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Characterization of chestnut starch acetate with different degrees of substitution 不同取代度板栗淀粉醋酸酯的表征
IF 1.6 4区 农林科学 Pub Date : 2023-03-01 DOI: 10.1515/ijfe-2022-0320
Na Hu, E. Tang, Shuo Wang, M. Yuan, S. Liu, X. Chu, Xuteng Xing, Xinying Liu, L. Jewell
Abstract Chestnut starch acetates (CSA) with different degrees of substitution (DS) were prepared. The structure and physicochemical properties of CSA were then determined, with scanning electron microscopy showing that most of the CSA granules were damaged and dented, and adhered with increased in DS. X-ray diffraction results indicated that the crystal form of CS and CSA was type C. Chemical structure analysis showed that the starch molecule was grafted with acetyl groups. The transparency, freeze–thaw stability, solubility and swelling power of CSA improved with an increase in DS. The viscosity and stability of CSA were significantly improved and pasting temperatures reduced compared with native CS. The cohesion, hardness, gumminess, chewiness and springiness of CSA decreased with an increase in DS, whereas adhesiveness increased. By comparing the properties of CSA with different DS, a new option was provided for the application of renewable natural polymer CSA in food fields.
摘要制备了不同取代度的栗淀粉醋酸酯(CSA)。然后测定了CSA的结构和理化性质,扫描电子显微镜显示,随着DS的增加,CSA颗粒大多出现损伤和凹陷,并粘附。X射线衍射结果表明,CS和CSA的结晶形式为C型。化学结构分析表明,淀粉分子上接枝有乙酰基。CSA的透明度、冻融稳定性、溶解度和溶胀力随着DS的增加而提高。与天然CS相比,CSA的粘度和稳定性显著提高,糊化温度降低。CSA的内聚力、硬度、粘性、咀嚼性和弹性随着DS的增加而降低,而粘附性增加。通过比较CSA与不同DS的性能,为可再生天然聚合物CSA在食品领域的应用提供了新的选择。
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引用次数: 1
Development, physiochemical and sensory evaluation of a new effervescent tablet formulation based on Moringa oleifera leaves extract 辣木叶提取物泡腾片配方的研制、理化及感官评价
4区 农林科学 Pub Date : 2023-03-01 DOI: 10.1515/ijfe-2022-0170
Ade Chandra Iwansyah, Hilman Fauzi, Wisnu Cahyadi, Hari Hariadi, Ashri Indriati, Riuh Wardhani, Hazrulrizawati Abd Hamid
Abstract New product development of Moringa oleifera effervescent tablet was optimization of the acid-base in the formula by using the D-optimal mix design. Chemical profiling and antioxidant activity of Moringa oleifera extract was evaluated. The physicochemical and sensory characteristics of Moringa oleifera effervescent tablet was measured. The results shows that chemical compounds of aqueous and ethanol extracts of Moringa oleifera extracts were hydrocarbons, esters, alcohols, and fatty acids. Both extracts exhibited high antioxidant by the IC 50 value at 240.27 μg/mL and 301.21 μg/mL respectively. The quadratic model was found to be the best fitted for evaluating the solubility time, colour, taste and aroma; meanwhile, the special cubic model appeared to be the best fitting model for assessing the hardness response. The optimization process suggested that citric acid (22.19% w/w), tartaric acid (11.17% w/w), and sodium bicarbonate (33.64% w/w) was the best solution for this combination of variables, with a desirability value of 0.798.
