Pub Date : 2019-01-30DOI: 10.30598//IJCR.2019.6-KAR
Karnelasatri Karnelasatri, Edi Mikrianto
Aurivillius compounds, SrBi4Ti4O15 (SBT four layers) have been synthesized by hydrothermal method at 200℃ with variation of times 48 hours, 72 hours and 96 hours. Single phase of SrBi4Ti4O15 Aurivillius compounds obtained at the 200 ˚ C, 96 hours and the concentration of NaOH 3M. The Rietica program shown the index Miller result is 1 1 5 1 1 3, 0 2 0, 0 2 4, 2 0 8 2 2 0, 0 2 1 0, 3 1 6, 1 1 1 6 and the space group is A21am with the orthorhombic crystal system. Cell parameters are a = 5.5754 Å, b = 5.5456 Å, c = 41.3642. Ferroelectric properties show the value of remanent polarization Pr (+) and Pr (-) 4,61 C/cm2 and 2,75 C/cm2 and that is much lower than the value of remanent polarization of other material that have been synthesized at 240℃, 72 hours with the same method.
{"title":"Perbandingan Sifat Feroelektrik Pada Sintesis Oksida Logam Aurivillius SrBi4Ti4O15 Empat Lapis Dengan Metode Hidrotermal","authors":"Karnelasatri Karnelasatri, Edi Mikrianto","doi":"10.30598//IJCR.2019.6-KAR","DOIUrl":"https://doi.org/10.30598//IJCR.2019.6-KAR","url":null,"abstract":"Aurivillius compounds, SrBi4Ti4O15 (SBT four layers) have been synthesized by hydrothermal method at 200℃ with variation of times 48 hours, 72 hours and 96 hours. Single phase of SrBi4Ti4O15 Aurivillius compounds obtained at the 200 ˚ C, 96 hours and the concentration of NaOH 3M. The Rietica program shown the index Miller result is 1 1 5 1 1 3, 0 2 0, 0 2 4, 2 0 8 2 2 0, 0 2 1 0, 3 1 6, 1 1 1 6 and the space group is A21am with the orthorhombic crystal system. Cell parameters are a = 5.5754 Å, b = 5.5456 Å, c = 41.3642. Ferroelectric properties show the value of remanent polarization Pr (+) and Pr (-) 4,61 C/cm2 and 2,75 C/cm2 and that is much lower than the value of remanent polarization of other material that have been synthesized at 240℃, 72 hours with the same method.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"8 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78494682","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-01-30DOI: 10.30598//IJCR.2019.6-NUR
Laily Nurliana, Rustam Musta
Research on kinetics antibacterial from pyrolysis product of cashew nut shell againts Staphylococcus aureus have been carried out. Cashew nuts are prepared by separating the shell and seeds for pyrolysis. The results of S. aureus antibacterial activity test results pyrolysis pyrolysis products shell cashew nut showed inhibition is different for each variation of the concentration of 12.5%, 25%, 50%, 75% and 100% with inhibition of successive 0.87; 0.97; 1.38; 1.47 and 1.61 (cm). Based on these results it can be said that the result of the pyrolysis of cashew nut shells provide a response inhibition that were at concentrations of 12.5 and 25%. While the concentration of 50%, 75%, and 100% response inhibitory power is included in the strong category on the growth of S. aureus. Order the reaction of the antibacterial activity of S. aureus from the pyrolysis products obtained cashew nut shell 0,3 with activity rate constant of 0.38. The concentration of pyrolysis products of pyrolysis results cashew nut shell the minimum recommended for use as an antibacterial S.aureus.
