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Nanoscale face-centered-cubic zirconium dispersed in omega zirconium 纳米级面心立方锆分散在欧米伽锆中
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-05-23 DOI: 10.1080/09500839.2022.2077999
Xinu Tan, R. Qiu, Yushun Liu, Fengxian Bi, Jinlong Zhang, Boran Tao, Qing Liu
ABSTRACT In contrast to lamella-like face-centered cubic zirconium (FCC-Zr) distributed inside an α-Zr matrix, as repeatedly reported previously, dispersed and nanoscale FCC-Zr with lattice parameter a = 0.520 nm has been found inside lamella-like and blocky ω-Zr by transmission electron microscopy (TEM). The orientation relationship between the FCC-Zr and the ω-Zr obeys [001]FCC//[1 02]ω, (100)FCC//(11 0)ω. A possible phase transformation mechanism between FCC-Zr, α-Zr and β-Zr is discussed. This finding introduces a new possibility in phase transformations during the fabrication of Zr alloys, potentially enlightening the design of new high-performance Zr alloys.
摘要与先前重复报道的分布在α-Zr基体内的片状面心立方锆(FCC Zr)不同,分散的纳米级FCC Zr具有晶格参数a = 0.520 透射电子显微镜(TEM)在ω-Zr片层状和块状内部发现了nm。FCC Zr与ω-Zr的取向关系服从[001]FCC//[1 02]ω,(100)FCC//(110)ω。讨论了FCC Zr、α-Zr和β-Zr之间可能的相变机制。这一发现为锆合金制造过程中的相变提供了一种新的可能性,可能对新型高性能锆合金的设计有所启发。
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引用次数: 1
Effect of secondary rolling on the interfacial bonding strength and mechanical properties of Al/Mg/Al clad plates 二次轧制对Al/Mg/Al复合板界面结合强度和力学性能的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-04-22 DOI: 10.1080/09500839.2022.2065702
Xiang-Zhi Cao, Chunhua Xu, Yu Li, Xuecheng Cao, Ruizhi Peng, J. Fang
ABSTRACT The effects of secondary rolling on the microstructure evolution and mechanical properties of Al/Mg/Al clad sheets have been investigated. The results indicate that a double-layer intermetallic compound (Mg2Al3 and Mg17Al12) forms and sandwiches the MgO film during the first rolling and annealing, while the sandwich structure shows a low peel strength owing to the intrinsic brittleness of intermetallic. However, a secondary rolling leads to a shear-induced breakage of the sandwich structure, whereupon the peel strength significantly increases from 1.3 N/mm to 12.7 N/mm on account of an effective bonding of the Mg/Al interface. The secondary rolling not only eliminates the influence of MgO on the interface, but also improves the bonding strength of the interface. Furthermore, the clad sheet can obtain an excellent elongation (21%) and remain of high interfacial strength (∼12 N/mm) after the recovery annealing.
研究了二次轧制对Al/Mg/Al复合板组织演变和力学性能的影响。结果表明,在第一次轧制和退火过程中,双层金属间化合物(Mg2Al3和Mg17Al12)形成并夹住了MgO膜,而夹层结构由于金属间化合物的固有脆性而表现出较低的剥离强度。然而,二次轧制导致夹层结构的剪切引起的断裂,因此剥离强度从1.3显著增加 N/mm至12.7 N/mm,这是由于Mg/Al界面的有效结合。二次轧制不仅消除了MgO对界面的影响,而且提高了界面的结合强度。此外,包层片材可以获得优异的伸长率(21%),并保持较高的界面强度(~12 N/mm)。
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引用次数: 1
Dislocation multiplication and dynamics in an aluminium alloy 铝合金中的位错倍增和动力学
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-04-22 DOI: 10.1080/09500839.2022.2065701
Tiantian Huang, Fei Liu, Zhiyi Liu, Guangyu He, Yangcheng Hu
ABSTRACT A mechanism of dislocation multiplication is introduced. The surface of the Al20Cu2Mn3 phase in an Al alloy can act as a barrier to impede dislocation movement. When two dislocations with opposite Burgers vectors approach each other, dislocations can annihilate if the pair remains at a distance less than the critical distance for annihilation. A dislocation loop is then formed around the Al20Cu2Mn3 phase or dislocations interact with the loop forming a dislocation tangle, which can promote dislocation multiplication. The driving force for dislocation reproduction, the dislocation glide velocity and the rate of dislocation multiplication are discussed.
