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Rapid detection of caffeic acid in food beverages using a non-enzymatic electrochemical sensor based on a Bi2S3/CNF nanocomposite 利用基于 Bi2S3/CNF 纳米复合材料的非酶电化学传感器快速检测食品饮料中的咖啡酸
Pub Date : 2024-03-25 DOI: 10.1039/D4FB00015C
Balaji Parasuraman, SathishKumar Chinnapayan, Hariprasath Rangaraju, Shanmugam Paramasivam, Sambasivam Sangaraju, Pazhanivel Thangavelu and Chi-Hsien Huang

Caffeic acid (CA), a naturally occurring polyphenol abundantly found in various plants, has garnered significant attention in recent years due to its diverse pharmacological properties and potential health benefits. Additionally, caffeic acid is used in a range of applications, including in the food industry, disease diagnostics, and environmental monitoring, underscoring the significance of its detection. In this investigation, Bi2S3/CNF nanocomposites were prepared by a simple ultrasonication method. The successful formation of the Bi2S3/CNF nanocomposites was validated through X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), high resolution transmission electron microscopy (HR-TEM), energy dispersive electron microscopy (EDX), elemental mapping, Brunauer–Emmett–Teller (BET) studies and X-ray photoelectron microscopy (XPS). Furthermore, the electrochemical behaviour of CA on the resulting electrode was investigated through cyclic voltammetry (CV) and differential pulse voltammetry (DPV). Based on above findings, the non-enzymatic electrochemical sensor has good performance for the electrochemical detection of CA under tailored conditions; the wide linear range of CA concentrations detectable by the modified GCE was 0.1–500 μM, and the LOD was 108 nM, with the sensitivity of the modified GCE calculated to be 2.56 μA μM−1 cm−2 and good selectivity, repeatability, reproducibility and stability. Additionally, the Bi2S3/CNF/GCE nanocomposite electrode material was used to detect CA in real samples, such as apple and grape juice, and acceptable results were achieved showing good practical applicability. Ultimately, this study demonstrated that the suggested sensor has enhanced the ability to determine CA in food industry and health care field.

咖啡酸(CA)是一种天然多酚类物质,大量存在于各种植物中,近年来因其多样的药理特性和潜在的健康益处而备受关注。此外,咖啡酸还被广泛应用于食品工业、疾病诊断和环境监测等领域,这也凸显了其检测的重要性。本研究采用简单的超声法制备了 Bi2S3/CNF 纳米复合材料。通过 X 射线衍射 (XRD)、场发射扫描电子显微镜 (FE-SEM)、高分辨率透射电子显微镜 (HR-TEM)、能量色散电子显微镜 (EDX)、元素图谱、Brunauer-Emmett-Teller (BET) 研究和 X 射线光电子显微镜 (XPS) 验证了 Bi2S3/CNF 纳米复合材料的成功制备。此外,还通过循环伏安法(CV)和微分脉冲伏安法(DPV)研究了 CA 在所得电极上的电化学行为。根据上述研究结果,该非酶电化学传感器在定制条件下具有良好的电化学检测 CA 的性能;改性 GCE 可检测的 CA 浓度的宽线性范围为 0.1-500 μM,LOD 为 108 nM,计算得出改性 GCE 的灵敏度为 2.56 μA μM-1 cm-2,并具有良好的选择性、重复性、再现性和稳定性。此外,Bi2S3/CNF/GCE 纳米复合电极材料还被用于检测苹果汁和葡萄汁等实际样品中的 CA,并取得了可接受的结果,显示出良好的实用性。这项研究最终证明,所建议的传感器提高了食品工业和医疗保健领域测定 CA 的能力。
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引用次数: 0
Modification of plant and algal proteins through the Maillard reaction and complex coacervation: mechanisms, characteristics, and applications in encapsulating oxygen-sensitive oils 通过马氏反应和复合共凝胶对植物和藻类蛋白质进行改性:机制、特征以及在封装氧敏感油类中的应用
Pub Date : 2024-03-15 DOI: 10.1039/D3FB00220A
Zijia Zhang, Bo Wang, Jie Chen and Benu Adhikari

