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Detection of an emerging contaminant in water by dielectric properties in microwave range 利用微波介电特性检测水中一种新出现的污染物
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-10-01 DOI: 10.1080/08327823.2020.1838047
E. Hernández-Gómez, J. Olvera-Cervantes, A. Corona‐Chavez, B. Corona-Vasquez, T. Kataria, M. Sosa‐Morales
Abstract The complex relative permittivity study of samples of liberdux® syrup dissolved in distilled–deionized water is presented. It should be mentioned that excess of this syrup as pharmaceutical residual in water is considered an emerging contaminant. The study covers liberdux® concentrations from 0% v/v to 100% v/v, which were measured from 500 MHz to 20 GHz. For each sample, the parameters of the Havriliak–Negami model are presented in the range of measurement. Also, the uncertainty study was carried out to determine the sensitivity of the open coaxial probe and it was established that, for concentrations between 8% v/v and 100% v/v, it is possible to determine the concentration of liberdux® in water by the dielectric constant and the loss factor. In addition, a linear relationship was found between the concentration of liberdux® and the α parameter of the Havriliak–Negami model. The study of liberdux® concentrations was also performed with a spectrophotometer and the Beer–Lambert equation. It was established that the spectrophotometer and the open coaxial probe can be used as complements to measure concentrations, the spectrophotometer being the instrument for measuring low concentrations by absorbance, and the open coaxial probe for high concentrations by microwave permittivity.
摘要对利必达糖浆在去离子水中溶解的复相对介电常数进行了研究。应该提到的是,过量的糖浆作为药物残留在水中被认为是一种新出现的污染物。该研究涵盖了从0% v/v到100% v/v的liberdux®浓度,测量频率为500 MHz至20 GHz。对于每个样本,Havriliak-Negami模型的参数都在测量范围内。此外,还进行了不确定度研究以确定开放式同轴探头的灵敏度,并确定了在8% v/v和100% v/v之间的浓度下,可以通过介电常数和损耗因子来确定水中liberdux®的浓度。此外,在Havriliak-Negami模型中,liberdux®的浓度与α参数之间存在线性关系。用分光光度计和Beer-Lambert方程对利必达®的浓度进行了研究。建立了分光光度计与开放式同轴探头互为补充的浓度测量方法,分光光度计通过吸光度测量低浓度,开放式同轴探头通过微波介电常数测量高浓度。
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引用次数: 0
Effect of input microwave power and insulation on microstructure and tensile properties of cast Al 7039 alloy produced at 2.45 GHz 输入微波功率和绝缘对2.45 GHz铸造Al 7039合金组织和拉伸性能的影响
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-10-01 DOI: 10.1080/08327823.2020.1838049
R. Mishra, A. Sharma
Abstract In the present work, microwave energy was used for casting Al 7039 alloy at 2.45 GHz in the ambient cavity environment. Effects of input power and insulation of the mould assembly during irradiation on charge melting and mould preheating were studied. Five different casts were produced at 1000 W, 1200 W, 1400 W, 1400 W with an insulated pouring basin and 1400 W with insulated mould assembly. Melting time of the charge was the least while using 1400 W with insulated mould assembly, whereas preheating of the mould was observed minimum during casting at 1400 W inside an insulated pouring basin. Cast microstructures revealed that less preheating of the mould resulted in finer grains and intermetallics, which improve tensile properties of the cast. Fractographic analyses showed the presence of coarse intermetallics in the casts produced with insulated mould assembly, which resulted in significant reduction of tensile properties.
