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Anti-corrosion Methods and Materials最新文献

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Review on aviation intelligent self-healing anti-corrosion coating 航空智能自修复防腐涂料综述
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-14 DOI: 10.1108/acmm-08-2023-2888
Yajun Chen, Zehuan Sui, Juan Du

Purpose

This paper aims to focus on the research progress of intelligent self-healing anti-corrosion coatings in the aviation field in the past few years. The paper provides certain literature review supports and development direction suggestions for future research on intelligent self-healing coatings in aviation.

Design/methodology/approach

This mini-review uses a systematic literature review process to provide a comprehensive and up-to-date review of intelligent self-healing anti-corrosion coatings that have been researched and applied in the field of aviation in recent years. In total, 64 articles published in journals in this field in the last few years were analysed in this paper.

Findings

The authors conclude that the incorporation of multiple external stimulus-response mechanisms makes the coatings smarter in addition to their original self-healing corrosion protection function. In the future, further research is still needed in the research and development of new coating materials, the synergistic release of multiple self-healing mechanisms, coating preparation technology and corrosion monitoring technology.

Originality/value

To the best of the authors’ knowledge, this is one of the few systematic literature reviews on intelligent self-healing anti-corrosion coatings in aviation. The authors provide a comprehensive overview of the topical issues of such coatings and present their views and opinions by discussing the opportunities and challenges that self-healing coatings will face in future development.

目的 本文旨在关注近几年航空领域智能自修复防腐涂料的研究进展。本文采用系统的文献综述流程,对近年来航空领域研究和应用的智能自修复防腐涂料进行了全面的最新综述。本文共分析了最近几年发表在该领域期刊上的 64 篇文章。研究结果作者认为,多种外部刺激-响应机制的加入使涂层在原有的自修复防腐功能之外变得更加智能。未来,在新型涂层材料的研发、多种自修复机制的协同释放、涂层制备技术和腐蚀监测技术等方面仍需进一步研究。 原创性/价值 据作者所知,这是为数不多的关于航空领域智能自修复防腐蚀涂层的系统性文献综述。作者全面概述了此类涂层的热点问题,并通过讨论自修复涂层在未来发展中面临的机遇和挑战,提出了自己的观点和看法。
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引用次数: 0
Mechanical and corrosion properties of nano ZrC reinforced FeCrAl alloys 纳米 ZrC 增强铁铬铝合金的机械和腐蚀特性
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-13 DOI: 10.1108/acmm-09-2023-2896
Zhenyu Ma, Yupeng Zhang, Xuguang An, Jing Zhang, Qingquan Kong, Hui Wang, Weitang Yao, Qingyuan Wang

Purpose

The purpose of this study is to investigate the effect of nano ZrC particles on the mechanical and electrochemical corrosion properties of FeCrAl alloys, providing a beneficial reference basis for the development of high-performance carbide reinforced FeCrAl alloys with good mechanical and corrosion properties in the future.

Design/methodology/approach

Nano ZrC reinforced FeCrAl alloys were prepared by mechanical alloying and spark plasma sintering. Phases composition, tensile fractography, corrosion morphology and chemical composition of nano ZrC reinforced FeCrAl alloys were analyzed by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray spectroscopy, respectively. Microhardness and tensile properties of nano ZrC reinforced FeCrAl alloys were investigated by mechanical testing machine and Vickers hardness tester. Electrochemical corrosion properties of nano ZrC reinforced FeCrAl alloys were investigated by electrochemical workstation in 3.5 wt.% NaCl solution.

Findings

The results showed that addition of nano ZrC can effectively improve the mechanical and corrosion properties. However, excessive nano ZrC could decrease the mechanical properties and reduce the corrosion resistance. In all the FeCrAl alloys, FeCrAl–0.6 wt.% ZrC alloy exhibits the optimum mechanical properties with an ultimate tensile strength, elongation and hardness of 990.7 MPa, 24.1% and 335.8 HV1, respectively, and FeCrAl–0.2 wt.% ZrC alloy has a lower corrosion potential (−0.179 V) and corrosion current density (2.099 µA/cm2) and larger pitting potential (0.497 V) than other FeCrAl–ZrC alloys, showing a better corrosion resistance.

