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Nutritional and functional aspects of fermented algae 发酵藻类的营养和功能方面
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17297
Sümeyye Sarıtaş, Hatice Duman, Sercan Karav
SummaryIn recent years, there has been an increasing emphasis on natural and healthy nutrition, leading to increased interest in fermented foods and their associated health benefits. In line with this trend, fermentation is employed to enhance the exceptional properties of algae, including their nutritional value and digestibility, rendering them suitable for consumption as food. Fermentation of algae involves the conversion of carbohydrates into alcohol or organic acids by microorganisms, including bacteria or yeast. First of all, the fermentation process results in enhanced antioxidant activity, antimicrobial effects, anti‐inflammatory properties, immunomodulatory effects, anti‐glycation activity, antihypertensive effects and neuroprotective activity by increasing the bioavailability of bioactive compounds in algae. In addition, this method encourages the incorporation of algae into food products. In this process, both the flavour and texture are enhanced, while simultaneously preserving and enriching the beneficial nutrients and compounds present in algae. Despite the availability of various fermented algae products in the market, their widespread adoption has yet to be realised. The incorporation of fermented algae into food products not only enhances their nutritional content but also fosters the emergence of a new segment within the fermented food market. Herein, the concept of fermented algae, the fermentation process, its nutritional value and its health benefits are explored.
摘要近年来,人们越来越重视天然健康的营养,从而对发酵食品及其相关的健康益处越来越感兴趣。为顺应这一趋势,发酵法被用来提高藻类的特殊属性,包括营养价值和消化率,使其适合作为食品食用。海藻发酵是指微生物(包括细菌或酵母)将碳水化合物转化为酒精或有机酸。首先,发酵过程可提高藻类中生物活性化合物的生物利用率,从而增强抗氧化活性、抗菌效果、抗炎特性、免疫调节效果、抗糖化活性、抗高血压效果和神经保护活性。此外,这种方法还有助于将海藻融入食品中。在这一过程中,风味和口感都得到了改善,同时还保留并丰富了海藻中有益的营养成分和化合物。尽管市场上有各种发酵海藻产品,但尚未得到广泛采用。在食品中加入发酵藻类不仅能提高食品的营养成分,还能促进发酵食品市场出现一个新的细分市场。本文探讨了发酵藻类的概念、发酵过程、营养价值及其对健康的益处。
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引用次数: 0
Physicochemical and nutritional characteristics of vegan protein bars formulated with sweet potato and rice protein 用甘薯和大米蛋白配制的素食蛋白棒的理化和营养特性
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17294
In‐Ha Baek, Ha‐Seong Cho, Nurul Saadah Said, Ibukunoluwa Fola Olawuyi, Kyu‐Rim Kim, Won‐Young Lee
SummaryIn response to the growing interest in plant‐based alternatives and vegan diets, this study aimed to develop novel sweet potato‐based vegan protein bars enriched with rice protein (RP) as an alternative protein source. The vegan protein bars (VPBs) formulated with varying RP content (0–32 g) were evaluated for nutritional, textural, microstructural and sensory properties. Nutritional analysis revealed a proportional increase in protein content (8.94%–21.77%) and energy value (310.29–353.32 kcal/100 g) with increasing RP content. The progressive inclusion of RP significantly (P < 0.05) improved the textural properties of VPBs, notably increasing cohesiveness (0.07%–0.60%), chewiness (8.71–105.02 g) and firmness (1453.80–3444.03 kg cm−2), with all VPBs receiving favourable sensory evaluation scores. Importantly, all VPBs received favourable sensory scores. Microstructural analysis revealed the mechanism for textural enhancement in enriched VPBs, indicating a positive correlation between higher RP content and the number and size of surface clumps. Amino acid profiling indicated over 50% increases in valine content and essential amino acid scores in enriched VPBs compared to those without RP. Moreover, protein‐enriched VPBs exhibited superior antioxidant activity. In conclusion, these findings suggest the potential of sweet potato and RP in developing VPBs, highlighting the value of plant‐based ingredients in vegan food products.
