饱满度分级贡献最大的波段。利用偏最小二乘法判别分析方法构建了荞麦谷物满足度分级模型。结果表明,高光谱图像是快速准确识别荞麦粒的潜在工具,可用于大规模谷物分类和谷物品质测定。
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引用次数: 0
Application Progress and Prospect of Defect Detection Technology for Timber Structure Members 木结构构件缺陷检测技术的应用进展与展望
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-08 DOI: 10.1134/S1061830924600217
Kai Zhao, Zhedong Ge, Liangliang Huo, Yisheng Gao, Yucheng Zhou, Zhihao Yao

Timber buildings show the exquisite skills of craftsmen in China. Under the influence of nature and human activities, damage and destruction of ancient timber structures lead to the loss of China’s cultural heritage. Therefore, it is particularly important to study the existing defect detection methods of timber members and provide excellent restoration plan for the preservation of timber structures. Defects of timber structure members were found to consist mainly of cracking, decay, insect-attack, bending and pullout of tenons, etc. These defects are the main factors that affect the mechanical properties of timber members and endanger the stability of timber structures. Pilodyn, resistograph, stress wave, radar, ultrasound, X-ray, infrared spectroscopy and piezoelectric transducers are all were studies for detection methods mentioned, which belong to semi-destructive testing and non-destructive testing. In detail, the principle, development status and application cases of wood building detection technology are elaborated to demonstrate the advantages and disadvantages of these technologies in various scenarios. New and feasible detection technology should be developed, and the development direction of damage detection technology for timber structures in the future is put forward.

摘要 木材建筑展现了中国工匠的精湛技艺。在自然和人类活动的影响下,古木结构的损坏和破坏导致了中国文化遗产的流失。因此,研究现有的木结构构件缺陷检测方法,为木结构的保护提供优秀的修复方案显得尤为重要。研究发现,木结构构件的缺陷主要包括开裂、腐朽、虫蛀、弯曲和榫头脱出等。这些缺陷是影响木结构构件机械性能和危及木结构稳定性的主要因素。上述检测方法包括皮洛迪、电阻仪、应力波、雷达、超声波、X 射线、红外光谱和压电传感器等,属于半破坏性检测和非破坏性检测。详细阐述了木结构建筑检测技术的原理、发展现状和应用案例,说明了这些技术在不同场景下的优缺点。应开发新的、可行的检测技术,并提出了未来木结构损伤检测技术的发展方向。
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引用次数: 0
Laser Ultrasonic High Precision Imaging Method for Internal Defects of Small-Diameter Cylindrical Components 针对小直径圆柱形部件内部缺陷的激光超声波高精度成像方法
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-08 DOI: 10.1134/S1061830924600047
Yanjie Zhang, Tianyou Li, Zhihui Xu, Ruipeng Jiang, Yaxing Liu, Wei Wang, Wei Shi, Yunfeng Song

An improved frequency-domain synthetic aperture focusing technique (F-SAFT) for laser ultrasonic testing (LUT) is proposed for internal defect detection of small-diameter cylindrical components. Firstly, a LUT automated detection platform is built, a pulsed laser is used to excite ultrasonic waves and a two-wave mixing (TWM) interferometer is used to detect ultrasonic waves. Since ultrasonic signals are affected by the thermal expansion of the pulsed laser, time-frequency analysis is used to obtain the frequency range for imaging longitudinal waves, and the influence of low-frequency clutter is eliminated through multiple filtering. Secondly, in order to balance signal acquisition efficiency and imaging quality, the peak signal-to-noise ratio (PSNR) is used to determine the optimal angular step size. Finally, the equivalent velocity of the longitudinal wave is corrected to compensate for the imaging position error caused by the separation of the ultrasonic excitation point and the detection point. The results show that the method proposed in this paper has high imaging accuracy, which could provide a new approach for in-service non-destructive testing of small-diameter cylindrical components.

