Pub Date : 2022-08-23DOI: 10.32734/jcnar.v3i1.9337
E. Zaidar
The preparation of edible film from carrot extracts (Daucus Carota, L) with the addition of tapioca flour, wheat flour, and glycerin was carried out. The edible film was prepared by mixing carrot extract, tapioca flour, and wheat flour, and then heated and added with glycerin and stirred up. The homogeneous solution was put into an acrylic plate to form an edible film and dried in an oven at 40oC for ± 2 days. The edible film formed was characterized and analyzed its nutrition content. The tensile strength and elasticity of edible film with a ratio of 5 g tapioca flour and 5 g wheat flour were 0.1028 KgF/mm2 and 39.83% respectively. The thickness of edible film with a ratio of 2.5 g of tapioca flour and 7.5 g of wheat flour 7.5 g was 0.26 mm. The better nutrition content was found on edible film with a ratio of 5 g tapioca flour and 5 g wheat flour which has 13.94% moisture content, 2.67% ash content, 4.93% protein content, and 2.90% fat, 75.56% carbohydrate content, and 410.34 ppm carotene content. Organoleptic test edible film of color, taste, texture, and aroma gave an average score of 3 (like), because of the shiny color, crunchy taste, smooth texture, and interesting edible film. Based on the test indicated that people accepted the edible film produced.
{"title":"Preparation of Edible Film from A Mixture of Carrot Extract (Daucus carota L.) with Tapioca Flour, Wheat Flour, and Glycerine","authors":"E. Zaidar","doi":"10.32734/jcnar.v3i1.9337","DOIUrl":"https://doi.org/10.32734/jcnar.v3i1.9337","url":null,"abstract":"The preparation of edible film from carrot extracts (Daucus Carota, L) with the addition of tapioca flour, wheat flour, and glycerin was carried out. The edible film was prepared by mixing carrot extract, tapioca flour, and wheat flour, and then heated and added with glycerin and stirred up. The homogeneous solution was put into an acrylic plate to form an edible film and dried in an oven at 40oC for ± 2 days. The edible film formed was characterized and analyzed its nutrition content. The tensile strength and elasticity of edible film with a ratio of 5 g tapioca flour and 5 g wheat flour were 0.1028 KgF/mm2 and 39.83% respectively. The thickness of edible film with a ratio of 2.5 g of tapioca flour and 7.5 g of wheat flour 7.5 g was 0.26 mm. The better nutrition content was found on edible film with a ratio of 5 g tapioca flour and 5 g wheat flour which has 13.94% moisture content, 2.67% ash content, 4.93% protein content, and 2.90% fat, 75.56% carbohydrate content, and 410.34 ppm carotene content. Organoleptic test edible film of color, taste, texture, and aroma gave an average score of 3 (like), because of the shiny color, crunchy taste, smooth texture, and interesting edible film. Based on the test indicated that people accepted the edible film produced.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"39 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90401195","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-08-23DOI: 10.32734/jcnar.v3i1.9341
A. Ginting
Essential oil of Baru Cina leaves (Artemisia vulgaris L.) has been successfully isolated by hydrodistillation method using the Stahl apparatus. Baru Cina leaves were hydrodistillation for ± 6 hours to produce the essential oil amount of 0.39 % (v/b). The essential oil obtained from Baru Cina leaves was characterized by using GC-MS spectroscopy. The GC-MS analysis results showed that there were 29 compounds and the main compounds identified as many as 14 compounds, such as Alpha-Pinene (0.33%), 1,8-Cineol (1.96% ), Filifoline (1.41 %), 1-Octen-3-Ol (2.99 %), 2,4-Cycloheptadien-1-0ne (Eucarvone) (30.61 %), 2-Cyclohexen-1-Ol (Cis) (2.86 %), Bicyclo-3,3,1-Hepta-3-One (1.62 %), Trans-Caryophyllene (4.82 %), 3-Cyclohexen-1-Ol (1, 71 %), 2-Cyclohexen-1-Ol(Trans) (2.75 %), 2-Cyclohexen-1-One (Piperitone) (30.92 %), Trans Carveol (0.31%), Ar-Dimethylphenethyl Alcohol (0.88%), Eugenol (2.42%). This study also showed antioxidant activity from the essential oil of Baru Cina leaves with the IC50 value was 95.76 mg/L.