{"title":"Studi Kinetika Antibakteri dari Hasil Pirolisis Cangkang Biji Jambu Mete terhadap Staphylococcus aureus","authors":"Laily Nurliana, Rustam Musta","doi":"10.30598//IJCR.2019.6-NUR","DOIUrl":"https://doi.org/10.30598//IJCR.2019.6-NUR","url":null,"abstract":"Research on kinetics antibacterial from pyrolysis product of cashew nut shell againts Staphylococcus aureus have been carried out. Cashew nuts are prepared by separating the shell and seeds for pyrolysis. The results of S. aureus antibacterial activity test results pyrolysis pyrolysis products shell cashew nut showed inhibition is different for each variation of the concentration of 12.5%, 25%, 50%, 75% and 100% with inhibition of successive 0.87; 0.97; 1.38; 1.47 and 1.61 (cm). Based on these results it can be said that the result of the pyrolysis of cashew nut shells provide a response inhibition that were at concentrations of 12.5 and 25%. While the concentration of 50%, 75%, and 100% response inhibitory power is included in the strong category on the growth of S. aureus. Order the reaction of the antibacterial activity of S. aureus from the pyrolysis products obtained cashew nut shell 0,3 with activity rate constant of 0.38. The concentration of pyrolysis products of pyrolysis results cashew nut shell the minimum recommended for use as an antibacterial S.aureus.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"2 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73115768","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-WAO
Waode Rustiah, Nur Umriani
Antioxidant activity test has been done on kawista fruit. This study aims to determine the antioxidant activity of kawista based on the test using UV-Vis spectrophotometer conducted wavelength (l) 516 nm. The kawista fruit is extracted by reflux using methanol solvent. The extracts were made at concentrations of 50 ppm, 100 ppm, 150 ppm, 200 ppm and 250 ppm. The results showed that the antioxidant activity based on IC50 values obtained on kawista fruit extract samples had a concentration of 1275 mg / ml. The results obtained are at the level of IC50> 150 mg/ml, this indicates that the kawista fruit have weak antioxidant ability.
{"title":"Uji Aktivitas Antioksidan Pada Ekstrak Buah Kawista (Limonia Acidissima) Menggunakan Spektrofotometer UV-Vis","authors":"Waode Rustiah, Nur Umriani","doi":"10.30598//IJCR.2018.6-WAO","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-WAO","url":null,"abstract":"Antioxidant activity test has been done on kawista fruit. This study aims to determine the antioxidant activity of kawista based on the test using UV-Vis spectrophotometer conducted wavelength (l) 516 nm. The kawista fruit is extracted by reflux using methanol solvent. The extracts were made at concentrations of 50 ppm, 100 ppm, 150 ppm, 200 ppm and 250 ppm. The results showed that the antioxidant activity based on IC50 values obtained on kawista fruit extract samples had a concentration of 1275 mg / ml. The results obtained are at the level of IC50> 150 mg/ml, this indicates that the kawista fruit have weak antioxidant ability.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"5 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73227881","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-CATH
Catherina M. Bijang, Helna Tehubijuluw, Terence Ghereds Kaihatu
The research about biosorption of Cadmium (Cd2+) metal ion in brown seaweed biosorben (Paladina australis) from Liti beach, Kisar island has been done. Analysis of decreasing Cd2+ content using Atomic Absorption Spectrophotometer (SSA) and also use FTIR to know functional groups contained in alginate compounds. A total of 0.5 g of brown seaweed powder was introduced into 25 mL of Cd2+ 50 ppm solution with variations of pH 1-7 and shaker for five hours. After the optimum pH was obtained, the adsorption process was applied on pH 5 solution with variation of contact time 1, 3, and 5 hours, after which it was filtered. The result of analysis and calculation showed that Cd2+ ion was optimum at pH 5 of 99.64% and 3 hours contact time was 74.54%.
对Kisar岛Liti海滩褐藻(Paladina australis)对镉(Cd2+)金属离子的吸附进行了研究。原子吸收分光光度法(SSA)和红外光谱法(FTIR)分析了藻酸盐化合物中Cd2+含量的下降。将0.5 g褐藻粉加入25 mL Cd2+ 50 ppm溶液中，pH值为1-7，摇瓶5小时。获得最佳pH后，在pH为5的溶液上进行吸附，吸附时间分别为1、3、5小时，然后进行过滤。分析计算结果表明，Cd2+离子在pH为99.64%、3 h接触时间为74.54%时的吸附效果最佳。
