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Coupling Interval Hyper-Active Drying (IHAD) with Instant Controlled Pressure Drop (D.I.C.) to define new swell-drying processes 将间歇超活性干燥(IHAD)与即时控制压降(D.I.C.)相结合,以确定新的溶胀干燥工艺
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-29 DOI: 10.1080/07373937.2023.2223278
W. Hajji, S. Bellagha, C. Téllez-Pérez, S. Mounir, Mohamed Salah Negm, T. Allaf, V. Lefrançois, C. Besombes, A. Mujumdar, K. Allaf
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引用次数: 0
Moisture transport and stress development in rice during drying, a Hybrid Mixture Theory-based model 水稻干燥过程中水分运移与胁迫发展——基于杂交理论的模型
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-24 DOI: 10.1080/07373937.2023.2220019
Fidèle Abédi, Sunil Kumar, N. Kumar, Deepak Kumar, P. Takhar
Abstract Internal fluid flow during rice drying generates a stress gradient inside the material. If the stress gradient becomes too large or certain rice layers undergo glass transition under a significant stress gradient, stress cracks can form. In this study, modeling equations based on the Hybrid Mixture Theory were solved to simulate moisture transport and the viscoelastic stress that occurs during rice drying. The model’s accuracy was evaluated using experimental moisture content data for two rice varieties: Pusa Basmati 1121 (MAEs: 0.0079–0.0162 g/g solids) and California M206 (MAEs: 0.0022–0.0061 g/g solids). Simulations were then conducted under continuous and time-varying drying conditions to determine the best drying strategy for minimizing stress crack formation. The results showed that gradually increasing the inlet air temperature by 5 °C every 5 min after an initial 28.5 min at 40 °C could reduce stress crack formation effectively while drying rice in only 38.5 min.
大米干燥过程中内部流体的流动会在物料内部产生应力梯度。如果应力梯度过大或某些米层在较大的应力梯度下发生玻璃化转变,就会形成应力裂纹。本文基于杂化理论求解了水稻干燥过程中水分运移和粘弹性应力的模型方程。利用两个水稻品种:Pusa Basmati 1121 (MAEs: 0.0079-0.0162 g/g固体)和California M206 (MAEs: 0.0022-0.0061 g/g固体)的实验水分含量数据,对模型的准确性进行了评估。然后在连续和时变干燥条件下进行了模拟,以确定最小应力裂纹形成的最佳干燥策略。结果表明,在40℃条件下,在初始28.5 min后,每5 min逐步提高5℃,可以有效减少应力裂纹的形成,而干燥时间仅为38.5 min。
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引用次数: 0
Hot-air drying behavior of lignite and quantitative characterization for its surface damage 褐煤热风干燥特性及其表面损伤的定量表征
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-24 DOI: 10.1080/07373937.2023.2223621
T. Zhang, Chenfei Lou, Daoguang Teng, Guosheng Li, Peng Li, Qinghang Yun, Guoli Zhou
Abstract Cracking and fragmentation problems that occur during lignite drying limit its utilization value. In this study, the dehydration, surface damage, and pulverization behaviors of lignite were investigated under hot-air drying conditions, and the effect of the dewatering process on shrinkage cracking was analyzed. Cracks first appear at the edges of the lignite, then gradually extend inward until they spread over the entire surface of the lignite, before beginning to shrink, and eventually stabilize. The crack rate exhibited three stages: rapid development, shrinkage, and stabilization. The crack rate and shrinkage percentage increased significantly with increase in the drying temperature. The moisture content had a greater influence on the crack rate and shrinkage percentage of the samples than the surface temperature. A uniaxial compression test revealed that lignite with different degrees of dryness exhibited different degrees of breakage. The drying process drives the lignite toward finer grain sizes and, with moisture content below 0.8 g/g, the degree of breakage increases significantly. Thus, the main factor affecting the shrinkage and cracking of lignite was the moisture content. Cracks occurred when the tensile strain caused by shrinkage was greater than the tensile strength of the lignite.
