Juliana Rincón‐López, Juanita Castro Chica, Victoria Eugenia Recalde Rojas, Liliana Moncayo Martínez, Ángela María Arango Gartner, Milton Rosero‐Moreano, Gonzalo Taborda‐Ocampo
SummaryThe Industria Licorera de Caldas (ILC) stands as a major liquor factory in Colombia, specialising in the production of various rum types including Tradicional, Juan de la Cruz, Carta de Oro, and Reserva Especial. These rums, as congeneric drinks, are known for their rich content of volatile compounds that define their sensory characteristics. To be commercialised, each rum batch must comply with Colombian standard NTC278 which defines rigorous assessment of congener content and various physicochemical parameters. Thus, the ILC has accumulated a vast amount of data over the years. This study conducts a comprehensive analysis of ILC rums, using chemometric techniques and machine‐learning classification models such as PCA, KNN, LDA, and RF. The aim was to distinguish between rum types based on parameters specified for standard compliance, streamlining the process without the need for additional or extensive new methodologies. As a result, through PCA data exploration, it was revealed that acetaldehyde, ethyl acetate, and isobutanol levels are instrumental in differentiating rum variants. Similarly, all classification models achieved accuracy levels exceeding 0.83 and precision surpassing 0.93. These findings pave the way for further research in the development of an ILC‐specific sensor for rapid and reliable liquor authenticity testing.
{"title":"Regulatory‐based classification of rums: a chemometric and machine learning analysis","authors":"Juliana Rincón‐López, Juanita Castro Chica, Victoria Eugenia Recalde Rojas, Liliana Moncayo Martínez, Ángela María Arango Gartner, Milton Rosero‐Moreano, Gonzalo Taborda‐Ocampo","doi":"10.1111/ijfs.17464","DOIUrl":"https://doi.org/10.1111/ijfs.17464","url":null,"abstract":"SummaryThe Industria Licorera de Caldas (ILC) stands as a major liquor factory in Colombia, specialising in the production of various rum types including Tradicional, Juan de la Cruz, Carta de Oro, and Reserva Especial. These rums, as congeneric drinks, are known for their rich content of volatile compounds that define their sensory characteristics. To be commercialised, each rum batch must comply with Colombian standard NTC278 which defines rigorous assessment of congener content and various physicochemical parameters. Thus, the ILC has accumulated a vast amount of data over the years. This study conducts a comprehensive analysis of ILC rums, using chemometric techniques and machine‐learning classification models such as PCA, KNN, LDA, and RF. The aim was to distinguish between rum types based on parameters specified for standard compliance, streamlining the process without the need for additional or extensive new methodologies. As a result, through PCA data exploration, it was revealed that acetaldehyde, ethyl acetate, and isobutanol levels are instrumental in differentiating rum variants. Similarly, all classification models achieved accuracy levels exceeding 0.83 and precision surpassing 0.93. These findings pave the way for further research in the development of an ILC‐specific sensor for rapid and reliable liquor authenticity testing.","PeriodicalId":181,"journal":{"name":"International Journal of Food Science & Technology","volume":"49 1","pages":""},"PeriodicalIF":3.713,"publicationDate":"2024-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142210083","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
SummaryThis study aimed to investigate the effects of different oxidation modes on the functional and gel properties of hazelnut proteins. The solubility of hazelnut protein showed a small trend when the oxidation level was low, and it decreased significantly with the increase in concentration. The maximum value of water‐holding capacity (WHC), emulsifying activity index (EAI), and emulsion stability index (ESI) was 343.33%, 56.00 m2 g−1, and 75.85 min at AAPH concentration of 1.0 mmol L−1, respectively. The functional properties of hazelnut proteins, except oil‐holding capacity (OHC), gradually reduced with the increase in malondialdehyde (MDA) concentration. H2O2 modified improved OHC, foaming capacity, foam stability, and EAI of hazelnut proteins, whereas WHC and ESI gradually decreased. The results of the secondary structure of hazelnut protein gels indicated a high ratio of α‐helix and β‐fold of the gels. Also, the increase in oxidation led to an increase in the gels' voids. Also, oxidation led to a rough and loose network structure of hazelnut protein gels. These results suggested that peroxyl radical, hydroxyl radical, and MDA produced during lipid peroxidation affected the interfacial properties of hazelnut protein and disrupted the formation of hazelnut protein gel, thus affecting the quality of hazelnut protein.
