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Comparative analysis of kokumi tastant intensity from mechanically deboned meat across three species through in vitro calcium‐sensing receptor activity 通过体外钙传感受体活性比较分析三个物种机械去骨肉的 Kokumi 味觉强度
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1111/ijfs.17293
Jihan Kim, Santanu Deb‐Choudhury, Arvind Subbaraj, Carolina E. Realini, Raise Ahmad
SummaryThe emergence of kokumi sensation as a flavour enhancer prompted the search for cost effective and the sustainable production of kokumi flavour substances (KS), including small γ‐glutamyl peptides (GGP) and aromatic free amino acids (FAA). We sought to investigate the potential of mechanically deboned meat (MDM) from beef, mutton, lamb and venison for KS production through enzymatic γ‐glutamylation. Liquid chromatography‐mass spectrometry (LC–MS) and in vitro calcium‐sensing receptor (CaSR) activity assays were utilised to identify GGPs and their kokumi intensity, respectively. The enzymatic method significantly increased GGP and FAA in all MDM samples with differences in individual peptides across the species. Notably, all four sources of MDM activated CaSR in a dose‐dependent manner, displaying varying potency and efficacy levels. Beef, lamb and mutton showed a similar range of higher potency, while venison exhibited lower potency but higher efficacy. The thermal stability of γ‐glutamylated beef samples, used as an exemplar, was confirmed at temperatures of 80 °C, 120 °C and 150 °C. Given these findings, MDM represents a promising substrate for KS production and warrants further investigation to assess its practical applicability for enhancing kokumi flavour in the food industry.
摘要作为一种增味剂,Kokumi 香味的出现促使人们寻找具有成本效益和可持续生产的 Kokumi 香味物质 (KS),包括小的γ-谷氨酰肽 (GGP) 和芳香游离氨基酸 (FAA)。我们试图研究牛肉、羊肉、羊肉和鹿肉的机械去骨肉(MDM)通过酶法γ-谷氨酰化生产 KS 的潜力。液相色谱-质谱法(LC-MS)和体外钙感受体(CaSR)活性测定法分别用于鉴定 GGPs 及其 Kokumi 强度。酶解法明显增加了所有 MDM 样品中的 GGP 和 FAA,但不同物种中的单个肽存在差异。值得注意的是,所有四种来源的 MDM 都能以剂量依赖的方式激活 CaSR,并显示出不同的效力和功效水平。牛肉、羔羊肉和羊肉显示出相似的较高效力范围,而鹿肉则显示出较低的效力,但效力较高。作为示例,γ-谷氨酰化牛肉样品在 80 ℃、120 ℃ 和 150 ℃ 的温度下具有热稳定性。鉴于这些发现,MDM 是一种很有前景的 KS 生产基质,值得进一步研究,以评估其在食品工业中增强 Kokumi 风味的实际应用性。
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引用次数: 0
Nutritional retention and browning minimisation in dehydrated onion slices through potassium metabisulphite and sodium chloride pre‐treatments 通过焦亚硫酸钾和氯化钠预处理保留脱水洋葱片的营养成分并减少褐变
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1111/ijfs.17334
Sajeel Ahamad, Vidya Ram Sagar, Ram Asrey, Sabina Islam, B. S. Tomar, B. R. Vinod, M. Menaka, Ajeet Kumar
SummaryThe global demand for dehydrated onion is on the rise, driven by the increasing consumer preference for ready‐to‐eat convenience foods. This study focused on enhancing the quality and functional properties of dehydrated onion slices (cv. Pusa Shobha) through different pre‐treatment and drying conditions. Fresh onion slices were subjected to pre‐treatment using NaCl (3%, 5% and 7%) and KMS (0.3%, 0.5% and 0.7%) solutions for 10 min, followed by tray drying at 50 °C, 60 °C and 70 °C temperatures for varying durations of 14, 12 and 10 h, respectively. Based on physicochemical and functional properties, onion slices pretreated with 5% NaCl + 0.5% KMS and dehydrated at 60 °C for 12 h retained higher bioactive compounds like total phenols (166.32 mg GAE 100 g−1 DW), total flavonoids (28.94 mg QE g−1 DW), ascorbic acid (12.45 mg 100 g−1 DW), quercetin (172.88 μg g−1 DW) and total antioxidant activity (24.59 μmol TE g−1 DW). Additionally, it maintained superior sensory acceptability with higher pungency (7.15 μmol g−1 DW), dehydration ratio (9.25%), rehydration ratio (5.20%), lower non‐enzymatic browning (0.36) and moisture content (5.75%). Hence, the optimised treatment of ‘Pusa Shobha’ slices with 5% NaCl + 0.5% KMS, followed by dehydration at 60 °C for 12 h, yields dehydrated onion slices with superior bioactive compounds, sensory acceptability, and enhanced functional properties. The findings of his research offer valuable technology for the food industry, providing a practical and efficient method to produce high‐quality dehydrated onion slices.