There is an increasing demand for plant and algal proteins as alternatives to animal proteins. This demand is driven by lifestyle choices and sustainability concerns. The demand for them is particularly strong as ingredients. However, the technofunctional properties of these proteins, such as solubility, emulsifying, encapsulating, and gelling, need improvement to meet the requirements of food products. Among the approaches to modify proteins, covalent conjugation with polysaccharides through the Maillard reaction and non-covalent complexation through complex coacervation have received increased research attention. This paper provides an overview of these two approaches in terms of their mechanisms, typical process protocols, and the characteristics of modified proteins. The application of covalent conjugates and complex coacervates as emulsifiers and encapsulating shell materials for unstable and oxygen-sensitive oils is also reviewed. Recent studies that have combined these two approaches to achieve improved emulsification and encapsulation outcomes are reviewed to provide insights into the mechanism by which previously conjugated proteins undergo complex coacervation with a second polysaccharide. Ultimately, this review intends to identify the most effective technologies for creating emulsifiers and encapsulating shell materials using plant and algal proteins, particularly to stabilise and protect oxygen-sensitive oils.

作为动物蛋白的替代品,人们对植物蛋白和海藻蛋白的需求与日俱增。这种需求是由生活方式的选择和对可持续发展的关注所驱动的。作为配料的需求尤为强劲。然而,这些蛋白质的技术功能特性,如溶解性、乳化性、包裹性和胶凝性,需要改进才能满足食品的要求。在改性蛋白质的方法中,通过马氏反应与多糖共价共轭,以及通过络合共凝胶进行非共价络合已受到越来越多的研究关注。本文从这两种方法的机理、典型工艺规程和改性蛋白质的特点等方面对其进行了概述。此外,还综述了共价共轭物和复合共凝胶作为乳化剂和封装外壳材料在不稳定油类和氧敏感油类中的应用。本综述还回顾了将这两种方法结合起来以实现更好的乳化和封装效果的最新研究,以便深入了解以前共轭的蛋白质与第二种多糖发生复合共凝结的机理。最后,本综述旨在确定使用植物和藻类蛋白质制造乳化剂和封装外壳材料的最有效技术,特别是用于稳定和保护对氧气敏感的油类。
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引用次数: 0
Bovine colostrum as a promising nutraceutical: a systematic review 牛初乳作为一种前景广阔的营养保健品:系统综述
Pub Date : 2024-03-14 DOI: 10.1039/D3FB00256J
Akshay Ramani, Sathiya Taherabbas and Subhadip Manik

Nowadays, it is essential to identify the benefits of sustainable living with nutritional food for the world's expanding population. This systematic review explores the unique composition of bovine colostrum, the initial milk produced by mammals post-parturition, compared to mature milk. We delve into extensive studies to examine its potential applications in human nutrition and health. Meticulous characterisation of its constituent fractions reveals a diverse array of potentially bioactive molecules, demonstrating their influence on neonatal development and their relevance in this era. Bovine colostrum can be a suitable alternative to mature milk as it is a rich source of numerous components such as bioactive proteins, fats, oligosaccharides, minerals and vitamins. Advance technologies were also used to preserve and commercialise it. So, a comprehensive discussion of its potential benefits for human health and exploring various preservation techniques for bovine colostrum presents a thorough overview of its multifaceted applications in promoting health and well-being.

如今,为不断增长的世界人口提供营养食品对确定可持续生活的益处至关重要。牛初乳是哺乳动物产后产生的最初乳汁,与成熟乳汁相比,牛初乳的成分更为独特。我们深入开展了大量研究,探讨牛初乳在人类营养和健康方面的潜在应用。对牛初乳成分的细致分析揭示了一系列潜在的生物活性分子,证明了它们对新生儿发育的影响以及在这个时代的意义。牛初乳富含多种成分,如生物活性蛋白质、脂肪、低聚糖、矿物质和维生素,是成熟牛奶的合适替代品。先进的技术也被用于牛初乳的保存和商业化。因此,全面讨论牛初乳对人类健康的潜在益处并探索各种牛初乳保存技术,可以全面了解牛初乳在促进健康和福祉方面的多方面应用。
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引用次数: 0
From kitchen scraps to delicacies to food waste 从厨余到美食,再到食物垃圾
Pub Date : 2024-03-13 DOI: 10.1039/D4FB00012A
Dietrich Knorr and Mary Ann Augustin

Food loss and waste occur along the whole food supply chain. The perceptions of food waste and how it is used have changed over time. Prior to and during WWII, household food scraps and leftovers were reused and even upgraded into delicacies which are still valued even today. Currently about one third of food produced for human consumption is wasted and this accounts for a carbon and water footprint of 4.4 giga tons of CO2 equivalents and 250 km3 of blue water, respectively. In addition, food waste is responsible for significant wastage of land used for agriculture and 3.3 billion tons of greenhouse gas emissions. Consumer food waste is a major source of the current food waste crisis. As consumer behavior is a key driver of food waste, strategies for reduction and avoidance of waste should appeal to consumers' individual values. Ways to prevent food waste, reuse and upscale recycling and recovery are reviewed. The potential of using waste for future food preparation, food waste avoidance tools and technologies are presented. Urgent action is needed for implementation of waste reduction interventions and more efficient food redistribution systems to improve food security and sustainability.

