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Pressure transient analysis of horizontal wells in multibranched fault-karst carbonate reservoirs: Model and application in SHB oilfield 多分支断裂岩溶碳酸盐岩油藏水平井压力瞬变分析模型及其在SHB油田的应用
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-10-29 DOI: 10.1016/j.petrol.2022.111167
Wenyang Shi , Jian Cheng , Yongchuan Liu , Min Gao , Lei Tao , Jiajia Bai , Qingjie Zhu

Current flow models for fault-karst reservoirs are mostly described as a single fault formation, which cannot be applied in recent-developed multibranched fault-karst reservoirs. This paper established a novel analytical model to investigate pressure response behavior of a horizontal well in multibranched fault-karst reservoirs. The model is able to describe the influence of the physical properties and spatial structure of fracture-cave system on pressure transient response. The flow model considers different flow behaviors in each region, which includes Darcy flow (gravity included) in fault-fracture, large-scale storage flow in karst-cave, and Poiseuille-law-based horizontal laminar flow in the horizontal wellbore, respectively. These assumptions enable the model to match complex situations in multibranched fault-karst reservoirs. Then, the model was retrograded to compare with a single fault-karst reservoir model to verify its accuracy. Further, the solutions were graphed on log-log plots, and we discussed the effect of fluids mobility, formation storability, and structure characteristics (e.g., length, angle, depth, distance) of fracture-cave branches on transient pressure responses. Results show that (a) the number of fracture-cave branches in a reservoir can be directly observed by counting the number of V-shaped appearances on the pressure derivative curve. (b) The exact shut-in time when V-shape appears is affected by volume and distance between two neighboring fracture-cave branches. (c)The characteristics of the V-shape are affected by fluid mobility, formation storability, and length of fracture region. (d) The slope of the pressure derivative curve in the boundary-dominated flow regime can be used to evaluate the gravity effect. (e) The pressure response behavior exhibits a near-well effect when a horizontal well commingled production in the multibranched fault-karst reservoir. Finally, we applied our model and resulting observations to analyze pressure build-up data tested from SHB Oilfield, which demonstrated a workflow to identify the number of fault-karst branches and also to estimate reservoir properties.

目前断层岩溶储层的渗流模型多为单断层构造,不适用于新近开发的多分支断层岩溶储层。本文建立了一种新的多分支断层岩溶油藏水平井压力响应分析模型。该模型能够较好地描述缝洞系统的物理性质和空间结构对压力瞬态响应的影响。该模型考虑了不同区域的不同流动行为,分别包括断层裂缝中的达西流动(含重力)、溶洞中的大规模储集流动和水平井筒中基于泊塞维尔定律的水平层流。这些假设使模型能够适应多分支断岩溶储层的复杂情况。然后对模型进行反演,与单一断层岩溶储层模型进行对比,验证模型的准确性。此外,将解绘制成对数-对数图,并讨论了流体流动性、地层储存性和缝洞分支结构特征(如长度、角度、深度、距离)对瞬态压力响应的影响。结果表明:(a)通过计算压力导数曲线上v形出现的次数,可以直接观察到储层缝洞分支的数量。(b) v形出现时的准确关井时间受相邻两个缝洞分支的体积和距离的影响。(c) v型特征受流体流动性、地层储存性和裂缝区域长度的影响。(d)边界主导流型的压力导数曲线斜率可以用来评价重力效应。(e)多分支断-岩溶油藏水平井混采时压力响应行为表现出近井效应。最后,我们将模型和观测结果应用于分析SHB油田的压力累积数据,该数据展示了识别断层喀斯特分支数量和估计储层性质的工作流程。
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引用次数: 4
Study of the trapping mechanism of merging drops moving under thermocapillary migration on a surface with wettability contrast 润湿性对比表面上热毛细迁移合并液滴的捕获机制研究
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-08 DOI: 10.1016/j.petrol.2022.111172
Gloire Imani , Lei Zhang , Chao Xu , Hai Sun , Yongfei Yang , Jun Yao

