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Tri-Nordammarane Triterpenoids and Neoclerodane Diterpenoids From Salvia Aspera (Labiatae) 鼠尾草(唇形科)中的三-北达玛烷三萜和新氯罗德烷二萜
Pub Date : 2002-01-01 DOI: 10.1080/10575630290020046
B. Esquivel, Francisco Guerrero, R. Toscano
From the aerial parts of Salvia aspera one new tri-nordammarane named amblyol ( 1 ) was isolated besides amblyone ( 2 ). An X-ray analysis was performed on compound 1 . In addition, three known neoclerodane diterpenoids were also isolated. The structures of these compounds were established by spectral and chemical methods. The presence of dammarane triterpenoids in a Mexican Salvia is described for the first time.
从鼠尾草(Salvia aspera)的地上部分离到一种新的三北丹参烷(amblyol),命名为amblyol(1)。对化合物1进行x射线分析。此外,还分离出3个已知的新氯罗丹二萜。通过光谱和化学方法确定了这些化合物的结构。首次在墨西哥鼠尾草中发现了达玛烷三萜。
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引用次数: 10
Triterpene Saponins from Craniotome Furcata
Pub Date : 2002-01-01 DOI: 10.1080/10575630290004233
C. Fan, Hai-Fang Sun, Shao-Nong Chen, J. Yue, Zhongwen Lin, Han-Dong Sun
Three saponins, craniosaponin A ( 1 ) and buddlejasaponins Ia ( 2 ) and I ( 3 ) were isolated from the n -butanol soluble fraction of Craniotome furcata for the first time. Among them, craniosaponin A ( 1 ) was identified to be a new compound. The structure of craniosaponin A was assigned mainly by spectral methods. A preliminary assay in vitro was applied to evaluate their cytotoxicity against several tumor cell-lines.
首次从开颅植物正丁醇溶性部位分离得到颅皂苷A(1)和茶皂素Ia(2)和I(3)。其中颅磷素A(1)为新化合物。颅皂苷A的结构主要通过光谱方法确定。体外初步测定了它们对几种肿瘤细胞系的细胞毒性。
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引用次数: 14
Labdane Diterpenes from Haplopappus Illinitus
Pub Date : 2002-01-01 DOI: 10.1080/10575630290020460
F. Faini, C. Labbé, R. Torres, G. D. Monache, F. Monache
A chemical study of aerial parts of Haplopappus illinitus afforded five labdane diterpenoids whose structures were elucidated by high field NMR spectroscopy and 2D techniques. Four of them are dicarboxylic acids previously reported as the corresponding dimethyl ester derivatives and the fifth is a new compound.
利用高场核磁共振波谱和二维光谱技术对五种唇丹二萜类化合物进行了化学分析。其中四种是二羧酸,先前报道为相应的二甲酯衍生物,第五种是新化合物。
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引用次数: 2
Isolation of Two New Ionone Glucosides from Quince ( Cydonia Oblonga Mill.) Leaves 昆柏(Cydonia Oblonga Mill)中两个新离子苷的分离叶子
Pub Date : 2002-01-01 DOI: 10.1080/10575630290020028
A. Lutz-Röder, Marc Schneider, P. Winterhalter
The 9- O - - d -glucopyranosides of (6 R )-3-oxo-4-hydroxy-7,8-dihydro- -ionol 1 and 3-oxo-5,6-epoxy- -ionol 2 were isolated from quince leaves. The glycosidic extract was obtained by XAD-2 adsorption and MeOH elution. After DCCC separation and flash chromatography, purification by high performance liquid chromatography was carried out. The novel quince leaf constituents were characterized as peracetates 1a and 2a .
从木瓜叶中分离得到(6 R)-3-氧-4-羟基-7,8-二氢-离子醇1和3-氧-5,6-环氧-离子醇2的9- O -d -葡萄糖吡喃苷。通过XAD-2吸附和甲醇洗脱得到糖苷提取物。经DCCC分离、闪蒸色谱后,进行高效液相色谱纯化。木瓜叶的新成分为过乙酸酯1a和过乙酸酯2a。
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引用次数: 16
Clerodane Diterpenoids from Ajuga Bracteosa Wall 取自小苞草的克罗丹二萜类化合物
Pub Date : 2002-01-01 DOI: 10.1080/10575630290020578
V. H. Verma, U. Mahmood, Bikram Singh
The whole plant of Ajuga bracteosa afforded five compounds including one new clerodane diterpenoid designated as Bracteonin-A ( 1 ) 6 f -acetoxy, 15 (R&S)-methoxy, 18-(4'-hydroxy, 3'- g -methyl, 3'- f -acetoxy, butyryloxy) neoclerodane. The other compounds identified were 14,15-dihydroajugapitin, 14-hydro-15-hydroxy ajugapitin, g -sitosterol, and stigmasterol. The structural elucidation was carried out by spectroscopic techniques.
在小苞草属植物中发现了5个新化合物,包括一种新的氯烷二萜类化合物,命名为小苞草素-a (1) 6 f -乙酰氧基,15 (R&S)-甲氧基,18-(4'-羟基,3'- g -甲基,3'- f -乙酰氧基,丁基氧基)新氯烷。其他化合物鉴定为14,15-二氢合欢素、14-氢-15-羟基合欢素、g -谷甾醇和豆甾醇。用光谱技术对其结构进行了解析。
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引用次数: 13
Synthesis and Antioxidant Activity of 3-Substituted Guaiazulene Derivatives 3-取代愈创唑烯衍生物的合成及抗氧化活性研究
Pub Date : 2002-01-01 DOI: 10.1080/10575630290013585
H. Pratsinis, S. Haroutounian
A series of 3-substituted guaiazulene derivatives has been synthesized and their antioxidant properties were evaluated by monitoring their capacity for scavenging the stable free-radical DPPH. 3-Vinylguaiazulene was the most potent, possessing antioxidant activity superior than f -tocopherol. These derivatives were also moderate inhibitors of the proliferation of human promyelocytic leukemia cells.