摘要由于消费者越来越偏爱即食方便食品,全球对脱水洋葱的需求不断增加。本研究的重点是通过不同的预处理和干燥条件提高脱水洋葱片(品种:Pusa Shobha)的质量和功能特性。使用 NaCl(3%、5% 和 7%)和 KMS(0.3%、0.5% 和 0.7%)溶液对新鲜洋葱片进行 10 分钟的预处理,然后分别在 50 ℃、60 ℃ 和 70 ℃ 的温度下进行 14、12 和 10 小时的托盘干燥。根据物理化学和功能特性,用 5% NaCl + 0.5% KMS 预处理并在 60 °C 下脱水 12 小时的洋葱片保留了较高的生物活性化合物,如总酚(166.32 毫克 GAE 100 克-1 DW)、总黄酮类化合物(28.94 毫克 QE 克-1 DW)、抗坏血酸(12.45 毫克 100 克-1 DW)、槲皮素(172.88 微克克-1 DW)和总抗氧化活性(24.59 微摩尔 TE 克-1 DW)。此外,它还具有较高的辛辣味(7.15 μmol g-1 DW)、脱水率(9.25%)、复水率(5.20%)、较低的非酶促褐变(0.36)和水分含量(5.75%),从而保持了极佳的感官可接受性。因此,用 5% NaCl + 0.5% KMS 对 "Pusa Shobha "切片进行优化处理,然后在 60 °C 下脱水 12 小时,可获得具有优质生物活性化合物、感官可接受性和更强功能特性的脱水洋葱切片。他的研究成果为食品工业提供了宝贵的技术,为生产高质量的脱水洋葱片提供了实用高效的方法。
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引用次数: 0
The effectiveness of garlic extracts on biogenic amine formation by foodborne pathogens and fish spoilage bacteria 大蒜提取物对食源性致病菌和鱼类腐败菌形成生物胺的影响
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1111/ijfs.17280
Hatice Yazgan, Esmeray Kuley, Yesim Ozogul, Fatih Ozogul, Elena Bartkiene, João Miguel Rocha
SummaryImpacts of aqueous and ethanolic extracts of garlic were investigated in suppressing bacterial growth and biogenic amine (BA) formation by selected foodborne pathogens (Candida albicans, Salmonella paratyphi A, Escherichia coli and Staphylococcus aureus) and fish spoilage bacteria (Enterococcus faecalis, Photobacterium damselae and Pseudomonas luteola). The spread‐plate method was used to monitor bacterial growth in histidine decarboxylase broth (HDB), whereas the rapid high‐performance liquid chromatographic (HPLC) method was used for BA analysis. Bacterial growth and their ammonia and BA production were monitored using HDB. The results showed that bacterial growth on HDB was in the range from 9.13, for P. luteola, to 9.54 log CFU (colony‐forming units) mL−1, for S. aureus and C. albicans. The presence of garlic extracts in HDB resulted considerably in lowering bacterial growth and BA formation (P < 0.05). The highest inhibitory activities of ethanolic and water garlic extracts were obtained for Gram‐positive S. aureus with 1.4 and 1.5 logarithmic reduction on bacterial growth, followed by Gram‐negative Salmonella Paratyphi A and E. coli. Application of garlic extracts, mainly ethanolic ones, showed a significant inhibitory effect on bacterial ammonia production, with 4‐100‐fold lower ammonia accumulation (P < 0.05). Bacteria produced all tested BAs, mainly dopamine, agmatine and tryptamine. The highest levels of histamine and tyramine (61.99 and 36.45 mg L−1) were produced by S. aureus. In the presence of aqueous or ethanolic garlic extracts, putrescine production by E. faecalis was around 110‐fold lower than that of the control group. Results revealed that both garlic extracts are potent antimicrobials that can control the growth of foodborne pathogens and their harmful BA formation.