Trapping of drops due to wettability contrast in porous materials emerges in a variety of subsurface and manufacturing applications. In carbon capture and storage, carbon dioxide must be trapped in order to avoid its release into the atmosphere, while trapped oil must be displaced. Both carbon dioxide and oil can exist as drops in porous media. The migration of a single drop attached to a wall can be hindered if the wall surface has a different wettability. However, the trapping condition becomes more complicated in the presence of two or more drops. In this work, we aim to study the trapping mechanism during thermocapillary migration of a merging drop on a heterogeneous surface. To do so, numerical simulations have been performed using the Front-Tracking/Finite Volume Method, where the Navier-Stokes equations are coupled with the conservation equations. The generalized Navier boundary condition (GNBC) has been used as the slip model to remove the viscous singularity. The combined finite-volume and tracking method is able to deal with different types of discontinuities in compressible or incompressible fluid flows, as e.g., interfaces. The material properties of the drop and the ambient fluid are different, and surface tension depends on the temperature. The results have shown that there exist three regimes characterizing the motion of merging drops, including the passage of the leading drop, the trapping of the merging drop, and the partial trapping, which correspond to the trapping of the leading drop but the passage of the merging drop. We show that there is a critical wettability contrast at which the merging drop gets trapped. The effects of Marangoni number (Ma) and viscosity ratio are investigated. The critical wettability contrast decreases with the increase of Ma number and the regime shift as a function of the viscosity and Marangoni number. These findings have implications for the design of geological carbon dioxide storage, improvement of oil recovery and microfluidic device development.

由于多孔材料中的润湿性对比而导致的液滴捕获出现在各种地下和制造应用中。在碳捕获和储存过程中,必须捕获二氧化碳以避免其释放到大气中,而捕获的石油必须被置换。二氧化碳和石油都可以以液滴的形式存在于多孔介质中。如果壁表面具有不同的润湿性,附着在壁上的单个液滴的迁移可能会受到阻碍。然而,在存在两个或多个液滴的情况下,捕获条件变得更加复杂。在这项工作中,我们旨在研究非均匀表面上合并液滴的热毛细迁移过程中的捕获机制。为此,使用前沿跟踪/有限体积法进行了数值模拟,其中Navier-Stokes方程与守恒方程相耦合。采用广义Navier边界条件(GNBC)作为滑移模型来消除粘性奇异性。有限体积和跟踪相结合的方法能够处理可压缩或不可压缩流体流中的不同类型的不连续性,例如界面。液滴和环境流体的材料特性不同,表面张力取决于温度。结果表明,存在三种表征合并液滴运动的状态,包括前导液滴的通过、合并液滴的捕获和部分捕获,这三种状态对应于前导液滴被捕获但合并液滴通过。我们表明,在合并液滴被捕获的临界润湿性对比。研究了马朗戈尼数(Ma)和粘度比对粘度的影响。临界润湿性对比度随着Ma数的增加而减小,并且作为粘度和Marangoni数的函数的状态偏移也随之减小。这些发现对地质二氧化碳储存的设计、石油开采的改进和微流体装置的开发具有启示意义。
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引用次数: 1
Hole cleaning and wet-granular rheology of rock cutting beds: Impact of drilling fluid composition 岩屑床的洗孔和湿颗粒流变:钻井液成分的影响
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-18 DOI: 10.1016/j.petrol.2022.111267
Camilo Pedrosa , Arild Saasen , Jan David Ytrehus

Cuttings-beds formation is an issue that must be considered during all wellbore drilling operations. This problem increases at highly deviated or horizontal wells, where cuttings removal efficiency becomes one of the most critical elements for the whole drilling operations. Removal of drilled cuttings is done through circulating the drilling fluid and then separate out the cuttings at the surface. When the wellbore is inclined or horizontal, the cuttings tend to settle and form cuttings-beds. The consolidation strength of these cuttings-beds is normally unknown. Traditional studies on cuttings-bed removal usually focus on the final result: effective cuttings-bed removal. The scope of this study is to analyze the wetted cuttings-bed particle bonding strength and the stress required to break the formed bed, by means of granular rheology methodology. In other words, the strength required to erode a formed cuttings-bed is addressed independently. Wet-granular rheology techniques, complemented by Mohr-Coulomb envelop analysis has shown to be an effective approach to describe the cohesive strength of consolidated cuttings-bed and flowability of the particles within the beds. We have analyzed simulated cuttings-beds’ shear strength and flowability using quartz particles saturated with water, water-based drilling fluid and oil-based drilling fluid. The results showed that the interstitial fluid and its composition significantly impact the shear strength of the bed, conveying higher cohesion for water-based drilling fluid in comparison to oil-based drilling fluids.