Originality/value

Adding proper nano ZrC particles can effectively improve the mechanical and corrosion properties, while the excessive nano ZrC is harmful to the mechanical and corrosion properties of FeCrAl alloys, which provides an instruction to develop high-performance FeCrAl cladding materials.

目的研究纳米ZrC颗粒对FeCrAl合金力学性能和电化学腐蚀性能的影响,为今后开发具有良好力学性能和腐蚀性能的高性能碳化物增强FeCrAl合金提供有益的参考依据。分别用 X 射线衍射、扫描电子显微镜和能量色散 X 射线光谱分析了纳米 ZrC 增强铁铬铝合金的相组成、拉伸断口形貌、腐蚀形貌和化学成分。用机械试验机和维氏硬度计研究了纳米 ZrC 增强铁铬铝合金的显微硬度和拉伸性能。结果表明,纳米 ZrC 的添加能有效改善铁铬铝合金的机械性能和腐蚀性能。然而,过量的纳米 ZrC 会降低力学性能和耐腐蚀性能。在所有铁铬铝合金中,FeCrAl-0.6 wt.% ZrC 合金的机械性能最佳,其极限抗拉强度、伸长率和硬度分别为 990.7 MPa、24.1% 和 335.8 HV1;与其他铁铬铝合金相比,FeCrAl-0.2 wt.% ZrC 合金的腐蚀电位(-0.179 V)和腐蚀电流密度(2.099 µA/cm2)更低,点蚀电位(0.497 V),显示出较好的耐腐蚀性能。原创性/价值添加适当的纳米ZrC颗粒可有效改善FeCrAl合金的力学性能和腐蚀性能,而过量的纳米ZrC对FeCrAl合金的力学性能和腐蚀性能有害,这为开发高性能的FeCrAl覆层材料提供了指导。
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引用次数: 0
Corrosion and protection of friction stir welding of magnesium alloy 镁合金搅拌摩擦焊的腐蚀与防护
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-12 DOI: 10.1108/acmm-07-2023-2853
Ziru Zhou, Songlin Zheng, Jiahuan Chen, Ting Zhang, Zhen He, Yuxin Wang

Purpose

The high specific strength makes magnesium alloys have a wide range of applications in aerospace, military, automotive, marine and construction industries. However, its poor corrosion resistance and weldability have limited its development and application. Friction stir welding (FSW) can effectively avoid the defects of fusion welding. However, the microstructure, mechanical properties and corrosion behavior of FSW joints in magnesium alloys vary among different regions. The purpose of this paper is to review the corrosion of magnesium alloy FSW joints, and to summarize the protection technology of welded joints.

Design/methodology/approach

The corrosion of magnesium alloy FSW joints includes electrochemical corrosion and stress corrosion. This paper summarizes corrosion protection techniques for magnesium alloys FSW joints, focusing on composition, microstructure changes and surface treatment methods.

Findings

Currently, this research is mainly focused on enhancing the corrosion resistance of magnesium alloy FSW joints by changing compositions, structural modifications and surface coating technologies. Refinement of the grains can be achieved by adjusting welding process parameters, which in turn minimizes the effects of the second phase on the alloy’s corrosion resistance.

Originality/value

This paper presents a comprehensive review on the corrosion and protection of magnesium alloys FSW joints, covering the latest research advancements and practical applications. It aims to equip researchers with a better insight into the field and inspire new studies on this topic.