摘要 针对小直径圆柱形零件的内部缺陷检测,提出了一种改进的频域合成孔径聚焦技术(F-SAFT)激光超声检测(LUT)。首先,构建了一个 LUT 自动检测平台,使用脉冲激光器激发超声波,并使用双波混合(TWM)干涉仪检测超声波。由于超声波信号会受到脉冲激光热膨胀的影响,因此采用时频分析法获得纵波成像的频率范围,并通过多重滤波消除低频杂波的影响。其次,为了平衡信号采集效率和成像质量,利用峰值信噪比(PSNR)来确定最佳角度步长。最后,对纵波的等效速度进行校正,以补偿超声波激发点和检测点之间的距离造成的成像位置误差。结果表明,本文提出的方法具有很高的成像精度,可为小直径圆柱形部件的在役无损检测提供一种新方法。
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引用次数: 0
High Precision Ultrasonic Testing Method for Density of Engineering Plastics 工程塑料密度的高精度超声波测试法
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-27 DOI: 10.1134/S1061830924600011
Chenggang Li, Lun Wang, Lihong Sun, Zhaojie Chu, Wei Liu, Jiagui Tao

The density of engineering plastics is a key parameter for ensuring their safety and reliability. In order to achieve rapid and high-precision on-site detection, a method based on the acoustic pressure reflection coefficient is proposed. First, finite element simulation analysis was conducted to obtain the acoustic field distribution during ultrasound propagation under water immersion conditions. The correlation between interface echo intensity and material density was determined. Optimal detection parameters were designed to reduce measurement errors caused by beam overlap and diffusion attenuation. A water immersion ultrasonic experimental system was constructed, and the measurement accuracy of the method was tested using chlorinated polyvinyl chloride pipes. The results show that, compared to the measurement results of the Archimedean drainage method, the maximum error of ultrasonic measurements does not exceed 1.7%, and the overall variance is less than 1.2%. The measurement accuracy of this method is compared with the regression results of different machine learning models. It is demonstrated that, compared to regression methods based on variable correlation, this method retains the advantages of high efficiency and low cost in ultrasonic density measurement, while achieving higher measurement accuracy. Additionally, it does not require a dataset for training support, making it promising and valuable for practical applications.

摘要 工程塑料的密度是确保其安全性和可靠性的关键参数。为了实现快速、高精度的现场检测,本文提出了一种基于声压反射系数的方法。首先,通过有限元模拟分析获得了超声波在浸水条件下传播时的声场分布。确定了界面回声强度与材料密度之间的相关性。设计了最佳检测参数,以减少由波束重叠和扩散衰减引起的测量误差。构建了水浸超声波实验系统,并使用氯化聚氯乙烯管道测试了该方法的测量精度。结果表明,与阿基米德排水法的测量结果相比,超声波测量的最大误差不超过 1.7%,总体方差小于 1.2%。该方法的测量精度与不同机器学习模型的回归结果进行了比较。结果表明,与基于变量相关性的回归方法相比,该方法既保留了超声波密度测量的高效率和低成本优势,又实现了更高的测量精度。此外,该方法不需要数据集的训练支持,因此在实际应用中具有广阔的前景和价值。
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引用次数: 0
Effect of Heat Treatment and Pigment Fraction on the Thermal Conductivity and Dynamic Behavior of Poly (Methyl Methacrylate) Pigmented with Titanium Dioxide 热处理和颜料组分对二氧化钛颜料聚(甲基丙烯酸甲酯)导热性和动态行为的影响
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-27 DOI: 10.1134/S1061830923601423
N. Ghebrid, D. Dadache, B. Barka, M. Guellal, F. Rouabah, M. Fois

The thermal behavior of a poly(methylmethacrylate) (PMMA) pigmented with titanium dioxide (TiO2) is studied in both Steady state and transient regimes in the present work. The numerical results of thermal conductivity, based on the finite element method, are compared to theoretical models and experimental measurements, which varies depending on the quenching temperature and pigment content. Time evolution of temperatures during the quenching of the composite is taken into account for different quenching temperatures and different pigment contents. It is noted that the heat exchange becomes slower for a pigment fraction of 0.5%, and the steady state is reached more rapidly for higher pigment content. The AFM image of the PMMA/TiO2 composite with content equal to 3% of titanium dioxide. This demonstrates a good distribution of the particles throughout the matrix, with the individual particles being uniformly dispersed and securely embedded in the polymer matrix, thereby avoiding any clustering. An improvement in heat exchange is observed in the composite with a high content of titanium dioxide. This improvement is attributed to the increase in the thermal conductivity of the PMMA/TiO2 composite.