岩屑床的形成是所有井筒钻井作业中必须考虑的问题。在大斜度井或水平井,岩屑去除效率成为整个钻井作业的最关键因素之一,这一问题会增加。钻屑的清除是通过循环钻井液来完成的,然后在地表分离出钻屑。当井筒倾斜或水平时,岩屑倾向于沉降并形成岩屑床。这些岩屑床的固结强度通常是未知的。传统的岩屑床去除研究通常侧重于最终结果:有效去除岩屑床。本研究的范围是通过颗粒流变学方法分析润湿岩屑床颗粒结合强度和破坏形成的岩屑床所需的应力。换句话说,侵蚀形成的岩屑床所需的强度是独立处理的。湿颗粒流变学技术,辅以莫尔-库仑包络分析,已被证明是描述固结岩屑床粘结强度和床内颗粒流动性的有效方法。我们使用饱和水的石英颗粒、水基钻井液和油基钻井液分析了模拟岩屑床的剪切强度和流动性。结果表明,与油基钻井液相比,间隙液及其成分显著影响了地层的剪切强度,为水基钻井液输送了更高的内聚力。
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引用次数: 2
Analytical model for transient pressure analysis in a horizontal well intercepting with multiple faults in karst carbonate reservoirs 碳酸盐岩岩溶储层多断层水平井暂态压力分析模型
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-03 DOI: 10.1016/j.petrol.2022.111183
Wenyang Shi , Zhenglin Jiang , Min Gao , Yongchuan Liu , Lei Tao , Jiajia Bai , Qingjie Zhu , Haoqin Ge

In recent years, the Shunbei karst-carbonate reservoirs becomes a huge productivity oilfield, which produced over one million tonnes crude oil annually. However, there are difficulties in understanding production contribution of each fault-karst branch in reservoirs, which significantly impacts the efficient development. Multibranched fault-karst reservoirs in the Shunbei have an obvious tree-shaped geostructure, in which the natural fractures and eroded cave develop along multiple large-scale faults. The existing models for pressure transient analysis (PTA) were mainly established for fracture-cave reservoirs only with single fault, which cannot be applicable to characterize the multibranched fault-karst reservoir. To fill this gap, a novel analytical PTA model for horizontal commingled production well in the multibranched fault-karst reservoir was established to describe pressure response and identify flow regimes. First, our model includes the Darcy flow with the fluid compressibility effect in fracture region, and the large-scale vertical storage flow in cave region as well as the horizontal laminar flow in the horizontal wellbore. Then, the accuracy of this PTA model is verified by comparing it with the existing single branch fault-karst pressure model. Further, we applied the model to analyze the Shunbei oilfield case data. Last, the effect of boundary type, fluid compressibility effect, fracture physical properties, and cave spatial distribution on the pressure response are discussed in detail. The sensitivity analysis results show (a) the cave storage flow regime exhibits an obvious unit-slope-line on pressure derivative curve, at the time the skin transient flow constitutes a V-shape characteristic. (b) The number of fracture-cave branches can be directly obtained by counting the number of V-shaped appearances on the pressure derivative curve. (c) The fluid compressibility effect leads to an upward trend on the pressure and its derivative, reservoir engineers should be cautious to explain that characteristic as a closed boundary effect. (d) The cave volume and cave position control the timing of the V-shape occurring. As the cave volume increases, the linear flow regime lasts longer and the V-shaped feature becomes apparent. With the cave distance and cave depth increasing, the V-shape characteristic comes later. This work can provide technical support for accurate characterization of multibranched fault-karst reservoirs, and give a type curve analysis method for rapidly diagnosing the spatial location of each karst cavity by analyzing bottom-hole pressure.