{"title":"Biosorpsi Ion Logam Kadmium (Cd2+) Pada Biosorben Rumput Laut Coklat (Padina australis) Asal Pantai Liti Pulau Kisar","authors":"Catherina M. Bijang, Helna Tehubijuluw, Terence Ghereds Kaihatu","doi":"10.30598//IJCR.2018.6-CATH","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-CATH","url":null,"abstract":"The research about biosorption of Cadmium (Cd2+) metal ion in brown seaweed biosorben (Paladina australis) from Liti beach, Kisar island has been done. Analysis of decreasing Cd2+ content using Atomic Absorption Spectrophotometer (SSA) and also use FTIR to know functional groups contained in alginate compounds. A total of 0.5 g of brown seaweed powder was introduced into 25 mL of Cd2+ 50 ppm solution with variations of pH 1-7 and shaker for five hours. After the optimum pH was obtained, the adsorption process was applied on pH 5 solution with variation of contact time 1, 3, and 5 hours, after which it was filtered. The result of analysis and calculation showed that Cd2+ ion was optimum at pH 5 of 99.64% and 3 hours contact time was 74.54%.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"4 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90736600","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ageratum Conyzoides L. has a toxic and bioactive component as anti-cancer and especially for the root, it has anti-tumor. In order to figure out the active component, it is necessary to do four steps; isolation, identification, characterization, and toxicity essay Brine Shrimp Lethality Test (BSLT) of non-polar fraction Ageratum conyzoides L plant. Isolation method consist of four parts; extraction, partitioning of Kupchan method, fractionation, and purification. Fractionation method uses press column chromatography (KTT). Furthermore, purification process uses thin layer chromatography (TLC) and characterization with spectroscopy FTIR, 1H-NMR and 13C-NMR. Then characterization utilizes spectroscopy FTIR, 1H-NMR and 13C-NMR. The toxicity essay toward Artemia Salina Leach n-hexane fraction and dichloromethane fraction showed that the fraction had toxic properties with number of LC50 are 0,0237 and 4,642 µg/mL respectively. Moreover, n-hexane fraction has succeed in isolating Stigmasterol compound shaped white crystalline needles with 19.6 mg weight, 143-144 °C melting point and and had toxic properties with number of LC50 are 30,33 µg/mL.
{"title":"Isolation, Identification, Characteriterization, And Toxicity Essay Of Non-polar Secondary Metabolite Fraction From Ageratum conyzoides L","authors":"Muhammad Irmawan, F. Mandey, S. Dali","doi":"10.30598/v12","DOIUrl":"https://doi.org/10.30598/v12","url":null,"abstract":"Ageratum Conyzoides L. has a toxic and bioactive component as anti-cancer and especially for the root, it has anti-tumor. In order to figure out the active component, it is necessary to do four steps; isolation, identification, characterization, and toxicity essay Brine Shrimp Lethality Test (BSLT) of non-polar fraction Ageratum conyzoides L plant. Isolation method consist of four parts; extraction, partitioning of Kupchan method, fractionation, and purification. Fractionation method uses press column chromatography (KTT). Furthermore, purification process uses thin layer chromatography (TLC) and characterization with spectroscopy FTIR, 1H-NMR and 13C-NMR. Then characterization utilizes spectroscopy FTIR, 1H-NMR and 13C-NMR. The toxicity essay toward Artemia Salina Leach n-hexane fraction and dichloromethane fraction showed that the fraction had toxic properties with number of LC50 are 0,0237 and 4,642 µg/mL respectively. Moreover, n-hexane fraction has succeed in isolating Stigmasterol compound shaped white crystalline needles with 19.6 mg weight, 143-144 °C melting point and and had toxic properties with number of LC50 are 30,33 µg/mL.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"11 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84650700","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-JOL
Jola Latupeirissa, M. F. Tanasale, Sigit Hardianto Musa
The adsorption of methylene blue dye by active carbon of hazelnut shell has been done. Through acquired active carbon composing process, where is the hazelnut shell at entry into furnace on temperature 350 for 2 hour, afterwards is cooled and at sieves by sieve 100 mesh. Then by the calsination process in furnace with temperature 450 one was streamed to gas N2 four 2 hours then characterized by X-ray diffraction (XRD) for carbon before activation. The next activated with KOH solution with a concentration 0f 50 four 5 hour, then dried in an ovenat 120℃ for 1 hour and thencharacterized. Weight of the solidacidity before and after activation consecutive (5.3848 x 10-3 dan 42.1554x 10-3) mol g-1. Isotherm adsorption of methylene blue dyes on active carbon was following the Freundlich isotherm. Adsorption kinetics of methylene blue dyes on active carbon in various concentration of hazelnut shell was controlled with temperature variety at 25 and 30 . The result showed that energy activation was kJ mol-1 and a value isg mg-1 menit-1. Adsorption mechanism of methylene blue dyes on active carbon at various concentration of hazelnut shell is chemical adsorption process.
