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Determination by scratch testing of the quality of thin-film oxide coatings formed by vacuum-arc plasma-assisted method 真空弧等离子体辅助法形成的氧化薄膜涂层质量的划痕试验测定
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-05-12 DOI: 10.1007/s11182-025-03445-9
N. N. Koval, N. A. Prokopenko, E. A. Petrikova, M. S. Vorobyov, Yu. F. Ivanov

Oxide coatings formed on the surface of medical instruments made of titanium-based alloys help physicians to protect patients from toxic titanium alloying elements and increase the resistance of the instruments to scratching and wearing. As a rule, the formation of a coating/substrate system is accompanied by an analysis of the adhesive properties of the applied coating. This paper presents an analysis of the results obtained by studying the structure and adhesive properties of titanium oxide and zirconium oxide films formed on the surface of titanium alloy samples of Grade 5 by vacuum arc plasma-assisted method with varying discharge current values of the plasma source operating on the basis of an independent arc discharge with glow and hollow cathodes. The studies showed that the oxide films contain droplet fraction particles the characteristics of which are determined by the film deposition mode. It has been established that the critical load force at which destruction of (peeling off) the film from the substrate (titanium alloy Grade 5) is observed in the ZrO2 film/Grade 5 substrate system is maximum at the “PINK” discharge current Ip = 0 A and minimum at Ip = 90 A. It was found that in the TiO2 film/Grade 5 substrate system, the maximum value of the critical load force is realized at the “PINK” discharge current Ip = 130 A and minimum at Ip = 0 A.

钛基合金制成的医疗器械表面形成的氧化物涂层有助于医生保护患者免受有毒钛合金元素的伤害,并增加器械对刮擦和磨损的抵抗力。通常,涂料/基材体系的形成伴随着对所涂涂料粘合性能的分析。本文分析了在辉光和空心阴极独立电弧放电的基础上,利用不同放电电流值的等离子体源,采用真空电弧等离子体辅助方法在5级钛合金样品表面形成氧化钛和氧化锆薄膜的结构和粘附性能。研究表明,氧化膜中含有液滴分数颗粒,其特征与膜的沉积方式有关。已经确定,在ZrO2薄膜/ 5级衬底体系中观察到薄膜从衬底(钛合金5级)上破坏(剥离)的临界负载力在“PINK”放电电流Ip = 0 A时最大,在Ip = 90 A时最小。研究发现,在TiO2薄膜/ 5级衬底体系中,临界负载力在“PINK”放电电流Ip = 130 A时达到最大值,在Ip = 0 A时达到最小值。
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引用次数: 0
Low resistivity measurement of chromium coatings on zirconium alloys E110 for the production of accident-resistant core components of nuclear reactors 核反应堆耐事故堆芯部件用E110锆合金铬涂层的低电阻率测量
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-05-12 DOI: 10.1007/s11182-025-03449-5
A. M. Salman, V. N. Kudiiarov, A. M. Lider

Non-destructive testing (NDT) techniques, including thermal electromotive force (ThermoEMF) and four-probe resistivity (FPP) measurements, offer an innovative approach to assessing chromium coatings on zirconium alloy E110, which are utilized in the manufacturing of core components resistant to emergencies in nuclear reactors. These methods quantify their critical properties, such as electrical conductivity, thermoelectric stability, and coating uniformity, providing insights into the coating structural quality and adhesion.

包括热电动势(ThermoEMF)和四探头电阻率(FPP)测量在内的无损检测(NDT)技术,为评估锆合金E110上的铬涂层提供了一种创新方法,这种方法可用于制造核反应堆中抗紧急情况的核心部件。这些方法量化了它们的关键性能,如导电性、热电稳定性和涂层均匀性,从而深入了解涂层的结构质量和附着力。
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引用次数: 0
Structure and properties of welding joints of 1370 aluminum alloy obtained by electron-beam welding 1370铝合金电子束焊接接头的组织与性能
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-08 DOI: 10.1007/s11182-025-03424-0
V. V. Solov’ev, V. Kh. Dammer, V. P. Krivobokov

The paper focuses on the structure and properties of welding joints of the high-strength 1370 aluminum alloy obtained by electron-beam welding (EBW). This issue is relevant to the housing assembly technique of space vehicle gyroscope sensors. The heat-affected zone geometry produced by the electron beam, is studied herein as well as the welding joint structure, depending on welding parameters. EBW of the 1370 aluminum alloy has a positive effect on the strength properties of the welding joint. The energy dose per unit length of the joint must be correct. Insufficient energy dose leads to lack of welding penetration and low joint strength, whereas its excess provides the liquid metal evaporation and the formation of pores and cracks. Feasibility is demonstrated for welding the aluminum alloy at a higher speed.