近年来,顺北岩溶-碳酸盐岩油藏已成为年产原油100多万吨的高产油田。然而,储层各断-岩溶分支的产量贡献难以准确认识,严重影响了储层的高效开发。顺北多分支断层岩溶储层具有明显的树状地质构造,其中天然裂缝和溶洞沿多条大型断层发育。现有的压力瞬态分析(PTA)模型主要是针对单断裂缝洞型储层建立的,不适用于多分支断裂岩溶储层的表征。为了填补这一空白,建立了一种新的多分支断层-岩溶油藏水平混采井分析PTA模型,以描述压力响应和识别流动形式。首先,我们的模型考虑了裂缝区域具有流体压缩性效应的达西流动,溶洞区域的大规模垂直储集流动以及水平井筒中的水平层流。然后,将PTA模型与现有的单分支断层-岩溶压力模型进行对比,验证了该模型的准确性。并将该模型应用于顺北油田的实例数据分析。最后,详细讨论了边界类型、流体可压缩性效应、裂缝物理性质和溶洞空间分布对压力响应的影响。敏感性分析结果表明:(a)洞库渗流流态在压力导数曲线上表现为明显的单位斜率线,同时表层瞬态渗流呈v型特征;(b)通过计算压力导数曲线上v形出现的次数,可以直接得到缝洞分支的数量。(c)流体压缩性效应导致压力及其导数呈上升趋势,油藏工程师应谨慎地将这一特征解释为封闭边界效应。(d)溶洞体积和溶洞位置控制着v形发生的时间。随着溶洞体积的增大,线性流态持续时间延长,v型流特征明显。随着洞距和洞深的增加,v型特征出现较晚。该工作可为多分支断岩溶储层的准确表征提供技术支持,并为通过分析井底压力快速诊断各溶洞的空间位置提供一种类型曲线分析方法。
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引用次数: 0
Prediction of nuclear magnetic resonance porosity well-logs in a carbonate reservoir using supervised machine learning models 基于监督机器学习模型的碳酸盐岩储层核磁共振孔隙度测井预测
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-03 DOI: 10.1016/j.petrol.2022.111169
Hugo Tamoto, Rafael dos Santos Gioria, Cleyton de Carvalho Carneiro

Porosity estimation is a fundamental input for reservoir management and petrophysical characterization, and this feature is usually estimated based on laboratory measurements or through the use of well-logs. As an important resource for porosity quantification, nuclear magnetic resonance (NMR) well-logs are extremely useful; they allow geologists and petrophysicists to rapidly quantify different types of porosities (including total, effective, and free fluid porosity), and to perform a full formation evaluation and a reservoir quality analysis. However, the activation of wireline tools, the signal-to-noise ratio, the environmental conditions, and the characteristics of the formation fluid can create expensive and adverse conditions for subsurface acquisition. This research aims to develop machine learning models for the creation of synthetic NMR well-logs, assisted by auxiliary well-logging features. Four supervised models: multilayer perceptron neural network, AdaBoost, XGBoost, and CatBoost, comparing the adjusted R2 and RMSE. Of these, the CatBoost regressor provided the most highly optimized model. It was able to reduce local dissimilarities with the real dataset, and returned a better global metric score, yielding an adjusted R2 of 0.87 and an RMSE of less than 0.01. Moreover, all of the machine learning models provided substantial improvements in total porosity estimation, particularly compared to conventional empirical calculations based on density and sonic well-logs. An improvement of 0.5520 in the adjusted R2 was achieved for the density porosity, and 0.2 for the sonic porosity. The differences between real NMR well-logs and the machine learning outputs were in general less than 5%, for most of the well-logging interval. In addition, a tree boosted porosity model based on well-logs is presented for the first time, and the contributions and impacts of the input features on the model predictions are explored. Finally, the behaviors of the linear and nonlinear features of the model are examined, which allows us to better understand the complex relationships among the features and the dataset used.