{"title":"Isolation and Analysis of Chemical Components of Essential Oil of Baru Cina (Artemisia vulgaris L) Leaves and Antioxidant Activities Test","authors":"A. Ginting","doi":"10.32734/jcnar.v3i1.9341","DOIUrl":"https://doi.org/10.32734/jcnar.v3i1.9341","url":null,"abstract":"Essential oil of Baru Cina leaves (Artemisia vulgaris L.) has been successfully isolated by hydrodistillation method using the Stahl apparatus. Baru Cina leaves were hydrodistillation for ± 6 hours to produce the essential oil amount of 0.39 % (v/b). The essential oil obtained from Baru Cina leaves was characterized by using GC-MS spectroscopy. The GC-MS analysis results showed that there were 29 compounds and the main compounds identified as many as 14 compounds, such as Alpha-Pinene (0.33%), 1,8-Cineol (1.96% ), Filifoline (1.41 %), 1-Octen-3-Ol (2.99 %), 2,4-Cycloheptadien-1-0ne (Eucarvone) (30.61 %), 2-Cyclohexen-1-Ol (Cis) (2.86 %), Bicyclo-3,3,1-Hepta-3-One (1.62 %), Trans-Caryophyllene (4.82 %), 3-Cyclohexen-1-Ol (1, 71 %), 2-Cyclohexen-1-Ol(Trans) (2.75 %), 2-Cyclohexen-1-One (Piperitone) (30.92 %), Trans Carveol (0.31%), Ar-Dimethylphenethyl Alcohol (0.88%), Eugenol (2.42%). This study also showed antioxidant activity from the essential oil of Baru Cina leaves with the IC50 value was 95.76 mg/L.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"254 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72757587","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-08-23DOI: 10.32734/jcnar.v3i1.9339
S. Lenny
Isolation of flavonoid compounds from leaves of Bangun-bangun (Plectranthus amboinicus (Lour.) Spreng.) has been conducted by maceration process with methanol solvent, added with ethyl acetate, and then partially extracted with n-hexane, acided by HCl 6% and partition extracted with chloroform. The concentrated extract of chloroform was separated using column chromatography with eluent n-hexane: ethyl acetate. The resulted tawny paste yielding was 10 mg with Rf= 0.38. The resulted compounds were characterized using UV-Vis, FT-IR, and 1H-NMR which was estimated as a flavonoid is a flavanone.
{"title":"Isolation of Flavonoid Compounds from Bangun-bangun Leaves (Plectranthus amboinicus (Lour.) Spreng.)","authors":"S. Lenny","doi":"10.32734/jcnar.v3i1.9339","DOIUrl":"https://doi.org/10.32734/jcnar.v3i1.9339","url":null,"abstract":"Isolation of flavonoid compounds from leaves of Bangun-bangun (Plectranthus amboinicus (Lour.) Spreng.) has been conducted by maceration process with methanol solvent, added with ethyl acetate, and then partially extracted with n-hexane, acided by HCl 6% and partition extracted with chloroform. The concentrated extract of chloroform was separated using column chromatography with eluent n-hexane: ethyl acetate. The resulted tawny paste yielding was 10 mg with Rf= 0.38. The resulted compounds were characterized using UV-Vis, FT-IR, and 1H-NMR which was estimated as a flavonoid is a flavanone.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"26 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90535417","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-08-23DOI: 10.32734/jcnar.v3i1.9335
H. Sihotang
Synthesis of 2-((furan-2-yl) methylene)-1-phenylhydrazone has been carried out by reaction of condensation of furfural aldehyde groups obtained from the isolation of corn cobs with phenylhydrazine. Furfural condensation with phenylhydrazine was carried out by refluxing in ethanol solvent for 1 hour. Of the 9.6 g (0.1 mol) furfural which was condensed with 5.4 g (0.05 mol) phenylhydrazine obtained yield of 10.54 g (67.02%) phenylhydrazone which was then analyzed by FT-IR spectroscopy showing the presence of vibration C = N in the area around 1597 cm-1. Fenilhidrazone was tested for inhibitor with 78.47% and compared with furfural as much as 58.18%, and phenylhydrazine as much as 50.04%. The results obtained by phenylhydrazone were more efficient at inhibiting the results of 78.47% while furfural and phenylhydrazine were only 58.18% and 50.04%.
