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Microstructure and properties of some extruded copper–phosphorus alloys 几种挤压型铜磷合金的组织与性能
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419782
T. Sheppard, H. L. Yiu
Abstract Five Cu-P alloys have been produced by extruding cast and heat treated billets. This paper reports the effects of the extrusion variables on the resultant structure and properties. It is shown that the recrystallized structure observed in the α phase is produced by dynamic recrystallization occurring during the deformation process. The α grain size is determined by the processing parameters, but considerably modified in the two phase alloys by the Cu3P phase such that it may be quantified only by expressing it as a function of both extrusion ratio and temperature compensated strain rate. The deformation process is considerably affected by the large volume of second phase: the Cu3P being either broken or elongated during the extrusion process. The mechanical properties are influenced by the extrusion conditions and may be further modified by an annealing process which causes precipitation in the α phase and coalescence of the Cu3P phase. The mechanism of fracture during tensile testing is also rep...
摘要:采用挤压铸造和热处理工艺制备了5种Cu-P合金。本文报道了挤压变量对合成组织和性能的影响。结果表明,α相的再结晶组织是变形过程中动态再结晶形成的。α晶粒尺寸由工艺参数决定,但在两相合金中受到Cu3P相的显著影响,因此只能用挤压比和温度补偿应变率的函数来量化α晶粒尺寸。第二相的大量存在对变形过程有很大的影响,在挤压过程中Cu3P被破坏或拉长。其力学性能受挤压条件的影响,并可通过α相的析出和Cu3P相的聚并进一步改善。并介绍了拉伸试验中断裂的机理。
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引用次数: 4
Microstructures of isothermally transformed Fe-Nb-C alloys 等温相变Fe-Nb-C合金的显微组织
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419791
T. Sakuma, R. Honeycombe
AbstractThe microstructures of an Fe-Nb-C alloy, with and without boron, developed by the γ → α transformation during isothermal holding were examined mainly by metallographic techniques. Ferrite formed above about 750°C is equiaxed or polygonal, while Widmanstatten ferrite is developed at lower transformation temperatures increasingly replacing polygonal ferrite, as commonly observed in low alloy steels. The carbide precipitation changes with transformation temperature. Above about 800°C, the structure is not uniform, i.e. almost carbide free ferrite is formed at first and later coarse interphase precipitation takes place. Interphase precipitation occurs readily around 800°C, while uniform precipitation of NbC from supersaturated ferrite is the principal structural change around 730°C. At the lower temperatures, ferrite often contains a high density of dislocations and coarse cementite. The observed structural changes are explained in terms of the γ → α reaction kinetics and the partition of carbon to au...
摘要采用金相技术研究了等温保温过程中γ→α相变形成的Fe-Nb-C合金的组织。在750°C以上形成的铁素体是等轴或多边形的,而在较低的转变温度下形成的魏氏铁素体逐渐取代多边形铁素体,这在低合金钢中很常见。碳化物析出随相变温度的变化而变化。在800℃以上,组织不均匀,即先形成几乎无碳化物的铁素体,而后发生粗相析出。在800°C左右容易发生相间析出,而在730°C左右主要的结构变化是过饱和铁氧体中均匀析出NbC。在较低温度下,铁素体通常含有高密度的位错和粗渗碳体。观察到的结构变化可以用γ→α反应动力学和碳对au的分配来解释。
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引用次数: 46
Phasestructure and morphology of rapidly solidified Fe-15Mn-8Al-2C alloy 快速凝固Fe-15Mn-8Al-2C合金的相组织和形貌
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419818
Z. Sun, H. Davies, J. Whiteman
AbstractAn attempt is made to resolve the apparent conflict between previous studies of the effects of rapid solidification on the microstructure and mechanical properties of Fe(Mn, Ni)-Al-C alloys. The phase structure and morphology of rapidly solidified Fe-15Mn-8Al-2C alloy were investigated by optical microscopy, transmission electron microscopy, and X-ray and electron diffraction. This paper presents the results of the investigation and a comparison is made with the results of previous workers.
