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Tannin determination in young coconut coir (Cocos nucifera L.) by FTIR and UV-Vis spectroscopy FTIR和UV-Vis光谱法测定幼椰子中单宁的含量
Pub Date : 2023-03-30 DOI: 10.54076/jumpa.v3i1.271
Yelfira Sari
The coir of young coconut is the largest by product of coconut. Young coconut coir has no important industrial uses and until now has been incinerated or dumped without control. This is because the utilization of young coconut coir is not easy as the old one. Tannin has pharmacological activities including anti-inflammatory, antioxidant, anti-tumor This study aims to determine tannin in young coconut coir (Cocos nucifera L.) using a complementary analytical technique, Fourier Transform Infra-RedFTIR) and Ultraviolet-Visible (UV-Vis) spectroscopy. Sample of young coconut coir was obtained from the waste of bargainer at the local market. Sample was maserated using ethanol as the solvent and then was evaporated to get concentrated extract.  The FTIR and UV-Vis spectra showed that the sample was indicated to contain tannin. The presence of tannin was indicated by appearance of peak at 283 nm and 326 nm in UV-Vis spectra and in the region between 1610-1445 cm-1 by FTIR. This research is an early stage in the characterization of tannin compounds from young coconut coir extract. It is expected that waste have economic value in the future.
幼椰子的椰壳是椰子最大的副产品。年轻的椰壳没有重要的工业用途,直到现在都被焚烧或随意倾倒。这是因为嫩椰壳的利用不如老椰壳容易。单宁具有抗炎、抗氧化、抗肿瘤等药理活性。本研究旨在利用互补分析技术——傅里叶变换红外光谱和紫外可见光谱——测定幼椰子中的单宁。幼龄椰壳的样本是从当地市场上小贩的废物中获得的。样品以乙醇为溶剂浸泡,然后蒸发得到浓缩提取物。红外光谱和紫外可见光谱分析表明,样品中含有单宁。紫外可见光谱在283 nm和326 nm处以及FTIR在1610 ~ 1445 cm-1之间出现了单宁峰,表明单宁的存在。本研究是早期阶段的单宁化合物的表征,从年轻椰子椰子提取物。预计废弃物在未来具有经济价值。
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引用次数: 0
Isolation and Identification of Secondary Metabolic Compounds Acetone Extract from Dutch Eggplant (Cyphomandra betacea) 荷兰茄子(Cyphomandra betacea)次生代谢化合物丙酮提取物的分离鉴定
Pub Date : 2022-09-26 DOI: 10.54076/jumpa.v2i2.230
M. Mawardi
Isolation and identification of secondary metabolite compound in acetone extract from fruit terong belanda (Cyphomandra betacea) have been carried out. The aim of this research is to isolate and identify the secondary metabolite compound in acetone extract from fruit terong belanda (Cyphomandra betacea) which obtain from Enrekang. The compound was obtained by isolation process that consist of several stages, including extraction, fractination, purification and identification. Extraction was carried out using maceration with acetone. The identification was coment by is color test, melt point, solubility and TLC. Base of identification are obtained compound in white powder with melting point 130-131 oC, and positively to the reagent Dragendorf and Wagner gives a brown precipitate that indicated as a alkaloid group. This result is supported by solubility compounds.
