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ATR–FTIR SPECTROSCOPY COMBINED WITH CHEMOMETRICS FOR RAPID CLASSIFICATION OF EXTRA VIRGIN OLIVE OILS AND EDIBLE OILS FROM DIFFERENT CULTIVARS AVAILABLE ON THE TURKISH MARKETS Atr-ftir光谱结合化学计量学快速分类特级初榨橄榄油和食用油从不同品种可在土耳其市场
F. Arslan
A combination of attenuated total reflectance–Fourier transform infrared (ATR–FTIR) spectroscopy and chemometric techniques was used to classify different trademarks of edible oils available on the Turkish markets. A total of 144 spectra of edible oil samples, including extra virgin olive oil (VOO), hazelnut oil (HNO), cottonseed oil (CSO), sunflower oil (SFO) and soybean oil (SBO), was recorded. The feasibility of ATR–FTIR with multivariate data analysis for discrimination of extra VOOs from other edible oils was also evaluated. Classification of edible oils was performed using principal components analysis (PCA), hierarchical cluster analysis (HCA), linear discriminant analysis (LDA) and soft independent modeling of class analogies (SIMCA). The spectra collected from wavelength region of 4000–650 cm-1 and 28 different wavelength ranges selected from full spectra were evaluated for optimal classification models. All multivariate analysis provided excellent discriminations between the edible oil classes with low classification error. LDA models constructed with five predictors, and a total of 100% of edible oil samples from different trademarks were correctly classified. Furthermore, no misclassification was reported for the discriminant analysis in supervised SIMCA models with an accuracy of 95%. Consequently, ATR–FTIR spectroscopy combined with multivariate data analyses provides excellent illustrations of the relative positions of the different brands of commercial edible oils according to their quality and purity.
采用衰减全反射-傅里叶变换红外光谱(ATR-FTIR)和化学计量技术相结合的方法对土耳其市场上的不同商标食用油进行了分类。对特级初榨橄榄油(VOO)、榛子油(HNO)、棉籽油(CSO)、葵花籽油(SFO)和大豆油(SBO)等144种食用油样品进行了光谱分析。采用多变量数据分析的ATR-FTIR方法对其他食用油中多余油脂进行鉴别的可行性进行了评价。采用主成分分析(PCA)、层次聚类分析(HCA)、线性判别分析(LDA)和类类比软独立建模(SIMCA)对食用油进行分类。在4000 ~ 650 cm-1波长范围内采集的光谱和从全光谱中选择的28个不同波长范围的光谱进行了评价,以获得最优的分类模型。多变量分析结果对食用油的分类具有良好的判别性,分类误差小。使用5个预测因子构建的LDA模型,对不同商标的食用油样品进行了100%的正确分类。此外,在有监督的SIMCA模型中,判别分析没有出现误分类,准确率达到95%。因此,ATR-FTIR光谱结合多变量数据分析,可以很好地说明不同品牌的商业食用油根据其质量和纯度的相对位置。
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引用次数: 4
READY MIXED CONCRETE CONSTITUENT MATERIALS; PLASTICIZING CHEMICAL ADMIXTURES AND EFFECTS ON FRESH AND HARDENED PROPERTIES 预拌混凝土组成材料;增塑化化学外加剂及其对新鲜和硬化性能的影响
Evren Ariöz, Omer Arıöz
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引用次数: 1
OPTIMIZATION OF THE SELECTIVE ADSORPTION OF CU2+ VERSUS NI2+ AND ZN2+ IN THE MULTI-ION SYSTEM WITH ACTIVATED CARBONS PREPARED BY ULTRASOUND 超声法制备活性炭在多离子体系中选择性吸附cu2 +、ni2 +和zn2 +的优化
Berrak Başar, Enes Şayan
Optimization of selective adsorption of Cu2+ from multi-ion media containing Cu2+, Zn2+ and Ni2+ on activated carbons prepared from ultrasound-assisted 10 % KOH impregnated hazelnut shells was investigated. The effects of independent variables such as particle size, ultrasound power density, impregnation rate, impregnation time, activation temperature and activation time for the production of suitable activated carbons were investigated by experiments with partial factorial design and central composite design. At the end of the adsorption experiments, activated carbons were evaluated by their adsorption capacities. In addition, the results were statistically modelled and optimized using a constrained optimization program via Matlab computer software. Optimum preparation conditions were obtained as follows particle size 1.75 mm, ultrasound power/volume 2 W/L, impregnation ratio 0.0168 g/mL, impregnation time 132 min, activation temperature 661°C and activation time 71,5 min, following with maximum adsorption capacity was found as 82,9 mg Cu2+/g Ac. On the basis of the distribution coefficient (Kd), the selectivity sequence for the multi-ion system of the prepared activated carbons is generally Cu+2 > Zn+2 > Ni+2. As a result, ultrasound-assisted prepared activated carbons can be used effectively to selectively adsorb Cu+2 from multiple ion systems.