摘要 鉴于人们对植物性替代品和素食的兴趣与日俱增,本研究旨在开发富含大米蛋白质(RP)的新型甘薯素食蛋白棒,作为替代蛋白质来源。研究人员对不同 RP 含量(0-32 克)的素食蛋白棒(VPBs)进行了营养、质地、微结构和感官特性评估。营养分析表明,随着 RP 含量的增加,蛋白质含量(8.94%-21.77%)和能量值(310.29-353.32 千卡/100 克)也成比例增加。逐步添加 RP 能显著改善 VPB 的质地特性(P < 0.05),尤其是增加了粘合度(0.07%-0.60%)、咀嚼感(8.71-105.02 克)和坚固度(1453.80-3444.03 千克/厘米-2),所有 VPB 都获得了良好的感官评价分数。重要的是,所有 VPB 都获得了良好的感官评分。微观结构分析揭示了富集 VPB 纹理增强的机制,表明较高的 RP 含量与表面团块的数量和大小呈正相关。氨基酸分析表明,与不含 RP 的 VPB 相比,富集 VPB 中的缬氨酸含量和必需氨基酸得分增加了 50%以上。此外,富含蛋白质的 VPB 还表现出卓越的抗氧化活性。总之,这些研究结果表明了甘薯和 RP 在开发 VPB 方面的潜力,凸显了植物性成分在素食食品中的价值。
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引用次数: 0
Characterisation of finger millet (Eleusine coracana) starch isolated by conventional and ultrasound‐assisted starch isolation methods 用传统方法和超声波辅助淀粉分离法分离出的小米(Eleusine coracana)淀粉的特征
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-30 DOI: 10.1111/ijfs.17303
Shweta Yadav, Sunita Mishra, Kambhampati Vivek, Sabyasachi Mishra
SummaryStarch is a versatile biomaterial with a wide range of applications across various industrial sectors. Therefore, starch isolation methods play a crucial role in fulfilling the demand for high‐quality starch required for different applications. Waxy maize starch is the most used starch for different food applications. It is isolated using an alkaline extraction method and available in the market at a high price. The traditional process of starch isolation involves labour‐intensive and costly downstream processing that leads to exploring cost‐effective isolation methods for various food applications. Finger millet (Eleusine coracana) is an underutilised cereal crop composed of 65–70% of starch. In the present study, the starch from finger millet is isolated using conventional and ultrasound‐assisted isolation methods to fulfil the current requirement. The isolated finger millet starch was characterised by morphological structure obtained by scanning electron microscopy (SEM), X‐ray diffractogram (XRD), infrared spectrum obtained by Fourier transform infrared spectrometer (FT‐IR), differential scanning calorimetry (DSC) analysis, and rheological analysis. The SEM images confirmed the reduced particle size and uniform grain size distribution in the starch isolated using ultrasound‐assisted isolation. The relative crystallinity of starch isolated using ultrasound‐assisted isolation method (69.05 ± 0.57%) was higher compared to other conventional isolation methods (57.18 ± 0.70%, 67.66 ± 1.00%, and 68.34 ± 0.33% for distilled water soaking, alkali soaking, and sodium bisulphite soaking, respectively). The FTIR analysis confirmed no significant changes in the functional group of starch with respect to different isolation methods. Thermal and rheological analysis of isolated starch using ultrasound‐assisted isolation indicated the lowest gelatinisation enthalpy (45.38 ± 1.67 J/g) and showed the lowest loss factor indicating the most elastic behaviour, respectively.