摘要褐煤干燥过程中出现的裂解和碎裂问题限制了其利用价值。本研究研究了褐煤在热风干燥条件下的脱水、表面损伤和粉碎行为,并分析了脱水过程对收缩开裂的影响。裂缝首先出现在褐煤的边缘,然后逐渐向内延伸,直到它们扩散到褐煤的整个表面,然后开始收缩,并最终稳定下来。裂纹率表现为三个阶段:快速发展、收缩和稳定。随着干燥温度的升高,裂纹率和收缩率显著增加。水分含量对试样的裂纹率和收缩率的影响大于表面温度。单轴压缩试验表明,不同干度的褐煤表现出不同程度的破碎。干燥过程使褐煤粒度变细,含水量低于0.8 g/g时,断裂程度显著增加。因此,影响褐煤收缩和开裂的主要因素是含水量。当收缩引起的拉伸应变大于褐煤的拉伸强度时,就会出现裂纹。
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引用次数: 0
Effect of ultrasonic power on moisture migration and microstructure of contact ultrasound enhanced far-infrared radiation drying on taro slices 超声波功率对接触超声增强远红外辐射干燥芋头片水分迁移及微观结构的影响
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-21 DOI: 10.1080/07373937.2023.2224429
Yu Yang, J. Zhong, Xinge Ma, Fang Li, Xiaoyan Fan, Yunhong Liu
Abstract To clarify the moisture migration and microstructure of taro in contact ultrasound enhanced far-infrared radiation drying (CUFRD), low-field nuclear magnetic resonance (NMR), scanning electron microscopy (SEM), paraffin sectioning and microscopic observation techniques were applied to explore the changes of the drying curves, water status, microstructure, porosity, microscopic images and distribution curves of cell microstructure parameters of taro under different ultrasound powers of 0, 40, and 80 W. The results showed that applying contact ultrasound (CU) during drying was beneficial to accelerating the dehydration process and improving the porosity of taro slice. With the augment of CU power, the drying times of taro reduced by 16.67% to 25.00%, and the effective water diffusion coefficient was improved by 14.72% to 31.38%. In addition, the application of CU resulted in an increase firstly and then decrease in the cross-sectional area and perimeter distribution curves of taro cells and a widening of the peak shape of the distribution curve of taro cell roundness. In conclusion, CU application could cause faster internal moisture migration, and higher CU power had more obvious effect on microstructure and cell morphological parameters of taro during CUFRD.
摘要为了阐明接触超声增强远红外辐射干燥(CUFRD)过程中芋头水分迁移和微观结构的变化,采用低场核磁共振(NMR)、扫描电镜(SEM)、石蜡切片和显微观察等技术,探讨了芋头干燥曲线、水分状态、微观结构、孔隙度、水分含量、水分含量和水分含量的变化。不同超声功率0、40、80 W下芋头细胞微观结构参数的显微图像及分布曲线。结果表明,在干燥过程中应用接触超声(CU)有利于加速芋头片的脱水过程,提高其孔隙率。随着CU功率的增加,芋头干燥次数减少16.67% ~ 25.00%,有效水分扩散系数提高14.72% ~ 31.38%。此外,CU的施用导致芋头细胞的横截面积和周长分布曲线先增大后减小,芋头细胞圆度分布曲线的峰形变宽。综上所述,CU能加快芋头内部水分迁移,且CU功率越大,对CUFRD过程中芋头微观结构和细胞形态参数的影响越明显。
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引用次数: 1
An adaptive optimization method toward batch-wise variable set point of outlet moisture content for the tobacco drying process 烟草干燥过程出口含水量批量可变设定点的自适应优化方法
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-21 DOI: 10.1080/07373937.2023.2222472
Yulei Gao, Tianyu Wang, X. Zhou, Mian Li, Chiyuan Zhang, Peng Qin, Yaojing Yang, Libin Zhang
Abstract The tobacco drying process in the cigarette production has an important effect on the final product quality. Therefore, the intelligent control methods have been widely investigated to ensure the stability of tobacco’s outlet moisture content. The existing work mostly uses a relatively fixed set point of the outlet moisture content for different tobacco batches, which can lead to unforeseen product quality after several processes following the drying process and inaccessible amount of dehydration for the rotary dryer. Some tobacco moisture prediction methods have been studied recently while the relationship with the intelligent control methods remain largely unexplored. To deal with these issues, a novel method is proposed in this paper to identify the optimal set point of the drying outlet moisture content for each tobacco batch. An encoder-decoder model is first developed to forecast the post-drying moisture trajectory. Then, an adaptive filter with specially designed mechanisms and a confidence interval of the dehydration level are constructed to obtain the design constraints. Based on all above, a constrained optimization problem is formulated and solved by the genetic algorithm. Extensive experiments on 895 tobacco batches from a large cigarette factory are carried out, which involves both algorithmic evaluation and field test. It turns out that the proposed method achieves the superior performance and leads to an improvement of the product quality in real production.