摘要 本研究对添加了二氧化钛(TiO2)颜料的聚(甲基丙烯酸甲酯)(PMMA)在稳态和瞬态下的热行为进行了研究。基于有限元法得出的导热系数数值结果与理论模型和实验测量结果进行了比较。针对不同的淬火温度和不同的颜料含量,考虑了复合材料淬火过程中温度的时间演变。结果表明,当颜料含量为 0.5% 时,热交换速度变慢,而颜料含量越高,达到稳定状态的速度越快。二氧化钛含量等于 3% 的 PMMA/TiO2 复合材料的原子力显微镜图像。这表明颗粒在整个基体中分布良好,单个颗粒均匀分散并牢固地嵌入聚合物基体中,从而避免了任何团聚现象。在二氧化钛含量较高的复合材料中可以观察到热交换的改善。这种改善归因于 PMMA/TiO2 复合材料热导率的提高。
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引用次数: 0
Visualization of Acoustic Emission Monitoring of Damage Evolution of Reinforced Concrete Beams under Bending 弯曲情况下钢筋混凝土梁损伤演变的声发射可视化监测
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-27 DOI: 10.1134/S1061830923601307
Ye Tian, Xudong Chen, Xin Shi, Bin Li, Yingjie Ning

Reinforced concrete (RC) structures combine steel and concrete to harness their respective advantages, making them a staple in contemporary architecture. With the aging of civil engineering structures, structural health monitoring grows increasingly critical. In this context, acoustic emission technology (AE) emerges as an effective nondestructive testing method for assessing the structural damage status. Building on this foundation, the AE technology was utilized to monitor the crack growth in the RC beam under the four-point bending test. Furthermore, a visual analysis method to assess the internal damage of the RC beam, based on the spatial b value of the AE, was introduced. This method integrates the spatial b value and the AE event density distributions to develop the T value. The results indicate that as the stirrup ratio decreases, the bearing capacity of RC beams increases; however, their ductility experiences a significant reduction, and the failure mode undergoes a transformation. Throughout each failure stage of RC beams, the AE ringing number and energy exhibit unique and easily distinguishable characteristics of change. Additionally, RA-AF correlation analysis can be applied to delve deeper into the analysis of the RC beams’ failure modes. Utilizing the spatial b value and T value facilitates the identification of damage locations within the RC beam, thereby offering a practical and feasible approach for structural damage analysis.

摘要钢筋混凝土(RC)结构结合了钢和混凝土各自的优势,使其成为当代建筑的主要组成部分。随着土木工程结构的老化,结构健康监测变得越来越重要。在此背景下,声发射技术(AE)作为一种有效的无损检测方法应运而生,用于评估结构的损坏状况。在此基础上,我们利用声发射技术监测了四点弯曲试验下 RC 梁的裂缝生长情况。此外,还引入了一种基于 AE 空间 b 值的可视化分析方法,用于评估 RC 梁的内部损坏情况。该方法综合了空间 b 值和 AE 事件密度分布,从而得出 T 值。结果表明,随着箍筋比的减小,RC 梁的承载能力会增加,但延性会显著降低,失效模式也会发生转变。在 RC 梁的每个破坏阶段,AE 振铃数和能量都表现出独特且易于区分的变化特征。此外,RA-AF 关联分析可用于深入分析 RC 梁的破坏模式。利用空间 b 值和 T 值有助于确定 RC 梁内的损坏位置,从而为结构损坏分析提供一种切实可行的方法。
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引用次数: 0
Applying Data Fusion Procedures to Evaluation of Impact Damage in Carbon Fiber Reinforced Plastic by Using Optical Infrared Thermography and Laser Vibrometry Techniques 利用光学红外热成像和激光测振技术,将数据融合程序应用于碳纤维增强塑料的冲击损伤评估
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-27 DOI: 10.1134/S1061830924601685
V. Yu. Shpil’noi, D. A. Derusova, V. P. Vavilov

