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Brazilian Journal of Thermal Analysis最新文献

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Análise Térmica no Brasil – O legado do Prof. Dr. Ivo Giolito
Pub Date : 2019-12-15 DOI: 10.18362/bjta.v8i2.78
M. Ionashiro
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引用次数: 0
Estudo do comportamento térmico das nanopartículas de Fe3O4@Quitosana e Fe3O4-EDTA
Pub Date : 2019-12-15 DOI: 10.18362/bjta.v8i2.79
I. R. D. Silva, Maria Laura Della Costa, Barbara de Oliveira Tessarolli, Rafael Turra Alarcon, Caroline Gaglieri, Gilbert Bannach, A. Magdalena
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引用次数: 0
Thermoanalytical study of a new norfloxacin solvate 新型诺氟沙星溶剂化物的热分析研究
Pub Date : 2019-12-15 DOI: 10.18362/bjta.v8i2.82
P. O. Ferreira, Carolina Torquetti, A. Almeida, É. D. Santos, F. Caires
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引用次数: 1
Study of thermal properties and flame propagation on epoxy nanocomposites reinforced with carbon nanotubes 碳纳米管增强环氧纳米复合材料的热性能及火焰传播研究
Pub Date : 2019-12-15 DOI: 10.18362/bjta.v8i2.80
Pedro Quirinus de Ruijter, G. B. Dutra, Pedro Romano Durigan Neto, Robin Bahr Junor, Pedro F. Zanetti
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引用次数: 0
Solid-state compounds of ciprofloxacin: Thermal characterization and antimicrobial activity against S. aureus, E. coli, P. aeruginosa, L. monocytogenes and C. albicans 环丙沙星固态化合物:对金黄色葡萄球菌、大肠杆菌、铜绿假单胞菌、单核细胞增生乳杆菌和白色念珠菌的热表征和抗菌活性
Pub Date : 2019-10-15 DOI: 10.18362/bjta.v8i1.1
A. Nascimento, Ana Carina Sobral Carvalho, B. Ekawa, Gustavo Brunelli Vallim, L. C. Nascimento, R. Mendes, M. Ionashiro, F. Caires
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引用次数: 0
STUDIES ON THE THERMAL BEHAVIOR OF POLYNUCLEAR PALLADIUM(II) COMPOUNDS CONTAINING PYRAZOLATO LIGANDS 含吡唑啉配体的多核钯化合物的热行为研究
Pub Date : 2019-10-15 DOI: 10.18362/bjta.v8i1.4
C. Silva, A. Mauro, R. Frem, A. C. Moro, P. B. D. Silva, A. Stevanato, E. D. Almeida, A. V. Netto
1UFGD Univ Federal da Grande Dourados, Faculdade de Ciências Exatas e Tecnologia Departamento de Química, , P.O. Box 364, 79.804-970, Dourados – MS – Brazil. 2UNESP Univ Estadual Paulista, Instituto de Química de Araraquara Departamento de Química Geral e Inorgânica, P.O. Box 355, 14801-970, Araraquara – SP – Brazil. 3UNESP Univ Estadual Paulista, Faculdade de Ciências Farmacêuticas, 14800-903, Araraquara – SP – Brazil. 4UTFPR Univ Tecnológica Federal do Paraná Departamento de Química, P.O. Box 135, 86036-370, Londrina – PR – Brazil. 5 UNIFAL -Univ Federal de Alfenas Instituto de Química, 37130-000, Alfenas – MG – Brazil.
1 ufgd联邦大学的金黄色,准确、科学技术学院化学系,79804—-970,邮政信箱364,金女士——巴西圣保罗州立2流大学,学院城市部门的普通化学和无机化学,355信箱,14801 - -970年城市—SP—巴西圣保罗州立,3流大学药物科学学院,14800年到-903年,城市—SP—巴西。4 utfpr巴拉那州联邦科技大学化学系,邮政信箱135,86036 -370,Londrina - PR - Brazil. 5 UNIFAL -Univ Federal de Alfenas institute of chemical, 37130-000, Alfenas - MG - Brazil。
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引用次数: 0
Non-isothermal kinetic study of andiroba and babassu oils 苦楝和巴巴苏油的非等温动力学研究
Pub Date : 2017-12-15 DOI: 10.18362/BJTA.V6.I4.22
Aniele Moura, C. Gaglieri, R. Alarcon, P. O. Ferreira, A. G. Magdalena, G. Bannach
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引用次数: 5
Thermal Analysis of Amphiphilic Quaternary Ammonium Chitosan Derivatives 两亲性季铵壳聚糖衍生物的热分析
Pub Date : 2017-12-15 DOI: 10.18362/BJTA.V6.I4.21
R. Pedro, Carla C Schmitt, É. Cavalheiro, M. Neumann
The thermal behaviour of amphiphilic systems involving (5-pentyl)trimethylammonium and dodecyl aldehyde-modified chitosans was studied. These amphiphilic chitosan derivatives were synthesized and characterized by 1HNMR and ATR-FTIR spectroscopies. Thermogravimetry (TGA) and differential scanning calorimetry (DSC) were used to determine their properties. It was found that the modification of the chitosan structure affects directly its thermal properties. The temperature at which water is released from the compounds showed that when adding the hydrophilic substituent water originally bound to an -NH2 group will bind to a less stronger >NH group requiring lower temperatures to be released. The addition of the hydrophobic C12 substituent confers a more micelle-like structure to the compound, leaving some water molecules within the core of the micelle, making its release more difficult. The decomposition peak observed around 300 °C, corresponding to the decomposition of the chitosan rings, is split in two peaks when adding the substituents, indicating the influence of the substituents on the ring decomposition reactions.
研究了(5-戊基)三甲基铵和十二烷基醛改性壳聚糖两亲体系的热行为。合成了这些两亲性壳聚糖衍生物,并用1HNMR和ATR-FTIR光谱对其进行了表征。用热重法(TGA)和差示扫描量热法(DSC)测定了它们的性质。研究发现,壳聚糖结构的改性直接影响其热性能。水从化合物中释放的温度表明,当加入亲水取代基时,原来与-NH2基团结合的水将与较弱的> nhh基团结合,需要较低的温度才能释放。疏水性C12取代基的加入使化合物具有更像胶束的结构,在胶束的核心留下一些水分子,使其更难释放。300℃左右观察到的分解峰与壳聚糖环的分解相对应,加入取代基时分解峰分裂为两个峰,表明取代基对壳聚糖环分解反应的影响。
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引用次数: 0
Estudo do efeito antioxidante da folha de acerola (Malpighia glabra) na estabilidade termo oxidativa do biodiesel de soja 针叶对大豆生物柴油热氧化稳定性的抗氧化作用研究
Pub Date : 2017-12-15 DOI: 10.18362/BJTA.V6.I4.23
Neuana Fernando Neuana, Jayne Carlos de Souza Barbosa, E. P. Santos, M. D. Silva
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引用次数: 0
Study of Isolated Starches of Pinhão Seeds Marketed in the Brazilian Southern Region 巴西南部地区销售的pinh<e:1>种子分离淀粉的研究
Pub Date : 2017-12-15 DOI: 10.18362/BJTA.V6.I4.25
Bárbara Mikulis Lemes, N. Ristow, C. D. Bet, Cristina Soltovski de Oliveira, M. Lazzarotto, E. Schnitzler
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引用次数: 0
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Brazilian Journal of Thermal Analysis
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