摘要本文试图解决以往关于快速凝固对Fe(Mn, Ni)-Al-C合金组织和力学性能影响的研究之间的明显矛盾。采用光学显微镜、透射电镜、x射线和电子衍射等方法研究了Fe-15Mn-8Al-2C合金快速凝固后的相组织和形貌。本文介绍了调查结果,并与前人的研究结果进行了比较。
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引用次数: 14
Effect of sulphur content in coating on development of (110)[001] texture of thin silicon–iron sheets 镀层中硫含量对硅铁薄板(110)[001]织构发展的影响
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419827
S. Szymura, A. Zawada
On peut obtenir de bonnes proprietes magnetiques dans des bandes de Fe-0% poids Si par recristallisation secondaire pour atteindre la texture (110) [001], l'inhibition de la croissance de grains apres achevement de la recristallisation primaire etant due aux precipites FeS et MnS qui se forment pendant la diffusion du soufre a partir du revetement. On determine le teneur en soufre du revetement et les limites a l'interieur desquelles, il est sur d'obtenir des bandes completement texturees
中可以获得良好的性能magnetiques Fe-0%波段的体重是否达到中等质地由结晶(110)[001],晶粒生长有抑制后再缴一次结晶由于海关对precipites FeS和MnS期间形成的传播起了硫岩。确定涂层的含硫量和极限,在此范围内可以获得完整的纹理条带。
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引用次数: 0
Role of microstructural instability in long time creep life prediction 微观组织不稳定性在长时间蠕变寿命预测中的作用
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419764
S. Claeys, J. Jones
AbstractThe influence of microstructural instability on long time creep life prediction has been investigated using Al alloy 6061 as a model material. The effect of microstructural changes on lifetime during long time creep, was determined by measuring the influence of microstructural degradation on steady state creep rate through the use of accelerated aging and short time creep tests. It was observed that at intermediate stresses at 260 and 288°C the creep life was strongly influenced by the rate of microstructural degradation and method proposed by other workers are effective in predicting creep life. At low stresses it was found that creep lives for times approaching 100000 hare adequately predicted by performing short time creep tests on fully overaged specimens and using simple extrapolation techniques. The results indicate that a knowledge of the aging response of alloys can be used to predict long time creep lives with reasonable accuracy.
摘要以6061铝合金为模型材料,研究了组织不稳定性对长时间蠕变寿命预测的影响。通过加速时效和短时间蠕变试验,测量微观组织退化对稳态蠕变速率的影响,确定了长时间蠕变过程中微观组织变化对寿命的影响。在260°C和288°C的中等应力下,蠕变寿命受到微观组织降解速率的强烈影响,其他工作者提出的方法可以有效地预测蠕变寿命。在低应力下,通过对完全超龄试样进行短时间蠕变试验并使用简单的外推技术,可以充分预测接近100000次的蠕变寿命。结果表明,了解合金的时效响应可以较准确地预测合金的长蠕变寿命。
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引用次数: 3
Impurity distribution In commercial Al-Ti and Al-Ti-B hardeners 商用Al-Ti和Al-Ti- b硬化剂中的杂质分布
Pub Date : 1984-09-01 DOI: 10.1179/030634584790419773
W. Youdelis, D. R. Grekul
AbstractThe concept of nucleation entropy has been developed in previous papers and applied to interpret the markedly enhanced grain refinement of Al by Ti when small amounts of Si (Refs. 2 and 3) and Be (Ref. 4) are added. In the theory, the nucleation entropy and the corresponding rate of nucleation of the peritectic compound increase if the third element concentrates in the peritectic compound. In the case of Si additions, incorporation of Si into the binary TiAl3 phase is required at a level which exceeds the concentration in the liquid alloy. The presence in an annealed and equilibrated Al-Ti-Si alloy of the compound TiAl2.4Si0.6, which has the body centred tetragonal (bct) structure of TiAl3, has been reported by Ramon and Schubert. In a more recent communication, Youdelis and Yang have shown that the bct Ti(Al, Si)3 compound (ranging in composition from TiAl1.83Si0.04 to TiAl2.38Si0.19)forms in a solidified non-equilibrated Al-Ti-Si alloy. The above conclusion that Si is incorporated into the TiAl3...