研究了采用电子束焊接技术获得的高强度1370铝合金焊接接头的组织和性能。该问题涉及航天飞行器陀螺仪传感器壳体装配技术。本文研究了电子束产生的热影响区几何形状以及焊接接头在不同焊接参数下的结构。1370铝合金的EBW对焊接接头的强度性能有积极的影响。关节单位长度的能量剂量必须正确。能量剂量不足导致焊透不足,接头强度低,能量剂量过高则导致液态金属蒸发,形成气孔和裂纹。论证了高速焊接铝合金的可行性。
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引用次数: 0
Structural features of low-stable phase states of aqueous solutions at ultrahigh dilution 超高稀释水溶液低稳定相态的结构特征
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-08 DOI: 10.1007/s11182-025-03436-w
A. I. Potekaev, V. V. Obukhov, S. D. Odintsov

A physical concept of thermodynamic structural-phase states of a physical system is proposed in application to ultrahigh diluted aqueous solutions low-stable to external impacts. The physical analogy between the states of these solutions and the condensed physical systems helps to understand physics of various effects observed in ultrahigh diluted aqueous solutions. In particular, this approach allows the role of shaking of the chemical solutions in the Epstein effect to be evaluated by mechanochemical methods. An analysis of the thermodynamic and structural-phase low-stable states of the physical system makes it possible to propose a possible mechanism for the system transition to a new phase state under a low-stable external impact on the example of an ordering alloy system. In this case, the small external impact (for example, shaking) can lead to significant phase changes of the system state in which the structural units are close thermodynamically, but can differ significantly in symmetry. It is discussed how the effect of the state of the suitable symmetric liquid solution of a substance under a small external impact (for example, in the form of shaking) can be experimentally realized.

提出了一个物理体系的热力学结构-相态的物理概念,并应用于对外界冲击不稳定的超高稀释水溶液。这些溶液的状态与凝聚态物理系统之间的物理类比有助于理解在超高稀释水溶液中观察到的各种效应的物理性质。特别是,这种方法允许通过机械化学方法来评估化学溶液在爱泼斯坦效应中的震动作用。通过对物理系统的热力学和结构相低稳定状态的分析,以有序合金系统为例,提出了在低稳定外部冲击下系统向新相状态转变的可能机制。在这种情况下,微小的外部冲击(例如,震动)可以导致系统状态的显著相变,其中结构单元在热力学上是接近的,但在对称性上可能存在显著差异。讨论了如何用实验方法来实现一种物质的合适的对称液体溶液的状态在一个小的外部冲击(例如,以震动的形式)下的影响。
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引用次数: 0
Monitoring of disturbances in the ionospheric layer as a result of solar flares on 31 Aug 2024 using IIOS station data 利用国际空间站数据监测2024年8月31日太阳耀斑引起的电离层扰动
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-08 DOI: 10.1007/s11182-025-03438-8
S. J. Hassan, H. Allawi, A. Gehad

The increasing electron density in the ionosphere at the D layer resulting from solar flare X‑rays, is likely to affect the propagation of very low frequency in both magnitudes and variations. The present study analyzes the observed events recorded by the Iraqi Ionospheric Observation Station IISO conducted on the 31st August, 2024 at Thi Qar University. The results show a match coincident with other observatories such as HWU and DHO and a high match with the X‑ray data detected by the GOES-16 satellite. The analysis focuses on three isolated incidents resulting from solar flares of class M and C, where sudden ionospheric disturbances appearing in the amplitude spike belong to classes M1.2, C9 and M1.8. The study and observation using the IISO, are compared with the French station, were signals are received from transmitters HWU, DHO and TTB, as well as GOES satellite data and appear to match these stations. It is found that the TBB signal shows no events well, despite its proximity to the receiver. In general, the obtained results indicate to a noise in the signal coming from several reasons including electromagnetic interference, weather, atmospheric conditions, problems with equipment, transmitter malfunctions at the TBB station, incompatibility, the need to reset transmitters, or solar disturbances such as solar storms and different reception angles, as well as physical obstacles and repeated reflections, which induce noise.