孔隙度估计是储层管理和岩石物理特征的基本输入,通常基于实验室测量或通过使用测井来估计这一特征。核磁共振测井作为孔隙度定量的重要资源,具有极其重要的应用价值;它们使地质学家和岩石物理学家能够快速量化不同类型的孔隙度(包括总孔隙度、有效孔隙度和自由流体孔隙度),并进行完整的地层评估和储层质量分析。然而,电缆工具的激活、信噪比、环境条件和地层流体的特性可能会为地下采集创造昂贵和不利的条件。本研究旨在开发用于创建合成NMR测井的机器学习模型,并辅以辅助测井特征。四个监督模型:多层感知器神经网络、AdaBoost、XGBoost和CatBoost,比较调整后的R2和RMSE。其中,CatBoost回归器提供了优化程度最高的模型。它能够减少与真实数据集的局部差异,并返回更好的全局度量得分,产生0.87的调整后R2和小于0.01的RMSE。此外,所有的机器学习模型都在总孔隙度估计方面提供了实质性的改进,特别是与基于密度和声波测井的传统经验计算相比。密度孔隙率的调整R2提高了0.5520,声波孔隙率提高了0.2。对于大多数测井间隔,真实NMR测井和机器学习输出之间的差异通常小于5%。此外,首次提出了一种基于测井曲线的树增强孔隙度模型,并探讨了输入特征对模型预测的贡献和影响。最后,检查了模型的线性和非线性特征的行为,这使我们能够更好地理解特征与所使用的数据集之间的复杂关系。
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引用次数: 0
Developing new correlations for asphaltene deposition involving SARA fractions and colloidal instability index 建立涉及SARA馏分和胶体不稳定性指数的沥青质沉积的新相关性
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-10-27 DOI: 10.1016/j.petrol.2022.111143
Aliyu Adebayo Sulaimon , Habineswaran A/L Rajan , Ali Qasim , Nwankwo Princess Christiana , Pearl Isabellah Murungi

Asphaltene deposition in pipelines disrupts the normal transportation of the fluid produced. The deposition within the pipeline depends on the content of saturates, aromatic, resin, and asphaltenes (SARA) in crude oil. SARA analysis is used in the petroleum industry to estimate the stability of asphaltenes. In this study, a new set of correlations has been developed using regression analysis and the MATLAB curve fitting tool. The SARA fractions and the colloidal instability index (CII) are correlated with density, viscosity, and the combination of density and viscosity. SARA analysis data from 310 crude oil samples were used to develop the correlations while field data from 29 unique crude oils were used for validation. The best-fit correlations are selected based on statistical indicators such as the correlation coefficient (R2), the root mean square error (RMSE), and the average absolute relative error (AARE). Asphaltene stability plots were also developed for the new density-based CII (DBCII), viscosity-based CII (VBCII), and the density-and-viscosity-based CII (DVBCII). Based on statistical indicators, analysis of results shows that the density-based correlations for the SARA fractions are relatively more accurate than the viscosity-based correlations. The R-squared value for the DBCII is 0.7031 compared to 0.3234 for the VBCII and 0.6875 for the DVBCII. However, the percentage accuracy of 83% for the DVBCII is higher than the accuracy of the existing methods. The newly developed deposition envelopes are divided into stable and unstable regions that can be used to determine the stability of the asphaltene based on the physical properties of crude oil. The newly developed correlations for each SARA fraction based on the oil density eliminate the requirement for the laborious and time-consuming SARA analysis. Therefore, it is useful to predict the stability of asphaltene based on the physical properties of crude oil.

管道中的沥青质沉积破坏了生产流体的正常运输。管道内的沉积取决于原油中饱和烃、芳香烃、树脂和沥青质(SARA)的含量。SARA分析在石油工业中用于估计沥青质的稳定性。在这项研究中,使用回归分析和MATLAB曲线拟合工具开发了一组新的相关性。SARA组分和胶体不稳定性指数(CII)与密度、粘度以及密度和粘度的组合相关。310个原油样本的SARA分析数据用于建立相关性,而29个独特原油的现场数据用于验证。基于诸如相关系数(R2)、均方根误差(RMSE)和平均绝对相对误差(AARE)之类的统计指标来选择最佳拟合相关性。还为新的基于密度的CII(DBCII)、基于粘度的CII和基于密度和粘度的CII(DVBCII)开发了沥青质稳定性图。基于统计指标,结果分析表明,基于密度的SARA组分相关性比基于粘度的相关性相对更准确。DBCII的R平方值为0.7031,而VBCII为0.3234,DVBCII为0.6875。然而,DVBCII 83%的百分比准确度高于现有方法的准确度。新开发的沉积包络线分为稳定区和不稳定区,可用于根据原油的物理性质确定沥青质的稳定性。新开发的基于油密度的每个SARA馏分的相关性消除了对费力和耗时的SARA分析的要求。因此,根据原油的物理性质预测沥青质的稳定性是有用的。
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引用次数: 1
A review of vertical closed-loop geothermal heating and cooling systems with an Emphasis on the importance of the subsurface 垂直闭环地热加热和冷却系统的综述,重点是地下的重要性
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-10-20 DOI: 10.1016/j.petrol.2022.111137
Keivan Khaleghi, Silviu Livescu