食物损失和浪费发生在整个食物供应链中。随着时间的推移,人们对食物浪费及其利用方式的看法也发生了变化。在二战之前和二战期间,家庭食物残渣和剩饭剩菜被重新利用,甚至被升级为美味佳肴,直到今天仍受到人们的重视。目前,供人类消费的食物中约有三分之一被浪费,造成的碳足迹和水足迹分别为 4.4 千兆吨二氧化碳当量和 250 立方公里的蓝水。此外,食物浪费还造成大量农业用地的浪费和 33 亿吨温室气体的排放。消费者的食物浪费是当前食物浪费危机的主要来源。由于消费者行为是造成食物浪费的关键因素,因此减少和避免浪费的战略应符合消费者的个人价值观。本文回顾了防止食物浪费、再利用以及提高回收和循环利用水平的方法。还介绍了利用废弃物制作未来食物的潜力、避免食物浪费的工具和技术。需要采取紧急行动,实施减少浪费的干预措施和更有效的粮食再分配系统,以改善粮食安全和可持续性。
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引用次数: 0
Storage stability, nutritional profiling and consumer acceptability of a milk-sorghum-based breakfast smoothie 牛奶-高粱早餐冰沙的储存稳定性、营养分析和消费者接受度
Pub Date : 2024-03-11 DOI: 10.1039/D4FB00038B
Rekha Rani, Latha Sabikhi and Sathish Kumar M. H.

This study was conducted to estimate the storage stability of a milk-sorghum-based functional breakfast smoothie (MSBS). The product was packed in 200 mL glass bottles and stored at 4 °C and 30 °C. The milk-sorghum-based smoothie was suitable for consumption for up to 75 days and 60 days at 4 °C and 30 °C, respectively; afterwards, the product lost its aroma and flavour. This product is nutritionally rich in dietary fibre (1.68%), calcium (560.46 ppm), iron (28.12 ppm), and vitamin A (679.3 IU/L); low in fat (0.65%) with a low calorific value (89.09 kcal per 100 g) and free of any synthetic preservatives and colour. The consumer acceptance study revealed that ∼88% consumers liked this product, 33% were willing to consume it daily and 89% were ready to purchase it at a price of Rs. 20 per 200 mL bottle. It is a convenient grab-and-go option for all age groups.

本研究旨在估测以牛奶-高粱为基础的功能性早餐冰沙(MSBS)的储存稳定性。产品包装在 200 mL 玻璃瓶中,分别在 4 °C 和 30 °C 下贮存。在 4 ℃ 和 30 ℃条件下,以牛奶和高粱为基础的冰沙分别可食用 75 天和 60 天;之后,产品的香气和风味消失。该产品营养丰富,富含膳食纤维(1.68%)、钙(560.46 ppm)、铁(28.12 ppm)和维生素 A(679.3 IU/L);脂肪含量低(0.65%),热量低(每 100 克 89.09 千卡),不含任何合成防腐剂和色素。消费者接受度研究表明,88%的消费者喜欢这种产品,33%的消费者愿意每天饮用,89%的消费者愿意以每瓶 200 毫升 20 卢比的价格购买。对于所有年龄段的人来说,这是一种方便的随手可取的选择。
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引用次数: 0
Recent advances in the fabrication, characterization and application of starch-based materials for active food packaging: hydrogels and aerogels 用于活性食品包装的淀粉基材料:水凝胶和气凝胶的制造、表征和应用方面的最新进展
Pub Date : 2024-03-08 DOI: 10.1039/D4FB00030G
Di Zhao, Xinyi Zhang, Yingying Zhang, Enbo Xu, Shengkun Yan, Huaide Xu and Mei Li

With the increasing awareness of the harmful effects of plastics on the environment, the demand for biodegradable packaging materials is growing. Over the last decade, starch-based colloidal materials including hydrogels and aerogels have attracted widespread attention owing to their abundant supply, complete biodegradability and unique properties. This review aimed to provide an overview of the fabrication methods of starch-based hydrogels and aerogels, summarize the effects of internal and external factors on the structural and physicochemical properties of starch-based hydrogels and aerogels, and focus on the evaluation of their application in active food packaging. Hydrogels are sensitive to environmental changes, giving them unique advantages in smart packaging applications. In addition, aerogels have a distinctive place in the delivery and release of active substances based on large surface areas and high porosity. Starch-based hydrogels and aerogels will provide great potential in the application of food packaging.