由太阳耀斑X射线引起的D层电离层中电子密度的增加,可能在量级和变化上影响极低频的传播。本文分析了伊拉克电离层观测站IISO于2024年8月31日在Thi Qar大学观测到的事件。结果表明,与其他天文台(如HWU和DHO)的匹配一致,与GOES-16卫星探测到的X射线数据高度匹配。分析的重点是由M级和C级太阳耀斑引起的三个孤立事件,其中在振幅峰值中出现的突然电离层扰动属于M1.2, C9和M1.8级。使用IISO进行的研究和观测与法国站进行了比较,法国站从发射机HWU、DHO和TTB接收信号,以及GOES卫星数据,似乎与这些站相匹配。发现TBB信号显示没有事件很好,尽管它接近接收器。总的来说,得到的结果表明,信号中的噪声是由几种原因引起的,包括电磁干扰,天气,大气条件,设备问题,TBB站发射机故障,不兼容,需要重置发射机,或太阳干扰,如太阳风暴和不同的接收角度,以及物理障碍和重复反射,这些都会引起噪声。
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引用次数: 0
Photoluminescence studies of Ce3+ doped phosphors: down/up-conversion luminescence Ce3+掺杂荧光粉的光致发光研究:下/上转换发光
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-08 DOI: 10.1007/s11182-025-03439-7
P. N. K. Chaitanya, D. Dinkar, P. Indira, A. S. Sai Prasad, M. Sree Ramana, Vikas Dubey, Shireen Aman, Ovica Manners, K. V. R. Murthy

The paper reports on the synthesis and characterisation of Ce3+ activated Mg3WO6 phosphor, with variable (0.5 to 2.5 mol%) concentration of doping Ce3+. The sample is synthesised via the combustion method. The crystal structure is determined by the X‑ray diffraction analysis, which shows the monoclinic structure with a P 1 2/c1 space group. The phosphor surface morphology is analysed by scanning electron microscopy, which shows the non-uniform particle distribution. The EDX analysis confirms the proper formation of phosphor. Photoluminescence study shows that prepared phosphor exhibits both the down- and up-conversion phenomenon. The notable peak at 275 nm is mainly due to the effective transitions from 4f ground state of Ce3+ to the field-splitting levels of 5d state. The emission peak at 475 nm is mainly due to the transitions of 5d excited state to 2F7/2 and 2F5/2 ground states.

本文报道了Ce3+在掺杂浓度为0.5 ~ 2.5 mol%的情况下,Ce3+活化Mg3WO6荧光粉的合成和表征。样品是通过燃烧法合成的。X射线衍射分析表明,该晶体结构为单斜斜结构,具有p2 /c1空间群。扫描电镜分析了荧光粉的表面形貌,发现其颗粒分布不均匀。EDX分析证实了磷光体的正确形成。光致发光研究表明,制备的荧光粉具有上下转换现象。275 nm处的显著峰主要是由于Ce3+从4f基态有效跃迁到5d态的场分裂能级。475 nm处的发射峰主要是5d激发态向2F7/2和2F5/2基态的跃迁所致。
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引用次数: 0
Fatigue strength of peek/carbon fiber laminates with copper and nickel micropowders 铜镍微粉peek/碳纤维层合板的疲劳强度
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-03 DOI: 10.1007/s11182-025-03435-x
A. A. Kononova, M. V. Burkov, A. V. Eremin

This study investigates the impact of incorporating copper and nickel micropowders on the fatigue life of polyetheretherketone (PEEK) carbon fiber reinforced composites. Powders are sprayed on the surface of PEEK/carbon fiber prepregs thus leading to modification of interlayers. The fatigue behavior of these hybrid composites is analyzed under two stress levels (0.77 and 0.8 of tensile strength). The research demonstrates that addition of copper and nickel micropowders to interlayers of the PEEK composites significantly enhances their fatigue resistance.

研究了铜镍微粉对聚醚醚酮(PEEK)碳纤维增强复合材料疲劳寿命的影响。粉末被喷涂在PEEK/碳纤维预浸料的表面,从而导致中间层的改性。在抗拉强度为0.77和0.8两种应力水平下,分析了复合材料的疲劳性能。研究表明,在PEEK复合材料中间层中加入铜和镍微粉可显著提高其抗疲劳性能。
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引用次数: 0
Microstructure and work hardening evolution of ultrafine-grained and coarse-grained alloys Ti–Nb–Zr and Mg–Y–Nd under tension Ti-Nb-Zr和Mg-Y-Nd超细晶和粗晶合金在拉伸作用下的组织和加工硬化演变
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-03 DOI: 10.1007/s11182-025-03418-y
A. Yu. Eroshenko, E. V. Legostaeva, I. A. Glukhov, A. I. Tolmachev, P. V. Uvarkin, Yu. P. Sharkeev