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引用次数: 0
Longitudinal Stability Analysis of a UAV under the Uncertainty of Two Stability Derivatives 两种稳定性导数不确定条件下无人机纵向稳定性分析
U. Ozdemir, M. Kavsaoglu, Zafer Öznalbant, Unver Kaynak
The longitudinal stability analysis of an aircraft is performed by the investigation of root locations of its transfer function’s denominator (the characteristic equation). However, this transfer function is obtained by linearizing aircraft dynamic model at a certain operation point (altitude and speed). However, aircraft have varying stability derivatives, therefore dynamic behavior, for different flight phases such as take-off, cruise, and landing. Thus, the stability investigation of the characteristic equation can be said to be valid only for a certain flight condition. In reality, stability derivatives have varying values depending on flight conditions. Therefore, an analysis including all possible values of stability derivatives in the flight envelope is required to guarantee stability. In this study, two most varying stability derivatives in the transfer function were taken as uncertain parameters. Gridding these two parameters to check the stability of the UAV for all possible flight conditions can be thought as a method, but it is very time-consuming, and it cannot assure the stability theoretically. A new simple approach, guaranteeing stability under the uncertainty of two stability derivatives, is developed by using the Edge and Bialas theorems. Here, the problem of the investigation of the stability under the uncertainty of two stability derivatives is reduced to the analysis of four polynomials. Thus, the stability characteristics of an airplane for a given flight envelope can be easily determined by just looking at the eigenvalues of the matrices obtained from these four polynomials.
飞机的纵向稳定性分析是通过研究其传递函数的分母(特征方程)的根位置来进行的。然而,该传递函数是通过在某一操作点(高度和速度)对飞机动力学模型进行线性化得到的。然而,飞机有不同的稳定性导数,因此动态行为,不同的飞行阶段,如起飞,巡航和着陆。因此,特征方程的稳定性研究可以说只对某一飞行条件有效。在现实中,稳定性导数的值随飞行条件的不同而变化。因此,为了保证稳定性,需要对飞行包线中所有可能的稳定性导数值进行分析。本文将传递函数中两个变化最大的稳定性导数作为不确定参数。网格化这两个参数来检验无人机在所有可能的飞行条件下的稳定性可以被认为是一种方法,但它非常耗时,并且不能保证理论上的稳定性。利用Edge定理和Bialas定理,提出了一种新的简单方法,在两个稳定性导数的不确定性下保证稳定性。本文将两个稳定性导数不确定下的稳定性研究问题简化为四个多项式的分析问题。因此,对于给定的飞行包线,飞机的稳定性特性可以很容易地通过观察从这四个多项式中得到的矩阵的特征值来确定。
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引用次数: 0
VOLTAMMETRIC DETERMINATION OF ESTRADIOL IN MILK AND PHARMACEUTICALS BASED ON FUMED-SILICA MODIFIED CARBON PASTE ELECTRODE 气相二氧化硅修饰碳糊电极伏安法测定牛奶和药品中的雌二醇
A. Özcan, Duygu Topçuoğulları, A. Özcan
In this study, modification of carbon paste electrode (CPE) with a nano-structured substance, fumed silica (FS), was investigated to develop a voltammetric method for the determination of an endocrine disrupting chemical, estradiol (EST). FS prominently increased the voltammetric response of CPE towards EST. The parameters that affect the volmametric performance of modified CPE were examined to find the optimal conditions. Modified electrode showed a linear response towards EST between the concentration values of 0.1 mM and 15.0 mM EST. Limit of detection value for the method developed was calculated as 0.023 mM. Production reproducibility of the modified electrode was obtained as 3.6 %. The voltammetric behavior of EST was also examined in the presence of different possible substances to evaluate their interference effects. The modified electrode successfully discriminated the oxidation potential of EST in the presence of different substances. The determination of EST was tested in milk and pharmaceutical samples to evaluate the analytical performance of the method. The recovery analysis of EST in milk samples showed that the modified electrode can be used safely in these samples. The modified electrode also achieved the determination of EST in pharmaceutical samples.
