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Antimicrobial Activities of Bioactive Compounds from Jatropha curcas 麻疯树生物活性化合物的抗菌活性研究
Pub Date : 2020-01-07 DOI: 10.24114/IJCST.V2I1.12366
Zona Octarya, Fitri Refelita, Novia Rahim
Jatropha curcas L is widely planted in people's homes. Jatropha has many bioactive compounds, including flavonoids, saponins, tannins, and alkaloids. In this research, phytochemical tests and antimicrobial activities of sap and water extraction of Jatropha curcas L leaves on Candida albicans, Aspergillus, and Pseudomonas aeruginosa were carried out. The results of the phytochemical test of sap and water extraction of leaves showed positive results in the test of flavonoids, saponins, alkaloids and tannins. While steroid testing showed negative results. The antimicrobial capabilities of sap and water extraction of leaves to Aspergillus were 10.5 mm and 11 mm and to Pseudomonas Aeruginosa were 15 mm and 11 mm. Whereas the antimicrobial ability of sap and water extraction of leaf to Candida albicans was negative. In this case, it means that Pseudomonas aeruginosa is including microbes that are sensitive to antimicrobial origin of plants.
麻疯树被广泛种植在人们的家中。麻疯树有许多生物活性化合物,包括类黄酮、皂苷、单宁和生物碱。本研究对麻疯树叶的树液和水提物进行了植物化学试验,并对白色念珠菌、曲霉菌和铜绿假单胞菌进行了抑菌活性研究。树液和叶水提液的植物化学试验结果表明,黄酮类化合物、皂苷类化合物、生物碱类化合物和单宁类化合物均呈阳性。而类固醇检测结果呈阴性。叶液和水提物对曲霉的抑菌能力分别为10.5 mm和11 mm,对铜绿假单胞菌的抑菌能力分别为15 mm和11 mm。而叶液和水提物对白色念珠菌的抑菌能力为阴性。在这种情况下,这意味着铜绿假单胞菌包括对植物抗菌素来源敏感的微生物。
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引用次数: 0
Potential of Bio-briquette of Pineapple Crown Waste (Ananas comosus (L.) merr 凤梨冠废弃物生物型煤的潜力
Pub Date : 2020-01-07 DOI: 10.24114/IJCST.V2I1.12370
Kurnia Nur Addina, Lazulva Lazulva
This study aims to determine the potential of pineapple crown waste to be used as natural fuel in the form of biobriquettes, The research method used in this study is an experimental method. The research carried out in several stages, namely collection of raw materials, dehydration of raw materials, carbonization, crushing and screening, mixing binder, molding and compressing, drying and briquettes quality determining. The research findings showed that the bio-briquette quality of pineapple crown was 5.2-2.2% based on water content test, kabout 200-150 minutes, heating a liter water wiyh 200 grams bio-briquette was 23-15 minutes. All results of bio-briquette quality test of pineapple crown passed the SNI 06-3730-1995.
本研究旨在确定菠萝冠废弃物作为生物燃料形式的天然燃料的潜力,本研究采用的研究方法为实验法。研究分几个阶段进行,即原料收集、原料脱水、炭化、破碎筛选、粘结剂混合、成型压缩、干燥和型煤质量确定。研究结果表明,以含水量测试为基础,菠萝冠的生物型煤质量为5.2-2.2%,约200-150分钟,用200克生物型煤加热1升水为23-15分钟。菠萝冠生物型煤质量检测结果均通过SNI 06-3730-1995。
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引用次数: 1
Synthesis and Characterization Nanomagnetite by Co-precipitation 共沉淀法合成纳米磁铁矿及表征
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.13995
R. Rahimah, A. Fadli, Yelmida Yelmida, N. Nurfajriani, Z. Zakwan
Magnetite (Fe3O4) nanoparticles becomes a new innovation that gets attention of biomedicine scientists. Magnetite can be applied to cancer treatment as a drug carrier because it’s good biocompatibility and very low toxicity. The aim of this study was to determine the effect of temperature and retention time on the magnetite particle characteristics prepared by co-precipitation method. The first, FeCl3 and FeCl2 with 2:1 mole ratio were reacted with 10% NH4OH at 40 - 80°C temperatures during 1 – 30 minutes in a beaker glass. Subsequently, the precipitate was separated using filter paper and it dried into air oven at 100°C. The characteristic of obtained magnetite powder were determined using XRD and SEM. From XRD pattern indicates that magnetite formed at all temperatures with crystallite diameter in the range of 7-13 nm. The SEM results indicate the agglomeration of the magnetite particles with size in the range of 1.37 to 1.72 μm. In the other hand, the higher of temperature and retention time will make the agglomeration of the particles become more uniform. The increasing of temperature and the retention time will increase the magnetite crystallinity level.