在卷烟生产中,烟叶干燥工艺对最终产品质量有重要影响。因此,为了保证烟草出口水分的稳定,智能控制方法得到了广泛的研究。现有的工作大多是针对不同批次的烟草采用相对固定的出口含水率设定值,这可能导致干燥过程后几道工序的产品质量不可预见,旋转干燥机脱水量难以达到。近年来研究了一些烟草水分预测方法,但与智能控制方法的关系仍未得到充分探讨。针对这些问题,本文提出了一种新的方法来确定每批烟草干燥出口水分含量的最佳设定值。首先建立了一个编码器-解码器模型来预测干燥后的水分轨迹。然后,构造具有特殊设计机制的自适应滤波器和脱水水平置信区间,以获得设计约束。在此基础上,提出了一个约束优化问题,并用遗传算法求解。对某大型卷烟厂的895批烟草进行了广泛的实验,包括算法评估和现场测试。实际生产中,该方法取得了较好的性能,提高了产品质量。
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引用次数: 0
Non-supercritical drying synthesis of hydrophobic, low-density, and high surface area silica aerogel using a sonication technique 利用超声技术非超临界干燥合成疏水、低密度、高表面积二氧化硅气凝胶
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-21 DOI: 10.1080/07373937.2023.2225100
J. Sharma, Shivangi Shukla, Javed Sheikh, B. Behera
Abstract Replacing the solvent in silica aerogel production with air is critical in getting the desired physical properties. Even though drying by evaporation under ambient pressure is thought to be the simplest way, it shrinks and collapses the gel network. In this research, uniform sol was prepared by sonication at room temperature. The surface of the developed wet gel was modified with trimethylchlorosilane (TMCS) after solvent exchange. The prepared aerogels underwent various characterization techniques to evaluate their functional, structural, morphological, surface, and thermal properties. The textural and physical characteristics of prepared silica aerogel were examined in relation to the precursor concentration, catalysts that affect the density of silica aerogel, volumetric shrinkage, and gelation time. The silica aerogel was found thermally stable up to 800 °C while hydrophobicity retained up to 350 °C. The contact angle of prepared aerogels confirms their hydrophobic nature. Field emission scanning electron microscopy (FE-SEM) and X-Ray Diffraction (XRD) results demonstrate the porous nature of silica aerogel. The Brunauer-Emmett-Teller (BET) surface area analysis revealed that the surface area and the pore radius were 784 m2/g and 36 Å, respectively.
摘要在硅胶气凝胶生产中,用空气代替溶剂是获得理想物理性能的关键。尽管在环境压力下通过蒸发干燥被认为是最简单的方法,但它会收缩并使凝胶网络崩溃。本研究采用室温超声法制备均匀溶胶。经溶剂交换,用三甲基氯硅烷(TMCS)对湿凝胶进行表面改性。制备的气凝胶通过各种表征技术来评估其功能、结构、形态、表面和热性能。考察了制备的二氧化硅气凝胶的结构和物理特性与前驱体浓度、影响二氧化硅气凝胶密度的催化剂、体积收缩率和凝胶化时间的关系。二氧化硅气凝胶的热稳定性可达800°C,疏水性可达350°C。所制备的气凝胶的接触角证实了其疏水性。场发射扫描电镜(FE-SEM)和x射线衍射(XRD)结果证实了二氧化硅气凝胶的多孔性。brunauer - emmet - teller (BET)表面积分析结果表明,其表面积为784 m2/g,孔隙半径为36 Å。
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引用次数: 0
Far infrared assisted refractance window drying: Influence on drying characteristics and quality of banana leather 远红外辅助折光窗干燥:对香蕉皮干燥特性及质量的影响
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-15 DOI: 10.1080/07373937.2023.2220777
Deependra Rajoriya, M. L. Bhavya, H. U. Hebbar
Abstract The market demand for fruit-based healthy snacks in dried form is increasing rapidly. Novel and efficient drying techniques are being explored to meet market demand of fruit-based snacks with better nutritive value and sensorial attributes. In this study, suitability of far infrared assisted refractance window (FIR + RW) drying to obtain banana leather was ascertained and drying behavior, bioactives, flavor, microstructure, and sensory attributes were compared with RW and hot air (HA) drying. FIR + RW and RW reduced the drying time by 60–75% and energy consumption by 38–45% as compared to HA. RW drying preserved color and retained higher phenolics (19%), ascorbic acid (22%) and antioxidant capacity (16–47%) compared to HA. Among the studied methods, HA resulted in higher browning index and hydroxymethylfurfural content. FIR + RW and RW dried banana samples had maximum flavor compounds, better overall consumer acceptance and improved cellular structure with widened pores. The study indicated that RW and FIR + RW have good potential to be considered as alternative drying techniques to HA for producing high-quality fruit leather.