在这项研究中,研究了纳米结构物质气相二氧化硅(FS)修饰碳糊电极(CPE),以建立一种测定内分泌干扰化学物质雌二醇(EST)的伏安法。FS显著提高了CPE对EST的伏安响应,考察了影响改性CPE伏安性能的参数,找出了最佳条件。在0.1 mM ~ 15.0 mM EST浓度范围内,修饰电极对EST呈线性响应,所建立方法的检出限为0.023 mM,生产重现性为3.6%。在不同可能的物质存在下,测试了EST的伏安行为,以评估它们的干扰效应。该修饰电极成功地区分了EST在不同物质存在下的氧化电位。在牛奶和药品样品中进行了EST的测定,以评价该方法的分析性能。对牛奶样品中EST的回收率分析表明,该修饰电极可安全用于牛奶样品中。该修饰电极也实现了药物样品中EST的测定。
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引用次数: 1
VISION BASED CONTROL OF GANTRY CRANE SYSTEM 基于视觉的龙门起重机系统控制
A. Okubanjo, O. Oyetola, O. Adekomaya
Heavy materials handling requires a sophisticated tool for efficient and optimum operations. In recent times, gantry cranes are considered as a dependable choice in terms of handling capacity, effectiveness, timeliness and safety. However, positioning of a trolley to the desired set point as fast as possible within minimum time without overshoot and payload induced oscillation have remained obstacles in crane dynamic control. Several control algorithms have been proposed, tested and implemented based on classical control. Recently, vision control has been introduced in the field of mechatronics as a bridging gap with little or no impact. In this paper, a vision based software control model is proposed such that webcam serves as a capturing sensor and the National Instrument LabVIEW is used as a programming tool for both image processing and crane control. Subsequently, the results of the proposed algorithm are experimentally validated by step increase in the trolley position. According to the results analysis, it is evident that the webcam performance is at an optimum level when compared with the installed sensor in positioning the trolley and minimizing the payload oscillation.
重型材料处理需要一个复杂的工具,以实现高效和最佳的操作。近年来,龙门吊在处理能力、有效性、及时性和安全性方面被认为是一种可靠的选择。然而,如何在最短的时间内使小车尽可能快地定位到所需的设定点,而不出现超调和载荷引起的振荡,一直是起重机动态控制中的难题。在经典控制的基础上,提出、测试和实现了几种控制算法。近年来,视觉控制已被引入到机电一体化领域,作为一个很小或没有影响的桥梁。本文提出了一种基于视觉的软件控制模型,其中网络摄像头作为捕获传感器,使用国家仪器LabVIEW作为编程工具进行图像处理和起重机控制。随后,通过小车位置阶跃递增的实验验证了算法的正确性。结果分析表明,与安装的传感器相比,网络摄像头在小车定位和载荷振荡最小化方面的性能处于最佳水平。
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引用次数: 4
THERMAL STRESS ANALYSIS OF AXIALLY LAYERED FUNCTIONALLY GRADED BEAMS USING FINITE ELEMENT AND TAGUCHI METHODS 用有限元和田口法分析轴向分层功能梯度梁的热应力
Savaş Evran
The aim of this paper is to investigate the thermal stress analysis of axially layered functionally graded beams under clamped-clamped (C-C) boundary conditions using finite element software which named ANSYS V13 parametric design language (APDL). The beams were made as three layers using functionally graded materials with Zirconia (ceramic) and Aluminum (metal) systems. The order of the layers of the beams was designed using L9 orthogonal array depending on Taguchi Method and thus nine different beam configurations were used. Analysis of signal-to-noise (S/N) ratio was performed to determine the effects of optimum levels of layers on the thermal stress characteristic. Analysis of Variance (ANOVA) was evaluated to carry out the meaningful layers and the percentage contributions of the layers on the thermal stress response. According to the results, the most effective layers on responses were found to be Layer 1 with 75.70 % contribution, Layer 2 with 21.05 % contribution, and Layer 3 with 3.23 % contribution respectively. In addition, the increase of Young's modulus and Thermal expansion values of the layers lead to the thermal stress results of axially layered functionally graded beams. This paper can be determined as a reference for thermal stress analysis of the axially layered beams produced functionally graded materials consists of ceramic and metal contents under clamped-clamped boundary conditions.