摘要成核熵的概念在以前的论文中得到了发展,并应用于解释当加入少量的Si(参考文献2和3)和Be(参考文献4)时,Ti对Al晶粒细化的显著增强。在理论上,如果第三元素集中在包晶化合物中,则包晶化合物的成核熵和相应的成核速率增大。在添加Si的情况下,需要在超过液态合金浓度的水平上将Si掺入二元TiAl3相。Ramon和Schubert报道了在退火和平衡的Al-Ti-Si合金中存在TiAl2.4Si0.6化合物,其具有TiAl3的体心四方(bct)结构。在最近的一篇论文中,Youdelis和Yang证明了bct Ti(Al, Si)3化合物(组成范围从TiAl1.83Si0.04到TiAl2.38Si0.19)在凝固的非平衡Al-Ti-Si合金中形成。以上结论认为Si被掺入TiAl3…
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引用次数: 1
Stress relief cracking phenomena in high strength structural steel 高强度结构钢的应力解除开裂现象
Pub Date : 1984-08-01 DOI: 10.1179/030634584790419845
C. You, C. A. Hippsley, J. Knott
AbstractStress relief cracking (SRC) is a potential risk during the post-weld heat treatment of fabrication welds. The present study investigates the susceptibility of Q1N (HY 80), a high strength weldable steel, to cracking in a recently developed stress relaxation test designed to simulate stress relief conditions. It has been found in previous investigations of the behaviour of 2.25Cr-1Mo and Mn-Mo-Ni steels in this test that the coarse grained heat affected zone (HAZ) is the most susceptible microstructure. In the present work, a comparison has been made of cracking behaviour in the HAZ of a metal inert gas butt weld and also in plate material in which the coarse grained HAZ microstructure has been simulated by application of an appropriate thermal cycle. The micromechanisms of cracking have been examined in both conditions and the prediction of SRC behaviour in service weldments from the observed behaviour of simulated HAZs is evaluated. It was found that cracking occurred under applied stresses of a...
摘要应力消除裂纹是制造焊缝焊后热处理过程中存在的潜在危险。本研究研究了Q1N (HY 80),一种高强度可焊钢,在最近开发的应力松弛试验中对开裂的敏感性,该试验旨在模拟应力释放条件。在先前对2.25Cr-1Mo和Mn-Mo-Ni钢的行为进行的研究中发现,粗晶热影响区(HAZ)是最易受影响的组织。在本工作中,对金属惰性气体对接焊缝的热影响区内的开裂行为进行了比较,并通过应用适当的热循环模拟了板材材料的粗晶热影响区内的微观结构。研究了这两种情况下裂纹的微观机制,并根据观察到的模拟haz行为评估了服役焊缝中SRC行为的预测。结果发现,在…
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引用次数: 12
Comparison of stress relief cracking in A 508 2 and A 533 B pressure vessel steels a5082与a533b压力容器钢应力解除开裂的比较
Pub Date : 1984-08-01 DOI: 10.1179/030634584790419836
J. Shin, C. Mcmahon
AbstractThe mechanisms of, and susceptibility to, stress relief cracking (SRC) were studied in A 508 class 2 and A 533 B pressure vessel steels by means of fixed displacement, load relaxation tests on notched specimens in pure bending at 823–923 K in vacuum. The specimens had previously been given heat affected zone simulation treatments in the range 1323–1573 K. The mechanisms of SRC were found to be the same as reported separately for A 508 2 steel, which was found to be generally more susceptible to SRC than A 533 B steel because of the faster formation of microcracks and coalescence of microcracks into a macrocrack. This can be rationalized in terms of the higher creep strength in A 508 2 steel owing to the presence of chromium, and the higher concentration of intergranular sulphur or reprecipitated sulphides owing to the lower manganese content of A 508 2 steel, which results in less stable sulphides. These factors are discussed in the framework of a recently proposed model for the brittle mode of SRC.