摘要淀粉是一种用途广泛的生物材料,在各个工业部门都有广泛的应用。因此,淀粉分离方法在满足不同应用对高质量淀粉的需求方面起着至关重要的作用。蜡质玉米淀粉是不同食品应用中使用最多的淀粉。它采用碱性提取法分离,在市场上售价不菲。传统的淀粉分离过程涉及劳动密集型和成本高昂的下游加工,这就需要为各种食品应用探索具有成本效益的分离方法。手指粟(Eleusine coracana)是一种未充分利用的谷类作物,其淀粉含量高达 65-70%。本研究采用传统和超声波辅助分离方法从小米中分离出淀粉,以满足当前的需求。通过扫描电子显微镜(SEM)获得的形态结构、X 射线衍射图(XRD)、傅立叶变换红外光谱仪(FT-IR)获得的红外光谱、差示扫描量热仪(DSC)分析和流变分析,对分离出的小米淀粉进行了表征。扫描电子显微镜图像证实,使用超声辅助分离技术分离出的淀粉粒度减小,粒度分布均匀。与其他传统分离方法(蒸馏水浸泡法、碱浸泡法和亚硫酸氢钠浸泡法分别为 57.18 ± 0.70%、67.66 ± 1.00% 和 68.34 ± 0.33%)相比,超声辅助分离法分离出的淀粉的相对结晶度(69.05 ± 0.57%)更高。傅立叶变换红外光谱分析证实,淀粉的官能团在不同分离方法下没有明显变化。使用超声波辅助分离法对分离出的淀粉进行的热分析和流变分析表明,其糊化焓(45.38 ± 1.67 焦耳/克)最低,损失因子最低,表明其弹性最好。
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引用次数: 0
Bioactive lipid‐enriched concentrates from squid discards by one‐step and two‐step extractions with non‐halogenated solvents 用无卤溶剂一步法和两步法萃取乌贼废弃物中富含生物活性的浓缩脂质
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-29 DOI: 10.1111/ijfs.17336
David Paz, Marcos Trigo, Sidonia Martínez, Santiago P. Aubourg
SummaryThis study focused on the preparation of lipid concentrates with high contents of bioactive molecules. Different one‐step and two‐step extractions with non‐halogenated solvents (hexane, HX; isopropanol, IP) were carried out on Patagonian squid (Doryteuthis gahi) discards. As a first step, HX extractions (one, two or three times) were carried out. The resulting substrates were extracted with IP (two, three or four times). Analysis of lipid extracts included total lipid, phospholipid (PL) and tocopherol values, and fatty acid (FA) profile. HX extractions led to remarkable α‐ and γ‐tocopherol values (ca. 1400 and 23 mg kg−1 lipids, respectively); no effect (P > 0.05) of the number of HX extractions was observed. IP extracts provided high PL values (383–501 mg kg−1 lipids); the highest average values were detected with four IP extractions after three HX extractions. Values obtained for tocopherols and PLs were higher (P < 0.05) than those obtained by employing the conventional (chloroform/methanol, 1:1) lipid extraction (ca. 496 and 11 mg kg−1 lipids and 400 g kg−1 lipids, respectively). Range values detected for eicosapentaenoic and docosahexaenoic acid values and the ω3/ω6 FA ratio were similar to those obtained by the conventional procedure. A valuable procedure is proposed for obtaining PL‐ and tocopherol‐enriched concentrates from marine waste with non‐halogenated solvents.
摘要 本研究的重点是制备生物活性分子含量高的脂质浓缩物。对巴塔哥尼亚鱿鱼(Doryteuthis gahi)废弃物进行了不同的一步法和两步法非卤溶剂(正己烷,HX;异丙醇,IP)萃取。第一步是进行 HX 提取(一次、两次或三次)。所得底物用 IP 提取(2、3 或 4 次)。脂质提取物的分析包括总脂质、磷脂(PL)和生育酚值以及脂肪酸(FA)概况。HX 提取物可产生显著的 α- 和 γ-生育酚值(分别约为 1400 和 23 毫克/千克-1 脂质);HX 提取物的提取次数没有影响(P > 0.05)。IP 提取物提供了较高的 PL 值(383-501 毫克/千克-1 脂质);在三次 HX 提取之后,四次 IP 提取物检测到的平均值最高。获得的生育酚和聚乳酸值(P< 0.05)高于采用传统(氯仿/甲醇,1:1)脂质萃取法获得的值(分别约为 496 和 11 毫克/千克-1 脂质和 400 克/千克-1 脂质)。检测到的二十碳五烯酸和二十二碳六烯酸值范围值以及ω3/ω6 FA 比值与传统方法得到的值相似。提出了一种利用非卤化溶剂从海洋废弃物中获得富含聚乳酸和生育酚浓缩物的有效方法。
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引用次数: 0
Stearic acid enhanced starch nanocrystal integration in cassava starch film 硬脂酸增强木薯淀粉膜中淀粉纳米晶的整合能力
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-26 DOI: 10.1111/ijfs.17310
Nkosingiphile L. Nzama, Alain Dufresne, Eric O. Amonsou
SummaryStarch nanocrystals (SNCs) have emerged as promising biodegradable nanomaterial for the enhancement of biopolymer films' properties. Nevertheless, using SNCs alone is difficult due to restricted capacity for nanocrystal integration within the film's matrix. The objective of this study was to enhance the properties of biopolymer films using waxy corn starch nanocrystals supplemented with stearic acid. Cassava starch films containing varying proportions of SNCs (0–20 wt.% starch) and steric acid (2%) were prepared and characterised. The inclusion of stearic acid substantially improved SNC integration from 5% to 15%, yielding nanocomposite films with better tensile strength, thermal stability and barrier properties than those prepared with native starch or starch‐fatty acid alone. The improvement in film properties was attributed to V‐amylose complexes formation, increased crystallinity and hydrophobicity. Microscopy images revealed homogenous film surfaces, depicting greater nanocrystal dispersibility. The supplementation of lipid additives offers a valuable strategy to improve the integration of SNCs in film matrices.