摘要:在常温空腔环境下,利用2.45 GHz微波能量铸造Al 7039合金。研究了辐照过程中输入功率和模具组件绝缘对装料熔化和模具预热的影响。生产了五种不同的铸件,分别为1000w、1200w、1400w、1400w带绝缘浇注盆和1400w带绝缘模具组件。当使用1400 W的绝缘模具组件时,装料的熔化时间最短,而在1400 W的绝缘浇注盆内浇注时,观察到模具的预热时间最短。铸型显微组织表明,减少模具预热使铸件的晶粒和金属间化合物更细小,从而提高了铸件的拉伸性能。断口分析表明,在使用绝缘模具组件生产的铸件中存在粗糙的金属间化合物,这导致拉伸性能显著降低。
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引用次数: 3
Editor’s message: the challenge of virus sanitizing with microwaves 编者的话:用微波炉消毒病毒的挑战
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-10-01 DOI: 10.1080/08327823.2020.1843986
J. Aguilar-Garib
Both microorganisms and viruses are germs; the difference is that the first ones are alive while the viruses are a sort of capsules with genetic material that reproduce themselves by replication in...
微生物和病毒都是细菌;不同之处在于,第一种病毒是活的,而病毒是一种带有遗传物质的胶囊,通过复制来繁殖自己。
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引用次数: 1
Dielectric properties, polarizability and molar refractive index of some VSrFeZnO glasses 几种VSrFeZnO玻璃的介电性能、极化率和摩尔折射率
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-10-01 DOI: 10.1080/08327823.2020.1838050
E. Ahmed, Bushra Al-Hasni
Abstract Dielectric properties of a set of glasses having the composition (70-x)%V2O5 - x%ZnO − 10%SrO − 20%FeO is studied in terms of their permittivity and electric modulus. The dielectric data are collected at the frequencies 120, 103, 104 and 105 Hz and in the temperature range 300 − 523 K. The electric moduli are treated with different theoretical models. Good fitting to the experimental data are obtained with Cole–Cole and Davidson–Cole equations. The static relaxation time τ0 values are found to vary between 7.6x10−9 sec and 22.7x10−9 sec, and the parameters α and γ are found to be (α = 0.056 − 0.065) and (γ = 0.94 − 0.95). The calculated optical basicity values are found to decrease with increasing the %ZnO. The molar refractive index is found to be between 2.6 and 3.2. The calculated single bond strength values suggest the transfer of bond nature from the covalent to the ionic form. The obtained third-order nonlinear optical susceptibility χ(3) results and electronic polarizability calculations suggests these glasses to be good nominees for nonlinear optical applications.
从介电常数和电模量的角度研究了(70-x)%V2O5 -x %ZnO - 10%SrO - 20%FeO玻璃的介电性能。电介质数据采集频率为120、103、104和105 Hz,温度范围为300 ~ 523 K。用不同的理论模型来处理电模量。用Cole-Cole方程和Davidson-Cole方程与实验数据拟合较好。静态弛豫时间τ0值在7.6 ~ 22.7x10−9 sec之间变化,参数α和γ分别为(α = 0.056 ~ 0.065)和(γ = 0.94 ~ 0.95)。计算出的光学碱度值随着ZnO含量的增加而减小。摩尔折射率在2.6 ~ 3.2之间。计算的单键强度值表明,键的性质从共价形式转移到离子形式。得到的三阶非线性光学磁化率χ(3)结果和电子极化率计算表明,这些玻璃是非线性光学应用的良好候选人。
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引用次数: 9
Editor’s message: a glance to virtual conferences 编辑的信息:浏览一下虚拟会议
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-28 DOI: 10.1080/08327823.2020.1800336
Juan Antonio Aguilar Garib
Coronavirus is a family of viruses, which are the cause of respiratory illnesses, and circulate among humans and animals. One of them, SARS-COV2, produces an illness known as COVID-19, which is ext...