以玉米芯分离得到的糠醛基团与苯肼缩合为原料，合成了2-((呋喃-2-基)亚甲基-1-苯腙。糠醛与苯肼在乙醇溶剂中回流反应1小时。将9.6 g (0.1 mol)糠醛与5.4 g (0.05 mol)苯肼缩合，得到10.54 g(67.02%)苯腙，并通过红外光谱分析，发现在1597 cm-1附近存在振动C = N。fenilhidra酮的抑制率为78.47%，而糠醛的抑制率为58.18%，苯肼的抑制率为50.04%。苯腙的抑制率为78.47%，糠醛和苯肼的抑制率分别为58.18%和50.04%。
{"title":"Synthesis 2-((Furan-2-yl) Methylene)-1-Phenilhydrazone from Furfural Results of Corn Isolation and Its Utilization as Corrosion Inhibitor in Zinc (Zn) Metal","authors":"H. Sihotang","doi":"10.32734/jcnar.v3i1.9335","DOIUrl":"https://doi.org/10.32734/jcnar.v3i1.9335","url":null,"abstract":"Synthesis of 2-((furan-2-yl) methylene)-1-phenylhydrazone has been carried out by reaction of condensation of furfural aldehyde groups obtained from the isolation of corn cobs with phenylhydrazine. Furfural condensation with phenylhydrazine was carried out by refluxing in ethanol solvent for 1 hour. Of the 9.6 g (0.1 mol) furfural which was condensed with 5.4 g (0.05 mol) phenylhydrazine obtained yield of 10.54 g (67.02%) phenylhydrazone which was then analyzed by FT-IR spectroscopy showing the presence of vibration C = N in the area around 1597 cm-1. Fenilhidrazone was tested for inhibitor with 78.47% and compared with furfural as much as 58.18%, and phenylhydrazine as much as 50.04%. The results obtained by phenylhydrazone were more efficient at inhibiting the results of 78.47% while furfural and phenylhydrazine were only 58.18% and 50.04%.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"532 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86922118","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-08-23DOI: 10.32734/jcnar.v3i1.9336
S. Lenny
Isolation of flavonoid compound from Suren leaves (Toona sureni) has been done using the extraction method. The suren leaves extract was separated by using the column chromatography method. The isolated compound results were yellow paste with weight 47 from fraction 55-67 and Rf = 0.44 of eluent n-hexane: ethylacetate 60:40 (v/v). The identification process was analyzed by UV-Vis, FT-IR spectroscopy, and 1H-NMR spectroscopy. The obtained result shows that the isolated compound was isoflavone.