摘要淀粉纳米晶体(SNCs)已成为增强生物聚合物薄膜性能的有前途的生物可降解纳米材料。然而,由于纳米晶体在薄膜基质中的整合能力受到限制,单独使用 SNCs 十分困难。本研究的目的是使用添加硬脂酸的蜡质玉米淀粉纳米晶体来增强生物聚合物薄膜的性能。制备了含有不同比例 SNCs(0-20 wt.% 淀粉)和硬脂酸(2%)的木薯淀粉薄膜,并对其进行了表征。硬脂酸的加入大大提高了 SNC 的整合度(从 5%提高到 15%),制备出的纳米复合薄膜与单独使用本地淀粉或淀粉脂肪酸制备的薄膜相比,具有更好的拉伸强度、热稳定性和阻隔性能。薄膜性能的改善归因于 V-amylose 复合物的形成、结晶度和疏水性的提高。显微镜图像显示薄膜表面均匀,纳米晶体分散性更高。补充脂质添加剂为改善 SNC 在薄膜基质中的整合提供了一种有价值的策略。
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引用次数: 0
A visual ratio PVA/curcumin/indigo nanofibre membrane based on natural pigments for detecting mutton freshness 一种基于天然色素的可视比 PVA/莪术/靛蓝纳米纤维膜,用于检测羊肉新鲜度
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-25 DOI: 10.1111/ijfs.17313
Lianye Li, Wenbo Li, Wuliang Sun, Yue Dong, Yaxin Yv, Wanting Shi, Wenxiu Sun
SummaryIn the storage process, meat is susceptible to external factors that produce corruption and deterioration, affecting consumers' health. Therefore, preparing an indicator membrane that can detect freshness in real time, non‐destructively, and visually is significant. Herein, an indicator membrane was prepared by electrostatic spinning technology using polyvinyl alcohol (PVA) as the substrate and curcumin (CUR) and indigo (IND) as the mixed indicator for freshness detection. When curcumin and indigo were mixed at 3:1 (w/w), CUR was transformed from ketone type to enol type with the gradual increase of pH, and IND underwent electron leaps, which resulted in green, brown, and reddish‐brown colour changes in the solution, and the colour development effect was effectively improved. The characterisation results showed that the average fibre diameter of the PVA/0.8 indicator membrane was 252 nm, the hybrid indicator was successfully loaded in the nanofibres, and the water contact angle was 103.6°, which was hydrophobic. In addition, the indicator membrane was sensitive to trimethylamine (limit of detection 17.38 ppm) and triethylamine (limit of detection 27.77 ppm) but insensitive to saline, ethanol, ethyl acetate, and other contaminants with detection specificity. Finally, the colour of the indicating membrane changes from green to brown during the storage of mutton in the mutton was rotten, indicating that the naked eye can judge the freshness of the mutton. Therefore, the PVA/CUR/IND indicator membrane has excellent potential for application in real‐time and non‐destructive detection of mutton freshness.
