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Effect of laser wavelength on ablation propulsion and plasma characteristics with acrylonitrile butadiene styrene target 激光波长对丙烯腈-丁二烯-苯乙烯靶烧蚀推进和等离子体特性的影响
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-07 DOI: 10.1088/1361-6463/ad6877
Yongfeng Xu, Liang Yang, Jiaqi Li, Dongjian Zhou, Qingwei Li, Wenbo Shi and Yuqi Jin
Propulsion performance produced by laser ablation of polymer made of acrylonitrile butadiene styrene is experimentally investigated using the first, second, and third harmonics of a Nd: YAG laser. A ballistic pendulum is employed to assess the impulse and coupling coefficient for laser propulsion application. Fast photography, target ablation, and optical emission spectroscopy are proposed to analyze the energy coupling characteristic. The impulse and coupling coefficient under different pressures are demonstrated to depend on the target ablation and plasma properties which are relevant to laser wavelength. As the laser wavelength decreases, the crater depth and ablation mass are enhanced. Meanwhile, the plasma plume separates at atmospheric pressure and its length extends continuously in the low-pressure range. As a result, plasma including more ejected particles with higher velocity contributes to obtaining excellent impulse and coupling coefficient. In addition, the decreased electron density and temperature indicate higher collision frequency and photoionization dominate rather than inverse bremsstrahlung absorption at shorter laser wavelengths. This work provides a better understanding of the energy conversion mechanism and a reference for improving propulsion performance.
利用掺钕钇钕石榴石(Nd: YAG)激光器的第一、第二和第三次谐波,对丙烯腈-丁二烯-苯乙烯聚合物激光烧蚀产生的推进性能进行了实验研究。采用弹道摆来评估激光推进应用的脉冲和耦合系数。提出了快速摄影、目标烧蚀和光学发射光谱来分析能量耦合特性。结果表明,不同压力下的脉冲和耦合系数取决于激光波长相关的目标烧蚀和等离子体特性。随着激光波长的减小,陨石坑深度和烧蚀质量都会增加。同时,等离子体羽流在大气压力下分离,其长度在低压范围内持续延长。因此,等离子体包括更多的喷射粒子和更高的速度,有助于获得出色的脉冲和耦合系数。此外,电子密度和温度的降低表明碰撞频率升高,在较短的激光波长下,光离子化占主导地位,而不是反轫致辐射吸收。这项工作有助于更好地理解能量转换机制,并为提高推进性能提供参考。
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引用次数: 0
The mechanism of tuning filler orientation degree in composites based on AC electric field assist: from microscopic dynamical model to macroscopic electrical properties 基于交流电场辅助的复合材料填料取向度调控机理:从微观动力学模型到宏观电学特性
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-07 DOI: 10.1088/1361-6463/ad699a
Huanmin Yao, Haibao Mu, He Li, Zhiyuan Qian, Chengshan Liu, Wendong Li, Daning Zhang and Guanjun Zhang
Using the AC electric field to induce the orientation of nonlinear conductive fillers in composites is an effective solution for alleviating electric field distortion in power modules. However, the mechanism by which the electric field affects the filler dynamic characteristics and the composites’ electrical properties remains unclear. In this paper, the correlation between the microscopic dynamic processes of fillers and the macroscopic current amplitude was analyzed. The results show that the current increases rapidly (0 ∼ 173 s) and then slowly (173 ∼ 869 s) at 600 V mm−1, influenced by the rotation and attraction processes of the fillers. This demonstrates that the orientation stops at about 869 s and the filler orientation state is a key factor in determining the dielectric properties. Secondly, the global orientation evaluation index D for the filler network was proposed, which can also derive the minimum time and energy loss required for preparation. Finally, the impact of different filler orientations on the composites’ conductivity was investigated. In the low electric field stress region, with the average carrier jump distance decreasing from 150.23 to 109.71 nm as the D increases from −0.93 to −0.05. On this basis, materials with nonlinear conductivity gradient distribution can be easily prepared. Before optimization, the electric field stress of the power module at the triple point was 35.79 kV. This composite can reduce the value to 15.42 kV, a decrease of 56.9%, while maintaining good electric field uniformity.