摘要研究了大蒜的水提取物和乙醇提取物在抑制细菌生长和某些食源性致病菌(白色念珠菌、副伤寒 A 型沙门氏菌、大肠杆菌和金黄色葡萄球菌)和鱼类腐败菌(粪肠球菌、大肠光杆菌和黄绿假单胞菌)形成生物胺(BA)方面的影响。采用展板法监测组氨酸脱羧酶肉汤(HDB)中细菌的生长情况,而采用快速高效液相色谱法(HPLC)分析 BA。使用 HDB 监测了细菌的生长及其氨和 BA 的产生。结果表明,在 HDB 上,金黄色葡萄球菌和白色念珠菌的细菌生长量在 9.13 至 9.54 log CFU(菌落形成单位)mL-1 之间。大蒜提取物在 HDB 中的存在大大降低了细菌的生长和 BA 的形成(P < 0.05)。大蒜乙醇提取物和水提取物对革兰氏阳性金黄色葡萄球菌的抑制活性最高,分别降低了 1.4 和 1.5 对数,其次是革兰氏阴性的副伤寒 A 沙门氏菌和大肠杆菌。应用大蒜提取物(主要是乙醇提取物)对细菌产生氨气有显著的抑制作用,氨气积累降低了 4-100 倍(P < 0.05)。细菌产生了所有测试的生物碱,主要是多巴胺、γ-氨基丁酸和色胺。金黄色葡萄球菌产生的组胺和酪胺含量最高(61.99 和 36.45 mg L-1)。在大蒜水提取物或乙醇提取物的作用下,粪肠球菌产生的腐胺比对照组低约 110 倍。结果表明,这两种大蒜提取物都是有效的抗菌剂,可以控制食源性病原体的生长及其有害 BA 的形成。
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引用次数: 0
Functional chocolate: exploring advances in production and health benefits 功能巧克力:探索生产和健康益处方面的进步
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17312
Sümeyye Sarıtaş, Hatice Duman, Burcu Pekdemir, João Miguel Rocha, Fatih Oz, Sercan Karav
SummaryChocolate has been a part of human consumption for millennia, serving as a confection, medicine and aphrodisiac. Chocolate consumption is increasing worldwide, and independent of the age or social background. The substantial content of chocolate may provide consumers with antioxidant, anti‐inflammatory, antimicrobial, antiallergenic, and anticarcinogenic benefits. Beyond such properties, diverse bioactive ingredients are utilised in the creation of functional chocolate products aiming at promoting health and meeting the modern consumers' demands and market orientations. These products are primarily focused on enhancing nutraceutical effects, such as antioxidant activity, protein content and prebiotic effects. Additionally, the use of A2 milk powder in chocolate production holds promising expectations towards enhancing the digestibility of the products. Due to the superior affinity of proteolytic enzymes, A2 milk can be digested more easily than A1 milk. In this way, with the addition of A2 milk to chocolate, it may become more easily digestible. The objectives of this review are a comprehensive understanding of the evolution of chocolate consumption, its health benefits, and the contemporary innovations in chocolate production. Additionally, the potential for developing easily digestible, functional chocolates made from A2 milk, which could rejuvenate functional chocolate production, is discussed in this article.