摘要:对辣木泡腾片的新产品开发,采用d-最优配比设计对配方中的酸碱进行优化。对辣木提取物的化学性质和抗氧化活性进行了评价。测定了辣木泡腾片的理化特性和感官特性。结果表明,辣木水提液和乙醇提液的化学成分主要为烃类、酯类、醇类和脂肪酸。两种提取物均表现出较高的抗氧化能力,其IC 50值分别为240.27 μg/mL和301.21 μg/mL。结果表明,二次元模型最适合评价溶解度、色、味、香;同时,特殊立方模型是评估硬度响应的最佳拟合模型。优选结果表明,柠檬酸(22.19% w/w)、酒石酸(11.17% w/w)和碳酸氢钠(33.64% w/w)是该组合的最佳方案,理想值为0.798。
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引用次数: 1
Physicochemical properties and structure of buckwheat flour modified by steam-treatment 蒸汽改性荞麦粉的理化性质及结构
IF 1.6 4区 农林科学 Pub Date : 2023-03-01 DOI: 10.1515/ijfe-2022-0289
Bo-Hai Yang, Jiake Wang, Tong Yang, Yi-fu Zhang, Yuhe Wang, Siqi Qiang, Junjun Zhou, Shuhong Li, Ye Chen
Abstract The natural buckwheat flour exhibits poor processing behaviour due to its conservative structure and the lack of gluten protein, thereby limiting its use in the food industry. The replacement of chemical modification with sustainable, environmentally friendly steam treatment is, currently, technically feasible and promising for most chemical modification methods. The data showed that the steam-treated buckwheat flour degree of gelatinization increased to 99.3 g/100 g, and water absorption increased to 3.93 g/100 g. Also, particle size of the samples in the trial group was significantly larger compared to the control group. Scanning electron microscopy and infrared tests showed that not only did the steam treatment disrupt the granular structure of the buckwheat flour, but its proximity crystalline ordering structure Importantly, rheological behaviour tests showed that the steam-treated buckwheat gel exhibited a better viscoelasticity. Consequently, steam-treated pre-gelatinized buckwheat flour readily forms a tight network structure and provided important information for potential processing applications.
摘要天然荞麦粉由于其结构保守和缺乏面筋蛋白而表现出较差的加工性能,从而限制了其在食品工业中的应用。目前,用可持续、环保的蒸汽处理取代化学改性在技术上是可行的,对大多数化学改性方法来说都很有前景。结果表明,经蒸汽处理的荞麦粉的糊化度提高到99.3 g/100 g、 吸水率提高到3.93 g/100 g.此外,与对照组相比,试验组样品的粒径明显更大。扫描电子显微镜和红外测试表明,蒸汽处理不仅破坏了荞麦粉的颗粒结构,而且破坏了其接近结晶的有序结构。重要的是,流变行为测试表明,经蒸汽处理的荞麦凝胶表现出更好的粘弹性。因此,经过蒸汽处理的预糊化荞麦粉很容易形成紧密的网络结构,并为潜在的加工应用提供了重要信息。
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引用次数: 0
The properties of potato gluten-free doughs: comparative and combined effects of propylene glycol alginate and hydroxypropyl methyl cellulose or flaxseed gum 马铃薯无麸质面团的特性:海藻酸丙二醇酯与羟丙基甲基纤维素或亚麻籽胶的比较及联合作用
IF 1.6 4区 农林科学 Pub Date : 2023-02-01 DOI: 10.1515/ijfe-2022-0227
Xueting Chen, Jingyan Gao, G. Cao, Shule Guo, Dingning Lu, Bingbing Hu, Zuoqian Yang, Yi Tong, Chengrong Wen
Abstract Different methods are often used to make gluten-free (GF) bread to get better bread characteristics. To explore the effects of emulsifiers and hydrocolloids on the characteristics of GF dough, different esterification levels of propylene glycol alginate (PGA), hydroxypropyl methyl cellulose (HPMC), flaxseed gum with (FG) different molecular weight, and the binary blends of HPMC/PGA and FG/PGA were added to GF dough, made with potato starch and potato protein in a ratio of 6:4. The results showed that the potato GF dough with FG and FG/PGA obtained a higher viscoelasticity than the other doughs. HPMC and FG promoted to the formation of network structure, but the network structure formed by PGA and their combination was more developed. It was found that all PGA, HPMC, FG and their combination could improve the softness of GF breads. The results provided a basis for optimizing the quality of potato GF bread.