利用交流电场诱导复合材料中非线性导电填料的取向是缓解功率模块中电场畸变的有效解决方案。然而,电场对填料动态特性和复合材料电气性能的影响机制仍不清楚。本文分析了填料微观动态过程与宏观电流幅值之间的相关性。结果表明,在 600 V mm-1 时,受填料旋转和吸引过程的影响,电流迅速增加(0 ∼ 173 秒),然后缓慢增加(173 ∼ 869 秒)。这表明取向在大约 869 秒时停止,而填料的取向状态是决定介电性能的关键因素。其次,提出了填料网络的全局取向评价指数 D,该指数还能推导出制备所需的最短时间和能量损失。最后,研究了不同填料取向对复合材料电导率的影响。在低电场应力区,当 D 从 -0.93 增加到 -0.05 时,平均载流子跃迁距离从 150.23 nm 减小到 109.71 nm。在此基础上,可以很容易地制备出具有非线性电导梯度分布的材料。优化前,电源模块在三点处的电场应力为 35.79 kV。这种复合材料可将该值降至 15.42 kV,降低了 56.9%,同时保持了良好的电场均匀性。
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引用次数: 0
Comparison of plasma-activated saline prepared with plasma gases with different N2/O2 ratios activated by gliding arc discharge 比较用滑弧放电激活的不同 N2/O2 比率等离子气体制备的等离子激活生理盐水
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-06 DOI: 10.1088/1361-6463/ad687e
Pengyu Zhao, Yikang Jia, Sihong Ma, Rui Zhang, Kaiyu Li, Tianyi Song, Jianbao Zheng, Jingyao Zhang, Li Guo, Dingxin Liu, Xiaohua Wang and Mingzhe Rong
Methicillin-resistant Staphylococcus aureus (MRSA) presents a significant threat due to the multiple resistance to antibiotics, leading to severe and challenging-to-treat infections. Plasma-activated saline (PAS) prepared by plasma gases, could efficiently inactivate various pathogenic bacteria including both sensitive and antibiotic-resistant bacteria. In this study, the PAS was prepared by plasma gases with different ratios of N2 and O2 activated by gliding arc discharge. First, the gaseous reactive species in the plasma gases were compared, revealing that the highest levels of NOx including NO2 and N2O5 were generated in the gases with the N2/O2 ratios of 4:6, 5:5, and 6:4. Subsequently, the PAS prepared by the two plasma-activated gases at the N2/O2 ratios of 5:5 and 6:4 exhibited the strongest inactivation effects on both planktic MRSA and biofilms. Furthermore, the aqueous reactive species in the PAS exhibited varied change trends with the increasing N2/O2 ratios. Additionally, ultraviolet spectroscopy combined with the probe of N, N-diethyl-p-phenylenediamine was applied for the detection of O2NOO− in the PAS, and the levels of O2NOO− in the PAS were positively correlated with the inactivation effects. Moreover, the PAS induced varying levels of nitration modification on the soluble proteins in MRSA cells, which were related to the intensities of O2NOO− in the PAS. This study regulated the reactive species in the PAS through gas composition and explored the inactivation mechanism of the PAS, providing a new strategy to promote the preparation efficiency of plasma-activated solutions for biomedical applications.