The paper investigates the influence of the ultrafine-grained (UFG) structure of Ti–42Nb–7Zr and Mg–2.9Y–1.3Nd alloys on their substructure and strain behavior induced by quasi-static tension. It is shown that the ultrafine grain (UFG) structure provides changes in stress-strain curves. Structural transformations due to quasi-static tension are described for both ultrafine- and coarse-grained structures of these alloys. The alloys with the coarse-grained structure demonstrate the formation of localized deformation bands with misoriented network substructure. The UFG Ti–42Nb–7Zr alloy structure is characterized by the formation of larger equiaxial grains with a lower dislocation density that indicates to a localized alloy softening before fracture. The fracture of the UFG Mg–2.9Y–1.3Nd alloy demonstrates the cellular-network substructure.

研究了Ti-42Nb-7Zr和Mg-2.9Y-1.3Nd合金超细晶(UFG)组织对其亚结构和准静态拉伸应变行为的影响。结果表明,超细晶粒(UFG)结构会引起应力-应变曲线的变化。描述了这些合金的超细组织和粗晶组织在准静态拉伸作用下的组织转变。晶粒粗大的合金表现为局部形变带的形成,并伴有取向错误的网状亚结构。UFG Ti-42Nb-7Zr合金的组织特征是形成较大的等轴晶粒,位错密度较低,表明合金在断裂前发生了局部软化。UFG Mg-2.9Y-1.3Nd合金断口呈细胞网状亚结构。
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引用次数: 0
Investigation of gas flow influence on acoustic waves, propagating downstream and upstream through gas flow in a cylindrical duct 气体流动对声波在圆柱形管道中沿下游和上游传播的影响研究
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-03 DOI: 10.1007/s11182-025-03433-z
A. V. Yamkin, N. V. Chukhareva, M. A. Bubenchikov, M. A. Yamkin

The physical and mechanical principles governing aeroacoustic vibrations within a cylindrical channel have been established through a series of numerical experiments aimed at investigating the impact of multidirectional turbulent gas flow on the propagation of these vibrations. The developed physical and mathematical model has demonstrated its efficacy, as verification processes confirmed a strong correspondence between the results of numerical simulations, experimental findings, and existing literature data. This validation allows us to assert the reliability of the model and its potential for further research endeavors. The outcomes of the numerical experiments distinctly reveal that the amplitude of waves propagating upstream surpassed that of downstream and non-flow waves at equal distances from the acoustic source within the cylindrical channel. The results obtained were corroborated through comparison with experimental and relevant literature data. The identified influence of flow can be practically applied in cross-correlation analyses of the amplitude of aeroacoustic vibrations resulting from leaks in gas pipelines, thereby enhancing the accuracy of leak detection systems.

通过一系列旨在研究多向湍流气体流动对这些振动传播影响的数值实验,建立了控制圆柱形通道内气动声学振动的物理和机械原理。开发的物理和数学模型已经证明了其有效性,因为验证过程证实了数值模拟结果、实验结果和现有文献数据之间的强烈对应关系。这种验证使我们能够断言模型的可靠性及其进一步研究努力的潜力。数值实验结果清楚地表明,在离声源相同距离的圆柱通道内,上游传播的波幅值超过了下游和非流动波的振幅。通过与实验数据和相关文献数据的比较,得到了较好的结果。确定的流量影响可以实际应用于天然气管道泄漏引起的气声振动幅值的互相关分析,从而提高泄漏检测系统的准确性。
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引用次数: 0
Maxwell and Einstein-Maxwell equations for homogeneous null Petrov spaces 齐次零彼得罗夫空间的麦克斯韦方程和爱因斯坦-麦克斯韦方程
IF 0.4 4区 物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY Pub Date : 2025-04-01 DOI: 10.1007/s11182-025-03440-0
V. V. Obukhov

Petrov homogeneous null spaces are considered. Using vector fields of the canonical reper, the vacuum Maxwell equations and the nonholonomic components of the momentum energy tensor of the electromagnetic field are derived. Examples of integration of these equations for spaces with motion groups of the first and second type according to the Bianchi classification are given.

考虑了Petrov齐次零空间。利用正则向量场,导出了真空麦克斯韦方程组和电磁场动量能量张量的非完整分量。给出了一类和二类运动群空间根据Bianchi分类对这些方程进行积分的例子。
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引用次数: 0
期刊
Russian Physics Journal
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