磁铁矿(Fe3O4)纳米颗粒是近年来备受生物医学界关注的一项新技术。磁铁矿具有良好的生物相容性和极低的毒性,可作为药物载体应用于癌症治疗。本研究的目的是确定温度和保留时间对共沉淀法制备的磁铁矿颗粒特性的影响。首先,FeCl3和FeCl2以2:1的摩尔比在烧杯中与10%的NH4OH在40 - 80℃的温度下反应1 - 30分钟。随后,用滤纸将沉淀分离,在100℃的空气烘箱中干燥。采用XRD和SEM对所得磁铁矿粉体进行了表征。XRD图谱表明,在所有温度下均形成了磁铁矿,晶粒直径在7 ~ 13 nm之间。扫描电镜结果表明,晶粒尺寸在1.37 ~ 1.72 μm之间的磁铁矿颗粒发生团聚。另一方面,较高的温度和停留时间将使颗粒的团聚变得更加均匀。温度的升高和保留时间的延长会提高磁铁矿的结晶度。
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引用次数: 1
Using Water Hyacinth Fiber ( Eichhornia Crassipes) as Heat Absorbers Media In Wall 水葫芦纤维作为墙体吸热介质的研究
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.13996
M. Amin, Sefri Wahyu Fernando Gultom, Fitrisia Krisa Bella, P. Luthan
Water hyacinth is aquatic weed plant that has medium fiber content with length about 1.75 – 2.12 mm and diameter about 11.15 – 11.65 μm in its stem. Water hyacinth contains 90% of water by weight reduction from 10 Kg when wet to 1 Kg when dry. In dry conditions, water hyacinth contains crude protein 13.03%, crude fiber 20.6%, fat 1.1%, ash 23.8% and the rest is vortex that contains polysaccharides and minerals. Research was done to obtain the design of heat absorbing product that modified with additional of water hyacinth. The method that was uesd begin with drying water hyacinth to obtain good fiber. water hyacinth fibers then mixed with cement and sand which are made as composites in order to reduce the heat of room. The result of the research is make a product that can overcome thermal comfort problems in deep room temperature condition. Water hyacinth was chosen because it is easy to obtain, cheap and can reduce environmental pollution (biodegradability) so that the composite can overcome environment ptoblem and its used doesn’t endanger health. Based on the test result by providing a heat source of 40 Watt bulb lamp to the media for 15 minutes, it was found that the final temperature of the media 1 without additional of water hyacinth fiber was 32.5oC, final temperature of media 2 with additional of 100 gr water hyacinth was 32.2oC, and the final temperature of media 3 with additional 150 gr water hyacinth was 31.7oC. it shows heat temperature that is released and cannot be absorbed by composite in media 3 is only 0.50C, in meida 2 is only 10C while in composite in media 1 without additional of water hyacinth fiber that release heat about 1.3oC. it shows that the product is suitable to use because composite with additional of water hyacinth can absorb heat and release less heat compared to composite without additional water hyacinth fiber so that the room become cooler.