耐甲氧西林金黄色葡萄球菌(MRSA)因对抗生素具有多重耐药性而构成重大威胁,导致严重的、难以治疗的感染。等离子体气体制备的等离子体活化生理盐水(PAS)可有效灭活各种病原菌,包括敏感菌和抗生素耐药菌。本研究采用滑弧放电激活不同比例的 N2 和 O2 等离子气体制备等离子体活化生理盐水。首先,比较了等离子气体中的气态活性物种,结果表明,N2/O2 比率为 4:6、5:5 和 6:4 的气体中产生的 NOx(包括 NO2 和 N2O5)含量最高。随后,N2/O2 比为 5:5 和 6:4 的两种等离子体激活气体制备的 PAS 对浮游 MRSA 和生物膜的灭活效果最强。此外,随着 N2/O2 比率的增加,PAS 中的水活性物质也呈现出不同的变化趋势。此外,紫外光谱结合 N,N-二乙基对苯二胺探针检测了 PAS 中的 O2NOO-,PAS 中的 O2NOO-含量与灭活效果呈正相关。此外,PAS还能诱导MRSA细胞中可溶性蛋白质发生不同程度的硝化修饰,这与PAS中O2NOO-的强度有关。该研究通过气体成分调节了等离子体活化体系中的活性物种,并探索了等离子体活化体系的灭活机理,为提高等离子体活化溶液的制备效率、促进生物医学应用提供了一种新策略。
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引用次数: 0
Parametric study of a vortex-enhanced supersonic inductive plasma torch 涡流增强型超音速感应等离子体火炬的参数研究
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-06 DOI: 10.1088/1361-6463/ad687d
A Pascale, T Lafleur and C S Corr
The feed gas injection configuration in radio-frequency (RF) inductively coupled plasma (ICP) torches plays a critical role in discharge stability, gas heating, and device thermal management: particularly if a supersonic nozzle is used to subsequently accelerate the hot gas. A novel injection configuration is the bidirectional vortex, which segments the internal ICP flow field into two counter-propagating vortices that can significantly enhance gas heating and reduce heat losses. The diameter of the interface between the vortices (known as the mantle) is expected to be an important dimensional parameter affecting torch operation, especially relative to the nozzle size. In this work, we investigate the effect of nozzle throat diameter on the behaviour and performance of a vortex-enhanced supersonic ICP torch. The system is operated at RF powers and argon mass flow rates between 200–1000 W and 0–400 mg s−1 respectively, and different nozzle diameters ranging from 1.5 to 4 mm are explored. Because of the high-temperature environment, and to prevent disruption of the vortex flow fields, non-invasive diagnostics are used to measure the gas temperature and plasma density, and to infer the torch thermal efficiency and achievable gas specific enthalpy change. The maximum temperature is between 8500–9500 K with the 1.5 mm nozzle giving the highest temperature for a given power and mass flow rate, while plasma densities vary between 1020–1021 m−3 depending on the operating conditions. The thermal efficiency increases from 29% for the 1.5 mm nozzle to just above 70% for the 4 mm nozzle with a similar maximum specific enthalpy of around 1.5 MJ kg−1. These results demonstrate the important coupling between torch properties, and how system optimization can lead to tailored performance of potential interest to several ground and space-based applications.