Geothermal heat pump (GHP) systems have been established as a proven technology for cooling and heating residential, public and commercial buildings. There is a geothermal solution to the ambitious goal of decarbonizing the space heating and cooling, which is contingent on the successful deployment of the GHP technology. This in turn requires accurate site characterization, sound design methodologies, effective control logic, and short and long-term (life-cycle) performance analysis and optimization. In this article, we review the aforementioned aspects of the vertical closed-loop GHPs specifically focusing on the important role of the subsurface. The basics of GHP technology are introduced along with relevant trends and statistics. GHPs are compared with similar technologies such as air source heat pumps (ASHP) along with the effects of deployment on the grid peak load. We then review the common system architectures and the growing trends for deeper boreholes and the drivers behind it. Various methods for design, sizing, and simulation of GHPs are introduced along with software tools common in research and industry. We then move to subsurface characterization, drilling and well construction of vertical boreholes. Long-term performance monitoring for GHP systems is an important source of information for model validation and engineering design and is garnering increasing attention recently. Data science is another field that is growing rapidly with its methods increasingly utilized in GHP applications. The environmental aspect of GHPs is briefly reviewed. Finally, concluding remarks are given to summarize the review and highlight the potential of petroleum engineering expertise and methods in GHP applications.

地热热泵(GHP)系统已被证明是一种用于住宅、公共和商业建筑制冷和供暖的成熟技术。有一个地热解决方案可以实现太空供暖和制冷脱碳的宏伟目标,这取决于GHP技术的成功部署。这反过来又需要准确的现场特征、完善的设计方法、有效的控制逻辑以及短期和长期(生命周期)性能分析和优化。在这篇文章中,我们回顾了垂直闭环GHP的上述方面,特别关注地下的重要作用。介绍了GHP技术的基本原理以及相关趋势和统计数据。将GHP与空气源热泵(ASHP)等类似技术以及部署对电网峰值负荷的影响进行了比较。然后,我们回顾了常见的系统架构、更深钻孔的增长趋势及其背后的驱动因素。介绍了GHP的各种设计、规模确定和模拟方法,以及研究和工业中常见的软件工具。然后,我们转向地下表征、钻井和垂直钻孔的井施工。GHP系统的长期性能监测是模型验证和工程设计的重要信息来源,近年来越来越受到关注。数据科学是另一个快速发展的领域,其方法越来越多地用于GHP应用。简要回顾了全球统一制度的环境方面。最后,对综述进行了总结,并强调了石油工程专业知识和方法在GHP应用中的潜力。
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引用次数: 2
Creep microindentation of low-density oil well cement and the implication on radial cracking risk of cement sheath 低密度油井水泥的蠕变微压痕及其对水泥环径向开裂风险的影响
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-10-28 DOI: 10.1016/j.petrol.2022.111155
Zhao Chen , Luca Sorelli , Philippe Benard

To better provide zonal isolation for the production of oil and gas, low-density oil well cement (LD-OWC) filling a deep oil well was developed to reduce the high hydrostatic pressure caused by the cement slurry. The key mechanical properties of LD-OWC and related cracking susceptibility, nevertheless, have not been fully understood. This work was to characterize the elastic and creep properties of LD-OWC using microindentation and assess the radial cracking risk of the cement sheath. With two types of LD-OWC cured at different temperatures, our measurement through mercury intrusion porosimetry (MIP) showed that their porosities depended on the slurry densities level, and the basic creep exhibited a logarithmic increase in the long term. Mechanical properties such as Young's modulus (E), indentation hardness (H), and creep modulus (C) of LD-OWC were statistically characterized, in particular, E and C were in line with those obtained by macroscopic tests. Moreover, a viscoelastic sheath model was developed to evaluate the stress redistribution in the steel casing, the cement sheath, and the formation in the long term. We found that lower slurry densities of OWC reduced the risk of radial cracking. Taking advantage of parametric analysis, the power-function correlation between the safety factor of radial cracking and the mechanical and geometrical sheath properties was also demonstrated.