摘要为了获得更好的面包特性,人们经常采用不同的方法制作无麸质面包。为了探讨乳化剂和水胶体对GF面团特性的影响,将不同酯化水平的海藻酸丙二醇酯(PGA)、羟丙基甲基纤维素(HPMC)、不同分子量的亚麻籽胶以及HPMC/PGA和FG/PGA二元共混物加入到以马铃薯淀粉和马铃薯蛋白按6:4的比例制成的GF面团中。结果表明,添加FG和FG/PGA的马铃薯GF面团比其他面团具有更高的粘弹性。HPMC和FG促进了网络结构的形成,但PGA及其组合形成的网络结构更为发达。结果表明,PGA、HPMC、FG及其组合均能提高GF面包的柔软度。研究结果为优化马铃薯GF面包的品质提供了依据。
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引用次数: 2
The influences of acidic electrolyzed water on quality and bacteria community of fresh-cut jackfruit in storage 酸性电解水对贮藏鲜切菠萝蜜品质及细菌群落的影响
IF 1.6 4区 农林科学 Pub Date : 2023-02-01 DOI: 10.1515/ijfe-2022-0210
Yangyang Yu, Yujuan Xu, Jijun Wu, Yuanshan Yu
Abstract This study evaluated the effects of acidic electrolyzed oxidizing water (AEW) on the quality and bacterial communities of fresh-cut jackfruit during storage. The result showed that AEW treatment, as compared to the CK group (without AEW treatment), could effectively inhibit the browning, maintain higher firmness and higher amounts of total titratable acidity (TTA) (0.21%), sugars (58.30 g/kg), ascorbic acids (28.72 mg/kg) and total phenolics (35.47 mg/kg) of fresh-cut jackfruits, and suppress the decrease of antioxidant ability during 4–8 days of storage. Additionally, the bacterial communities were significantly affected by AEW during storage. In particular, the AEW treated samples showed lower abundance of Pseudomonas and Lactobacillus than the CK group after storage of 8 day. And energy metabolism, nucleotide metabolism has the significantly lower (p < 0.05) relative abundance in the AEW group than in CK group. These results suggested that AEW (pH: 4.2–4.5, ACC: 35–38 mg/L) treatment could maintain the quality of fresh-cut jackfruit during storage. It could be attributed to that AEW treatment affect the growth and metabolism of bacterial communities, resulting in the decrease of nutrients consumption.
摘要本研究研究了酸性电解氧化水(AEW)对鲜切菠萝蜜贮藏期间品质和细菌群落的影响。结果表明,与CK组相比,AEW处理能有效抑制菠萝蜜褐变,在贮藏4 ~ 8 d期间保持较高的硬度和较高的总可滴定酸度(TTA)(0.21%)、糖(58.30 g/kg)、抗坏血酸(28.72 mg/kg)和总酚(35.47 mg/kg),抑制抗氧化能力下降。此外,在贮藏过程中,AEW对细菌群落有显著影响。贮藏8 d后,AEW处理的样品中假单胞菌和乳酸杆菌的丰度低于CK组。AEW组能量代谢、核苷酸代谢相对丰度显著低于CK组(p < 0.05)。结果表明,AEW (pH: 4.2 ~ 4.5, ACC: 35 ~ 38 mg/L)处理能保持鲜切菠萝蜜的贮藏品质。这可能是由于AEW处理影响了细菌群落的生长和代谢,导致养分消耗减少。
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引用次数: 0
Frontmatter 头版头条
4区 农林科学 Pub Date : 2023-02-01 DOI: 10.1515/ijfe-2023-frontmatter1-2
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引用次数: 0
Effect of water-retention agents on Scomberomorus niphonius surimi after repeated freeze–thaw cycles: low-field NMR and MRI studies 保水剂对日本Scomberomorus鱼糜重复冻融循环后的影响:低场NMR和MRI研究
IF 1.6 4区 农林科学 Pub Date : 2023-02-01 DOI: 10.1515/ijfe-2022-0270
Shan Sun, Zhuyi Lin, Shasha Cheng, A. M. Abd El-Aty, M. Tan
Abstract Repeated freeze–thaw cycles can directly cause the changes in the water distribution, physicochemical characteristics, and microstructure of Scomberomorus niphonius surimi. To improve the quality of S. niphonius surimi, the effect of water retention agents (phosphate and trehalose) was investigated during freeze-thaw cycles. The results of low-field nuclear magnetic resonance (LF-NMR) combined with magnetic resonance imaging (MRI) analysis showed that the water retention agents could obviously decrease the water loss and water mobility during repeated freeze–thaw cycles. Water retention agent significantly reduced the cook loss and improved the surimi quality by decreasing the surimi protein denaturation. The scanning electron microscopy (SEM) characterization revealed that water retention agents could obviously ameliorate the protein structure damage. In addition, the principal component analysis combined with LF-NMR parameters showed clear discrimination between samples supplemented with different water retention agents. In a word, the LF-NMR and MRI might provide useful information in a non-invasive manner for monitoring the effects of water-retention agents on surimi after repeated freeze–thaw cycles.