射频(RF)电感耦合等离子体(ICP)火炬中的馈入气体注入配置在放电稳定性、气体加热和设备热管理方面起着至关重要的作用:尤其是在使用超音速喷嘴对热气体进行后续加速的情况下。双向漩涡是一种新颖的注入结构,它将内部 ICP 流场分割成两个反向传播的漩涡,可显著增强气体加热并减少热量损失。涡流之间的界面(称为幔)直径预计将成为影响火炬运行的重要尺寸参数,尤其是相对于喷嘴尺寸而言。在这项工作中,我们研究了喷嘴喉部直径对涡流增强超音速 ICP 火炬的行为和性能的影响。该系统在射频功率和氩气质量流量分别为 200-1000 W 和 0-400 mg s-1 的条件下运行,喷嘴直径从 1.5 毫米到 4 毫米不等。由于是在高温环境下,为防止涡流场受到破坏,采用了非侵入式诊断方法来测量气体温度和等离子体密度,并推断出火炬热效率和可实现的气体比热焓变化。最高温度在 8500-9500 K 之间,在给定功率和质量流量下,1.5 毫米喷嘴的温度最高,而等离子体密度则在 1020-1021 m-3 之间,具体取决于工作条件。热效率从 1.5 毫米喷嘴的 29% 提高到 4 毫米喷嘴的 70%,最大比热约为 1.5 MJ kg-1。这些结果表明了火炬特性之间的重要耦合关系,以及系统优化如何实现量身定制的性能,这对一些地面和空间应用具有潜在的意义。
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引用次数: 0
Pulsed corona discharge: an advanced treatment method for antibiotic-contaminated water 脉冲电晕放电:抗生素污染水的先进处理方法
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-06 DOI: 10.1088/1361-6463/ad6882
Florin Bilea, Corina Bradu, Andrei V Medvedovici, Dunpin Hong and Monica Magureanu
Water pollution is one of the most significant problems of the current century. With the increase in medicine availability and use, pharmaceutical pollutants such as antibiotics become more prevalent in natural environments with potentially negative impact. In this study, a pulsed corona discharge was investigated as a possible treatment method of water contaminated with amoxicillin (AMX). Two system configurations were used: plasma and plasma-ozonation. In order to better grasp the effect of system and water matrix on degradation, different pulse widths, solutions pH and conductivity values, as well as the nature of the dissolved salts were investigated. Decreasing the pulse width from 300 ns to 106 ns (full width at half maximum) led to almost a two-fold increase in energy yield at 50% pollutant removal, and the addition of the ozonation reactor resulted six times enhancement in efficiency. While the water matrix had little impact on AMX degradation, the buffering capacity of carbonates has proven beneficial by preventing pH decrease during treatment. Under optimum conditions, the energy yield was 57 g kWh−1 at 93% removal of AMX in tap water. A number of 26 potential degradation products have been identified, resulting from hydroxylation of the benzene ring, oxidation of the thioester and amine groups, hydrolysis, and cleavage of the benzene, β-lactam and thiazole rings, along with fragmentation of the resulting compounds. All but seven degradation intermediates are completely removed by extending treatment duration to 60 min and the persistent ones are less toxic than the parent compound.
水污染是本世纪最重要的问题之一。随着药品供应和使用的增加,抗生素等药物污染物在自然环境中变得越来越普遍,并可能产生负面影响。本研究将脉冲电晕放电作为处理受阿莫西林(AMX)污染的水的一种可能方法进行了研究。采用了两种系统配置:等离子和等离子-臭氧。为了更好地掌握系统和水基质对降解的影响,研究了不同的脉冲宽度、溶液 pH 值和电导率以及溶解盐的性质。将脉冲宽度从 300 毫微秒降低到 106 毫微秒(半最大全宽),在污染物去除率为 50%的情况下,能量产量几乎增加了两倍,而增加臭氧反应器则使效率提高了六倍。虽然水基质对 AMX 降解的影响很小,但碳酸盐的缓冲能力可防止处理过程中 pH 值下降,因此证明是有益的。在最佳条件下,自来水中 AMX 的去除率为 93%,能量产量为 57 g kWh-1。通过苯环的羟基化、硫酯基和胺基的氧化、水解、苯环、β-内酰胺环和噻唑环的裂解以及由此产生的化合物的碎片化,确定了 26 种潜在降解产物。将处理时间延长至 60 分钟后,除七种降解中间体外,所有降解中间体都会被完全去除,而且持续存在的降解中间体的毒性低于母体化合物。
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引用次数: 0
Facile synthesis and characterization of Cu2Se thin films and self-powered p-Cu2Se/n-Si heterojunction with high-performance photoresponse Cu2Se 薄膜和具有高性能光响应的自供电 p-Cu2Se/n-Si 异质结的简易合成与表征