{"title":"Isolation of Flavonoid Compounds from Suren Leaves (Toona sureni)","authors":"S. Lenny","doi":"10.32734/jcnar.v3i1.9336","DOIUrl":"https://doi.org/10.32734/jcnar.v3i1.9336","url":null,"abstract":"Isolation of flavonoid compound from Suren leaves (Toona sureni) has been done using the extraction method. The suren leaves extract was separated by using the column chromatography method. The isolated compound results were yellow paste with weight 47 from fraction 55-67 and Rf = 0.44 of eluent n-hexane: ethylacetate 60:40 (v/v). The identification process was analyzed by UV-Vis, FT-IR spectroscopy, and 1H-NMR spectroscopy. The obtained result shows that the isolated compound was isoflavone.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"28 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76974153","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-08-28DOI: 10.32734/jcnar.v1i2.1252
F. Sebayang
The utilization of carboxymethyl cellulose (CMC) from groundnut (Arachis hypogaea L) cellulose as stabilizer for cow milk yogurt has been done in three steps. The first step was α-cellulose isolation from groundnut skin powder which was analysed with FTIR. The result was compared to FTIR analysis of commercial cellulose to verify the compound obtained is cellulose. The second step involves alkalization process using isopropanol and NaOH, carboxymethylation process with sodium chloroacetate (NaMCA), neutralization using CH3COOH 90% and ethanol, purification with aquadest and followed by centrifugation and addition of acetone to produce carboxymethyl cellulose. The CMC produced gave positive result in the qualitative anlysis, the FTIR spectrum was similar to commercial CMC and the degree of substitution obtained was 0.71. The last step is yogurt making process. In this stage, the CMC concentration added was varied from 0 – 0.5%. Then, the yogurt produced went through quality analysis such as syneresis, pH, viscosity, protein, fat content and organoleptic tests. The best result was obtained at the addition of 0.5% CMC concentration with 7.69% and 2.11% protein and fat content, pH 4.6, viscosity was 1676.01 x 102 cP, low syneresis with 90.66% stability and 22 days of storage life. Organoleptic result shows that yogurt with 0.3% CMC addition gave the best result with distinctive aroma and sourness, and rather thick texture. The panelists preferred such yogurt to others. The quality analysis for yogurt with CMC stabilizer still meets SNI standard. [Use 10 pt Times New Roman for the abstract body with single spacing and 10 pt spacing for the next heading. Left indent is 2 cm and right indent is 0 cm. Please write abstract paper in English with maximum length is 200 words.
以花生羧甲基纤维素(CMC)为原料，分三步研究了其在牛奶酸奶中的稳定作用。第一步从花生皮粉中分离α-纤维素，用FTIR对其进行分析。结果与工业纤维素的FTIR分析结果进行了比较，验证了所得化合物为纤维素。第二步:异丙醇和NaOH碱化，氯乙酸钠(NaMCA)羧甲基化，90% CH3COOH和乙醇中和，aquadest纯化，离心加丙酮制羧甲基纤维素。所制CMC定性分析结果为阳性，FTIR光谱与市售CMC相似，取代度为0.71。最后一步是酸奶制作过程。在这一阶段，CMC的添加浓度在0 - 0.5%之间变化。然后，对生产的酸奶进行了质量分析，如协同作用、pH值、粘度、蛋白质、脂肪含量和感官测试。结果表明，添加0.5% CMC，蛋白和脂肪含量分别为7.69%和2.11%，pH为4.6，粘度为1676.01 × 102 cP，低协同作用，稳定性为90.66%，保鲜期为22 d。感官测试结果表明，添加0.3% CMC的酸奶效果最佳，香气和酸味独特，质地较厚。与其他酸奶相比，小组成员更喜欢这种酸奶。添加CMC稳定剂的酸奶质量分析仍符合SNI标准。摘要正文使用10 pt Times New Roman，间距为1，下一个标题使用10 pt spacing。左缩进为2厘米，右缩进为0厘米。请用英文撰写论文摘要，不超过200字。
{"title":"The Utilization of Carboxymethyl Cellulose (Cmc) from Groundnut (Arachis Hypogaea L) Cellulose as Stabilizer for Cow Milk Yogurt","authors":"F. Sebayang","doi":"10.32734/jcnar.v1i2.1252","DOIUrl":"https://doi.org/10.32734/jcnar.v1i2.1252","url":null,"abstract":"The utilization of carboxymethyl cellulose (CMC) from groundnut (Arachis hypogaea L) cellulose as stabilizer for cow milk yogurt has been done in three steps. The first step was α-cellulose isolation from groundnut skin powder which was analysed with FTIR. The result was compared to FTIR analysis of commercial cellulose to verify the compound obtained is cellulose. The second step involves alkalization process using isopropanol and