随着人们越来越意识到塑料对环境的有害影响,对可生物降解包装材料的需求也在不断增长。在过去十年中,淀粉基胶体材料(包括水凝胶和气凝胶)因其丰富的供应、完全的生物可降解性和独特的性能而受到广泛关注。本综述旨在概述淀粉基水凝胶和气凝胶的制备方法,总结内外因素对淀粉基水凝胶和气凝胶结构和理化性质的影响,并重点评估其在活性食品包装中的应用。水凝胶对环境变化非常敏感,因此在智能包装应用中具有独特的优势。此外,气凝胶具有大表面积和高孔隙率,在输送和释放活性物质方面具有独特的优势。淀粉基水凝胶和气凝胶将为食品包装应用提供巨大潜力。
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引用次数: 0
Optimisation of lactic acid production using cost effective agro residue for food applications† 利用具有成本效益的农业残留物优化乳酸生产,用于食品应用†。
Pub Date : 2024-03-04 DOI: 10.1039/D3FB00213F
Janifer Raj Xavier, Ilaiyaraja Nallamuthu, Muthiah Pal Murugan and Om Prakash Chauhan

Lactic acid (LA) (CH3CHOHCOOH) is utilised in a variety of industrial processes, including production of polymers, emulsifiers, pharmaceutical, and cosmetic formulations. Biological synthesis of useful products by fermentation of renewable resources has advantages over chemical methods. Focus on optimised usage of cost effective regional substrates is necessary to achieve environmentally sustainable practices and efficient biomass fermentation for production of organic acid such as lactic acid. The present study was carried out to optimize lactic acid production using Limosilactobacillus fermentum DFRM8 with cost effective regional carbon substrate (sugarcane bagasse). Experimental design used for the optimization of lactic acid production was 34 full factorial design using four factors such as sugarcane bagasse (%), inoculation level (%), incubation temperature (°C) and pH. The conditions optimized with sugarcane bagasse hydrolysate at 5.0% (v/v), inoculum level at 5.0% (v/v), and incubation temperature at 30 °C with an initial pH of 6.0 produced the maximum lactic acid (22.2 g L−1 on dry weight basis) after 48 h. Simple sugars when used as carbon source in fermentation medium produced (g L−1) LA in the range of 4.5 to 13.5 while agro residues such as mango peel, grape peel and banana peel produced (g L−1) LA at 18.0, 4.5 and 2.7 on dry weight basis. Lactic acid synthesised by the isolate L. fermentum DFRM8 is suitable for food and biomedical applications as the bacterium has GRAS status.

乳酸(LA)(CH3CHOHCOOH)可用于多种工业流程,包括生产聚合物、乳化剂、药品和化妆品配方。与化学方法相比,利用可再生资源发酵进行有用产品的生物合成具有优势。要实现环境可持续发展和高效的生物质发酵生产有机酸(如乳酸),就必须注重优化使用具有成本效益的地区基质。本研究采用具有成本效益的地区性碳基质(甘蔗渣),利用 Limosilactobacillus fermentum DFRM8 对乳酸生产进行了优化。优化乳酸生产的实验设计采用 34 全因子设计,使用甘蔗渣(%)、接种水平(%)、培养温度(°C)和 pH 值等四个因素。甘蔗渣水解物含量为 5.0%(v/v),接种量为 5.0%(v/v),培养温度为 30 °C,初始 pH 值为 6.0 的优化条件在 48 小时后产生的乳酸最多(干重为 22.2 g L-1)。在发酵培养基中使用单糖作为碳源时,产生的乳酸(克/升-1)在 4.5 至 13.5 之间,而农业残留物(如芒果皮、葡萄皮和香蕉皮)产生的乳酸(克/升-1)(按干重计算)分别为 18.0、4.5 和 2.7。由分离菌 L. fermentum DFRM8 合成的乳酸适用于食品和生物医学应用,因为该细菌已获得 GRAS 认证。
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引用次数: 0
Unlocking the potential of rice bran through extrusion: a systematic review† 通过挤压发掘米糠的潜力:系统综述†。
Pub Date : 2024-03-04 DOI: 10.1039/D4FB00027G
Yadav KC, Jaquie Mitchell, Bhesh Bhandari and Sangeeta Prakash