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-06 DOI: 10.1088/1361-6463/ad687c
Der-Yuh Lin, Yu-Tai Shih, De-Jin Qiu, Yee-Mou Kao, Sheng-Beng Hwang, Ming-Cheng Kao and Chia-Feng Lin
A facile, cost-effective, and scalable chemical vapor deposition technique was used to synthesize p-type Cu2Se thin films on glass and n-type Si substrates. Thorough characterization confirmed the films’ β-phase structure with the correct stoichiometric ratio and exceptional crystalline quality, exhibiting behavior akin to a degenerate semiconductor. Measurements unveiled a work function of 4.83 eV and a bandgap of 2.13 eV for Cu2Se. The fabrication of a p-Cu2Se/n-Si heterojunction was achieved by depositing the p-type Cu2Se thin film onto the n-type Si substrate. The resulting heterostructure displayed rectification behavior, and its energy band diagram resembled a Schottky diode. Further exploration into its photoelectric properties showcased the p-Cu2Se/n-Si heterostructure’s favorable self-powered attribute, characterized by fast, steady, reproducible, sensitive, and robust photoresponsive performance. Consequently, it proves highly suitable for applications in high-frequency photodetectors. Additionally, the p-Cu2Se/n-Si heterojunction’s photovoltaic power conversion efficiency exceeded the reported values of the CuO/Si and Cu2O/Si systems. Here, this study contributes significantly to the pivotal evaluation of p-Cu2Se/n-Si heterostructures for promising optoelectronic applications.
该研究采用了一种简便、经济、可扩展的化学气相沉积技术,在玻璃和 n 型硅基底上合成了 p 型 Cu2Se 薄膜。彻底的表征证实了薄膜的 β 相结构具有正确的化学计量比和优异的结晶质量,表现出类似于退变型半导体的行为。测量结果显示,Cu2Se 的功函数为 4.83 eV,带隙为 2.13 eV。通过在 n 型硅衬底上沉积 p 型 Cu2Se 薄膜,实现了 p-Cu2Se/n-Si 异质结的制造。由此产生的异质结显示出整流行为,其能带图类似于肖特基二极管。对其光电特性的进一步研究表明,p-Cu2Se/n-Si 异质结构具有良好的自供电特性,其特点是快速、稳定、可重现、灵敏和稳健的光致发光性能。因此,它非常适合应用于高频光电探测器。此外,p-Cu2Se/n-Si 异质结的光电转换效率超过了 CuO/Si 和 Cu2O/Si 系统的报告值。这项研究为评估对铜2硅/非晶硅异质结构的光电应用前景做出了重要贡献。
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引用次数: 0
On the modes of nanosecond pulsed plasmas for combustion ignition of quiescent CH4-air mixtures 纳秒脉冲等离子体在静态 CH4 空气混合物燃烧点火中的应用模式
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-05 DOI: 10.1088/1361-6463/ad6876
Chunqi Jiang, Akash C Dhotre, Meimei Lai, Sayan Biswas, James R MacDonald and Isaac W Ekoto
The effect of transient plasma modes on ignition kernel development are discussed here for a quiescent CH4-air combustion model system. A 10 ns high-voltage pulse was applied to a pin-to-pin electrode in lean fuel-air mixtures at room temperature and atmospheric pressure. High-impedance streamer, transient spark and low-impedance spark discharges were identified based on pulse waveforms of voltage and current. A sustained ignition kernel expansion was observed when the plasma discharge transitioned into a transient spark or spark discharge. The minimum ignition energy was obtained at the transient spark mode, which has less than a third of the energy or Coulomb transfer compared to the low-impedance spark. Employing repetitive 10-pulse sequence at 10 kHz, the lean-fuel limit was extended from an equivalence ratio of 0.6 for the single pulse ignition to 0.5. The use of repetitive pulses also allowed streamer breakdown or spark initiation to occur at a lower voltage.