摘要市场对干果类健康零食的需求正在迅速增长。为了满足市场对具有更好营养价值和感官特性的水果零食的需求,人们正在探索新的高效干燥技术。在本研究中,远红外辅助折射窗口(FIR)的适用性 + RW)干燥得到香蕉皮,并与RW和热空气(HA)干燥进行了干燥行为、生物活性、风味、微观结构和感官特性的比较。冷杉 + 与HA相比,RW和RW使干燥时间减少了60-75%,能耗减少了38-45%。与HA相比,RW干燥保留了颜色,并保留了更高的酚类物质(19%)、抗坏血酸(22%)和抗氧化能力(16-47%)。在所研究的方法中,HA导致较高的褐变指数和羟甲基糠醛含量。冷杉 + RW和RW干香蕉样品具有最大的风味化合物,更好的整体消费者接受度,并改善了细胞结构,使孔隙变宽。研究表明,RW和FIR + RW具有很好的潜力,可以作为HA的替代干燥技术来生产高质量的果皮。
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引用次数: 0
Application of experimental, numerical, and machine learning methods to improve drying performance and decrease energy consumption of tunnel-type food dryer 应用实验、数值和机器学习方法提高隧道式食品干燥机的干燥性能和降低能耗
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-08 DOI: 10.1080/07373937.2023.2216781
Murat Catalkaya, O. Akay, M. Das, E. Akpinar
Abstract In this study, to distribute the drying air uniformly on the product surface, straight and trapeze air barriers were designed in the drying chamber of the existing tunnel dryer. The effects of air barriers on product surface temperature changes were investigated by computational fluid dynamics analysis (CFD). Drying time in the experiment without an air barrier decreased by 45% with the trapeze barrier and 20% with the straight barrier. Likewise, the trapeze barrier provided 53.9% energy savings, and the straight barrier 37.4% energy saving compared to the drying process carried out in the current system. Also, using the experimental data, mathematical equations that can calculate activation energy (Ea) in the drying process were produced with the help of regression-based artificial intelligence methods (Pace and Elastic.Net). With the help of these equations, the Ea values of the drying process performed under different experimental conditions were determined, and a 1.03% error value was calculated between the obtained Ea values and the experimental values.
摘要在本研究中,为了使干燥空气均匀地分布在产品表面,在现有的隧道式干燥机的干燥室中设计了直的和梯形的空气屏障。通过计算流体动力学分析(CFD)研究了空气屏障对产品表面温度变化的影响。在没有空气屏障的实验中,梯形屏障的干燥时间减少了45%,直线屏障的干燥速度减少了20%。同样,与在当前系统中进行的干燥过程相比,梯形屏障提供了53.9%的能量节省,而直屏障提供了37.4%的能量节省。此外,利用实验数据,借助基于回归的人工智能方法(Pace和Elastic.Net),建立了可以计算干燥过程中活化能(Ea)的数学方程。借助这些方程,确定了不同实验条件下干燥过程的Ea值,并且在所获得的Ea值和实验值之间计算出1.03%的误差值。
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引用次数: 0
Modeling and simulation of single droplet drying in an acoustic levitator 声学悬浮器中单液滴干燥的建模与仿真
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-08 DOI: 10.1080/07373937.2023.2218162
M. Doß, N. Ray, E. Bänsch
Abstract We present a mathematical model for the full drying process of a single protein formulation droplet taking into account the convective impact arising from its levitation by a standing ultrasound wave. Using the finite element method allows us to compute the evaporation rate directly from the fully resolved heat and mass transfer within and around the levitated droplet. We apply our model to simulate the drying kinetics of pure water and aqueous phosphoglycerate kinase (PGK) droplets under various levitation and drying conditions. Empirical data from the literature are used to validate and discuss our numerical results. The acoustic streaming turns out to accelerate not only the first but also the second drying stage. Moreover, the dehydration of the protein molecules is found to be primarily responsible for their enzymatic inactivation throughout the drying process.