为了更好地为油气生产提供层间隔离,开发了充填深井的低密度油井水泥(LD-OWC),以降低水泥浆造成的高静水压力。然而,LD-OWC的关键力学性能和相关的开裂敏感性尚未完全了解。这项工作是利用微压痕来表征LD-OWC的弹性和蠕变特性,并评估水泥环的径向开裂风险。在不同温度下固化两种类型的LD-OWC,通过压汞孔隙度法(MIP)测量表明,它们的孔隙度取决于料浆密度水平,长期来看,基本蠕变呈对数增长。对LD-OWC的杨氏模量(E)、压痕硬度(H)、蠕变模量(C)等力学性能进行了统计表征,其中E、C与宏观试验结果一致。此外,建立了粘弹性套管模型,以评估钢套管、水泥环和地层的长期应力重新分布。我们发现较低的OWC浆体密度降低了径向开裂的风险。利用参数分析方法,论证了径向开裂安全系数与护套力学和几何性能之间的幂函数关系。
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引用次数: 2
Using laser scanning confocal microscopy combined with saturated oil experiment to investigate the pseudo in-situ occurrence mechanism of light and heavy components of shale oil in sub-micron scale 利用激光扫描共聚焦显微镜结合饱和油实验研究亚微米级页岩油轻、重组分的伪原位生成机制
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-17 DOI: 10.1016/j.petrol.2022.111234
Zhiye Gao , Longfei Duan , Zhenxue Jiang , Liliang Huang , Jiaqi Chang , Guowei Zheng , Zhiwei Wang , Feng An , Weihang Wei

The occurrence characteristics of shale oil have a significant impact on its mobility and the ultimate oil recovery. How to quantitatively characterize the occurrence and distribution characteristics of shale oil is a challenging task. Accordingly, the laser scanning confocal microscopy (LSCM) combined with saturated oil experiment is used to quantitatively characterize the pseudo in-situ occurrence characteristics of light and heavy components of shale oil in sub-micron scale in Fengcheng Formation of Mahu Sag. Furthermore, the main controlling factors of light and heavy components’ occurrence characteristics are comprehensively investigated in this study. The results show that: (1) Shale wettability significantly affects the occurrence state of shale oil. The heavy components are prone to exist on the surface of oil-wet minerals and organic matter of shale compared with light components. (2) Shale oil is relatively rich in bright laminas and the content of light components is higher in contrast to dark laminas. (3) The temperature has a greater impact on the heavy components and pressure has a multistage impact on the occurrence state of shale oil. The microscopic preferential fluid occurrence index, ΔHL, is proposed to interpret the microscopic occurrence mechanism of the light and heavy components under different pressure conditions, which provides a new perspective on the shale oil occurrence mechanism. (4) Shale oil is not easy to be enriched in dolomitic lumps and alkaline minerals due to their low pore development level. Overall, the outcomes of this study are of great significance to the understanding of shale oil enrichment mechanism.

页岩油的产状特征对其流动性和最终采油率有着重要影响。如何定量表征页岩油的产状和分布特征是一项具有挑战性的任务。因此,采用激光扫描共聚焦显微镜(LSCM)结合饱和油实验,定量表征了马湖凹陷丰城组亚微米级页岩油轻、重组分的伪原位产状特征。此外,本研究还全面探讨了轻、重组分赋存特征的主要控制因素。结果表明:(1)页岩润湿性显著影响页岩油的赋存状态。与轻组分相比,重组分容易存在于页岩的油湿矿物和有机质表面。(2) 页岩油相对富含明亮的薄片,与深色薄片相比,轻质成分的含量更高。(3) 温度对重组分的影响较大,压力对页岩油的赋存状态有多阶段的影响。提出了微观优先流体赋存指数Δ∅H−L来解释不同压力条件下轻组分和重组分的微观赋存机制,为研究页岩油赋存机制提供了新的视角。(4) 页岩油由于孔隙发育水平低,不易富集白云质块状物和碱性矿物。总体而言,本研究成果对理解页岩油富集机制具有重要意义。
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引用次数: 5
A novel experimental-theoretical method to improve MMP estimation using VIT technique 利用VIT技术改进MMP估算的一种新的实验理论方法
2区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2023-01-01 Epub Date: 2022-11-08 DOI: 10.1016/j.petrol.2022.111182
Ali Safaei , Masoud Riazi , Saman Shariat