{"title":"Effects of different oxidation methods on the functional properties and gel characteristics of hazelnut proteins","authors":"Hongyu Jiang, Hao Hu, Ziyi Huang, Meichu Liu, Chunmao Lyu","doi":"10.1111/ijfs.17596","DOIUrl":"https://doi.org/10.1111/ijfs.17596","url":null,"abstract":"SummaryThis study aimed to investigate the effects of different oxidation modes on the functional and gel properties of hazelnut proteins. The solubility of hazelnut protein showed a small trend when the oxidation level was low, and it decreased significantly with the increase in concentration. The maximum value of water‐holding capacity (WHC), emulsifying activity index (EAI), and emulsion stability index (ESI) was 343.33%, 56.00 m<jats:sup>2</jats:sup> g<jats:sup>−1</jats:sup>, and 75.85 min at AAPH concentration of 1.0 mmol L<jats:sup>−1</jats:sup>, respectively. The functional properties of hazelnut proteins, except oil‐holding capacity (OHC), gradually reduced with the increase in malondialdehyde (MDA) concentration. H<jats:sub>2</jats:sub>O<jats:sub>2</jats:sub> modified improved OHC, foaming capacity, foam stability, and EAI of hazelnut proteins, whereas WHC and ESI gradually decreased. The results of the secondary structure of hazelnut protein gels indicated a high ratio of α‐helix and β‐fold of the gels. Also, the increase in oxidation led to an increase in the gels' voids. Also, oxidation led to a rough and loose network structure of hazelnut protein gels. These results suggested that peroxyl radical, hydroxyl radical, and MDA produced during lipid peroxidation affected the interfacial properties of hazelnut protein and disrupted the formation of hazelnut protein gel, thus affecting the quality of hazelnut protein.","PeriodicalId":181,"journal":{"name":"International Journal of Food Science & Technology","volume":"32 1","pages":""},"PeriodicalIF":3.713,"publicationDate":"2024-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142210082","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Shanmugam Alagappan, Sam Mallard, Daniel Cozzolino, Deirdre Mikkelsen, Peter James, Sandra Olarte Mantilla, Olympia Yarger, Louwrens Hoffman
The use of black soldier fly larvae (BSFL) to valorise different organic waste streams and the subsequent use of resulting larvae as a feedstock ingredient is increasing rapidly in several regions across the globe. The lack of knowledge about several safety issues including chemical contaminants (e.g. heavy metals) seems to affect the upscaling and commercialisation of this product. This study evaluates the safety of the BSFL against chemical contaminants including heavy metals and mycotoxins in both BSFL and frass samples reared with different food waste streams (e.g. soy waste, customised bread-vegetable diet, food waste mixture, supermarket and childcare centre) from two commercial production facilities. The effect of larval instars and post-harvest treatments (e.g. blanching and drying) on the safety of the BSFL was also investigated. The concentration of heavy metals was primarily influenced by the concentration in the food waste streams. The concentration was also higher in 6th instar compared to 5th instar larvae. The effect of blanching and drying have a varied effect on the concentration of heavy metals. Mycotoxins were found to be below the limit of quantification for all samples. The outcomes of this study indicated that BSFL grown on food waste streams and the resulting frass is safe against different heavy metals analysed. The findings of this study will assist the commercial BSFL manufacturers with the identification of relevant control points to ensure the chemical safety of their products. Therefore, encourage the use of different food waste streams as feedstock for rearing BSFL.
{"title":"Effect of larval instar and post-harvest treatments on heavy metals in BSFL and frass reared on commercial food waste streams","authors":"Shanmugam Alagappan, Sam Mallard, Daniel Cozzolino, Deirdre Mikkelsen, Peter James, Sandra Olarte Mantilla, Olympia Yarger, Louwrens Hoffman","doi":"10.1111/ijfs.17511","DOIUrl":"10.1111/ijfs.17511","url":null,"abstract":"<p>The use of black soldier fly larvae (BSFL) to valorise different organic waste streams and the subsequent use of resulting larvae as a feedstock ingredient is increasing rapidly in several regions across the globe. The lack of knowledge about several safety issues including chemical contaminants (e.g. heavy metals) seems to affect the upscaling and commercialisation of this product. This study evaluates the safety of the BSFL against chemical contaminants including heavy metals and mycotoxins in both BSFL and frass samples reared with different food waste streams (e.g. soy waste, customised bread-vegetable diet, food waste mixture, supermarket and childcare centre) from two commercial production facilities. The effect of larval instars and post-harvest treatments (e.g. blanching and drying) on the safety of the BSFL was also investigated. The concentration of heavy metals was primarily influenced by the concentration in the food waste streams. The concentration was also higher in 6th instar compared to 5th instar larvae. The effect of blanching and drying have a varied effect on the concentration of heavy metals. Mycotoxins were found to be below the limit of quantification for all samples. The outcomes of this study indicated that BSFL grown on food waste streams and the resulting frass is safe against different heavy metals analysed. The findings of this study will assist the commercial BSFL manufacturers with the identification of relevant control points to ensure the chemical safety of their products. Therefore, encourage the use of different food waste streams as feedstock for rearing BSFL.</p>","PeriodicalId":181,"journal":{"name":"International Journal of Food Science & Technology","volume":"59 11","pages":"8214-8223"},"PeriodicalIF":2.6,"publicationDate":"2024-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1111/ijfs.17511","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142210085","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}