目的 镁合金的高比强度使其在航空航天、军事、汽车、海洋和建筑行业有着广泛的应用。然而,镁合金较差的耐腐蚀性和可焊性限制了其发展和应用。搅拌摩擦焊(FSW)可以有效避免熔化焊的缺陷。然而,不同地区镁合金 FSW 接头的微观结构、机械性能和腐蚀行为各不相同。本文旨在回顾镁合金 FSW 接头的腐蚀情况,并总结焊接接头的保护技术。设计/方法/途径镁合金 FSW 接头的腐蚀包括电化学腐蚀和应力腐蚀。本文总结了镁合金 FSW 接头的腐蚀防护技术,重点关注成分、微观结构变化和表面处理方法。研究结果目前,这项研究主要集中在通过改变成分、结构改性和表面涂层技术来增强镁合金 FSW 接头的耐腐蚀性。通过调整焊接工艺参数可实现晶粒细化,进而将第二相对合金耐腐蚀性的影响降至最低。 原创性/价值 本文全面综述了镁合金 FSW 接头的腐蚀和保护问题,涵盖了最新的研究进展和实际应用。其目的是让研究人员更好地了解该领域,并激发对该主题的新研究。
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引用次数: 0
New understanding on the critical factors determining stability of passive film on Fe-Cr alloy based on aberration-corrected TEM study 基于像差校正 TEM 研究的铁铬合金被动膜稳定性关键因素新认识
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-11 DOI: 10.1108/acmm-09-2023-2891
B. Zhang, X.X. Wei, X.L. Ma

Purpose

In recent years, using aberration-corrected transmission electron microscopy, the authors have achieved precisely detecting the structural evolution of passive film as well as its interface zone at atomic scale. The purpose of this paper aims to make a brief review to show the authors’ new understanding and perspective on the issue of critical factors determining stability of passive film of Fe-Cr alloy.

Design/methodology/approach

The introduction of single crystal enabled the authors to obtain a distinct metal/passive film interface and better characterize the structure of the interface region. The authors use aberration-corrected TEM to conduct cross-sectional observation and directly capture the details across the entire film at a high spatial and energy resolution.

Findings

Apart from the passive film itself, the interface zone, including metal/film (Me/F) interface and the adjacent metal side, is also the site which is attacked. Accordingly, the nature of the interface zone, such as microstructure, composition and atomic configuration, is one of the critical factors determining the stability of passive film.

Originality/value

Deciphering the critical factors determining the stability of passive film is of great significance and has been a fundamental issue in corrosion science. Great attention has been paid to the nature of the passive film itself. In contrast, the possible role of the interface between the passive film and the metal is rarely taken into account. Based on the advanced analytical tool with high spatial resolution, the authors have specified the significant role of interface structures on the macro-scale stability of passive film.

目的 近年来,作者利用像差校正透射电子显微镜,在原子尺度上实现了对被动膜结构演变及其界面区的精确检测。本文旨在对决定铁铬合金被动膜稳定性的关键因素这一问题进行简要评述,以展示作者对这一问题的新理解和新观点。设计/方法/途径单晶的引入使作者能够获得清晰的金属/被动膜界面,并更好地表征界面区的结构。研究结果除被动膜本身外,界面区(包括金属/薄膜 (Me/F) 界面和相邻金属侧)也是被攻击的部位。因此,界面区的微观结构、组成和原子构型等性质是决定被动膜稳定性的关键因素之一。人们对被动膜本身的性质给予了极大的关注。相比之下,被动膜与金属之间的界面可能发挥的作用却很少被考虑在内。基于先进的高空间分辨率分析工具,作者明确了界面结构对被动膜宏观稳定性的重要作用。
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引用次数: 0
Research on the corrosion resistance and the passive film growth of Ni-based superalloy surface treated by ultrasonic impact 超声冲击处理镍基高温合金表面的耐蚀性及钝化膜生长研究
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-06 DOI: 10.1108/acmm-09-2023-2899
Hairui Jiang, Jianjun Guan, Yan Zhao, Yanhong Yang, Jinglong Qu

Purpose

The purpose of this study is to investigate the corrosion resistance of superalloys subjected to ultrasonic impact treatment (UIT). The passive film growth on the superalloys’ surface is analyzed to illustrate the corrosion mechanism.