摘要几千年来,巧克力一直是人类消费的一部分,它既是糖果,也是药品和壮阳药。巧克力的消费量在全球范围内不断增长,而且不受年龄和社会背景的影响。巧克力中的大量成分可为消费者带来抗氧化、抗炎、抗菌、抗过敏和抗癌等益处。除了这些特性外,人们还利用各种生物活性成分制作功能性巧克力产品,旨在促进健康,满足现代消费者的需求和市场导向。这些产品主要侧重于增强营养保健功效,如抗氧化活性、蛋白质含量和益生元功效。此外,在巧克力生产中使用 A2 奶粉有望提高产品的消化率。由于蛋白水解酶的亲和力更强,A2 牛奶比 A1 牛奶更容易被消化。因此,在巧克力中添加 A2 牛奶后,巧克力可能会变得更容易消化。本综述旨在全面了解巧克力消费的演变、其对健康的益处以及当代巧克力生产的创新。此外,本文还讨论了开发由 A2 牛奶制成的易消化功能性巧克力的潜力,这将为功能性巧克力的生产注入新的活力。
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引用次数: 0
Nutritional and functional aspects of fermented algae 发酵藻类的营养和功能方面
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17297
Sümeyye Sarıtaş, Hatice Duman, Sercan Karav
SummaryIn recent years, there has been an increasing emphasis on natural and healthy nutrition, leading to increased interest in fermented foods and their associated health benefits. In line with this trend, fermentation is employed to enhance the exceptional properties of algae, including their nutritional value and digestibility, rendering them suitable for consumption as food. Fermentation of algae involves the conversion of carbohydrates into alcohol or organic acids by microorganisms, including bacteria or yeast. First of all, the fermentation process results in enhanced antioxidant activity, antimicrobial effects, anti‐inflammatory properties, immunomodulatory effects, anti‐glycation activity, antihypertensive effects and neuroprotective activity by increasing the bioavailability of bioactive compounds in algae. In addition, this method encourages the incorporation of algae into food products. In this process, both the flavour and texture are enhanced, while simultaneously preserving and enriching the beneficial nutrients and compounds present in algae. Despite the availability of various fermented algae products in the market, their widespread adoption has yet to be realised. The incorporation of fermented algae into food products not only enhances their nutritional content but also fosters the emergence of a new segment within the fermented food market. Herein, the concept of fermented algae, the fermentation process, its nutritional value and its health benefits are explored.
摘要近年来,人们越来越重视天然健康的营养,从而对发酵食品及其相关的健康益处越来越感兴趣。为顺应这一趋势,发酵法被用来提高藻类的特殊属性,包括营养价值和消化率,使其适合作为食品食用。海藻发酵是指微生物(包括细菌或酵母)将碳水化合物转化为酒精或有机酸。首先,发酵过程可提高藻类中生物活性化合物的生物利用率,从而增强抗氧化活性、抗菌效果、抗炎特性、免疫调节效果、抗糖化活性、抗高血压效果和神经保护活性。此外,这种方法还有助于将海藻融入食品中。在这一过程中,风味和口感都得到了改善,同时还保留并丰富了海藻中有益的营养成分和化合物。尽管市场上有各种发酵海藻产品,但尚未得到广泛采用。在食品中加入发酵藻类不仅能提高食品的营养成分,还能促进发酵食品市场出现一个新的细分市场。本文探讨了发酵藻类的概念、发酵过程、营养价值及其对健康的益处。
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引用次数: 0
Physicochemical and nutritional characteristics of vegan protein bars formulated with sweet potato and rice protein 用甘薯和大米蛋白配制的素食蛋白棒的理化和营养特性
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17294
In‐Ha Baek, Ha‐Seong Cho, Nurul Saadah Said, Ibukunoluwa Fola Olawuyi, Kyu‐Rim Kim, Won‐Young Lee
SummaryIn response to the growing interest in plant‐based alternatives and vegan diets, this study aimed to develop novel sweet potato‐based vegan protein bars enriched with rice protein (RP) as an alternative protein source. The vegan protein bars (VPBs) formulated with varying RP content (0–32 g) were evaluated for nutritional, textural, microstructural and sensory properties. Nutritional analysis revealed a proportional increase in protein content (8.94%–21.77%) and energy value (310.29–353.32 kcal/100 g) with increasing RP content. The progressive inclusion of RP significantly (P < 0.05) improved the textural properties of VPBs, notably increasing cohesiveness (0.07%–0.60%), chewiness (8.71–105.02 g) and firmness (1453.80–3444.03 kg cm−2), with all VPBs receiving favourable sensory evaluation scores. Importantly, all VPBs received favourable sensory scores. Microstructural analysis revealed the mechanism for textural enhancement in enriched VPBs, indicating a positive correlation between higher RP content and the number and size of surface clumps. Amino acid profiling indicated over 50% increases in valine content and essential amino acid scores in enriched VPBs compared to those without RP. Moreover, protein‐enriched VPBs exhibited superior antioxidant activity. In conclusion, these findings suggest the potential of sweet potato and RP in developing VPBs, highlighting the value of plant‐based ingredients in vegan food products.