冠状病毒是导致呼吸道疾病的病毒家族,在人类和动物之间传播。其中一种是SARS-COV2,它会产生一种被称为COVID-19的疾病,这是下一种…
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引用次数: 0
Determination and modelling of dielectric properties of the cherry leaves of varying moisture content over 3.30–7.05 GHz frequency range 3.30-7.05 GHz频率范围内不同含水率樱桃叶片介电特性的测定与建模
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-21 DOI: 10.1080/08327823.2020.1794724
Habib Dogan, I. Basyigit, A. Genç
Abstract In order to exploit the use of remote sensing, microwave heating/drying and water stress in the agricultural sector, it is necessary to determine the dielectric properties of plant materials (branches, leaves, roots, fruits). In this way, the yield and quality of agricultural products can be increased. In this study, dielectric parameters of the sweet cherry and sour cherry leaves are measured by waveguide transmission line Method. The dielectric properties of the leaves (varying moisture content) are measured over a frequency ranging from (3.30–7.05 GHz) using WR229 (3.30–4.90 GHz) and WR159 (4.90–7.05 GHz) waveguide structures. A novel curve fitting technique is used to characterize dielectric properties of sweet cherry leaves. In order to verify the accuracy of the model the data obtained using this methodology is compared with measurement data of sour cherry leaves belonging to the same family. The determination coefficient R2 of the model for WR229 and WR159 are 0.996 and 0.998, respectively. Similarly, the Root Mean Square Error (RMSE) values of the model for WR229 and WR159 are 0.852 and 0.236, respectively.
摘要为了在农业领域开发利用遥感、微波加热/干燥和水分胁迫,有必要对植物材料(枝、叶、根、果)的介电特性进行测定。这样,就可以提高农产品的产量和质量。本文采用波导传输线法测量了甜樱桃和酸樱桃叶片的介电参数。使用WR229 (3.30-4.90 GHz)和WR159 (4.90-7.05 GHz)波导结构在(3.30-7.05 GHz)频率范围内测量叶片的介电特性(不同含水量)。提出了一种新的曲线拟合方法来表征甜樱桃叶的介电特性。为了验证模型的准确性,将该方法获得的数据与同科酸樱桃叶片的测量数据进行了比较。WR229和WR159的模型决定系数R2分别为0.996和0.998。同样,WR229和WR159的模型均方根误差(RMSE)值分别为0.852和0.236。
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引用次数: 14
Equivalent analytical model of plain weave composite fabric for electromagnetic shielding applications 电磁屏蔽用平纹复合织物的等效解析模型
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-02 DOI: 10.1080/08327823.2020.1794722
A. O. Kizilçay, Y. Akinay
Abstract In this paper, the electromagnetic shielding effectiveness results of the plain weave composite fabric and the analytical solution of metal mesh were investigated. The composite fabric made of cotton yarns twisted with 50 µm copper filaments was used in the experiment. As the fabric was weaved and stretched, it had square shaped apertures which had length of 1.2 mm. The electromagnetic shielding effectiveness of these fabrics was measured in the frequency range of 1.7–2.6 GHz via WR430 waveguide system. In order to model the shielding results of the aforementioned fabric, an analytical solution which facilitates to calculate shielding effectiveness of metal mesh, was taken into consideration. Due to the physical similarity between the fabric geometry and metal mesh structure, the values of fabric characteristics were substituted in analytical solution. A statistical approach showed that the measured SE results of plain weave composite fabric fitted in the analytical solution for metal mesh in 1.82–2.6 GHz frequency range with strength of 30–36 dB. Thus, depending on desired shielding efficiency the physical texture of shielding fabric can be determined analytically.