This study is devoted to the development of fusion techniques for data obtained by one or several nondestructive testing (NDT) methods. Experimental results were obtained by applying laser vibrometry and optical infrared thermography to evaluation of impact damage to carbon fiber composites. These NDT techniques are different by their physical nature and supply specific testing results. The proposed data fusion method allows increasing the reliability of inspection results and enables estimating defect parameters. It involves both averaging data of each single NDT technique and merging the results obtained by two methods. Vibrograms obtained by laser vibrometry are used to analyze acoustic response of the test sample to stimulation at various frequencies. In turn, infrared thermographic NDT supplies the sample response to thermal stimulation. It has been shown that the fusion of these two techniques supplies a comprehensive information on defect size and location. Also, the automation of the fusion procedure increases NDT productivity and reduces subjectivity of testing results.

摘要 本研究致力于开发一种或几种无损检测(NDT)方法所获数据的融合技术。通过应用激光测振仪和光学红外热成像技术对碳纤维复合材料的冲击损伤进行评估,获得了实验结果。这些无损检测技术具有不同的物理特性,并提供特定的检测结果。所提出的数据融合方法可以提高检测结果的可靠性,并能估算缺陷参数。该方法既包括对每种单一无损检测技术的数据进行平均,也包括对两种方法获得的结果进行合并。激光测振仪获得的振动图用于分析检测样本对不同频率刺激的声学响应。而红外热成像无损检测则提供样品对热刺激的响应。研究表明,这两种技术的融合可提供有关缺陷大小和位置的全面信息。此外,融合程序的自动化还能提高无损检测的效率,减少检测结果的主观性。
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引用次数: 0
Dynamic Laser Speckle Imaging as a Nondestructive Method for Tracking the Dynamics in Slow Curing Epoxy Resin 动态激光斑点成像是跟踪慢固化环氧树脂动态的一种无损方法
IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-27 DOI: 10.1134/S106183092360123X
S. H. Keerthana, A. Mujeeb, P. Radhakrishnan

Dynamic laser speckle imaging (DLSI) is an emerging nondestructive optical method used for the characterization of turbid materials. The microscopic dynamics of the turbid materials can be quantified using this imaging technique with high spatio temporal resolution. In recent decades, epoxy resins became indispensable for industries due to its fascinating mechanical properties, high chemical resistance, etc. The physical, mechanical and electrical characteristics of epoxy resins depend on the curing process. However, the techniques for monitoring the microscopic dynamics of the curing process are in-sufficient. Hence this work reports the application of dynamic laser speckle imaging to monitor the curing stages of Araldite, a 2 part epoxy resin. The computational methods incorporated with the technique include cross-correlation, inertia moment, Fujii method, etc. Conventional characterization techniques such as Differential Scanning Calorimetry and Fourier Transform Infrared Spectroscopy were also employed to confirm the results. The experimental results were also confirmed using the theoretical analysis.

摘要 动态激光斑点成像(DLSI)是一种新兴的无损光学方法,用于表征浑浊材料。利用这种高时空分辨率的成像技术,可以对浑浊材料的微观动态进行量化。近几十年来,环氧树脂因其迷人的机械性能和高耐化学腐蚀性等特点成为工业中不可或缺的材料。环氧树脂的物理、机械和电气特性取决于固化过程。然而,对固化过程的微观动态监测技术还不够充分。因此,这项工作报告了应用动态激光斑点成像技术监测 Araldite(一种双组分环氧树脂)固化阶段的情况。该技术采用的计算方法包括交叉相关法、惯性矩法、藤井法等。此外,还采用了差示扫描量热法和傅立叶变换红外光谱法等常规表征技术来确认结果。理论分析也证实了实验结果。
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引用次数: 0
期刊
Russian Journal of Nondestructive Testing
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