摘要 鉴于人们对植物性替代品和素食的兴趣与日俱增,本研究旨在开发富含大米蛋白质(RP)的新型甘薯素食蛋白棒,作为替代蛋白质来源。研究人员对不同 RP 含量(0-32 克)的素食蛋白棒(VPBs)进行了营养、质地、微结构和感官特性评估。营养分析表明,随着 RP 含量的增加,蛋白质含量(8.94%-21.77%)和能量值(310.29-353.32 千卡/100 克)也成比例增加。逐步添加 RP 能显著改善 VPB 的质地特性(P < 0.05),尤其是增加了粘合度(0.07%-0.60%)、咀嚼感(8.71-105.02 克)和坚固度(1453.80-3444.03 千克/厘米-2),所有 VPB 都获得了良好的感官评价分数。重要的是,所有 VPB 都获得了良好的感官评分。微观结构分析揭示了富集 VPB 纹理增强的机制,表明较高的 RP 含量与表面团块的数量和大小呈正相关。氨基酸分析表明,与不含 RP 的 VPB 相比,富集 VPB 中的缬氨酸含量和必需氨基酸得分增加了 50%以上。此外,富含蛋白质的 VPB 还表现出卓越的抗氧化活性。总之,这些研究结果表明了甘薯和 RP 在开发 VPB 方面的潜力,凸显了植物性成分在素食食品中的价值。
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引用次数: 0
Characterisation of finger millet (Eleusine coracana) starch isolated by conventional and ultrasound‐assisted starch isolation methods 用传统方法和超声波辅助淀粉分离法分离出的小米(Eleusine coracana)淀粉的特征
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17303
Shweta Yadav, Sunita Mishra, Kambhampati Vivek, Sabyasachi Mishra
SummaryStarch is a versatile biomaterial with a wide range of applications across various industrial sectors. Therefore, starch isolation methods play a crucial role in fulfilling the demand for high‐quality starch required for different applications. Waxy maize starch is the most used starch for different food applications. It is isolated using an alkaline extraction method and available in the market at a high price. The traditional process of starch isolation involves labour‐intensive and costly downstream processing that leads to exploring cost‐effective isolation methods for various food applications. Finger millet (Eleusine coracana) is an underutilised cereal crop composed of 65–70% of starch. In the present study, the starch from finger millet is isolated using conventional and ultrasound‐assisted isolation methods to fulfil the current requirement. The isolated finger millet starch was characterised by morphological structure obtained by scanning electron microscopy (SEM), X‐ray diffractogram (XRD), infrared spectrum obtained by Fourier transform infrared spectrometer (FT‐IR), differential scanning calorimetry (DSC) analysis, and rheological analysis. The SEM images confirmed the reduced particle size and uniform grain size distribution in the starch isolated using ultrasound‐assisted isolation. The relative crystallinity of starch isolated using ultrasound‐assisted isolation method (69.05 ± 0.57%) was higher compared to other conventional isolation methods (57.18 ± 0.70%, 67.66 ± 1.00%, and 68.34 ± 0.33% for distilled water soaking, alkali soaking, and sodium bisulphite soaking, respectively). The FTIR analysis confirmed no significant changes in the functional group of starch with respect to different isolation methods. Thermal and rheological analysis of isolated starch using ultrasound‐assisted isolation indicated the lowest gelatinisation enthalpy (45.38 ± 1.67 J/g) and showed the lowest loss factor indicating the most elastic behaviour, respectively.