介绍了位错倍增的机理。Al20Cu2Mn3相的表面可以起到阻挡位错运动的屏障作用。当两个具有相反的Burgers向量的位错相互接近时,如果这对位错保持在小于湮灭的临界距离,则位错可以湮灭。在Al20Cu2Mn3相周围形成位错环或位错与位错环相互作用形成位错缠结,促进位错增殖。讨论了位错再生的驱动力、位错滑动速度和位错增殖速率。
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引用次数: 0
Deformation mechanisms in the directionally solidified nickel-based CM247LC at room temperature 室温定向凝固镍基CM247LC的变形机理
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-03-17 DOI: 10.1080/09500839.2022.2049908
Zhenhuan Gao, Peng Zhang, Q. Niu, Jiao Li, L. Nie, X. Gong, Xiaolong Song
ABSTRACT After solutionizing and aging at 980°C for various durations, the compressive deformation behaviour and mechanisms of the directionally solidified nickel-based superalloy CM247LC are investigated at room temperature. Experimental results show that the yield strength decreases gradually from 991 ± 1.2–672 ± 7.5 MPa with increasing the γ′ precipitate size from 145 ± 2–604 ± 19 nm. Transmission electron microscope observations on the slightly deformed specimens reveal that, in contrast to previous researches, plastic deformation of all the specimens is controlled by strongly coupled dislocations cutting through γ′ precipitates. Based on these experimental results, the relationship between the yield strength and precipitate size is discussed.
摘要研究了定向凝固镍基高温合金CM247LC在980°C不同时间的固溶和时效后的室温压缩变形行为和机理。实验结果表明,屈服强度从991开始逐渐降低 ± 1.2–672 ± 7.5 MPa,随着γ′沉淀尺寸从145增加 ± 2–604 ± 19 nm。对轻微变形试样的透射电镜观察表明,与以往的研究相比,所有试样的塑性变形都是由切割γ′析出相的强耦合位错控制的。基于这些实验结果,讨论了屈服强度与沉淀物尺寸之间的关系。
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引用次数: 1
Ex-situ study of diffusion in liquid Al–Cu melts under a transverse magnetic field using X-ray imaging X射线成像在横向磁场作用下Al–Cu液态熔体扩散的原位研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-03-09 DOI: 10.1080/09500839.2022.2048111
Ying Liu, Wen-Chih Lin, Bangfei Zhou, Xianghui Guo, Hao Cai, T. Zheng, B. Ding, Y. Zhong, Lei Zhang
ABSTRACT Al–Cu melts were used to study interdiffusion under a transverse magnetic field (TMF) using X-ray imaging. A novel gravity-assisted automatic docking device was used to create a long capillary of the diffusion couple. Compared with the results acquired using energy-dispersive spectroscopy, X-ray imaging is more convenient and accurate to determine concentration profiles along long capillaries using the numerous gray value intensities in the imaging. Because a TMF can inhibit melt convection, the interdiffusion coefficient (D AlCu) was reduced after applying a TMF of 2 T. Our results demonstrate that the application of X-ray imaging is an efficient way to study ex-situ diffusion in liquid melts.
摘要:采用x射线成像技术研究了Al-Cu熔体在横向磁场(TMF)作用下的相互扩散。采用一种新型的重力辅助自动对接装置,形成了扩散偶的长毛细管。与能量色散光谱的结果相比,x射线成像利用成像中的众多灰度值强度来确定长毛细血管的浓度分布更加方便和准确。由于TMF可以抑制熔体对流,施加2 T的TMF后,相互扩散系数(dalcu)降低。我们的结果表明,应用x射线成像是研究液体熔体中非原位扩散的有效方法。
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引用次数: 3
Modelling of cavity growth during the superplastic flow of a fine-grained Ti–6Al–4V titanium alloy processed by direct rolling 直轧细晶Ti-6Al-4V钛合金超塑性流动过程中空洞生长的模拟
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-02-23 DOI: 10.1080/09500839.2022.2036380
Xin Wang, Ge Zhou, Chao Liu, Siqian Zhang, Haoyu Zhang, Feng Li, Lijia Chen
ABSTRACT Ti–6Al–4V fine-grained plates were manufactured using a rolling method and then subjected to superplastic tensile tests at varying temperatures and strain rates on an AG 250KNE electronic tensile testing machine. The superplastic behaviours of the plates were also tested. A cavity-growth model was established and the changing laws of energy during cavity growth and microstructure evolution of superplastic deformation were predicted. The Ti–6Al–4V alloy possessed the maximum elongation rate of 886% at 840°C and a strain rate of 5 × 10−4 s−1. The strain-rate sensitivity index m for this alloy was 0.54. The mechanism of superplastic deformation was established to be strain-induced grain-boundary slip, and the mechanism of cavity growth to be plasticity-controlled cavity coalescence and growth.