本文讨论了静态 CH4 空气燃烧模型系统中瞬态等离子体模式对点火核发展的影响。在室温和大气压力下,对贫油-空气混合物中的针对针电极施加了 10 毫微秒的高压脉冲。根据电压和电流的脉冲波形,确定了高阻抗流、瞬态火花和低阻抗火花放电。当等离子体放电过渡到瞬态火花放电或火花放电时,可观察到持续的点火内核膨胀。瞬态火花模式获得的点火能量最小,与低阻抗火花相比,其能量或库仑传递不到三分之一。采用频率为 10 kHz 的 10 个重复脉冲序列后,贫油极限从单脉冲点火的 0.6 等效比扩大到 0.5。重复脉冲的使用还允许在较低电压下发生流线击穿或火花启动。
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引用次数: 0
Floquet-engineered valley topotronics in Kekulé-Y bond textured graphene superlattice Kekulé-Y 键纹理石墨烯超晶格中的浮凸工程谷拓扑技术
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-08-01 DOI: 10.1088/1361-6463/ad5e90
Sushmita Saha, Alestin Mawrie
The exquisite distortion in a Kekulé -Y (Kek-Y) superlattice merges the two inequivalent Dirac cones (from the K- and the K′- points) into the highest symmetric Γ-point in the hexagonal Brillouin zone. Here, we report that UV circularly polarized light not only opens up a topological gap at the Γ-point, but also lifts the valley degeneracy at that point. Endowed with Floquet dynamics and by devising a scheme of high-frequency approximation, we propose that the left/right-handedness in polarized light offers the possibility to realize valley-selective circular dichroism in a Kek-Y-shaped graphene superlattice. In addition, the non-vanishing Berry curvature and enumeration of the valley-resolved Chern number CK/CK=+1/1 enable us to assign two pseudospin flavors (up/down) with the two valleys. Thereby, the above observations confirm the topological transition, suggesting the ease of realizing the valley quantum anomalous Hall state within the photon-dressed Kek-Y. These findings further manifest a non-zero optical valley polarization that is maximal at the Γ-point. Our paper thus proposes an optically switchable topological valley filter, which is desired in the evolving landscape of valleytronics.
Kekulé -Y(Kek-Y)超晶格中的精致变形将两个不等价的狄拉克锥(来自 K- 点和 K′-点)合并成六边形布里渊区中最高的对称 Γ 点。在这里,我们报告了紫外圆偏振光不仅在Γ点打开了拓扑缺口,而且还解除了该点的谷退性。借助 Floquet 动力学并通过设计一种高频近似方案,我们提出偏振光的左右手性为在 Kek-Y 形石墨烯超晶格中实现谷选择性圆二色性提供了可能性。此外,由于贝里曲率的非消失和枚举的山谷分辨切尔恩数 CK/CK′=+1/-1,我们可以为两个山谷赋予两种伪自旋味道(上/下)。因此,上述观察结果证实了拓扑转变,表明在光子压制的 Kek-Y 中很容易实现谷量子反常霍尔态。这些发现进一步表明,光谷极化不为零,且在Γ点处达到最大。因此,我们的论文提出了一种可光学切换的拓扑山谷滤波器,这正是不断发展的山谷电子学所需要的。
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引用次数: 0
Deformation theory and nonlinear dynamic behavior of PVC gel actuators 聚氯乙烯凝胶致动器的变形理论和非线性动态行为
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-07-29 DOI: 10.1088/1361-6463/ad6455
Zhuoao Du, Bin Luo, Zhigang Chen, Meiyu Zhu, Kejun Zhu, Yanjie Wang
Polyvinyl chloride (PVC) gel generates complex nonlinear vibration behavior under an alternating current voltage excitation, which has potential application as a dynamic electromechanical actuator. However, there are few studies on the deformation theory of PVC gel actuators, especially the dynamic nonlinear response theory. In this paper, a complex dynamic model is established according to the electrodeformation mechanism of PVC film, and the nonlinear dynamic behavior of the actuator is numerically studied by a differential equation. The effects of applied voltage amplitude, voltage frequency, dibutyl adipate content, mechanical tension, and bias voltage on the dynamic properties of PVC film were analyzed under the condition of equal biaxial tension. The variation of amplitude and the generation and disappearance of the beat frequency during vibration are analyzed by using time-domain characteristics. The degree of PVC actuator nonlinearity as well as vibration stability and periodicity is also reflected based on the phase path and Poincare map. Finally, the law of influence of external condition parameters on the dynamic response of the PVC actuator is obtained.