本文对槟榔果丙酮提取物中次生代谢产物进行了分离鉴定。本研究的目的是分离鉴定恩热康产的槟榔果丙酮提取物中的次生代谢产物。该化合物经过萃取、分离、纯化和鉴定等几个步骤分离得到。用丙酮浸渍法提取。通过显色法、熔点法、溶解度法和薄层色谱法进行鉴定。碱基鉴定所得化合物为白色粉末,熔点为130-131℃,正向试剂Dragendorf和Wagner给出棕色沉淀,表明为生物碱基团。这一结果得到了溶解度化合物的支持。
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引用次数: 0
Determination of Protein Content by Spectrophotometric Method and Fat Content by Soxhletation Method on Purple Kopek Eggplant and Green Kopek Eggplant 紫外分光光度法测定紫Kopek茄子和绿Kopek茄子的蛋白质含量和索氏法测定脂肪含量
Pub Date : 2022-09-26 DOI: 10.54076/jumpa.v2i2.229
Kartika Hasan
The type of research is quantitative research which is concerned with determining how much certain substances are contained in a sample. The formulation of the problem in this study is how much protein and fat levels are contained in the green kopek green eggplant kopeksangegg plant. The study was conducted to determine how many grams of protein and fat content in purple kopek eggplant and green kopek eggplant samples. With a spectrophotometric method (Lowry) for the determination of protein content and one method of hot extraction is the soxhletation method for the determination of fat content. The results showed that the protein content in 50 g of eggplant purple kopek was 0.0323 g and 50 g eggplant green kopek was 0.0375 g. The fat content in 10 grams of eggplant purple kopek is 0.1794% and 10 grams of eggplant green kopek is 0.1612%. Based on the results of the research that has been carried out, it was found that the protein content of eggplant kopek did not meet the DKBM standard, namely 1.4-2 g in a sample of 100 g. While the standard fat content obtained by DKBM is 1.1 g in a sample of 100 g.
这类研究是定量研究,涉及确定样品中含有多少某些物质。本研究的拟定问题是绿kopek绿茄子kopeksangegg植株中含有多少蛋白质和脂肪水平。这项研究是为了确定紫色kopek茄子和绿色kopek茄子样品中蛋白质和脂肪的含量。用分光光度法(Lowry)测定蛋白质含量,用热萃取法(soxletation)测定脂肪含量。结果表明:50g紫紫kopek的蛋白质含量为0.0323 g, 50g绿kopek的蛋白质含量为0.0375 g。10克茄子紫kopek的脂肪含量为0.1794%,10克茄子绿kopek的脂肪含量为0.1612%。根据已经开展的研究结果,发现茄子kopek的蛋白质含量不符合DKBM标准,即100 g样品中的1.4-2 g。而DKBM获得的标准脂肪含量为每100克样品1.1克。
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引用次数: 0
Corncob Activated Carbon Adsorption Capacity (Zea mays L.) Against Rhodamine B. Dyes 玉米芯活性炭吸附量(Zea mays L.)对罗丹明b染料
Pub Date : 2022-09-26 DOI: 10.54076/jumpa.v2i2.231
Sudarmi Sudarmi
The aims of this experimental research are to determine the optimum of contact time, influence of stirring against absorbing power, and adsorption capacity of activated carbon corn cob to pigmen Rhodamin B. This research was done to vary contact time and first concentration of pigmen Rhodamin B. The result of this research showed that optimum of time contact needed activated carbon corn cob to adsorption pigmen Rhodamin B 45 minutes, rapid process way would be more biggest with more big the contact time until reach optimum time and adsorption capacity of activated carbon corn  cob against pigmen Rhodamin B were 2,2255 mg/g. The value was more biggest than the adsorption capacity of activated carbon waste of sugar cane against pigment Rhodamin B were 2,078 mg/g. Isoterm system of the activated carbon corn cob to pigmen Rhodamin B followed isoterm system Langmuir with adsorption capacity were 2,2255 mg/g. Isoterm system Freundlich value of adsorption capacity were 1,481 mg/g.