{"title":"Kinetika Adsorpsi Zat Warna Metilen Biru Oleh Karbon Aktif Dari Kulit Kemiri (Aleurites moluccana (L) Willd)","authors":"Jola Latupeirissa, M. F. Tanasale, Sigit Hardianto Musa","doi":"10.30598//IJCR.2018.6-JOL","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-JOL","url":null,"abstract":"The adsorption of methylene blue dye by active carbon of hazelnut shell has been done. Through acquired active carbon composing process, where is the hazelnut shell at entry into furnace on temperature 350 for 2 hour, afterwards is cooled and at sieves by sieve 100 mesh. Then by the calsination process in furnace with temperature 450 one was streamed to gas N2 four 2 hours then characterized by X-ray diffraction (XRD) for carbon before activation. The next activated with KOH solution with a concentration 0f 50 four 5 hour, then dried in an ovenat 120℃ for 1 hour and thencharacterized. Weight of the solidacidity before and after activation consecutive (5.3848 x 10-3 dan 42.1554x 10-3) mol g-1. Isotherm adsorption of methylene blue dyes on active carbon was following the Freundlich isotherm. Adsorption kinetics of methylene blue dyes on active carbon in various concentration of hazelnut shell was controlled with temperature variety at 25 and 30 . The result showed that energy activation was kJ mol-1 and a value isg mg-1 menit-1. Adsorption mechanism of methylene blue dyes on active carbon at various concentration of hazelnut shell is chemical adsorption process.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"22 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84709338","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-MAT
M. F. Tanasale, A. Bandjar, Natasya Sewit
Chitosan isolated from mushroom (Vollariella volvaceae) as adsorbent of lead (Pb) metal has been done. The isolation of chitosan was obtained 2.94% from total weight of mushroom. Fungtional groups of chitin and chitosan were indentified by using FTIR spectrophotometry. The chitosan had 74.66% degree of deacetylation and 2.09 x 104 g/mol viscosity molecular weight. The experimental data of the chitosan as adsorbent for Pb metal were correlated with the Langmuir and Freundlich isotherm model. The maximum adsorption capacity of Pb based on the Langmuir isotherm model was 2.66 mg/g.
{"title":"Isolasi Kitosan Dari Tudung Jamur Merang (Vollvariella Volvaceae) Dan Aplikasinya Sebagai Absorben Logam Timbal (Pb)","authors":"M. F. Tanasale, A. Bandjar, Natasya Sewit","doi":"10.30598//IJCR.2018.6-MAT","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-MAT","url":null,"abstract":"Chitosan isolated from mushroom (Vollariella volvaceae) as adsorbent of lead (Pb) metal has been done. The isolation of chitosan was obtained 2.94% from total weight of mushroom. Fungtional groups of chitin and chitosan were indentified by using FTIR spectrophotometry. The chitosan had 74.66% degree of deacetylation and 2.09 x 104 g/mol viscosity molecular weight. The experimental data of the chitosan as adsorbent for Pb metal were correlated with the Langmuir and Freundlich isotherm model. The maximum adsorption capacity of Pb based on the Langmuir isotherm model was 2.66 mg/g.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"106 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85530693","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//ijcr.2018.6-cat
Catherina M. Bijang, Jola Latupeirissa, Marike Ratuhanrasa
The research on the biosorption of Cu2+ metal ions in brown seaweed biosorbent (Padina australis) has been done. This study aims to determine moisture content, ash content, biomass content, pH and optimum contact time of Cu2+ metal ions absorption pH and optimum contact time of Cu2+ metal ions absorption. The method used is batch method. The adsorption result of Cu2+ metal ions was analyzed by using atomic absorption spectrophotometer (AAS). The results showed that the optimum pH was 7 with 99.8308 % absorption ability of biosorbent and the optimum contact time was 5 hours with 99.5570 % biosorbent absorbency.
{"title":"Biosorpsi Ion Logam Tembaga (Cu2+) Pada Biosorben Rumput Laut Coklat (Padina australis)","authors":"Catherina M. Bijang, Jola Latupeirissa, Marike Ratuhanrasa","doi":"10.30598//ijcr.2018.6-cat","DOIUrl":"https://doi.org/10.30598//ijcr.2018.6-cat","url":null,"abstract":"The research on the biosorption of Cu2+ metal ions in brown seaweed biosorbent (Padina australis) has been done. This study aims to determine moisture content, ash content, biomass content, pH and optimum contact time of Cu2+ metal ions absorption pH and optimum contact time of Cu2+ metal ions absorption. The method used is batch method. The adsorption result of Cu2+ metal ions was analyzed by using atomic absorption spectrophotometer (AAS). The results showed that the optimum pH was 7 with 99.8308 % absorption ability of biosorbent and the optimum contact time was 5 hours with 99.5570 % biosorbent absorbency.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"5 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90578106","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-SER
S. J. Sekewael, K. Wijaya, Triyono
The thermal treatment of the silica-zirconia montmorillonite K10 and silica-ferri oxide montmorillonite K10 nanocomposites at 300 and 500 °C has been carried out, respectively as part of a study of their function as the catalyst. The heating effect on the crystallinity and the lattice parameter calculation of both nanocomposites was studied using XRD and FTIR instruments. The results showed that the nanocomposite silica-zirconia montmorillonite K10 has a thermal resistance and the crystallinity better than the silica-ferri oxide montmorillonite K10, and both have values varying lattice parameters.