摘要 在贮藏过程中,肉类容易受到外界因素的影响而腐败变质,影响消费者的健康。因此,制备一种能实时、无损、直观地检测肉类新鲜度的指示膜意义重大。本文以聚乙烯醇(PVA)为基材,姜黄素(CUR)和靛蓝(IND)为混合指示剂,通过静电纺丝技术制备了一种指示剂膜,用于新鲜度检测。当姜黄素和靛蓝以3:1(重量比)混合时,随着pH值的逐渐升高,姜黄素由酮型转变为烯型,而靛蓝则发生了电子跃迁,从而使溶液中的颜色发生了绿色、棕色和红棕色的变化,显色效果得到了有效改善。表征结果表明,PVA/0.8 指示剂膜的平均纤维直径为 252 nm,纳米纤维中成功负载了混合指示剂,水接触角为 103.6°,具有疏水性。此外,指示膜对三甲胺(检测限为 17.38 ppm)和三乙胺(检测限为 27.77 ppm)敏感,但对生理盐水、乙醇、乙酸乙酯和其他污染物不敏感,具有检测特异性。最后,在羊肉腐烂的贮藏过程中,指示膜的颜色由绿色变为褐色,说明肉眼可以判断羊肉的新鲜程度。因此,PVA/CUR/IND 指示膜在实时、无损检测羊肉新鲜度方面具有很好的应用潜力。
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引用次数: 0
Exploring the impact of harvest year on the mineral composition of Mimosa scabrella Bentham honeydew honey from Santa Catarina (Brazil) using ICP‐MS and chemometric tools 利用 ICP-MS 和化学计量学工具探索收获年份对巴西圣卡塔琳娜州含羞草蜜露中矿物质成分的影响
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-25 DOI: 10.1111/ijfs.17251
Bibiana Silva, Luciano Valdemiro Gonzaga, Heloísa França Maltez, Kátia Bennett Samochvalov, Roseane Fett, Ana Carolina Oliveira Costa
SummaryThis study investigated the variation in mineral elements in bracatinga (Mimosa scabrella Bentham) honeydew honeys produced biannually over three consecutive harvest years. The aim was to assess the relationship between the year of production and the concentration of fourteen rare earth elements and six trace elements analysed using ICP‐MS. The concentrations of the twenty elements varied (P < 0.001) among all the honey samples. The dominant rare earth elements were Eu, followed by Nd and La, while Pd and Au were the major trace elements. Cluster analysis (CA) and linear discriminant analysis (LDA) were performed using all the elements identified. The LDA categorised (83.3% accuracy) the bracatinga honeydew honey samples according to their harvest year. Discriminant functions, influenced by Ce, Tb, and Th, show distinct elemental patterns in bracatinga honeydew honeys, varying with harvest year. This reflects fluctuations in yearly climatic conditions and is important to guarantee accurate characterisation.
摘要 本研究调查了连续三个收获年中每两年生产一次的布拉卡廷加(Mimosa scabrella Bentham)蜜露中矿物质元素的变化。目的是评估生产年份与使用 ICP-MS 分析的 14 种稀土元素和 6 种微量元素浓度之间的关系。在所有蜂蜜样品中,这 20 种元素的浓度各不相同(P < 0.001)。主要的稀土元素是 Eu,其次是 Nd 和 La,而 Pd 和 Au 是主要的微量元素。利用所有确定的元素进行了聚类分析(CA)和线性判别分析(LDA)。线性判别分析(LDA)根据收获年份对布拉卡廷加蜜露蜂蜜样本进行了分类(准确率为 83.3%)。受 Ce、Tb 和 Th 的影响,判别函数显示了布拉卡廷加蜜露蜂蜜的独特元素模式,随收获年份而变化。这反映了每年气候条件的波动,对保证准确定性非常重要。
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引用次数: 0
Recent progress in metabolomics research: insights into fruit metabolome, harvesting techniques and health‐promoting bioactives 代谢组学研究的最新进展:对水果代谢组、采摘技术和促进健康的生物活性物质的深入了解
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-25 DOI: 10.1111/ijfs.17308
Vikas Dadwal, Manoj S. Aroor, Robin Joshi, Mahesh Gupta
SummaryThe use of cutting‐edge omics technology to edible fruits has transformed the disciplines of fruit biology, pre‐ and post‐harvest investigations, metabolite biosynthesis and the identification of novel therapeutic fruit bioactives for health by leveraging varied omics data. Combining modern analytical chromatography tools (LC, GC) with mass spectrometry has significantly improved our ability to examine complex fruit tissues or extracted components, advancing our understanding of the fruit metabolome. Studies aiming at understanding the full metabolome and future quality characteristics have concentrated on quantifying the number of metabolites in edible fruit species and cultivars from diverse geographical locations. These studies have also helped to develop new databases for precise and comprehensive qualitative analysis of metabolites, allowing for the analysis of metabolite biosynthesis pathways to identify differences in metabolites among developed hybrids, metabolite origins and potential derivatives. Bioactive metabolite information is currently being utilised to manage illnesses, provide nutrition and creation of novel food products. Furthermore, this research has helped us better understand fruit quality and how metabolites interact with biological systems. In conclusion, this review emphasises the importance of metabolomics approaches in studying fruit metabolomes in the context of current research perspectives.