本实验研究的目的是确定最佳接触时间、搅拌对活性炭玉米芯对罗达明B的吸附能力的影响以及活性炭玉米芯对罗达明B的吸附能力,研究了不同的接触时间和罗达明B的首次浓度。研究结果表明,活性炭玉米芯吸附罗达明B的最佳接触时间为45分钟。接触时间越长,快速处理效果越好,活性炭玉米芯对罗丹明B的吸附量分别为2、2255 mg/g。甘蔗活性炭对色素罗丹明B的吸附量最大,为2078 mg/g。活性炭玉米芯对罗丹明B的吸附量遵循Langmuir体系,吸附量分别为2、2255 mg/g。体系的Freundlich吸附量值为1481 mg/g。
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引用次数: 0
Design of a Light Intensity Regulator with Remote Control for Incandescent Lamps 白炽灯遥控光强调节器的设计
Pub Date : 2022-09-26 DOI: 10.54076/jumpa.v2i2.227
A. Yani
Research has been carried out on the design of a light intensity regulator with a remote control on incandescent lamps. This study aims to design and manufacture a light intensity controller that can be controlled remotely. This research uses Infrared Light Emitting Diode (LED) as transmitter and phototransistor module as receiver. The results of this study indicate that the tool that has been successfully designed and made can function up to a distance of 300 cm.
对白炽灯进行了一种远程控制光强调节器的设计研究。本课题旨在设计和制造一种可远程控制的光强控制器。本研究采用红外发光二极管(LED)作为发射端,光电晶体管模块作为接收端。这项研究的结果表明,已经成功设计和制造的工具可以在300厘米的距离内工作。
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引用次数: 0
Design of a Light Intensity Regulator with Remote Control for Incandescent Lamps 白炽灯遥控光强调节器的设计
Pub Date : 2022-09-26 DOI: 10.54076/jumpa.v2i2.228
Januar Januar
One of the uses of rice washing water is to make nata de rice or bacterial cellulose. This study was conducted to determine the effect of glucose mass and fermentation time on the viscosity of nata de rice. The study was conducted using 1000 ml of water to wash rice then added 10 ml of acetic acid, glucose with 50 grams, 75 grams and 100 grams, 5 grams urea, Acebacter xylinum starter as much as 100 ml then fermented. up to 14 days. Parameters analyzed were glucose mass and time of optimum fermentation conditions on the thickness of nata de rice. Thickness measurements were carried out using shear anchors. The results showed that the optimum thickness of nata was the addition of 100 grams of glucose with an optimum thickness of 17 mm and the optimum time was on the 14th day during fermentation.
淘米水的用途之一是制造天然大米或细菌纤维素。研究了葡萄糖质量和发酵时间对糯米黏度的影响。本研究采用1000ml水洗米,然后加入乙酸10ml,葡萄糖加50克,75克加100克,尿素加5克,木质菌发酵剂加100毫升左右再发酵。最多14天。分析了葡萄糖质量和最佳发酵条件对大米厚度的影响。厚度测量采用剪切锚进行。结果表明,nata的最佳厚度为添加100 g葡萄糖,最佳厚度为17 mm,最佳发酵时间为发酵第14天。
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引用次数: 0
The Signage Placement Directions On The Pedestarian Path, Iskandar Muda Road, Medan City 棉兰市依斯干达慕达路行人路指示牌放置指引
Pub Date : 2022-09-05 DOI: 10.54076/jumpa.v2i1.224
Hibnul Walid, Indra Kesuma Hadi, Muhammad Amin, Surta Ria Nurliana Panjaitan, Rizky Franchitika
The  city  of  Medan  as the  capital  city  of North  Sumatra  Province  has  made  significant progress.  This  coTechnology and Computer Sciencemmercial buildings  in several places, one of which was in the Jalan Iskandar Muda corridor. In general, these buildings are spread along road corridors  that function  as commercial areas in the city of Medan.  Presence signage on Jalan Iskandar Muda, Medan  City,  it turns  out that  they  tend  to maximize the economic potential  of the region, resulting  in a shift in the function of urban space into a space for advertising media expression.  As  an  effort  to  create  city comfort  that  supports  visual  aesthetics  and  does  not interfere  with  pedestrian comfort,  this research   produces   a  design  concept  in  the  form  of  placement  signage   according  to  the designated zone, namely  in the pedestrian zone, the design  of the height  proportion signage to the width of the pedestrian path using a human  scale approach, panel or plane dimension design signage by using the concept golden section, as well as setting the point of placement or spread signage using the concept  of rhythm  and local regulations  that have been established with the aim of limiting  the number of signage  on the pedestrian path.