合成了一系列3-取代的愈创唑烯衍生物,并通过监测其清除稳定自由基DPPH的能力来评价其抗氧化性能。3-乙烯基愈创蓝烯的抗氧化活性最强,其抗氧化活性优于f -生育酚。这些衍生物也是人类早幼粒细胞白血病细胞增殖的中度抑制剂。
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引用次数: 10
A New Steroidal Saponin from Tribulus Terrestris Linn 蒺藜中一种新的甾体皂苷
Pub Date : 2002-01-01 DOI: 10.1080/10575630290020541
Wen-ji Sun, Jin-Min Gao, G. Tu, Z. Guo, Yongming Zhang
A new steroidal saponin containing six monosaccharides was obtained from the total plant of Tribulus terrestris and elucidated based on chemical spectroscopic analysis, especially on 2D-NMR technology as 26- O - g - d -glucopyranosyl-22-methoxy-furostane-3- O -{ g - d -xylopyranosyl(1 M 3)-[ g - d -xylopyranosyl(1 M 2)- g - d -glucopyranosyl(1 M 4)]}-[ f - l -rhamnopyranosy(1 M 2)]- g - d -galactopyranoside.
获得了一个新的包含六个单糖甾体皂苷的总植物刺蒺藜,阐明基于化学光谱分析,尤其是在2 d-nmr技术为26 - O g - d -glucopyranosyl-22-methoxy-furostane-3 - O - {g - d -xylopyranosyl(1米3)- (g - d -xylopyranosyl(1米2)- g d -glucopyranosyl(1米4)]}- [f - l -rhamnopyranosy(1米2)]- g d -galactopyranoside。
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引用次数: 30
Isolation and Structure Elucidation of Three Glycosides and a Long Chain Alcohol from Polianthes Tuberosa Linn 牡丹中三个苷和一个长链醇的分离与结构解析
Pub Date : 2002-01-01 DOI: 10.1080/713604303
K. Khan, S. Perveen, S. A. M. Ayattollahi, N. Saba, A. Rashid, S. Firdous, Syed Moazzam Haider, Z. Ullah, Shagufta Rahat, Zarrar Khan
Three glycosides and a long chain alcohol were isolated from the bulbs of Polianthes tuberosa , these were identified as 3,29-dihydroxystigmast-5-ene-3- O - g - d -galactopyranoside ( 1 ) 1 , ethyl g - d -galactopyranoside ( 2 ), ethyl- f - d -galactopyranoside ( 3 ), and 1-tricosanol ( 4 ). The structures were determined by extensive spectroscopic and chemical methods. All four isolated compounds were screened for their cytotoxicity, antibacterial and antifungal activities, none of the compounds showed any significant activity.
从牡丹鳞茎中分离到3种糖苷和1种长链醇,分别鉴定为3,29-二羟基柱状体-5-烯-3- O -g -d -半乳糖苷(1)1、乙基g -d -半乳糖苷(2)、乙基- f -d -半乳糖苷(3)和1-三葡萄糖醇(4)。通过广泛的光谱和化学方法确定了其结构。对4个分离得到的化合物进行了细胞毒性、抗菌和抗真菌活性的筛选,均未显示出明显的活性。
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引用次数: 11
A Novel Flavonol Lyxoside of Orostachys Japonicus Herb 一种新的黄酮类醇苷类化合物
Pub Date : 2002-01-01 DOI: 10.1080/1057563029001/4818
S. Sung, W. J. Jung, Y. Kim
A novel flavonol lyxoside was isolated from the aerial part of Orostachys japonicus (Crassulaceae). Its structure was determined as gossypetin 8-O-f-D-lyxopyranoside using several spectral data and chemical methods. Lyxoside of flavonoid was isolated for the first time from nature.
从天竺葵地上部分离到一种新的黄酮醇苷。利用多种光谱数据和化学方法确定其结构为棉sypetin 8-O-f-D-lyxopyranoside。本文首次从自然界中分离到黄酮类化合物中的溶糖苷。
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引用次数: 16
A New Drimane from the Heartwood of the Japanese Yew, Taxus Cuspidata 日本红豆杉(Taxus Cuspidata)心材的一种新动力
Pub Date : 2002-01-01 DOI: 10.1080/1057563029001/4791
H. Kiyota, Q. Shi, T. Oritani
A new drimane sesquiterpenoid was isolated from the heartwood of the Japanese yew, Taxus cuspidata Sieb. et Zucc. Its structure was established as 1 g -acetoxyisodrimeninol (1 g -acetoxy-11,12-epoxy-7-drimen-11-ol, 1 ). This compound was gradually oxidized to give n -lactone (1 g -acetoxy-8-drimeno-11,12-lactone, 4 ).
从日本红豆杉(Taxus cuspidata Sieb)心材中分离到一个新的驱动倍半萜类化合物。调查。确定其结构为1 g -乙酰氧基异丙胺醇(1 g -乙酰氧基-11,12-环氧-7-乙酰氧基-11-醇,1)。该化合物被逐渐氧化生成n -内酯(1g -乙酰氧基-8-基氨基-11,12-内酯,4)。
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引用次数: 10
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Natural Product Letters
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