NaOH, carboxymethylation process with sodium chloroacetate (NaMCA), neutralization using CH3COOH 90% and ethanol, purification with aquadest and followed by centrifugation and addition of acetone to produce carboxymethyl cellulose. The CMC produced gave positive result in the qualitative anlysis, the FTIR spectrum was similar to commercial CMC and the degree of substitution obtained was 0.71. The last step is yogurt making process. In this stage, the CMC concentration added was varied from 0 – 0.5%. Then, the yogurt produced went through quality analysis such as syneresis, pH, viscosity, protein, fat content and organoleptic tests. The best result was obtained at the addition of 0.5% CMC concentration with 7.69% and 2.11% protein and fat content, pH 4.6, viscosity was 1676.01 x 102 cP, low syneresis with 90.66% stability and 22 days of storage life. Organoleptic result shows that yogurt with 0.3% CMC addition gave the best result with distinctive aroma and sourness, and rather thick texture. The panelists preferred such yogurt to others. The quality analysis for yogurt with CMC stabilizer still meets SNI standard. [Use 10 pt Times New Roman for the abstract body with single spacing and 10 pt spacing for the next heading. Left indent is 2 cm and right indent is 0 cm. Please write abstract paper in English with maximum length is 200 words.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"50 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-08-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74977835","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-08-28DOI: 10.32734/jcnar.v1i2.1251
D. R. Gusti
Surface coverage and corrosion rate of taro tuber methanol extract on mild steel in dilute 0.5 M sulfuric acid solution were studied through weight loss method, FT-IR spectroscopy and SEM.The result obtained in 0.5 M sulfuric acid solution for 72 hours with optimal surface coveragewas 0.86. The corrosion ratewas found to be decreased and surface coveragewas increased with the increasing concentration of taro tuber methanol extract which was added. The results showed that taro tuber methanol extract was a good corrosion inhibitor.
{"title":"The Surface Coverage and Corrosive Rate of Methanol Extract from Taro Tuber (Colocasia esculenta) on Mild Steel in Sulfuric Acid","authors":"D. R. Gusti","doi":"10.32734/jcnar.v1i2.1251","DOIUrl":"https://doi.org/10.32734/jcnar.v1i2.1251","url":null,"abstract":"Surface coverage and corrosion rate of taro tuber methanol extract on mild steel in dilute 0.5 M sulfuric acid solution were studied through weight loss method, FT-IR spectroscopy and SEM.The result obtained in 0.5 M sulfuric acid solution for 72 hours with optimal surface coveragewas 0.86. The corrosion ratewas found to be decreased and surface coveragewas increased with the increasing concentration of taro tuber methanol extract which was added. The results showed that taro tuber methanol extract was a good corrosion inhibitor.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"41 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-08-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83090479","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-08-28DOI: 10.32734/jcnar.v1i2.1250
Desy Kurniawaty
In this study, the effect of of Cd(II) in biosorption of Pb(II) by lengkeng seed and sheel from a binary metal mixture was studied and compared with the single metal ion situation and other way. The purpose studied by the metal ion competition in the solution is to know the effect and the absorption capacity of one type of metal ion in a solution containing several metal ions inside which will be applied to the waste. The optimum conditions used were for Pb at pH 3 and Cd at pH 5 with a particle size of 250μm. The results showed a decrease in the absorption of Pb metal ions reached 42.14% (for lengkeng sheel) and 57.07% (for lengkeng seed). And decrease of Cd metal ion to 68,11% for seed and 64,77% for lengkeng shell.