摘要淀粉是一种用途广泛的生物材料,在各个工业部门都有广泛的应用。因此,淀粉分离方法在满足不同应用对高质量淀粉的需求方面起着至关重要的作用。蜡质玉米淀粉是不同食品应用中使用最多的淀粉。它采用碱性提取法分离,在市场上售价不菲。传统的淀粉分离过程涉及劳动密集型和成本高昂的下游加工,这就需要为各种食品应用探索具有成本效益的分离方法。手指粟(Eleusine coracana)是一种未充分利用的谷类作物,其淀粉含量高达 65-70%。本研究采用传统和超声波辅助分离方法从小米中分离出淀粉,以满足当前的需求。通过扫描电子显微镜(SEM)获得的形态结构、X 射线衍射图(XRD)、傅立叶变换红外光谱仪(FT-IR)获得的红外光谱、差示扫描量热仪(DSC)分析和流变分析,对分离出的小米淀粉进行了表征。扫描电子显微镜图像证实,使用超声辅助分离技术分离出的淀粉粒度减小,粒度分布均匀。与其他传统分离方法(蒸馏水浸泡法、碱浸泡法和亚硫酸氢钠浸泡法分别为 57.18 ± 0.70%、67.66 ± 1.00% 和 68.34 ± 0.33%)相比,超声辅助分离法分离出的淀粉的相对结晶度(69.05 ± 0.57%)更高。傅立叶变换红外光谱分析证实,淀粉的官能团在不同分离方法下没有明显变化。使用超声波辅助分离法对分离出的淀粉进行的热分析和流变分析表明,其糊化焓(45.38 ± 1.67 焦耳/克)最低,损失因子最低,表明其弹性最好。
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引用次数: 0
Bioactive lipid‐enriched concentrates from squid discards by one‐step and two‐step extractions with non‐halogenated solvents 用无卤溶剂一步法和两步法萃取乌贼废弃物中富含生物活性的浓缩脂质
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-29 DOI: 10.1111/ijfs.17336
David Paz, Marcos Trigo, Sidonia Martínez, Santiago P. Aubourg
SummaryThis study focused on the preparation of lipid concentrates with high contents of bioactive molecules. Different one‐step and two‐step extractions with non‐halogenated solvents (hexane, HX; isopropanol, IP) were carried out on Patagonian squid (Doryteuthis gahi) discards. As a first step, HX extractions (one, two or three times) were carried out. The resulting substrates were extracted with IP (two, three or four times). Analysis of lipid extracts included total lipid, phospholipid (PL) and tocopherol values, and fatty acid (FA) profile. HX extractions led to remarkable α‐ and γ‐tocopherol values (ca. 1400 and 23 mg kg−1 lipids, respectively); no effect (P > 0.05) of the number of HX extractions was observed. IP extracts provided high PL values (383–501 mg kg−1 lipids); the highest average values were detected with four IP extractions after three HX extractions. Values obtained for tocopherols and PLs were higher (P < 0.05) than those obtained by employing the conventional (chloroform/methanol, 1:1) lipid extraction (ca. 496 and 11 mg kg−1 lipids and 400 g kg−1 lipids, respectively). Range values detected for eicosapentaenoic and docosahexaenoic acid values and the ω3/ω6 FA ratio were similar to those obtained by the conventional procedure. A valuable procedure is proposed for obtaining PL‐ and tocopherol‐enriched concentrates from marine waste with non‐halogenated solvents.
摘要 本研究的重点是制备生物活性分子含量高的脂质浓缩物。对巴塔哥尼亚鱿鱼(Doryteuthis gahi)废弃物进行了不同的一步法和两步法非卤溶剂(正己烷,HX;异丙醇,IP)萃取。第一步是进行 HX 提取(一次、两次或三次)。所得底物用 IP 提取(2、3 或 4 次)。脂质提取物的分析包括总脂质、磷脂(PL)和生育酚值以及脂肪酸(FA)概况。HX 提取物可产生显著的 α- 和 γ-生育酚值(分别约为 1400 和 23 毫克/千克-1 脂质);HX 提取物的提取次数没有影响(P > 0.05)。IP 提取物提供了较高的 PL 值(383-501 毫克/千克-1 脂质);在三次 HX 提取之后,四次 IP 提取物检测到的平均值最高。获得的生育酚和聚乳酸值(P< 0.05)高于采用传统(氯仿/甲醇,1:1)脂质萃取法获得的值(分别约为 496 和 11 毫克/千克-1 脂质和 400 克/千克-1 脂质)。检测到的二十碳五烯酸和二十二碳六烯酸值范围值以及ω3/ω6 FA 比值与传统方法得到的值相似。提出了一种利用非卤化溶剂从海洋废弃物中获得富含聚乳酸和生育酚浓缩物的有效方法。
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引用次数: 0
Stearic acid enhanced starch nanocrystal integration in cassava starch film 硬脂酸增强木薯淀粉膜中淀粉纳米晶的整合能力
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-26 DOI: 10.1111/ijfs.17310
Nkosingiphile L. Nzama, Alain Dufresne, Eric O. Amonsou
SummaryStarch nanocrystals (SNCs) have emerged as promising biodegradable nanomaterial for the enhancement of biopolymer films' properties. Nevertheless, using SNCs alone is difficult due to restricted capacity for nanocrystal integration within the film's matrix. The objective of this study was to enhance the properties of biopolymer films using waxy corn starch nanocrystals supplemented with stearic acid. Cassava starch films containing varying proportions of SNCs (0–20 wt.% starch) and steric acid (2%) were prepared and characterised. The inclusion of stearic acid substantially improved SNC integration from 5% to 15%, yielding nanocomposite films with better tensile strength, thermal stability and barrier properties than those prepared with native starch or starch‐fatty acid alone. The improvement in film properties was attributed to V‐amylose complexes formation, increased crystallinity and hydrophobicity. Microscopy images revealed homogenous film surfaces, depicting greater nanocrystal dispersibility. The supplementation of lipid additives offers a valuable strategy to improve the integration of SNCs in film matrices.