采用有限元软件ANSYS V13参数化设计语言(APDL)对轴向分层功能梯度梁在夹紧-夹紧(C-C)边界条件下进行热应力分析。梁采用氧化锆(陶瓷)和铝(金属)系统的功能梯度材料制成三层。根据田口法,采用L9正交阵列设计光束层序,共设计了9种不同的光束结构。通过信噪比(S/N)分析确定最佳层数对热应力特性的影响。方差分析(ANOVA)进行评估,以进行有意义的层和各层对热应力响应的贡献百分比。结果表明,对响应最有效的层是层1,贡献75.70%,层2贡献21.05%,层3贡献3.23%。此外,层的杨氏模量和热膨胀值的增加导致了轴向分层功能梯度梁的热应力结果。本文可作为夹固边界条件下由陶瓷和金属成分组成的功能梯度材料制作的轴向层状梁热应力分析的参考。
{"title":"THERMAL STRESS ANALYSIS OF AXIALLY LAYERED FUNCTIONALLY GRADED BEAMS USING FINITE ELEMENT AND TAGUCHI METHODS","authors":"Savaş Evran","doi":"10.18038/AUBTDA.448786","DOIUrl":"https://doi.org/10.18038/AUBTDA.448786","url":null,"abstract":"The aim of this paper is to investigate the thermal stress analysis of axially layered functionally graded beams under clamped-clamped (C-C) boundary conditions using finite element software which named ANSYS V13 parametric design language (APDL). The beams were made as three layers using functionally graded materials with Zirconia (ceramic) and Aluminum (metal) systems. The order of the layers of the beams was designed using L9 orthogonal array depending on Taguchi Method and thus nine different beam configurations were used. Analysis of signal-to-noise (S/N) ratio was performed to determine the effects of optimum levels of layers on the thermal stress characteristic. Analysis of Variance (ANOVA) was evaluated to carry out the meaningful layers and the percentage contributions of the layers on the thermal stress response. According to the results, the most effective layers on responses were found to be Layer 1 with 75.70 % contribution, Layer 2 with 21.05 % contribution, and Layer 3 with 3.23 % contribution respectively. In addition, the increase of Young's modulus and Thermal expansion values of the layers lead to the thermal stress results of axially layered functionally graded beams. This paper can be determined as a reference for thermal stress analysis of the axially layered beams produced functionally graded materials consists of ceramic and metal contents under clamped-clamped boundary conditions.","PeriodicalId":7757,"journal":{"name":"Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering","volume":"93 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84214294","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
SITEM for the Conformable Space-Time Fractional Coupled KD Equations 符合时空-分数阶耦合KD方程的SITEM
H. Yaslan, A. Girgin
In the present paper, new analytical solutions for the space-time fractional coupled Konopelchenko-Dubrovsky (KD) equations are obtained by using the simplified $tan(frac{phi (xi) }{2})$-expansion method (SITEM). Here, fractional derivatives are described in conformable sense. The obtained traveling wave solutions are expressed by the trigonometric, hyperbolic, exponential and rational functions. Simulation of the obtained solutions are given at the end of the paper.