Design/methodology/approach

Electrochemical tests were used to investigated the corrosion resistance of GH4738 superalloys with different UIT densities. The microstructure was compared before and after the corrosion tests. The passive film characterization was described by electrochemical impedance spectroscopy (EIS) and X-ray photoelectron spectroscopy (XPS) tests.

Findings

The compressive residual stress and corrosion resistance of the specimens significantly increased after UIT. The order of corrosion resistance is related to the UIT densities, i.e. 1.96 s/mm2 > 1.71 s/mm2 > 0.98 s/mm2 > as-cast. The predominant constituents of the passive films are TiO2, Cr2O3, MoO3 and NiO. The passive film on the specimen with 1.96 s/mm2 UIT density has the highest volume fraction of Cr2O3 and MoO3, which is the main reason for its superior corrosion resistance.

Originality/value

This study provides quantitative corrosion data for GH4738 superalloys treated by ultrasonic impact. The corrosion mechanism is explained by the passive film’s characterization.

目的研究高温合金经超声冲击处理后的耐腐蚀性能。分析了高温合金表面钝化膜的生长情况,阐述了钝化膜的腐蚀机理。设计/方法/方法采用电化学试验研究了不同密度的GH4738高温合金的耐蚀性。对比了腐蚀试验前后的微观组织。通过电化学阻抗谱(EIS)和x射线光电子能谱(XPS)测试描述了钝化膜的表征。结果:经高温压缩处理后,试样的残余压应力和抗腐蚀性能明显提高。合金的耐蚀等级与合金密度有关,铸态为1.96 s/mm2 > 1.71 s/mm2 > 0.98 s/mm2 >钝化膜的主要成分是TiO2、Cr2O3、MoO3和NiO。当UIT密度为1.96 s/mm2时,钝化膜中Cr2O3和MoO3的体积分数最高,这是钝化膜具有优异耐蚀性的主要原因。本研究为超声波冲击处理的GH4738高温合金提供了定量的腐蚀数据。钝化膜的特性解释了钝化膜的腐蚀机理。
{"title":"Research on the corrosion resistance and the passive film growth of Ni-based superalloy surface treated by ultrasonic impact","authors":"Hairui Jiang, Jianjun Guan, Yan Zhao, Yanhong Yang, Jinglong Qu","doi":"10.1108/acmm-09-2023-2899","DOIUrl":"https://doi.org/10.1108/acmm-09-2023-2899","url":null,"abstract":"<h3>Purpose</h3>\u0000<p>The purpose of this study is to investigate the corrosion resistance of superalloys subjected to ultrasonic impact treatment (UIT). The passive film growth on the superalloys’ surface is analyzed to illustrate the corrosion mechanism.</p><!--/ Abstract__block -->\u0000<h3>Design/methodology/approach</h3>\u0000<p>Electrochemical tests were used to investigated the corrosion resistance of GH4738 superalloys with different UIT densities. The microstructure was compared before and after the corrosion tests. The passive film characterization was described by electrochemical impedance spectroscopy (EIS) and X-ray photoelectron spectroscopy (XPS) tests.</p><!--/ Abstract__block -->\u0000<h3>Findings</h3>\u0000<p>The compressive residual stress and corrosion resistance of the specimens significantly increased after UIT. The order of corrosion resistance is related to the UIT densities, i.e. 1.96 s/mm<sup>2</sup> &gt; 1.71 s/mm<sup>2</sup> &gt; 0.98 s/mm<sup>2</sup> &gt; as-cast. The predominant constituents of the passive films are TiO<sub>2</sub>, Cr<sub>2</sub>O<sub>3</sub>, MoO<sub>3</sub> and NiO. The passive film on the specimen with 1.96 s/mm<sup>2</sup> UIT density has the highest volume fraction of Cr<sub>2</sub>O<sub>3</sub> and MoO<sub>3</sub>, which is the main reason for its superior corrosion resistance.</p><!--/ Abstract__block -->\u0000<h3>Originality/value</h3>\u0000<p>This study provides quantitative corrosion data for GH4738 superalloys treated by ultrasonic impact. The corrosion mechanism is explained by the passive film’s characterization.</p><!--/ Abstract__block -->","PeriodicalId":8217,"journal":{"name":"Anti-corrosion Methods and Materials","volume":"1 1","pages":""},"PeriodicalIF":1.2,"publicationDate":"2023-12-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138539871","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Study on the scale-forming mechanism of magnesium phosphate by polyepoxysuccinic acid based on solution conductivity method 基于溶液电导率法的聚氧琥珀酸磷酸镁结垢机理研究
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-05 DOI: 10.1108/acmm-07-2023-2851
Huihong Feng, Jianxiang Zhao, Jiarui Hou, Huixia Feng