{"title":"Effect Of Heating On The Crystalinity And The Lattice Parameter Of Silica-Zirconia Montmorillonite K10 And Silica-Ferri Oxide Montmorillonite K10 Nanocomposites","authors":"S. J. Sekewael, K. Wijaya, Triyono","doi":"10.30598//IJCR.2018.6-SER","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-SER","url":null,"abstract":"The thermal treatment of the silica-zirconia montmorillonite K10 and silica-ferri oxide montmorillonite K10 nanocomposites at 300 and 500 °C has been carried out, respectively as part of a study of their function as the catalyst. The heating effect on the crystallinity and the lattice parameter calculation of both nanocomposites was studied using XRD and FTIR instruments. The results showed that the nanocomposite silica-zirconia montmorillonite K10 has a thermal resistance and the crystallinity better than the silica-ferri oxide montmorillonite K10, and both have values varying lattice parameters.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"121 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76115970","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-07-31DOI: 10.30598//IJCR.2018.6-MUH
Muhammad Irmawan, Frederyk Mandey, S. Dali
Ageratum Conyzoides L. has a toxic and bioactive component as anti-cancer and especially for the root, it has anti-tumor. In order to figure out the active component, it is necessary to do four steps; isolation, identification, characterization, and toxicity essay Brine Shrimp Lethality Test (BSLT) of non-polar fraction Ageratum conyzoides L plant. Isolation method consist of four parts; extraction, partitioning of Kupchan method, fractionation, and purification. Fractionation method uses press column chromatography (KTT). Furthermore, purification process uses thin layer chromatography (TLC) and characterization with spectroscopy FTIR, 1H-NMR and 13C-NMR. Then characterization utilizes spectroscopy FTIR, 1H-NMR and 13C-NMR. The toxicity essay toward Artemia Salina Leach n-hexane fraction and dichloromethane fraction showed that the fraction had toxic properties with number of LC50 are 0,0237 and 4,642 µg/mL respectively. Moreover, n-hexane fraction has succeed in isolating Stigmasterol compound shaped white crystalline needles with 19.6 mg weight, 143-144 °C melting point and and had toxic properties with number of LC50 are 30,33 µg/mL.
{"title":"Isolasi, Identifikasi, Karakterisasi Dan Uji Toksisitas Senyawa Metabolit Sekunder Fraksi Nonpolar Akar Babandotan (Ageratum conyzoides L)","authors":"Muhammad Irmawan, Frederyk Mandey, S. Dali","doi":"10.30598//IJCR.2018.6-MUH","DOIUrl":"https://doi.org/10.30598//IJCR.2018.6-MUH","url":null,"abstract":"Ageratum Conyzoides L. has a toxic and bioactive component as anti-cancer and especially for the root, it has anti-tumor. In order to figure out the active component, it is necessary to do four steps; isolation, identification, characterization, and toxicity essay Brine Shrimp Lethality Test (BSLT) of non-polar fraction Ageratum conyzoides L plant. Isolation method consist of four parts; extraction, partitioning of Kupchan method, fractionation, and purification. Fractionation method uses press column chromatography (KTT). Furthermore, purification process uses thin layer chromatography (TLC) and characterization with spectroscopy FTIR, 1H-NMR and 13C-NMR. Then characterization utilizes spectroscopy FTIR, 1H-NMR and 13C-NMR. The toxicity essay toward Artemia Salina Leach n-hexane fraction and dichloromethane fraction showed that the fraction had toxic properties with number of LC50 are 0,0237 and 4,642 µg/mL respectively. Moreover, n-hexane fraction has succeed in isolating Stigmasterol compound shaped white crystalline needles with 19.6 mg weight, 143-144 °C melting point and and had toxic properties with number of LC50 are 30,33 µg/mL.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"50 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2018-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89502836","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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