摘要本文研究了平纹复合织物的电磁屏蔽效果和金属网的解析解。实验采用棉纱加50µm铜丝捻制而成的复合织物。由于织物经过编织和拉伸,它具有长度为1.2毫米的方形孔。通过WR430波导系统在1.7 ~ 2.6 GHz频率范围内测量了这些织物的电磁屏蔽效果。为了对上述织物的屏蔽效果进行建模,采用了一种便于计算金属网屏蔽效果的解析解。由于织物几何形状与金属网结构的物理相似性,将织物特性值代入解析解中。统计结果表明,平纹复合织物的SE测量结果符合1.82 ~ 2.6 GHz频率范围内强度为30 ~ 36 dB的金属网解析解。因此,根据所需的屏蔽效率,可以解析地确定屏蔽织物的物理结构。
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引用次数: 0
Comparison of chemical composition, antioxidant and antibacterial activity of Callistemon citrinus skeels (bottlebrush) essential oil obtained by conventional and microwave-assisted hydrodistillation 常规蒸馏法与微波辅助加氢蒸馏法提取香茅(瓶刷)精油的化学成分、抗氧化及抗菌活性比较
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-02 DOI: 10.1080/08327823.2020.1794721
P. Mande, N. Sekar
Abstract Microwave-assisted hydrodistillation and conventional hydrodistillation (MAHD and HD) were used for a comparative study of extraction Callistemon citrinus Skeels leaf essential oils. The time required for a MAHD method is 75 minutes that for HD method is 3.5 hours, so MAHD requires lesser time. The increases in yield of extracted oil by MAHD (0.84%) is found compared oil extracted by HD (0.6%). Essential oils were examined by GC–MS. MAHD extracted essential oils were wealthier in oxygenated molecules. The main constituent was 1, 8-cineole, followed by α-pinene in the case of MAHD. Percentage of the major component increases from 80% to 90% as compared to HD. Their antibacterial activity was examined on ‘Gram-negative’ and ‘Gram-positive bacteria’. In the case of both bacteria, MAHD extracted oil shows better activity than HD extracted one. Antioxidant action was studied by using 2, 2-diphenyl-1-picrylhydrazyl (DPPH•) radical scavenging and β-carotene/linoleic acid assay it is shown that MAHD extract has better activity than HD extract. Surface morphology of Callistemon leaves was studied with scanning electronic microscopy (SEM) which reveals that the MAHD leaves surface undergo major damage to the conventional HD.
摘要采用微波辅助加氢蒸馏法和常规加氢蒸馏法(MAHD和HD)对桔梗叶精油的提取工艺进行了比较研究。MAHD法所需时间为75分钟,HD法所需时间为3.5小时,因此MAHD法所需时间更短。与HD提取的油收率(0.6%)相比,MAHD提取的油收率增加了0.84%。采用气相色谱-质谱法测定精油含量。MAHD提取的精油含氧分子更丰富。MAHD的主要成分为1,8 -桉叶油脑,其次为α-蒎烯。与HD相比,主成分的百分比从80%增加到90%。研究了它们对革兰氏阴性菌和革兰氏阳性菌的抑菌活性。在两种细菌的情况下,MAHD提取油比HD提取油表现出更好的活性。通过清除DPPH自由基和β-胡萝卜素/亚油酸试验研究了MAHD提取物的抗氧化活性,结果表明MAHD提取物的抗氧化活性优于HD提取物。利用扫描电子显微镜(SEM)研究了茉莉叶片的表面形貌,发现MAHD叶片表面对常规HD损伤较大。
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引用次数: 5
Effects of different drying methods on quality changes and energy characteristics of tilapia fillets 不同干燥方式对罗非鱼鱼片品质变化及能量特性的影响
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-02 DOI: 10.1080/08327823.2020.1794725
Linbao Wei, Weiqiang Qiu, Yingshan Jin, Ruilin Zheng, K. Row, Yudong Cheng, Yinzhe Jin
Abstract The effects of different drying methods (hot air drying (HAD), microwave drying (MD), and hot air-microwave combined drying (HAMCD) processes) on the drying characteristics, rehydration ability, colour, texture, moisture state, microstructure, and energy characteristics of tilapia fillets have been investigated. The best rehydration and recovery ratios of tilapia fillets were obtained using HAMCD (58.96 and 39.24%, respectively). Tilapia fillets quickly become a burnt-yellow colour by MD. HAMCD can improve the hardness, chewiness, and elasticity values, and can obtain crispy tilapia fillets. In the moisture state peak image, the symmetry of the T21 (fixed water) peak obtained at 70 °C + 250 W (H3M) was the best with an asymmetry factor (As) of 1.04. In the MRI image, the brightness of the proton density weighted image was arranged from high to low as follows: HAD > HAMCD > MD. Using SEM, the microstructure of the tilapia fillets prepared using HAMCD showed a large number of small holes. The specific energy consumption was reduced ∼1.8 fold and the thermal efficiency increased ∼5 fold using HAMCD when compared with the HAD process. It was concluded that HAMCD can be used for to process tilapia fillets with high quality and low operating costs.