Rice bran (RB) is a by-product of the rice milling process and is rich in nutrients and bioactive compounds making it a valuable ingredient for extruded foods. Preferred Reporting Items for Systematic reviews and Meta-Analysis (PRISMA) was applied that involved screening large databases (Google Scholar, PubMed, Web of Science, ScienceDirect and Scopus) and analysing the most relevant peer-reviewed forty-four journal articles. This review discusses the benefits of incorporating RB into various food product formulations, including meat analogues, biscuits, cookies, cakes, noodles, breads, and pasta. The review also examines how extrusion conditions, such as temperature, screw speed, and moisture content affect the physicochemical parameters of the expanded extrudates from the feed formulation incorporated with RB. In extrusion, 0–30% RB was used as feed in 52.27% of the studies, and 71.42% of the studies used screw speed below 250 rpm. Almost all studies had extrusion temperatures below 150 °C, and plant-based meat used a higher moisture content (60–70%) during extrusion. The extrusion of RB results in increased hardness and bulk density, and reduced expansion. However, depending on the feed's composition, moisture content, extrusion temperature, and screw speed, its addition to the feed mixture could cause variability of results for the water solubility index (WSI), water absorption index (WAI), thermal behaviour and viscosity. RB in foods processed through extrusion enhances their nutritional profiles, especially total phenolics, antioxidant activity, and functional properties and supports sustainable practices. Overall, the use of RB in food extrusion holds promise for the development of nutritious, functional, and sustainable food products.

米糠(RB)是碾米过程中产生的副产品,富含营养和生物活性化合物,是挤压食品的重要配料。本综述采用了系统综述和元分析首选报告项目(PRISMA),包括筛选大型数据库(Google Scholar、PubMed、Web of Science、ScienceDirect 和 Scopus)和分析最相关的 44 篇同行评审期刊文章。本综述讨论了在各种食品配方中添加 RB 的益处,包括肉类类似物、饼干、曲奇、蛋糕、面条、面包和意大利面。综述还探讨了挤压条件(如温度、螺杆转速和水分含量)如何影响掺入 RB 的饲料配方的膨化挤出物的理化参数。在挤压过程中,52.27% 的研究使用 0-30% 的 RB 作为饲料,71.42% 的研究使用低于 250 rpm 的螺杆转速。几乎所有研究的挤压温度都低于 150 °C,植物肉在挤压过程中的含水量较高(60-70%)。挤压 RB 可提高硬度和体积密度,减少膨胀。然而,根据饲料成分、含水量、挤压温度和螺杆转速的不同,在饲料混合物中添加 RB 会导致水溶性指数(WSI)、吸水指数(WAI)、热性能和粘度结果的变化。挤压加工食品中的 RB 可提高其营养成分,尤其是总酚类、抗氧化活性和功能特性,并有助于可持续发展。总之,在食品挤压中使用 RB 有望开发出营养、功能和可持续的食品。
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引用次数: 0
Transitioning of petroleum-based plastic food packaging to sustainable bio-based alternatives 将石油基塑料食品包装过渡为可持续生物基替代品
Pub Date : 2024-03-04 DOI: 10.1039/D4FB00028E
Yue Yin and Meng Wai Woo

Motivated by the urgent need to address environmental concerns associated with traditional food packaging, this review explores the shift towards sustainable, bio-based packaging solutions. It highlights the evolution of food packaging functions, emphasizing not only the basic roles but also the innovative methods developed to enhance food quality. The focus extends to well-researched bio-based plastics, particularly in promoting their mechanical properties. Additionally, the review explores the innovative use of plant-based and animal-based materials in creating sustainable packaging solutions. These materials have shown considerable promise in improving mechanical properties, prolonging shelf life, and providing antimicrobial and antioxidant benefits. A critical aspect of the review is the practical application of bio-based biodegradable materials in the food packaging industry. Despite significant theoretical advancements, there remains a gap in understanding how these materials can be effectively utilized in real-world scenarios.