In the gas injection process for enhanced oil recovery (EOR), the interfacial tension (IFT) and the minimum miscibility pressure (MMP) are two key parameters for evaluating the miscibility condition. The vanishing interfacial tension (VIT) method is an efficient method for measuring the interfacial tension of oil and gas versus pressure and can estimate the minimum miscibility pressure. A problem in the VIT test of a hydrocarbon system is that during this test, oil and gas densities vary due to the composition variation of both phases. But in the conventional interfacial measurement, this issue is ignored, and the initial and non-equilibrium densities are utilized for estimating the interfacial tension. In this study, it is tried to nominate a novel method for estimating the most accurate value of IFT. Hence, for this purpose, first a VIT test has been performed for a hydrocarbon gas and a live oil system and using the axisymmetric drop shape analysis (ADSA), the oil droplet has been analyzed, and the geometry factor, which has been defined in this paper, was calculated. After that, the volume of oil droplet and the gas have been measured and were used for vapor-liquid-equilibrium (VLE) or flash calculation using Peng-Robinson equation of state (PR-EOS). By VLE calculation fulfillment, the final composition of two phases is determined. Eventually, the densities of two phases have been calculated for VIT modification. Finally, the IFT results were plotted versus the pressure steps, and the MMP were estimated. Furthermore, to evaluate the results of VIT test and its modification, slim tube displacement (STD) test, which is known as the most reliable laboratory method for measuring the MMP in the oil industry, has been performed. The results show that the values obtained for MMP values for the VIT test with the corrected densities which are lower than the values obtained for the VIT test for not-corrected densities and the suggested experimental-theoretical method has been estimated the MMP more accurately. The MMP obtained by VIT test and modified VIT method was equal to 3858.72 and 3722.0 psi, respectively. Meanwhile, the slim tube test has measured the MMP equal to 3667.13 psi.

在提高采收率的注气过程中,界面张力(IFT)和最小混相压力(MMP)是评价混相条件的两个关键参数。消失界面张力(VIT)法是一种测量油气界面张力与压力关系的有效方法,可以估计最小混溶压力。碳氢化合物系统的VIT测试中的一个问题是,在该测试过程中,由于两相的组成变化,油气密度发生变化。但在传统的界面测量中,这一问题被忽略了,而是利用初始密度和非平衡密度来估计界面张力。在本研究中,试图提出一种新的方法来估计IFT的最准确值。因此,为此,首先对烃类气体和活油系统进行了VIT测试,并使用轴对称液滴形状分析(ADSA)对油滴进行了分析,并计算了本文中定义的几何因子。然后,测量油滴和气体的体积,并使用Peng-Robinson状态方程(PR-EOS)进行汽液平衡(VLE)或闪蒸计算。通过VLE计算的实现,确定了两相的最终组成。最后,计算了VIT改性的两相密度。最后,绘制了IFT结果与压力阶跃的关系图,并估计了MMP。此外,为了评估VIT测试及其修改的结果,进行了细管位移(STD)测试,该测试被认为是石油工业中测量MMP最可靠的实验室方法。结果表明,具有校正密度的VIT试验获得的MMP值低于未校正密度的VIT试验获得的值,并且建议的实验理论方法已经更准确地估计了MMP。通过VIT试验和改良的VIT方法获得的MMP分别等于3858.72和3722.0 psi。同时,细管试验测得MMP等于3667.13 psi。
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引用次数: 2
期刊
Journal of Petroleum Science and Engineering
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