摘要我们提出了一个单一蛋白质制剂液滴完全干燥过程的数学模型,该模型考虑了驻波悬浮产生的对流影响。使用有限元方法,我们可以直接从悬浮液滴内部和周围的完全解析的传热和传质计算蒸发率。我们应用我们的模型模拟了纯水和磷酸甘油酸激酶(PGK)水液滴在各种悬浮和干燥条件下的干燥动力学。使用文献中的经验数据来验证和讨论我们的数值结果。声学流不仅加速了第一干燥阶段,而且加速了第二干燥阶段。此外,发现蛋白质分子的脱水是其在整个干燥过程中酶失活的主要原因。
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引用次数: 0
Thermodynamic and exergoeconomic analyses of two-stage spray drying plant for skim milk powder production 脱脂奶粉两级喷雾干燥装置的热力学和运行经济分析
IF 3.3 3区 工程技术 Q1 Chemical Engineering Pub Date : 2023-06-08 DOI: 10.1080/07373937.2023.2219736
A. Juneja, P. Barnwal, A. K. Sharma, Banashree Naskar, Amit Kumar
Abstract Spray drying of milk is a highly energy intensive process. In this study, thermodynamic and exergoeconomic analyses of two-stage spray drying plant have been executed. This plant was analyzed on the basis of various parameters such as energy efficiency, exergy efficiency, energy improvement potential, exergy improvement potential, etc. The energy and exergy efficiency of the plant were 72.90 and 35.15%, respectively. The maximum energy improvement potential was for drying whereas maximum exergy improvement potential was for homogenizer. It indicates huge scope in the technical improvement for drying chamber and homogenizer of the plant. The highest cost of processing was for cyclone separator (percentage relative cost difference: 44%) followed by drying chamber (percentage relative cost difference: 40.71%). Highest energy destroyed was calculated for drying chamber (195.83 kJ/kg) followed by VFBD (87.62 kJ/kg). Lowest energy efficiency was calculated for VFBD (34.64%) followed by drying chamber (50.04%). Highest energy improvement potential was estimated for drying chamber (97.86 kJ/kg). Highest relative energy destruction ratio was calculated for drying chamber (52.04%) followed by VFBD (23.30%). Highest energetic factor was calculated for drying chamber (28.22%) followed by homogenizer (16.71%). Based on these analyses, it was realized that performance of the spray drying plant may be substantially improved by some design improvement of drying chamber and homogenizer only.
牛奶喷雾干燥是一个高能耗的过程。本文对两段喷雾干燥装置进行了热力学和功耗经济分析。对该装置进行了能源效率、火用效率、能源改善潜力、火用改善潜力等参数分析。该装置的能量和火用效率分别为72.90%和35.15%。能量改进潜力最大的是干燥机,而能量改进潜力最大的是均质机。说明该厂干燥室和均质机的技术改进空间巨大。处理成本最高的是旋风分离器(相对成本差百分比为44%),其次是干燥室(相对成本差百分比为40.71%)。干燥室的能量破坏最高(195.83 kJ/kg),其次是VFBD (87.62 kJ/kg)。VFBD的能量效率最低(34.64%),其次是干燥室(50.04%)。估计干燥室的能量改善潜力最高(97.86 kJ/kg)。干燥室的相对能量破坏比最高(52.04%),其次是VFBD(23.30%)。干燥室的能量因子最高(28.22%),其次是均质器(16.71%)。在此基础上,认识到只要对干燥室和均质机进行设计改进,就可以大大提高喷雾干燥装置的性能。
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引用次数: 0
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Drying Technology
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