作为北苏门答腊省首府的棉兰市取得了重大进展。这个联合技术和计算机科学的商业建筑在几个地方,其中一个在Jalan Iskandar Muda走廊。一般来说,这些建筑分布在棉兰市作为商业区的道路走廊上。在棉兰市Jalan Iskandar Muda的存在标牌,事实证明,它们倾向于最大化该地区的经济潜力,导致城市空间功能转变为广告媒体表达空间。为了创造既支持视觉美学又不影响行人舒适度的城市舒适度,本研究提出了按指定区域放置标识的设计理念,即在步行区,采用人性化尺度的方法设计标识的高度与行人路径的宽度比例,采用黄金分割的概念设计面板或平面尺寸的标识;以及使用节奏和当地法规的概念来设置放置或传播标志的点,这些法规的目的是限制人行道上的标志数量。
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引用次数: 0
Manufacturing of Ceramic Reinforced Metal Matrix Composites (Al/Sicp) And Their Characterization Through Powder Metallurgy Methods 陶瓷增强金属基复合材料(Al/Sicp)的制备及其粉末冶金表征
Pub Date : 2022-05-19 DOI: 10.54076/jumpa.v2i1.209
Jepriandi Ginting
Metal Matrix Composites is two or more combination material with aluminum metal as matrix and devolved to fix metal act, strength, high temperature stability and hardness. Metal matrix composites have been developed so many because it has low density, corrosion proof, cheap and easy fabrication. Powder metallurgy technique is one of metal matrix composites fabrication process in solid state that is still developed because more economic, doesn't need difficult equipment. Aluminum that use in this research is Al alloy type 2124. Metal matrix composites fabrication process with powder metallurgy method using wet mixing with pure ethanol, cold compaction 300 MPa and inert gas atmospheric using Nitrogen gas (N2) at sintering process. Variation of sinter temperature that used is 450, 500, 550, and 600 oC with highly temperature average 5 oC/min and holding time for 1 hour and with speed flow Nitrogen gas (N2) 5 lt/min with pressure 1000 kgf/cm2. From research result can be concluded the mechanical properties and physical properties from metal matrix composites reinforced ceramics Al/SiCp increase with sinter temperature highly and with reinforcement particle addition SiC can increase mechanical properties and physical properties such as: hardness, wear resistance, coefficient of thermal expansion and corrosion resistance. From microstructure analysis, particle Sic distributed homogeneously at test specimen based on SEM analysis, and structure crystal analysis test result XRD show that dominant phase appear is Al, and Sic.
金属基复合材料是以铝金属为基体,具有固定金属作用、强度、高温稳定性和硬度的两种或两种以上的复合材料。金属基复合材料以其低密度、耐腐蚀、价格低廉、易于制造等优点得到了广泛的应用。粉末冶金技术是固体金属基复合材料的一种制备方法,由于其经济、不需要复杂的设备,目前仍在发展中。本研究使用的铝为2124型铝合金。金属基复合材料的制备工艺采用粉末冶金法,采用纯乙醇湿法混合,300 MPa冷压,惰性气体常压,烧结过程中采用氮气(N2)。使用的烧结温度变化为450、500、550和600℃,高温平均5℃/min,保温时间1小时,高速流量氮气(N2) 5 lt/min,压力1000 kgf/cm2。研究结果表明,金属基复合材料增强陶瓷Al/SiCp的力学性能和物理性能随着烧结温度的升高而显著提高,添加增强颗粒SiC可以提高材料的硬度、耐磨性、热膨胀系数和耐腐蚀性等力学性能和物理性能。从显微组织分析来看,SEM分析表明试样中Sic颗粒分布均匀,XRD分析结果表明,主要相为Al和Sic。
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引用次数: 0
The Effect of Addition of Ash from Burning Wood Powder to the Mechanical and Physical Properties of Concrete 燃烧木粉灰分掺加对混凝土力学物理性能的影响
Pub Date : 2022-03-01 DOI: 10.54076/jumpa.v2i1.208
Yusnitaerna Erna
The wood powder is the waste from woods industry that further used as a mixture of plant soil. Scientist have used the powder of wood to make a particle board. This research, We used the ash of wood powder as an additive thing in the concrete mixture. The test is done for physics and mechanics of the concrete. The sample is made from the ingredients 1 cement : 2 sand : 3 pebble. In variation add to ash of the wood powder for cement is 5%, 10%, and 15%. The result of the researching show that the used of the ash of wood powder can build the impact of the concrete is 9.54% from normal concrete with the mixture of the ash of wood powder is 15%. Orther side for the physics, the water absorption and porosity with the ash of the wood powder is from 4.94% to 14.35% and from 4.16% to 14.89% higher than the normal concrete.