由于迫切需要解决与传统食品包装相关的环境问题,本综述探讨了向可持续的生物基包装解决方案的转变。文章重点介绍了食品包装功能的演变,不仅强调了其基本作用,还介绍了为提高食品质量而开发的创新方法。重点延伸到经过深入研究的生物基塑料,尤其是在提高其机械性能方面。此外,本综述还探讨了如何创新使用植物基和动物基材料来创造可持续包装解决方案。这些材料在改善机械性能、延长保质期以及提供抗菌和抗氧化功效方面已显示出相当大的前景。审查的一个重要方面是生物基可生物降解材料在食品包装行业中的实际应用。尽管在理论上取得了重大进展,但在了解如何在实际应用中有效利用这些材料方面仍然存在差距。
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引用次数: 0
Extractability of oleuropein, hydroxytyrosol, tyrosol, verbascoside and flavonoid-derivatives from olive leaves using ohmic heating (a green process for value addition) 利用欧姆加热法从橄榄叶中提取油菜素、羟基酪醇、酪醇、马鞭草苷和黄酮类衍生物(一种绿色增值工艺)
Pub Date : 2024-02-26 DOI: 10.1039/D3FB00252G
Fereshteh Safarzadeh Markhali and José A. Teixeira

The aim of this study was to determine the influence of ohmic heating (OH) as a green processing approach on the extraction of principal polar phenols from olive leaves, with special attention on oleuropein content. The concentrations were quantified using ultra-high-performance liquid chromatography (UHPLC). Other target analytes including total flavonoid content (TFC) and total condensed tannins (TCT) were also assessed as secondary response variables. The key predictor variables were (i) extraction method: ohmic heating (OH) and conventional heating (conven), (ii) solvent ratio (40–80% aqueous ethanol), and (iii) extraction temperature: 45–75 °C. In addition, control samples were prepared through solvent extraction at room temperature using the same solvent ratios applied for OH and conven. The length of processing time (15 min) was the same for all extraction methods. Overall, the data showed that intensified extractability of major polyphenols from olive leaves is readily achievable by using ohmic heating rather than the other aforementioned methods (p < 0.05). Importantly, the recovery of oleuropein through the ohmic system, that reached up to 26.18 mg per g extract at 75 °C with 80% ethanol was significantly higher than other examined approaches (7.98–14.55 mg per g in conven groups, and 8.64–10.81 mg per g in control groups). Other major polyphenols that reached the maximum levels via the ohmic approach, were as follows: (i) luteolin 7-O-glucoside (4.12 mg per g extract), apigenin 7-O-glucoside (3.47 mg per g extract), rutin (3.78 mg per g extract), and tyrosol (0.34 mg per g extract) using 60% ethanol at 55 °C, (ii) verbascoside (1.04 mg per g extract) using 80% ethanol at 75 °C, and (iii) hydroxytyrosol (1.38 mg per g extract) using 80% ethanol at 55 °C. The findings of this study demonstratethat ohmic heating is potentially a method of preference for efficient recovery of representative phenols of olive leaves.

本研究旨在确定欧姆加热(OH)作为一种绿色加工方法对从橄榄叶中提取主要极性酚类的影响,尤其关注油菜素的含量。采用超高效液相色谱法(UHPLC)对其浓度进行了量化。其他目标分析物包括总黄酮含量(TFC)和总缩合单宁含量(TCT)也作为次要响应变量进行了评估。主要预测变量包括:(i) 提取方法:欧姆加热法(OH)和传统加热法(CH);(ii) 溶剂比例(40-80% 的乙醇水溶液);(iii) 提取温度:45-75 °C.此外,还使用与 OH 和 conven 相同的溶剂比例,在室温下通过溶剂萃取制备了对照样品。所有萃取方法的处理时间(15 分钟)相同。总之,数据表明,与上述其他方法相比,使用欧姆加热法很容易提高橄榄叶中主要多酚的提取率(p < 0.05)。重要的是,通过欧姆系统,油菜素的回收率高达 26.18 毫克/克(75 °C、80% 乙醇提取),明显高于其他研究方法(召集组为 7.98-14.55 毫克/克,对照组为 8.64-10.81 毫克/克)。通过欧姆法达到最高含量的其他主要多酚如下:(i) 叶黄素 7-O-葡萄糖苷(每克萃取物 4.12 毫克)、芹菜素 7-O-葡萄糖苷(每克萃取物 3.47 毫克)、芦丁(每克萃取物 3.78 毫克)和酪醇(每克萃取物 0.34 毫克),使用 60% 的乙醇,温度为 55 °C;(ii) 马鞭草苷(每克萃取物 1.04 毫克),使用 80% 的乙醇,温度为 75 °C;(iii) 羟基酪醇(每克萃取物 1.38 毫克),使用 80% 的乙醇,温度为 55 °C。该研究结果表明,欧姆加热法是高效回收橄榄叶中代表性酚类的首选方法。
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引用次数: 0
期刊
Sustainable Food Technology
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