Purpose

This study aims to investigate the influence of polyepoxysuccinic acid sodium (PESA), a green antiscalant, on the nucleation, crystallization and precipitation of magnesium phosphate.

Design/methodology/approach

The conductivity method was used to investigate the maximum relative supersaturation of magnesium phosphate across various PESA dosages. Subsequently, a magnesium phosphate scale was prepared using the static scale inhibition method (GB/T16632-1996) and then analyzed via scanning electron microscopy.

Findings

The findings showed that PESA extends the induction period of magnesium phosphate crystallization, reduces crystal growth rate and elevates the solution’s relative supersaturation. Notably, PESA exerts a low dosage effect on inhibition of the magnesium phosphate scale, with the optimal dosage identified at 10 mL. Scanning electron microscopy revealed that PESA dispenses a dispersing effect on the magnesium phosphate scale, generating numerous concave, convex and deeper pores on the scale particles’ surface, and thereby significantly enhancing the surface area, especially when using an antiscalant with variable dosages.

Originality/value

This study sheds new light on the impact of PESA, a green antiscalant, on the crystallization and precipitation of magnesium phosphate, thus paving the way for the development of enhanced and eco-friendly scale inhibition strategies in future applications.

目的研究绿色抗垢剂聚氧琥珀酸钠(PESA)对磷酸镁成核、结晶和沉淀的影响。设计/方法/方法:采用电导率法研究磷酸镁在不同PESA剂量下的最大相对过饱和度。随后,采用静态阻垢法(GB/T16632-1996)制备磷酸镁阻垢剂,并通过扫描电镜对其进行分析。结果表明:PESA延长了磷酸镁结晶的诱导期,降低了结晶的生长速率,提高了溶液的相对过饱和度。值得注意的是,PESA对磷酸镁水垢的抑制作用较小,最佳剂量为10 mL。扫描电镜结果显示,PESA对磷酸镁垢具有分散作用,在磷酸镁垢颗粒表面产生大量凹、凸和更深的孔隙,从而显著增加表面积,特别是在使用可变剂量的抗垢剂时。原创性/价值本研究揭示了绿色阻垢剂PESA对磷酸镁结晶和沉淀的影响,从而为未来应用中开发增强型和环保型阻垢策略铺平了道路。
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引用次数: 0
Hot corrosion behavior of hot isostatic pressing treated TiC/GTD222 composite fabricated by selective laser melting 选择性激光熔化热等静压处理TiC/GTD222复合材料的热腐蚀行为
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-05 DOI: 10.1108/acmm-08-2023-2870
Yuting Lv, Yaojie Liu, Rui Wang, Hongyao Yu, Zhongnan Bi, Guohao Liu, Guangbao Sun

Purpose

This paper aims to design a novel TiC/GTD222 nickel-based high-temperature alloy with excellent hot corrosion resistance by incorporating appropriate amounts of C, Al and Ti elements into GTD222 alloy.

Design/methodology/approach

The composite material was prepared using the selective laser melting (SLM) technology, followed by a hot isostatic pressing (HIP) treatment. Subsequently, the composite underwent a hot corrosion test in a 75% Na2SO4 + 25% NaCl mixed salt environment at 900 °C.