摘要在可食用水果中使用尖端的全息技术改变了水果生物学、采前和采后研究、代谢物生物合成以及利用各种全息数据鉴定新型治疗性水果生物活性物质等学科。现代色谱分析工具(液相色谱、气相色谱)与质谱技术相结合,大大提高了我们研究复杂水果组织或提取成分的能力,促进了我们对水果代谢组的了解。旨在了解完整代谢组和未来质量特征的研究主要集中在对不同地理位置的食用水果品种和栽培品种的代谢物数量进行量化。这些研究还有助于开发新的数据库,用于对代谢物进行精确和全面的定性分析,从而分析代谢物的生物合成途径,确定已培育杂交种之间代谢物的差异、代谢物的来源和潜在衍生物。生物活性代谢物信息目前正被用于控制疾病、提供营养和创造新型食品。此外,这项研究还有助于我们更好地了解水果质量以及代谢物如何与生物系统相互作用。总之,本综述强调了代谢组学方法在当前研究视角下研究水果代谢组的重要性。
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引用次数: 0
Jet milling‐activated direct synthesis of octenyl succinic anhydride modified starch: an analysis of structural and application properties 喷射研磨激活直接合成辛烯基琥珀酸酐改性淀粉:结构和应用特性分析
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-24 DOI: 10.1111/ijfs.17268
Shuangjing Lang, Chunguang Sui, Lidong Wang
SummaryThe synthesis of octenyl succinic anhydride‐modified starch was achieved through a fluidised bed activated by jet milling with graded revolution rates of 1200, 1800, 2400, 3000, and 3600 rpm. This study investigated the changes in the structural, physicochemical, and application properties of modified starch after jet milling. The results showed that modified starch can be synthesised using a one‐step jet milling process. The degree of substitution increased with a decrease in the starch particle size, resulting in a rough granule morphology. Structural analysis revealed that crystalline areas were destroyed in the modified starches. In the Fourier‐infrared spectrum, typical peaks appeared at 1724 and 1573 cm−1 upon introduction of the octenyl succinic anhydride group, whereas a new sodium peak appeared in the XPS spectrogram. The 1H‐NMR spectrum indicated that the esterification reaction mainly occurred on OH2 groups. The emulsification properties of the modified starch were significantly enhanced and increased with the crushing strength. The octenyl succinic anhydride‐modified starch has potential as a wall material for microcapsules, with good embedding rate and thermal stability. This novel synthesis method represents an innovative method for the synthesis of OSA‐starches.