摘要研究了热风干燥(HAD)、微波干燥(MD)和热风-微波复合干燥(HAMCD)工艺对罗非鱼鱼片干燥特性、复水化能力、色泽、质地、水分状态、微观结构和能量特性的影响。采用HAMCD对罗非鱼鱼片的复水率和回收率最高,分别为58.96和39.24%。经MD处理后,罗非鱼鱼片迅速呈焦黄色。hammcd能提高罗非鱼鱼片的硬度、嚼劲和弹性值,并能得到酥脆的罗非鱼鱼片。在水分状态峰图像中,70°C + 250 W (H3M)条件下获得的T21(固定水)峰的对称性最好,不对称系数(As)为1.04。在MRI图像中,质子密度加权图像亮度由高到低排列为:HAD > HAMCD > MD。利用SEM对HAMCD制备的罗非鱼鱼片进行微观结构分析,发现鱼片表面存在大量小孔。与HAD工艺相比,使用HAMCD的比能耗降低了1.8倍,热效率提高了5倍。结果表明,HAMCD可用于罗非鱼鱼片的高质量加工和低成本生产。
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引用次数: 8
Optimal design of compact microwave fractional order differentiator 紧凑微波分数阶微分器的优化设计
IF 1.5 4区 工程技术 Q2 Materials Science Pub Date : 2020-07-02 DOI: 10.1080/08327823.2020.1794723
U. Gautam, T. Rawat, Apoorva Aggarwal, D. Upadhyay
Abstract This paper presents a stable, accurate and wideband microwave fractional order differentiator (MFOD) based on infinite impulse response filter. The fractional order differentiator (FOD) design problem is formulated in the z-domain. This formulation alliances with the transmission line elements in cascading. Real coded genetic algorithm (RCGA), particle swarm optimization (PSO) and cuckoo search algorithm (CSA) are applied to determine the optimum values of the characteristic impedances of the transmission line elements. The performance measure criterion of CSA algorithm as compared with other nature inspired algorithms-based differentiator are carried by the magnitude response, absolute magnitude error, phase response, pole-zero response, percentage improvement graph and convergence rate. The simulation and statistical analysis clearly affirm that the proposed MFOD using CSA outperforms RCGA and PSO in all state-of-the-art. The absolute magnitude error for the designed fifth order is as low as 2.9022. The designed fractional order differentiator is implemented in the form of microstrip on RT/Duroid substrate with dielectric constant 2.2 and thickness 0.762 mm. that is eligible for wideband microwave differentiator. The proposed design is compact in size and has low absolute magnitude error over the entire bandwidth. The measured result agrees well with the simulated result in the frequency range 1–12.5 GHz in MATLAB and advanced design software (ADS) environment.
摘要提出了一种基于无限脉冲响应滤波器的稳定、精确、宽带微波分数阶微分器。分数阶微分器(FOD)的设计问题是在z域中表述的。该公式与级联的传输线元件相结合。采用实编码遗传算法(RCGA)、粒子群算法(PSO)和布谷鸟搜索算法(CSA)确定传输线单元特征阻抗的最优值。CSA算法与其他基于自然启发算法的微分器相比,其性能衡量标准为幅度响应、绝对幅度误差、相位响应、极零响应、改进百分比图和收敛速度。仿真和统计分析清楚地证实,使用CSA的MFOD在所有先进技术中都优于RCGA和PSO。设计的五阶绝对数量级误差低至2.9022。所设计的分数阶微分器以微带形式实现在介电常数为2.2、厚度为0.762 mm的RT/Duroid衬底上。这符合宽带微波微分器的要求。所提出的设计尺寸紧凑,在整个带宽内具有低的绝对幅度误差。在MATLAB和高级设计软件(ADS)环境下,在1 ~ 12.5 GHz频率范围内的仿真结果与实测结果吻合较好。
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引用次数: 1
期刊
Journal of Microwave Power and Electromagnetic Energy
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