摘要反复冻融循环可直接导致日本Scomberomorus鱼糜水分分布、理化特性和微观结构的变化。为了提高日本鱼糜的质量,研究了保水剂(磷酸盐和海藻糖)在冻融循环中的作用。低场核磁共振(LF-NMR)与核磁共振成像(MRI)分析相结合的结果表明,保水剂在反复冻融循环中可以显著降低水分损失和水分流动性。保水剂通过降低鱼糜蛋白质变性,显著降低煮失量,改善鱼糜品质。扫描电子显微镜(SEM)表征表明,保水剂能明显改善蛋白质结构损伤。此外,结合LF-NMR参数的主成分分析显示,添加不同保水剂的样品之间有明显的区别。总之,LF-NMR和MRI可能以非侵入性的方式提供有用的信息,用于监测重复冻融循环后保水剂对鱼糜的影响。
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引用次数: 1
Dietary modeling of greenhouse gases using OECD meat consumption/retail availability estimates 使用经合组织肉类消费/零售可用性估计的温室气体饮食建模
IF 1.6 4区 农林科学 Pub Date : 2023-01-25 DOI: 10.1515/ijfe-2021-0352
S. Lincke, Joy J. Wolf
Abstract Research has demonstrated different carbon footprints, based on portion estimations. However, previous estimates are low and often omit the impact of food waste. For example, a high-level of daily meat consumption has been estimated at 100 g, which is less than a typical “quarter pounder” hamburger. We used the Organization for Economic Co-operation and Development (OECD) annual estimates of national retail availability, and applied a mathematical model to prorate other research results to determine a meat portion equal to current OECD statistics, and also projected the diets to 2500 and 3250 kcal, to include consumer and retail waste. Once prorated, the 14 national studies are contrasted and analyzed for reasonableness against OECD data pertaining to U.S., U.K., E.U., vegetarian and vegan diets. We quantify how previous studies underestimated greenhouse gas (GHG) emissions and show that previous GHG study results for the highest tier most accurately predict average national dietary consumption.
摘要研究已经证明了不同的碳足迹,基于部分估计。然而,以前的估计数很低,往往忽略了食物浪费的影响。例如,据估计,高水平的每日肉类消费量为100克,比典型的“四分之一磅”汉堡还少。我们使用了经济合作与发展组织(OECD)对全国零售供应量的年度估计,并应用数学模型按比例分配其他研究结果,以确定与当前经合组织统计数据相等的肉类份额,还预测了2500和3250千卡的饮食,包括消费者和零售废物。一旦按比例分配,将14项国家研究与经合组织关于美国、英国、欧盟、素食和纯素饮食的数据进行对比和分析,以确定其合理性。我们量化了之前的研究是如何低估温室气体排放的,并表明之前最高级别的温室气体研究结果最准确地预测了全国平均饮食消费。
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引用次数: 0
An application of citric acid as a carrier for solid dispersion to improve the dissolution and uric acid-lowering effect of kaempferol 应用柠檬酸作为固体分散载体,提高山奈酚的溶出度和降尿酸效果
IF 1.6 4区 农林科学 Pub Date : 2023-01-19 DOI: 10.1515/ijfe-2022-0214
Danni Song, Chang-ming Xie, Rong Yang, Aijinxiu Ma, Honghui Zhao, Fengmao Zou, Xiangrong Zhang, Xu-Jie Zhao
Abstract Kaempferol (KPF) is a flavonoid compound, which has a variety of pharmacological activities, and widely exists in daily diet. However, its application is limited due to poor solubility. Citric acid (CA) is a common food additive with high solubility. In this study, solid dispersion (SD) was prepared with CA as the carrier to improve the solubility of KPF. KPF-CA-SD (weight ratio 1:20) was obtained by ultrasonic for 20 min at 40 °C. The in vitro dissolution of KPF in SD was increased from about 50% to more than 80%. The physicochemical characterizations were analyzed by X-ray diffraction, differential scanning calorimetry, Fourier transform infrared spectroscopy, and scanning electron microscope. In hyperuricemia mice, KPF-SD (equivalent to 100 mg/kg KPF) can effectively reduce serum uric acid and exert nephroprotective effects. In conclusion, the preparation of SD with CA might provide a safe and effective selection to facilitate application of KPF in food and medicine.