水葫芦是一种中等纤维含量的水草植物,茎长约1.75 ~ 2.12 mm,直径约11.15 ~ 11.65 μm。水葫芦含有90%的水,重量从湿时的10公斤减少到干时的1公斤。在干燥条件下,水葫芦的粗蛋白质含量为13.03%,粗纤维含量为20.6%,脂肪含量为1.1%,灰分含量为23.8%,其余为含多糖和矿物质的漩涡。对添加水葫芦改性的吸热产品进行了设计研究。所采用的方法是从干燥水葫芦入手,以获得良好的纤维。然后将水葫芦纤维与水泥和沙子混合制成复合材料,以减少房间的热量。研究的结果是研制出一种能够克服深室温条件下热舒适问题的产品。选择水葫芦是因为水葫芦容易获得,价格便宜,并且可以减少对环境的污染(可生物降解性),因此复合材料可以克服环境问题,而且使用时不危害健康。通过对介质提供40瓦灯泡热源15分钟的测试结果,发现不添加水葫芦纤维的介质1的最终温度为32.5oC,添加100克水葫芦的介质2的最终温度为32.2oC,添加150克水葫芦的介质3的最终温度为31.7oC。由图可知,复合材料在介质3中放出的不能被吸收的热温度仅为0.50℃,在介质2中放出的热温度仅为10C,而在不添加水葫芦纤维的复合材料中放出的热温度约为1.3℃。结果表明,与不添加水葫芦纤维的复合材料相比,添加水葫芦纤维的复合材料吸收热量和释放热量更少,使室内温度降低,是适合使用的。
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引用次数: 2
Synthesis of Biodiesel From Rubber Seed Oil with Acid and Base Activated Natural Zeolite Catalyst 酸碱活化天然沸石催化剂催化橡胶籽油合成生物柴油
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.14001
Tiamina Nasution, Akhir Mauludin Pulungan, Yuli Asih Wiliranti, J. Sihombing, A. Pulungan
 In this study, biodiesel synthesis was carried out using Z-AH and Z-OH Zeolite catalysts to obtain a cheaper and environmentally friendly process. The catalysts were prepared from Sarulla Indonesian natural zeolite       (Z-AS) through a chemical activation process with certain HCl 3 M and NaOH 2 M, then calcined at 500°C with Nitrogen gas for 4 hours to obtain Z-AH ang Z-OH catalyst. The catalysts were characterized by FT-IR and XRD. The conversion of rubber seed oil into biodiesel was carried out at temperature of 30 oC, 60 oC and 90 oC. The ratio of methanol: rubber seed oil is 6: 1 (v / v) and the catalyst concentration used is 1% wt. The XRD and FTIR data show that Z-AS activation increases the crystallinity of zeolite and does not damage the zeolite skeletal structure.The Z-AH catalyst has a better catalytic activity than the Z-OH catalyst with the conversion value of the biodiesel product obtained at 69.79%.
在本研究中,采用Z-AH和Z-OH沸石催化剂进行生物柴油的合成,以获得更便宜和环保的工艺。以印尼Sarulla天然沸石(Z-AS)为原料,用一定量的HCl 3 M和NaOH 2 M进行化学活化,然后在500℃下用氮气煅烧4 h,得到Z-AH和Z-OH催化剂。采用FT-IR和XRD对催化剂进行了表征。橡胶籽油在30℃、60℃和90℃的温度下转化为生物柴油。甲醇与橡胶籽油的比例为6:1 (v / v),催化剂浓度为1% wt。XRD和FTIR数据表明,活化Z-AS提高了沸石的结晶度,且不破坏沸石的骨架结构。Z-AH催化剂的催化活性优于Z-OH催化剂,生物柴油产品的转化率为69.79%。
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引用次数: 2
Application of Humid Silica Plus Fertilizer with Various Combinations of Planting Media 湿润二氧化硅+肥料与不同种植介质组合的应用
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.14000
Thomson A.S. Girsang, V. Apriyani, Desti S.N Pasaribu, Lisnawaty Simatupang
Volcanic ash contains minerals needed by soil and plants with the highest composition of total elements, namely Ca, Na, K and Mg, other macro elements in the form of P and S, while micro elements consist of Fe, Mn, Zn, Cu. The layer of volcanic dust that has the potential to contain nutrients for soil fertilization for agriculture can actually only be used about 10 years after the spread of volcanic ash. Soil fertilization can be accelerated if mixed with organic materials such as by using chicken manure fertilizer which has nutrients from chicken manure: N = 1.7%, P2O5 = 1.9%, K2O = 1.5%. Humic acid helps regulate clay and soil improvement, binds and transfers micro elements from the soil to plants, increases water absorption, and stimulates the development of microorganisms in the soil. Therefore, this study was conducted to make humic silica fertilizer in the planting medium by utilizing volcanic ash in combination with chicken manure mixed with soil. In this study apart from being a source of humic acid, chicken manure is also beneficial because it contains microorganisms which will be useful in accelerating the fertilizer incubation process. The composition of the fertilizer mixture used in this study is: volcanic ash sinabung: chicken manure: soil = 20: 50: 30; 30: 50:20; 40: 50: 10. The mixture is stirred evenly and then incubated for 30 days. After 30 days, the nutrient content of these fertilizers was tested and the highest content of the nutrients obtained in the combination was 20:50:30 namely: Organic C-1.35%, N-total 0.2%, P-available 20.16 ppm , K-available 0.527 me / 100g, C / N 6.75%, and humic acid contained in 3.925%