聚氯乙烯(PVC)凝胶在交流电压激励下会产生复杂的非线性振动行为,具有作为动态机电致动器的潜在应用价值。然而,关于聚氯乙烯凝胶致动器的变形理论,尤其是动态非线性响应理论的研究很少。本文根据 PVC 薄膜的电变形机理建立了一个复杂的动态模型,并通过微分方程对致动器的非线性动态行为进行了数值研究。在双轴拉力相等的条件下,分析了外加电压振幅、电压频率、己二酸二丁酯含量、机械拉力和偏置电压对 PVC 薄膜动态特性的影响。利用时域特性分析了振幅的变化以及振动过程中节拍频率的产生和消失。此外,还根据相位路径和 Poincare 地图反映了 PVC 激励器的非线性程度以及振动稳定性和周期性。最后,得出了外部条件参数对 PVC 激励器动态响应的影响规律。
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引用次数: 0
Study on the effect of heat treatment on the structure, mechanical and electrical properties of alumina fiber insulation 研究热处理对氧化铝纤维绝缘层的结构、机械和电气性能的影响
IF 3.4 3区 物理与天体物理 Q2 PHYSICS, APPLIED Pub Date : 2024-07-25 DOI: 10.1088/1361-6463/ad6456
Li Xie, Yongjin Han and Yang Huang
In this paper, the heat treatment of alumina fiber was studied. The infiltration agent on the fiber surface was removed after heat treatment at 450 °C for 6 h. TG-DSC, scanning electron microscope, x-ray diffraction, Fourier infrared spectrometer, energy dispersive spectrometer, and patterning were used to analyze the thermal weight loss, fiber surface morphology, crystal structure, and composition of alumina fibers. The results show that the aluminum oxide fiber has excellent temperature resistance and does not undergo crystal phase transformation during thermal weight loss. After heat treatment, the fiber surface infiltration agent ablates and dissolves from the fiber surface, and the internal crystal structure of the fiber remains stable. The tensile testing machine was utilized to test the breaking strength of alumina fiber. The fiber still maintained high strength after heat treatment, and the retention rate of breaking strength was greater than 74%. ZC-90G high insulation resistance measuring instrument and WDY-Ⅱ automatic voltage tester were utilized to analyze the insulation resistivity and breakdown strength of alumina fiber before and after heat treatment. The results show that heat treatment can effectively improve the insulation performance and breakdown strength of alumina fiber.
本文研究了氧化铝纤维的热处理。采用 TG-DSC、扫描电子显微镜、X 射线衍射仪、傅立叶红外光谱仪、能量色散光谱仪和图案分析了氧化铝纤维的热失重、纤维表面形貌、晶体结构和成分。结果表明,氧化铝纤维具有优异的耐温性,在热失重过程中不会发生晶相转变。热处理后,纤维表面的浸润剂从纤维表面烧蚀溶解,纤维内部晶体结构保持稳定。利用拉伸试验机测试氧化铝纤维的断裂强度。热处理后的纤维仍保持高强度,断裂强度保持率大于 74%。利用 ZC-90G 高绝缘电阻测量仪和 WDY-Ⅱ 自动电压测试仪分析了热处理前后氧化铝纤维的绝缘电阻率和击穿强度。结果表明,热处理能有效改善氧化铝纤维的绝缘性能和击穿强度。
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Journal of Physics D: Applied Physics
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