摘要通过823 ~ 923 K真空纯弯曲缺口试样的固定位移、载荷松弛试验,研究了a508 2级和a533b压力容器钢的应力解除开裂机理和敏感性。在1323-1573 K范围内对试样进行热影响区模拟处理。a5082钢的SRC机制与单独报道的相同,由于微裂纹的形成和微裂纹合并成大裂纹的速度更快,因此通常比a533 B钢更容易受到SRC的影响。这可以合理地解释为,由于铬的存在,a5082钢的蠕变强度较高,而由于a5082钢的锰含量较低,晶间硫或再沉淀硫化物浓度较高,导致硫化物不稳定。在最近提出的SRC脆性模式模型的框架内讨论了这些因素。
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引用次数: 22
Computer simulated dissolution of carbide precipitates in alloys 计算机模拟了合金中碳化物沉淀的溶解
Pub Date : 1984-08-01 DOI: 10.1179/030634584790419872
W. Voice, R. Faulkner
AbstractConventional theory on the dissolution of a spherical particle of a second phase in an alloy is shown to be inappropriate when considering carbide species. In particular, the assumptions of an error function solute concentration profile and a constant equilibrium solute concentration level at the interface cannot be made. A model for computer simulated dissolution is therefore proposed which is based on the diffusion of solute away from a carbide particle across discrete shell increments. The method is used to predict times for complete and partial dissolutions of M23C6 particles in Nimonic 80A (registered trade mark of Henry Wiggin and Co. Ltd). As a result, the effect of solution heat treatment of the alloy is more clearly understood and practical improvements are recommended.
摘要传统的第二相球形颗粒在合金中溶解的理论在考虑碳化物种类时是不合适的。特别是,不能假设误差函数的溶质浓度分布和恒定的平衡溶质浓度水平在界面上。因此,提出了一个计算机模拟溶解的模型,该模型基于溶质从碳化物颗粒扩散到离散壳增量的过程。该方法用于预测M23C6颗粒在Nimonic 80A (Henry Wiggin and Co Ltd .的注册商标)中完全和部分溶解的时间。从而对该合金固溶热处理的效果有了更清晰的认识,并提出了切实可行的改进建议。
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引用次数: 7
Hot deformation and dynamic recrystallization of Al-5Mg-0.8Mn alloy Al-5Mg-0.8Mn合金的热变形与动态再结晶
Pub Date : 1984-08-01 DOI: 10.1179/030634584790419854
H. Mcqueen, E. Evangelista, J. Bowles, G. Crawford
AbstractThe AA 5083 alloy was deformed in torsion in the ranges 300–500°C and 0.1–1 S−1 to a strain of 5. The flow stress as a function of strain rose to a maximum value then gradually decreased towards a steady state and had a dependence on temperature and strain rate of the traditional form with an activation energy higher than that for pure Al. Optical microstructures of specimens quenched after working ranged from elongated grains at 300°C to recrystallized grains at 500°C. Transmission electron microscope subgrain structures from all conditions of working were more recovered at higher temperatures and lower strain rates. The subgrain diameters are smaller than those in commercial Al mainly as a result of the increased density of particles and this is in agreement with observations in extrusions. Since the degree of recovery is not substantially less than in commercial Al, one is led to confirm the theory that the dynamic recrystallization is caused by particles of <0.6 μm.
摘要:对AA 5083合金在300 ~ 500℃、0.1 ~ 1 S−1条件下进行了应变为5的扭转变形。流动应力随应变的变化先达到最大值,然后逐渐减小,且与温度和应变速率有关,其活化能高于纯Al。加工后淬火试样的光学组织从300℃时的细长晶粒到500℃时的再结晶晶粒不等。在较高的温度和较低的应变速率下,所有工作条件下的透射电镜亚晶结构都得到了更好的恢复。亚晶粒直径比商业铝的小,主要是由于颗粒密度的增加,这与挤压中的观察结果一致。由于回收程度并不明显低于商用Al,因此可以证实动态再结晶是由<0.6 μm的颗粒引起的理论。
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引用次数: 103
期刊
Metal science
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