山奈酚是一种黄酮类化合物,具有多种药理活性,广泛存在于日常饮食中。然而,由于溶解性差,其应用受到限制。柠檬酸是一种常见的高溶解度食品添加剂。本研究以CA为载体制备了固体分散体(SD),以提高KPF的溶解度。通过在40°C下超声20分钟获得KPF-CA-SD(重量比1:20)。KPF在SD中的体外溶出度从约50%增加到80%以上。通过X射线衍射、差示扫描量热法、傅立叶变换红外光谱和扫描电子显微镜对其理化性质进行了分析。在高尿酸血症小鼠中,KPF-SD(相当于100mg/kg KPF)可以有效降低血清尿酸并发挥肾保护作用。总之,用CA制备SD可能为促进KPF在食品和药物中的应用提供一种安全有效的选择。
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引用次数: 0
Alginate and β-lactoglobulin matrix as wall materials for encapsulation of polyphenols to improve efficiency and stability 海藻酸盐和β-乳球蛋白基质作为壁材包埋多酚,提高效率和稳定性
IF 1.6 4区 农林科学 Pub Date : 2022-12-12 DOI: 10.1515/ijfe-2022-0202
R. Sasikumar, Paras Sharma, A. Jaiswal
Abstract The present study aimed at developing novel encapsulate materials of calcium-alginate and β-lactoglobulin complex for polyphenols using the jet-flow nozzle vibration method. Encapsulated microbeads were characterized using SEM, FTIR, DSC, and MSI. The encapsulation efficiency of the microbeads varied depending upon the coating material in the range of 74.17–84.87%. Calcium-alginate-β-lactoglobulin microbeads (CABM) exhibited a smooth surface and uniform shape with an average particle size of 1053.73 nm. CABM also showed better thermal and storage stabilities as compared to calcium alginate microbeads. The CABM resulted in excellent target release of polyphenols (84%) in the intestine, which was more than 3-fold the bio-accessibility offered by free polyphenol powder. Further study on individual phenolic acids after simulated in-vitro digestion (SIVD), photo-oxidative and osmotic stress revealed that CABM significantly retained a higher amount of polyphenols and exhibited improved antioxidant capacity after SIVD environment, and may have high industrial application for nutraceutical production.
摘要本研究旨在利用射流喷嘴振动法制备海藻酸钙- β-乳球蛋白复合物多酚包封材料。采用扫描电镜(SEM)、红外光谱(FTIR)、差示量热分析(DSC)和微细扫描(MSI)对微珠进行了表征。微珠的包封率随包封材料的不同而变化,包封率在74.17 ~ 84.87%之间。海藻酸钙-β-乳球蛋白微球(CABM)表面光滑,形状均匀,平均粒径为1053.73 nm。与海藻酸钙微球相比,CABM还表现出更好的热稳定性和储存稳定性。CABM可使多酚在肠道内的靶释放率达到84%,是游离多酚粉末的3倍以上。在体外模拟消化(SIVD)、光氧化和渗透胁迫下对单个酚酸的进一步研究表明,经过SIVD环境后,CABM显著保留了更多的多酚,并表现出更强的抗氧化能力,可能在营养保健产品的工业生产中具有很高的应用价值。
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引用次数: 1
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International Journal of Food Engineering
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