火山灰中含有土壤和植物所需的矿物质,总元素含量最高,即Ca、Na、K和Mg,其他宏量元素以P和S的形式存在,微量元素包括Fe、Mn、Zn、Cu。火山灰层有可能含有用于农业土壤施肥的营养物质,实际上只能在火山灰扩散后10年左右使用。鸡粪肥是一种有机肥,其营养成分N = 1.7%, P2O5 = 1.9%, K2O = 1.5%,与有机肥混合可加速土壤施肥。腐植酸有助于调节粘土和土壤的改善,将土壤中的微量元素结合并转移到植物中,增加水分吸收,并刺激土壤中微生物的发育。因此,本研究利用火山灰与鸡粪混合土壤,在种植介质中制备腐殖质硅肥。在这项研究中,除了作为腐植酸的来源外,鸡粪也是有益的,因为它含有有助于加速肥料孵化过程的微生物。本研究使用的混合肥料组成为:火山灰:鸡粪:土壤= 20:50:30;30: 50:20;40:50: 10。搅拌均匀后孵育30天。30 d后,对各肥料进行养分含量测定,得到的最高养分含量为20:50:30,即有机碳1.35%,全氮0.2%,速效磷20.16 ppm,速效钾0.527 me / 100g, C / N 6.75%,腐植酸含量3.925%
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引用次数: 1
Combination of Sinabung Volcanic Ash and Humic Acid Against Characteristics of Humid Silica Fertilizers 锡纳朋火山灰与腐植酸复合对湿法二氧化硅肥料特性的影响
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.13998
V. Apriyani, Thomson A.S. Girsang, Ribka J Sirait, Lisnawaty Simatupang
Volcanic ash from Mount Sinabung has a large silica (SiO2) content of 69,93% and contains minerals needed by soil and plants. This potential cannot be directly utilized due to the acidic nature of volcanic ash which can damage plants. To be used as fertilizer, the process can be accelerated by adding humic acid from chicken manure. So the purpose of this study is to manufacture humic silica fertilizer by combining volcanic ash with humic acid from chicken manure and and  the characteristics of humic silica fertilizer. In this study a method of extracting humic acid from chicken manure was used using sodium hydroxide (NaOH) 0,25 M solution and mixing volcanic ash with humic acid. The results of humic acid extract from chicken manure were then combined with volcanic ash from sinabung. Nutrients from the combination obtained at variation 60:40 with the highest organic C were 1.37%, N total 0.24%, Phosphate 20.64 ppm and Potassium 0.664 me / 100g with pH fertilizer 6 and crumb texture and free neutral which indicates the fertilizer is ready to use.
锡纳朋火山的火山灰含有大量二氧化硅(SiO2),含量高达69.93%,其中含有土壤和植物所需的矿物质。这种潜力不能直接利用,因为火山灰的酸性会损害植物。作为肥料,加入鸡粪中的腐植酸可以加速这一过程。因此,本研究的目的是利用火山灰与鸡粪中的腐植酸结合,制备腐植酸硅肥,并分析腐植酸硅肥的特性。采用氢氧化钠(NaOH) 0,25 M溶液,将火山灰与腐植酸混合,从鸡粪中提取腐植酸。然后将鸡粪腐植酸提取液与锡纳朋火山的火山灰相结合。在60:40变化条件下,有机碳最高的组合为1.37%,总氮为0.24%,磷酸盐为20.64 ppm,钾为0.664 me / 100g, pH值为6,颗粒状,游离中性,表明肥料可以使用。
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引用次数: 3
Red Spinach (Alternanthera amoena voss) as an Environmental Friendly Acid Base Indicator 红菠菜(Alternanthera amoena voss)作为环境友好的酸碱指示剂
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.13997
Sri Adelila Sari, Suriati Nilmarito
Natural indicators are indicators that are continuously developed to determine whether a sample is acidic or basic. This study examined how red spinach can be developed into an environmentally friendly acid-base indicator that intends to be non-toxic, easy to obtain, and affordable. The natural indicator used in this study was red spinach leaf extract (Alternanthera amoena voss). The samples used were salt water, tea, pineapple, detergent, and oranges. Red spinach leaf extract was dropped on each sample which had a volume of 150mL resulting in a color change. The results of this study indicated that red discoloration occurs in samples of salt water, tea, oranges, and pineapples according to their acidic properties. Furthermore, detergent water turned to a bluish green color, and according to the basic properties of a detergent. This study concluded that red spinach leaf extract can be used as an environmental friendly natural indicator.