本文采用简化$tan(frac{phi (xi) }{2})$ -展开法(SITEM),得到了时空分数阶耦合的Konopelchenko-Dubrovsky (KD)方程的新的解析解。这里,分数阶导数的描述是符合逻辑的。得到的行波解分别用三角函数、双曲函数、指数函数和有理函数表示。本文最后对所得解进行了仿真。
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引用次数: 1
MULTIPLE REGRESSION ANALYSIS SYSTEM IN MACHINE LEARNING AND ESTIMATING EFFECTS OF DATA TRANSFORMATION&NORMALIZATION 多元回归分析系统在机器学习和估计效果的数据转换与归一化
A. Sayli, Ceyda Akbulut, Kemal Kosuta
Machine learning area is a recent topic in data analysis and a researcher or worker of the area is called “Data Scientist” which nowadays has been a highly preferred job title in computing. In this study, we have two aims that the first is to implement a multiple regression analysis system which is developed in Ubuntu operating system on the Anaconda platform using Python3 in order to construct models of each attribute to make their estimations for future decisions taking less risk in advance of past experiences hided in cumulated data and the second aim is to find out effects of data transformation and min-max normalization in the data preparation before building models. After the system implementation, we test the system to determine the best estimation model of each attribute of the vehicles sold in the five European countries between 1970 and 1999. We have constructed six versions of the original dataset and these versions are used to construct regression models for further estimations. Finally, we compute the regression criterion value of R-Squared for each constructed-model and we compare the models according to these values. Computational results are very promising that the system can be used efficiently and the effects of the data transformation and min-max normalization are significant for some attributes.
机器学习领域是数据分析领域的一个最新话题,该领域的研究人员或工作人员被称为“数据科学家”,这是当今计算领域一个非常受欢迎的职位。在这项研究中,我们有两个目标,第一是实现多元回归分析系统开发在蟒蛇Ubuntu操作系统平台使用Python3为了构建模型的每个属性估计未来决定提前采取风险较小的累积数据中隐藏的过去的经验,第二个目的是找出影响数据转换和min-max正常化前的数据准备建筑模型。在系统实现后,我们对系统进行了测试,以确定1970年至1999年间在欧洲五国销售的汽车的各个属性的最佳估计模型。我们构建了原始数据集的六个版本,这些版本用于构建回归模型以进行进一步估计。最后,我们计算了每个模型的回归准则R-Squared的值,并根据这些值对模型进行比较。计算结果表明,该系统可以有效地使用,对某些属性进行数据转换和最小-最大归一化处理效果显著。
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引用次数: 0
AN ANALYSIS OF INDUSTRIAL CHANGE IN TURKEY. II: SECTORAL DEVELOPMENT AND VALUE ADDING 土耳其工业变革分析。二:部门发展和增值
A. Yücekaya
The success of companies in each sector is related not only with the performance of the company but also with the sectoral development. The value adding level in each sector also creates extra gains that make companies successful. In this paper, regional distribution of the largest companies in Turkey is analyzed. The annual data of the largest companies in the country based on the company performances, sectoral changes, ownership structure and value adding levels are examined below. Trend analysis for sectoral development is made and sectors are classified as rising and falling based on their performances. The data illustrates that the country replaces high value adding sectors with the low value adding ones. The value adding analysis confirms these results. It is also interesting to see that the share of the state rapidly decreases over time while the share of the private ownerships and foreign companies rise rapidly. A trend analysis is also employed for the changes in ownership structure and the results are presented. The overall results depict that the country is becoming a more industrialized; however, new policies and incentives are needed to increase the value adding in each sector.
各个行业企业的成功不仅与企业的业绩有关,而且与行业的发展有关。每个行业的增值水平也会创造额外的收益,使企业成功。本文对土耳其大型企业的区域分布进行了分析。根据公司业绩、部门变化、所有权结构和增值水平,对该国最大公司的年度数据进行了审查。对行业发展进行趋势分析,并根据行业表现将其划分为上升和下降。数据表明,我国以低附加值产业取代高附加值产业。增值分析证实了这些结果。同样有趣的是,随着时间的推移,国家的份额迅速下降,而私人所有权和外国公司的份额迅速上升。本文还对股权结构的变化进行了趋势分析,并给出了结果。总体结果表明,该国正在成为一个更加工业化的国家;然而,需要新的政策和激励措施来提高每个部门的附加值。
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引用次数: 0
期刊
Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering
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