木粉是木材工业的废料,进一步用作植物土壤的混合物。科学家们用木粉制作了刨花板。本研究将木粉灰分作为混凝土混合料的添加剂。这项试验是为了测试混凝土的物理和力学性能。样品由1水泥:2沙子:3鹅卵石组成。水泥用木粉在灰分中的添加量分别为5%、10%和15%。研究结果表明,木粉灰分掺量为15%时,对混凝土的影响比普通混凝土大9.54%。另一方面,在物理性能方面,木粉灰分掺量比普通混凝土的吸水率和孔隙率分别提高4.94% ~ 14.35%和4.16% ~ 14.89%。
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引用次数: 0
ISOLATION AND NODULATION TEST OF Rhizobium sp. FROM Pueraria javanica (Benth.) Benth. AND LIABILITY TEST ON THE CARRIER MEDIUM OF PEAT AND COMPOST FROM PALM OIL PALM EMPTY FRUITS 土葛根瘤菌的分离与结瘤试验Benth。并对棕榈空果中泥炭和堆肥的载体介质进行了负荷试验
Pub Date : 2022-03-01 DOI: 10.54076/jumpa.v2i1.205
Agnes Siska Situmorang
Isolation and Nodulation Rhizobium sp. from Pueraria javanica (Benth.) Benth. and Study of  Its Survival on Peat Soil and Compost of Oil Palm Empty Fruit Bunch was done from March to July 2008, in the Laboratory of Plant Biotechnology of Indonesian Oil Palm Research Institute (IOPRI) Marihat Research Station in Pematang Siantar, and Laboratory of Microbiology, Department of Biology, FMIPA USU. The sampel of nodules were taken from the roots of Pueraria javanica growing in the oil palm plantation at Sei Aek Pancur, Marihat, and University of North Sumatera. Ten isolates were isolated from the nodules and all of them could form root nodule after 8 weeks of inoculation in a nodulation trial. Another trial was conducted to study the survival of the Rhizobium in 2 different types of media: peat soil and compost of oil palm empty fruit bunch. It was found that all of the isolates could survive in both media during 4 weeks of observation. Statistically, the Rhizobium had a more stable viability in compost.
土葛根瘤菌的分离与结瘤研究Benth。2008年3月至7月,在印尼油棕研究所(IOPRI)位于Pematang Siantar的Marihat研究站植物生物技术实验室和USU FMIPA生物系微生物实验室进行了油棕空果串在泥炭土和堆肥上的生存研究。瘤样取自生长在马里哈特市Sei Aek Pancur和北苏门答腊大学油棕种植园的爪哇葛根。从根瘤中分离出10株菌株,接种8周后均能形成根瘤。研究了根瘤菌在泥炭土和油棕空果束堆肥2种不同培养基上的生存情况。在4周的观察中,所有分离株均能在两种培养基中存活。据统计,根瘤菌在堆肥中具有更稳定的生存能力。
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引用次数: 0
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Jurnal Matematika Dan Ilmu Pengetahuan Alam LLDikti Wilayah 1 (JUMPA)
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