摘要辛烯基琥珀酸酐改性淀粉的合成是通过流化床活化喷射研磨实现的,其转速分级为 1200、1800、2400、3000 和 3600 rpm。本研究调查了喷射研磨后改性淀粉在结构、理化和应用特性方面的变化。结果表明,改性淀粉可通过一步喷射研磨工艺合成。随着淀粉粒径的减小,取代度也随之增加,从而形成了粗糙的颗粒形态。结构分析表明,改性淀粉中的结晶区域被破坏。在傅立叶红外光谱中,引入辛烯基琥珀酸酐基团后,在 1724 和 1573 cm-1 处出现了典型的峰值,而在 XPS 光谱图中出现了一个新的钠峰。1H-NMR 光谱表明,酯化反应主要发生在 OH2 基团上。改性淀粉的乳化性能明显增强,并随着粉碎强度的增加而增加。辛烯基琥珀酸酐改性淀粉具有良好的包埋率和热稳定性,可作为微胶囊的壁材。这种新型合成方法是合成辛烯基琥珀酸酐淀粉的一种创新方法。
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引用次数: 0
The effects of rice bran oil, coconut oil and homogenisation pressure on the properties of oil‐in‐water emulsion loaded baicalein 米糠油、椰子油和均质压力对负载黄芩素的水包油乳液特性的影响
IF 3.713 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-23 DOI: 10.1111/ijfs.17284
Witcha Treesuwan, Khemmapas Treesuwan, Aunchalee Aussanasuwannakul
SummaryBaicalein is a functional flavonoid that has been intensively studied for its health benefits. Loading baicalein in oil‐in‐water (O/W) emulsions could provide advantages for its application in foods. This work investigated the characteristics of O/W emulsions loaded with baicalein formulated by combination of vegetable oils and homogenisation pressures. Rice bran oil (RBO) and coconut oil (CCO), classified as long‐chain triglycerides and medium‐chain triglyceride, were used in the homogenisation process at 600–1200 bar. The rice bran oil‐in‐water emulsion loaded with baicalein (RBOb/W) produced at 1200 bar provided the emulsion with the smallest particle size of the surface‐weighted mean diameter (d3,2) of 220 nm. The result showed that loading baicalein into RBO could reduce the particle size of O/W emulsion while it increased the particle size of coconut oil‐in‐water emulsion loaded with baicalein (CCOb/W). The RBOb/W and CCOb/W emulsions were physically stable in terms of droplet size during storage at 4 °C for 28 days. The change in viscosity of freshly prepared emulsion loaded with baicalein was dominant compared with the emulsion unloaded baicalein, however, the viscosity profiles of emulsions loaded with baicalein are like emulsions unloaded with baicalein after storage. The influence of baicalein on the viscoelastic properties of emulsion was observed in the storage modulus (G′) at low frequencies. These results suggest that baicalein could potentially interfere with the stabilising effect of Tween 20, contribute to droplet interactions, and migrate from the surface of RBO but not CCO. High baicalein retention of 91–98% was observed in the RBOb/W emulsions. This study recommends that RBO is preferable over CCO to produce O/W emulsion loaded with baicalein in terms of droplet size, stability and retention. It would be useful information to produce functional ingredients for the food industry.
摘要黄芩素是一种功能性黄酮类化合物,其对健康的益处已得到深入研究。在水包油(O/W)乳液中添加黄芩素可为其在食品中的应用提供优势。这项工作研究了通过植物油组合和均质压力配制的添加黄芩素的水包油型乳液的特性。米糠油(RBO)和椰子油(CCO)分为长链甘油三酯和中链甘油三酯,在 600-1200 巴的均质过程中使用。在 1200 巴条件下生产的水包米糠油乳液中添加了黄芩素(RBOb/W),其表面加权平均直径(d3,2)为 220 nm,是粒径最小的乳液。结果表明,在 RBO 中添加黄芩素可以减小水包油型乳液的粒径,而添加黄芩素的水包椰油型乳液(CCOb/W)的粒径则有所增加。RBOb/W 和 CCOb/W 乳剂在 4 °C 下储存 28 天后,液滴大小保持稳定。与未添加黄芩素的乳液相比,新制备的添加黄芩素的乳液的粘度变化较大,但添加黄芩素的乳液在储存后的粘度曲线与未添加黄芩素的乳液相似。黄芩素对乳液粘弹性能的影响表现在低频下的储存模量(G′)上。这些结果表明,黄芩素有可能干扰吐温 20 的稳定作用,导致液滴相互作用,并从 RBO 表面迁移,而不是从 CCO 表面迁移。在 RBOb/W 乳剂中观察到黄芩素的保留率高达 91-98%。本研究建议,就液滴大小、稳定性和保留率而言,RBO 比 CCO 更适合用于生产负载黄芩素的 O/W 乳剂。这将为食品工业生产功能性配料提供有用的信息。
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International Journal of Food Science & Technology
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