Findings

The HIP-SLMed TiC/GTD222 composite exhibits a relatively low weight loss rate. First, the addition of alloying elements facilitates the formation of multiple protective oxide films rich in Al, Ti and Cr. These oxide films play a crucial role in enhancing the material’s resistance to hot corrosion. Second, the HIP treatment results in a reduction of grain size in the composite and an increased number of grain boundaries, which further promote the formation of protective films.

Originality/value

The hot corrosion behavior of the TiC/GTD222 nickel-based composite material prepared through SLM and HIP processing has not been previously studied. This research provides a new approach for designing nickel-based superalloys with excellent hot corrosion resistance.

目的通过在GTD222合金中加入适量的C、Al和Ti元素,设计一种新型的具有优异耐热腐蚀性能的TiC/GTD222镍基高温合金。采用选择性激光熔化(SLM)技术制备复合材料,然后进行热等静压(HIP)处理。随后,复合材料在900℃的75% Na2SO4 + 25% NaCl混合盐环境中进行热腐蚀试验。发现HIP-SLMed TiC/GTD222复合材料具有较低的减重率。首先,合金元素的加入有利于形成富含Al, Ti和Cr的多层氧化保护膜,这些氧化膜对增强材料的耐热腐蚀能力起着至关重要的作用。其次,HIP处理导致复合材料晶粒尺寸减小,晶界数量增加,进一步促进了保护膜的形成。通过SLM和HIP加工制备的TiC/GTD222镍基复合材料的热腐蚀行为尚未得到研究。本研究为设计耐高温腐蚀性能优异的镍基高温合金提供了新的途径。
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引用次数: 0
Prediction of hot corrosion behavior of Inconel 617 via machine learning 基于机器学习的Inconel 617热腐蚀行为预测
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-12-01 DOI: 10.1108/acmm-07-2023-2854
Amir Rezaei

Purpose

This paper aims to study the feasibility of using machine learning in hot corrosion prediction of Inconel 617 alloy.

Design/methodology/approach

By examination of the experimental studies on hot corrosion of Inconel 617, a data set was built for machine learning models. Apart from the alloy composition, this paper included the condition of hot corrosion like time and temperature, and the composition of the saline medium as independent features, while the specific mass change is set as the target feature. In this paper, linear regression, random forest and XGBoost are used to predict the specific mass gain of Inconel 617.

Findings

XGBoost yields the coefficient of determination (R2) of 0.98, which was highest among models. Also, this model recorded the lowest value of mean absolute error (0.20). XGBoost had the best performance in predicting specific mass gain of the alloy in different times at temperature of 900°C. In sum, XGBoost shows highest accuracy in predicting specific mass gain for Inconel 617.

Originality/value

Using machine learning to predict hot corrosion in Inconel 617 marks a substantial progress in this domain and holds promise for simplifying the development and evaluation of novel materials featuring enhanced hot corrosion resilience.

目的研究机器学习在Inconel 617合金热腐蚀预测中的可行性。设计/方法/方法通过对Inconel 617热腐蚀的实验研究,建立了一个用于机器学习模型的数据集。除合金成分外,本文还将热腐蚀条件(如时间、温度)和含盐介质成分作为独立特征,而将比质量变化作为目标特征。本文采用线性回归、随机森林和XGBoost来预测Inconel 617的比质量增益。发现sxgboost的决定系数(R2)为0.98,是所有模型中最高的。该模型的平均绝对误差最小(0.20)。在900℃温度下,XGBoost对合金在不同时间的比质量增益的预测效果最好。总之,XGBoost在预测Inconel 617的比质量增益方面显示出最高的准确性。独创性/价值使用机器学习来预测Inconel 617的热腐蚀标志着该领域的重大进展,并有望简化具有增强热腐蚀弹性的新材料的开发和评估。
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引用次数: 0
Development of a Cr-Ni-Mo alloyed stress corrosion-resistant anchor bolt steel Cr-Ni-Mo合金抗应力腐蚀地脚螺栓钢的研制
IF 1.2 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-24 DOI: 10.1108/acmm-08-2023-2873
Hailong Du, Zengyao Chen, Xiyan Wang, Yongliang Li, Renshu Yang, Zhiyong Liu, Aibing Jin, Xiaogang Li

Purpose

The purpose of this paper is to develop new types of anchor bolt materials by adding corrosion-resistant elements for alloying and microstructure regulation.