摘要淀粉纳米晶体(SNCs)已成为增强生物聚合物薄膜性能的有前途的生物可降解纳米材料。然而,由于纳米晶体在薄膜基质中的整合能力受到限制,单独使用 SNCs 十分困难。本研究的目的是使用添加硬脂酸的蜡质玉米淀粉纳米晶体来增强生物聚合物薄膜的性能。制备了含有不同比例 SNCs(0-20 wt.% 淀粉)和硬脂酸(2%)的木薯淀粉薄膜,并对其进行了表征。硬脂酸的加入大大提高了 SNC 的整合度(从 5%提高到 15%),制备出的纳米复合薄膜与单独使用本地淀粉或淀粉脂肪酸制备的薄膜相比,具有更好的拉伸强度、热稳定性和阻隔性能。薄膜性能的改善归因于 V-amylose 复合物的形成、结晶度和疏水性的提高。显微镜图像显示薄膜表面均匀,纳米晶体分散性更高。补充脂质添加剂为改善 SNC 在薄膜基质中的整合提供了一种有价值的策略。
{"title":"Stearic acid enhanced starch nanocrystal integration in cassava starch film","authors":"Nkosingiphile L. Nzama, Alain Dufresne, Eric O. Amonsou","doi":"10.1111/ijfs.17310","DOIUrl":"https://doi.org/10.1111/ijfs.17310","url":null,"abstract":"SummaryStarch nanocrystals (SNCs) have emerged as promising biodegradable nanomaterial for the enhancement of biopolymer films' properties. Nevertheless, using SNCs alone is difficult due to restricted capacity for nanocrystal integration within the film's matrix. The objective of this study was to enhance the properties of biopolymer films using waxy corn starch nanocrystals supplemented with stearic acid. Cassava starch films containing varying proportions of SNCs (0–20 wt.% starch) and steric acid (2%) were prepared and characterised. The inclusion of stearic acid substantially improved SNC integration from 5% to 15%, yielding nanocomposite films with better tensile strength, thermal stability and barrier properties than those prepared with native starch or starch‐fatty acid alone. The improvement in film properties was attributed to V‐amylose complexes formation, increased crystallinity and hydrophobicity. Microscopy images revealed homogenous film surfaces, depicting greater nanocrystal dispersibility. The supplementation of lipid additives offers a valuable strategy to improve the integration of SNCs in film matrices.","PeriodicalId":181,"journal":{"name":"International Journal of Food Science & Technology","volume":null,"pages":null},"PeriodicalIF":3.713,"publicationDate":"2024-06-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141503035","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A visual ratio PVA/curcumin/indigo nanofibre membrane based on natural pigments for detecting mutton freshness 一种基于天然色素的可视比 PVA/莪术/靛蓝纳米纤维膜,用于检测羊肉新鲜度
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-25 DOI: 10.1111/ijfs.17313
Lianye Li, Wenbo Li, Wuliang Sun, Yue Dong, Yaxin Yv, Wanting Shi, Wenxiu Sun
SummaryIn the storage process, meat is susceptible to external factors that produce corruption and deterioration, affecting consumers' health. Therefore, preparing an indicator membrane that can detect freshness in real time, non‐destructively, and visually is significant. Herein, an indicator membrane was prepared by electrostatic spinning technology using polyvinyl alcohol (PVA) as the substrate and curcumin (CUR) and indigo (IND) as the mixed indicator for freshness detection. When curcumin and indigo were mixed at 3:1 (w/w), CUR was transformed from ketone type to enol type with the gradual increase of pH, and IND underwent electron leaps, which resulted in green, brown, and reddish‐brown colour changes in the solution, and the colour development effect was effectively improved. The characterisation results showed that the average fibre diameter of the PVA/0.8 indicator membrane was 252 nm, the hybrid indicator was successfully loaded in the nanofibres, and the water contact angle was 103.6°, which was hydrophobic. In addition, the indicator membrane was sensitive to trimethylamine (limit of detection 17.38 ppm) and triethylamine (limit of detection 27.77 ppm) but insensitive to saline, ethanol, ethyl acetate, and other contaminants with detection specificity. Finally, the colour of the indicating membrane changes from green to brown during the storage of mutton in the mutton was rotten, indicating that the naked eye can judge the freshness of the mutton. Therefore, the PVA/CUR/IND indicator membrane has excellent potential for application in real‐time and non‐destructive detection of mutton freshness.