{"title":"Effect of Cadmium in Biosorption of Lead by Lengkeng Seed and Shell (Euphoria logan lour)","authors":"Desy Kurniawaty","doi":"10.32734/jcnar.v1i2.1250","DOIUrl":"https://doi.org/10.32734/jcnar.v1i2.1250","url":null,"abstract":"In this study, the effect of of Cd(II) in biosorption of Pb(II) by lengkeng seed and sheel from a binary metal mixture was studied and compared with the single metal ion situation and other way. The purpose studied by the metal ion competition in the solution is to know the effect and the absorption capacity of one type of metal ion in a solution containing several metal ions inside which will be applied to the waste. The optimum conditions used were for Pb at pH 3 and Cd at pH 5 with a particle size of 250μm. The results showed a decrease in the absorption of Pb metal ions reached 42.14% (for lengkeng sheel) and 57.07% (for lengkeng seed). And decrease of Cd metal ion to 68,11% for seed and 64,77% for lengkeng shell.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"8 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-08-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78084736","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-08-28DOI: 10.32734/jcnar.v1i2.1256
Masriani
Cancer has been considered as problematic medical issues both in developed and developing countries. Pycnarrhena cauliflora or Sengkubak (Pycnarrhena cauliflora) has a potential value as alternatives for anticancer medication. This study aims to evaluate the cytotoxic activities of Sengkubak (Pycnarrhena cauliflora), and investigate the induction for apoptosis mechanisms from the extracts n-hexane, dichloromethane, and methanol from roots, branches the leaves to HeLa cancer cells. The cytotoxic activities were analyzed by performing MTT methods, while induction analysis of apoptosis was conducted by utilizing the Acridine Orange/Ethidium Bromide (AO/EB) as visual nuclear methodologies. The extracts of roots dichloromethane showed the highest cytotoxic activities accounted for IC50 70µg/mL and these extracts were able to induce the apoptosis mechanisms. This study concludes that the Sengkubak (Pycnarrhena cauliflora) has the ability as a potential alternative for anticancer medications.
{"title":"The Cytotoxic Activities of the Extracts of Sengkubak (Pycnarrhena cauliflora) As Apoptosis Inducers to Hela Cervical Cancer Cells","authors":"Masriani","doi":"10.32734/jcnar.v1i2.1256","DOIUrl":"https://doi.org/10.32734/jcnar.v1i2.1256","url":null,"abstract":"Cancer has been considered as problematic medical issues both in developed and developing countries. Pycnarrhena cauliflora or Sengkubak (Pycnarrhena cauliflora) has a potential value as alternatives for anticancer medication. This study aims to evaluate the cytotoxic activities of Sengkubak (Pycnarrhena cauliflora), and investigate the induction for apoptosis mechanisms from the extracts n-hexane, dichloromethane, and methanol from roots, branches the leaves to HeLa cancer cells. The cytotoxic activities were analyzed by performing MTT methods, while induction analysis of apoptosis was conducted by utilizing the Acridine Orange/Ethidium Bromide (AO/EB) as visual nuclear methodologies. The extracts of roots dichloromethane showed the highest cytotoxic activities accounted for IC50 70µg/mL and these extracts were able to induce the apoptosis mechanisms. This study concludes that the Sengkubak (Pycnarrhena cauliflora) has the ability as a potential alternative for anticancer medications.","PeriodicalId":15309,"journal":{"name":"Journal of Chemical Natural Resources","volume":"32 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-08-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87497279","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-08-28DOI: 10.32734/jcnar.v1i2.1248
A. Ginting
Cellulose was isolated from plantain skin and then carboxymethylated with trichloroacetic acid which resulted a 0.9936 gram of carboxymethylcellulose. The FT-IR spectroscopy analysis of carboxymethyltricellulose indicated the –OH vibration at wavelength of 3448.72 cm-1.Moreover, a wavenumber in the region of 1026.13 cm-1 is attributed to ether vibration (-O-) and carboxyl vibration at 1651.07 cm-1. The results of morphological analysis using SEM also showed a smoother, homogeneous pore, and a larger surface area. The adsorption capability for Cu2+ ions at concentration of 100 ppm was analyzed by atomic adsorption spectrophotometer (AAS). It shows that the optimum adsorption was found to be at a 90 minutes agitation process for both carboxymethyltricellulose and cellulose with about 97.266% and 21.602% respectively.
从车前草皮中分离纤维素，用三氯乙酸进行羧甲基化，得到0.9936 g羧甲基纤维素。羧基甲基三纤维素在3448.72 cm-1波长处存在-OH振动。此外，1026.13 cm-1区域的波数归属于醚振动(- o -)和羧基振动(1651.07 cm-1)。SEM形貌分析结果也显示出更光滑、均匀的孔隙和更大的表面积。采用原子吸附分光光度计(AAS)分析了其对浓度为100ppm的Cu2+离子的吸附能力。结果表明，搅拌时间为90 min时，羧甲基三纤维素和纤维素的最佳吸附率分别为97.266%和21.602%。
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