Design/methodology/approach

Three new anchor bolt materials were designed around the 1Ni system. The stress corrosion cracking resistance of the new materials was characterized by microstructure observation, electrochemical testing and slow strain rate tensile testing.

Findings

The strength of the new anchor bolt materials has been improved, and the stress corrosion sensitivity has been reduced. The addition of Nb makes the material exhibit excellent stress corrosion resistance under –1,200 mV conditions, but the expected results were not achieved when Nb and Sb were coupled.

Originality/value

The new anchor bolt materials designed around 1Ni have excellent stress corrosion resistance, which is the development direction of future materials. Nb allows the material to retain its ability to extend in hydrogen-evolution environments.

目的通过添加抗腐蚀元素进行合金化和组织调控,开发新型锚杆材料。设计/方法/方法围绕1Ni系统设计了三种新的地脚螺栓材料。通过显微组织观察、电化学测试和慢应变速率拉伸测试对新材料的抗应力腐蚀开裂性能进行了表征。结果新型锚杆材料的强度得到提高,应力腐蚀敏感性降低。Nb的加入使材料在- 1200 mV条件下表现出优异的抗应力腐蚀性能,但当Nb和Sb耦合时却没有达到预期的效果。围绕1Ni设计的新型地脚螺栓材料具有优异的抗应力腐蚀性能,是未来材料的发展方向。Nb允许材料在析氢环境中保持其扩展的能力。
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引用次数: 0
Effect of post-treated methods on corrosion resistance of MF-DC magnetron sputtering Al coating on TC4 后处理方法对MF-DC磁控溅射铝涂层耐蚀性的影响
4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-10 DOI: 10.1108/acmm-07-2023-2857
Wensheng Li, Yiding Zhang, Yanwei Xu, Guangming Jiao, Dunwen Zuo, Wenting Lu, Quanshi Cheng, Jiaqi Yu, Yajun Chen
Purpose This study aims to investigate the effect of post-treatment on anti-corrosion performance of Al coating on the surface of Ti-6Al-4V (TC4) fastener. Design/methodology/approach The Al coatings with different layer structures were prepared on TC4 by middle-frequency and direct-current combined magnetron sputtering. The cross-sectional morphology and surface roughness of coatings were characterized by scanning electron microscope and atomic force microscope. The corrosion resistance was evaluated by electrochemical method. The monolayer coating was post-treated by Alodine chemical conversion, Ar + bombardment and a combination of two methods above. Findings The results show that the interfaces in bilayer and trilayer coatings reduce the defects. Ar + bombardment reduces the corrosion current density, and Alodine chemical conversion leads to a higher pitting corrosion potential. The combined post-treatment has the highest polarization resistance. Originality/value The corrosion resistance of the Al coating is enhanced as the layer quantity increases. The combination of two post-treatments, Ar + bombardment and Alodine chemical conversion, could achieve an overall improvement in corrosion resistance of Al coating.
目的研究后处理对Ti-6Al-4V (TC4)紧固件表面Al涂层防腐性能的影响。采用中频和直流复合磁控溅射技术在TC4上制备了不同层状结构的Al涂层。采用扫描电镜和原子力显微镜对涂层的横截面形貌和表面粗糙度进行了表征。用电化学方法对其耐蚀性进行了评价。采用Alodine化学转化、Ar +轰击及以上两种方法相结合的后处理方法对单层涂层进行后处理。结果表明,双层和三层涂层中的界面减少了缺陷。Ar +轰击降低了腐蚀电流密度,Alodine化学转化导致更高的点蚀电位。复合后处理具有最高的极化电阻。随着层数的增加,铝涂层的耐蚀性增强。结合Ar +轰击和Alodine化学转化两种后处理,可以全面提高Al涂层的耐蚀性。
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Anti-corrosion Methods and Materials
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