自然指标是不断发展的指标,用于确定样品是酸性还是碱性。本研究探讨了如何将红菠菜开发成一种无毒、容易获得、价格合理的环境友好型酸碱指示剂。本研究采用的天然指示剂为红菠菜叶提取物(Alternanthera amoena voss)。使用的样品是盐水、茶、菠萝、洗涤剂和橙子。将红色菠菜叶提取物滴在每个样品上,其体积为150mL,导致颜色变化。这项研究的结果表明,在盐水、茶、橙子和菠萝的样品中,根据它们的酸性特性,会发生红色变色。此外,洗涤剂水变成蓝绿色,并根据洗涤剂的基本性质。本研究表明,红菠菜叶提取物可作为一种环境友好型天然指标。
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引用次数: 5
Utilization of Glycerol from Used Oil as an Ester Glycerol Surfactant 废油中甘油用作酯甘油表面活性剂的研究
Pub Date : 2019-07-12 DOI: 10.24114/ijcst.v2i2.13999
Dian Wardana, A. Ramadhan, Dinda Prihatini Fitri Amne, E. Eddiyanto
The development of biodiesel which is currently increasing has helped increase glycerol as a by-product. The glycerol can be obtained from a transesterification reaction in either vegetable or animal oils or fats and even used cooking oil. Glycerol buildup without further processing can reduce the selling price of glycerol. One solution to overcome this is to convert it to surfactants such as glycerol esters which are widely used in various industries such as chemistry, food, cosmetics, medicine and textiles. This study aims to utilize used cooking oil as a source of glycerol used in the synthesis of glycerol ester surfactants, as well as to compare the quality of glycerol ester surfactants produced by the use of commercial glycerol. The process begins by isolating glycerol from used cooking oil and then purifying it to improve its quality. Then glycerol ester was synthesized by using stearic acid, palmitic acid and oleic acid at reaction times of 120, 150 and 180 minutes. The highest yield of ester glycerol produced was at the reaction time of 180 minutes for each use of fatty acids. The test results showed that the glycerol ester produced was able to reduce the surface tension of the water. The value of hydrophylic-lipophylic balance (HLB) is not much different in the range of 5, and the use of various fatty acids and different sources of glycerol results in % of the stability of different emulsions.
随着生物柴油的发展,作为副产品的甘油也在不断增加。甘油可以在植物油或动物油或脂肪甚至用过的食用油中通过酯交换反应得到。未经进一步处理的甘油堆积可以降低甘油的销售价格。解决这一问题的一种方法是将其转化为表面活性剂,如甘油酯,这种表面活性剂广泛应用于化学、食品、化妆品、医药和纺织等各个行业。本研究旨在利用废食用油作为合成甘油酯表面活性剂的甘油来源,并比较使用商品甘油生产的甘油酯表面活性剂的质量。这个过程首先从用过的食用油中分离甘油,然后对其进行净化以提高其质量。然后以硬脂酸、棕榈酸和油酸为原料,分别反应120、150和180分钟,合成甘油酯。每次使用脂肪酸,反应时间为180分钟时酯甘油得率最高。试验结果表明,所制得的甘油酯能够降低水的表面张力。水酚脂平衡(HLB)值在5的范围内差别不大,不同脂肪酸的使用和不同来源的甘油对乳剂稳定性的影响也不同。
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引用次数: 4
Effect of Dragon Fruit Juice Addition on Changes in Peroxide Numbers and Acid Numbers of Used Cooking Oil 添加火龙果汁对废食用油过氧化氢和酸值变化的影响
Pub Date : 2019-07-10 DOI: 10.24114/ijcst.v2i2.15449
Sri Adelila Sari, T. Putri, Muhammad Rudi Ar
Many foods from Indonesia are cooked through the frying process using cooking oil. Good cooking oil is oil that has a low amount of peroxide and acid. The purpose of this study was to find the effect of adding dragon fruit juice (Hylocereus undatus)to peroxide numbers and acid numbers in used cooking oil. Peroxide numbers were measured using the iodometry method, whereas acidic numbers were carried out by the acid-base method. The results of this study indicated that after the addition of dragon fruit juice the peroxide number was dropped to 2.4 meg / kg, whereas in acid numbers an acid number was increased to 6.08 percent.
印度尼西亚的许多食物都是用食用油油炸的。好的食用油是含有少量过氧化氢和酸的油。本研究的目的是研究龙果汁(Hylocereus undatus)对废油中过氧化值和酸值的影响。过氧化氢数用碘量法测定,酸性数用酸碱法测定。研究结果表明,加入火龙果汁后,过氧化氢含量降至2.4 meg / kg,而酸含量则增加到6.08%。
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引用次数: 4
期刊
Indonesian Journal of Chemical Science and Technology (IJCST)
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