摘要 在贮藏过程中,肉类容易受到外界因素的影响而腐败变质,影响消费者的健康。因此,制备一种能实时、无损、直观地检测肉类新鲜度的指示膜意义重大。本文以聚乙烯醇(PVA)为基材,姜黄素(CUR)和靛蓝(IND)为混合指示剂,通过静电纺丝技术制备了一种指示剂膜,用于新鲜度检测。当姜黄素和靛蓝以3:1(重量比)混合时,随着pH值的逐渐升高,姜黄素由酮型转变为烯型,而靛蓝则发生了电子跃迁,从而使溶液中的颜色发生了绿色、棕色和红棕色的变化,显色效果得到了有效改善。表征结果表明,PVA/0.8 指示剂膜的平均纤维直径为 252 nm,纳米纤维中成功负载了混合指示剂,水接触角为 103.6°,具有疏水性。此外,指示膜对三甲胺(检测限为 17.38 ppm)和三乙胺(检测限为 27.77 ppm)敏感,但对生理盐水、乙醇、乙酸乙酯和其他污染物不敏感,具有检测特异性。最后,在羊肉腐烂的贮藏过程中,指示膜的颜色由绿色变为褐色,说明肉眼可以判断羊肉的新鲜程度。因此,PVA/CUR/IND 指示膜在实时、无损检测羊肉新鲜度方面具有很好的应用潜力。
{"title":"A visual ratio PVA/curcumin/indigo nanofibre membrane based on natural pigments for detecting mutton freshness","authors":"Lianye Li, Wenbo Li, Wuliang Sun, Yue Dong, Yaxin Yv, Wanting Shi, Wenxiu Sun","doi":"10.1111/ijfs.17313","DOIUrl":"https://doi.org/10.1111/ijfs.17313","url":null,"abstract":"SummaryIn the storage process, meat is susceptible to external factors that produce corruption and deterioration, affecting consumers' health. Therefore, preparing an indicator membrane that can detect freshness in real time, non‐destructively, and visually is significant. Herein, an indicator membrane was prepared by electrostatic spinning technology using polyvinyl alcohol (PVA) as the substrate and curcumin (CUR) and indigo (IND) as the mixed indicator for freshness detection. When curcumin and indigo were mixed at 3:1 (w/w), CUR was transformed from ketone type to enol type with the gradual increase of pH, and IND underwent electron leaps, which resulted in green, brown, and reddish‐brown colour changes in the solution, and the colour development effect was effectively improved. The characterisation results showed that the average fibre diameter of the PVA/0.8 indicator membrane was 252 nm, the hybrid indicator was successfully loaded in the nanofibres, and the water contact angle was 103.6°, which was hydrophobic. In addition, the indicator membrane was sensitive to trimethylamine (limit of detection 17.38 ppm) and triethylamine (limit of detection 27.77 ppm) but insensitive to saline, ethanol, ethyl acetate, and other contaminants with detection specificity. Finally, the colour of the indicating membrane changes from green to brown during the storage of mutton in the mutton was rotten, indicating that the naked eye can judge the freshness of the mutton. Therefore, the PVA/CUR/IND indicator membrane has excellent potential for application in real‐time and non‐destructive detection of mutton freshness.","PeriodicalId":181,"journal":{"name":"International Journal of Food Science & Technology","volume":null,"pages":null},"PeriodicalIF":3.713,"publicationDate":"2024-06-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141518072","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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International Journal of Food Science & Technology
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