摘要采用轧制方法制造了Ti–6Al–4V细晶板,然后在AG 250KNE电子拉伸试验机上进行了不同温度和应变速率下的超塑性拉伸试验。还测试了板材的超塑性行为。建立了空洞生长模型,预测了空洞生长过程中能量的变化规律和超塑性变形的微观组织演变。Ti–6Al–4V合金在840°C下的最大伸长率为886%,应变速率为5 × 10−4 s−1。该合金的应变速率敏感性指数m为0.54。建立了超塑变形机制为应变诱导晶界滑移,空穴生长机制为塑性控制的空穴聚结和生长。
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引用次数: 4
Orientation relationship of quasicrystalline approximate phase η-Al5(Mn,Cr) in AA5083 aluminium alloy AA5083铝合金准晶近似相η-Al5(Mn,Cr)的取向关系
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-02-23 DOI: 10.1080/09500839.2022.2038802
Xiaoling Xiao, Hongwei Liu, Huilan Huang, Wenlong Chen, Yanfang Ma
ABSTRACT A quasicrystalline approximate monoclinic phase η-Al5(Mn,Cr) with a plate-like or rod-like morphology in AA5083 aluminium alloy was investigated using transmission electron microscopy. Several types of orientation relationships (ORs) between the η-Al5(Mn,Cr) phase and the α-Al matrix were observed and these ORs could be correlated with a rotation operation around the axis with an angle that is an integer times 18.5°. These multiple ORs were interpreted by utilizing an invariant deformation element model – a simplified version of three-dimensional invariant line strain analysis.
摘要:用透射电镜研究了AA5083铝合金中近似单斜晶的片状或棒状η-Al5(Mn,Cr)相。观察到η-Al5(Mn,Cr)相与α-Al基体之间存在几种类型的取向关系(ORs),这些取向关系可能与绕轴旋转18.5°的整数倍的角度有关。使用不变变形单元模型-三维不变线应变分析的简化版本来解释这些多个ORs。
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引用次数: 0
A note on mixed-mode fracture by the smoothing gradient damage model 用平滑梯度损伤模型研究混合模式断裂
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-02-23 DOI: 10.1080/09500839.2022.2041214
T. Bui, Chanh Dinh Vuong
ABSTRACT The objective of this technical note is to illustrate twofold. The first issue is devoted to the ability of the recently developed smoothing gradient-enhanced damage model (SGDM), which is associated with the modified von Mises equivalent strain in modelling mixed-mode fracture problems, in particular the common Nooru–Mohamed's test. We show that the developed approach works pretty well for this test, yielding appropriate structural damage response and crack paths for all three specimen sizes, i.e. and . The second issue is, in a similar manner, to discuss the less accuracy of another damage model, the localising gradient damage scheme recently studied by Shedbale et al. Int. J. Mech Sci 2021, 199:106410, in reproducing crack paths and structural responses for the same mixed-mode problem.
摘要本技术说明的目的是说明两个方面。第一个问题是最近开发的平滑梯度增强损伤模型(SGDM)的能力,该模型与模拟混合模式断裂问题时的修正von Mises等效应变有关,特别是常见的Nooru–Mohamed试验。我们表明,所开发的方法在该测试中效果良好,对所有三种试样尺寸(即和)产生了适当的结构损伤响应和裂纹路径。第二个问题是,以类似的方式,讨论另一个损伤模型的精度较低的问题,Shedbale等人最近研究的局部梯度损伤方案。Int.J.Mech Sci 2021199:106410,在再现相同混合模式问题的裂纹路径和结构响应时。
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引用次数: 0
Electric field influenced coordinate jump of the guiding centre and magnetotransport 电场对导引中心坐标跳跃和磁输运的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-02-16 DOI: 10.1080/09500839.2022.2152505
Jingjing Feng, Yang Gao, Q. Niu
ABSTRACT Our studies formulate a classical theory to study the influence of in-plane electric field on electron-impurity scattering process and magnetotransport in a two-dimensional space, in the presence of a strong out-of-plane magnetic field. Our studies connect classical scattering and quantum Landau Level broadening, as will be reviewed in this report. We derived an electric current formula in agreement with the current derived from the Drude theory under a strong magnetic field. Our electric current formula is derived microscopically from the migration of the guiding centres at strong magnetic field regime . The electron-impurity scattering under electromagnetic field not only shifts the guiding centre coordinates X and Y, but also changes cyclotron radius R. The change of cyclotron radius R compensates the change of the electric potential energy during the scattering process. The broadening of cyclotron radius is a classical manifestation of Landau Levels broadening. Our conductivity derived from our current formula in the linear response regime results in the same as the current derived from Kubo current fluctuation theory, providing a special case of the fluctuation-dissipation theorem.
摘要我们的研究提出了一个经典理论来研究在强平面外磁场存在的情况下,平面内电场对二维空间中电子杂质散射过程和磁输运的影响。我们的研究将经典散射和量子朗道能级加宽联系起来,这将在本报告中进行综述。我们导出了一个与强磁场下德鲁德理论导出的电流一致的电流公式。我们的电流公式是从强磁场下引导中心的迁移微观上推导出来的。电磁场作用下的电子杂质散射不仅改变了引导中心坐标X和Y,而且改变了回旋半径R。回旋半径R的变化补偿了散射过程中势能的变化。回旋半径的加宽是朗道能级加宽的经典表现。我们从线性响应状态下的电流公式推导出的电导率与从Kubo电流波动理论推导出的电流相同,提供了波动耗散定理的一个特例。
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引用次数: 0
Experimental determination of effective atomic radii of constituent elements in CrMnFeCoNi high-entropy alloy CrMnFeCoNi高熵合金中组成元素有效原子半径的实验测定
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2022-01-25 DOI: 10.1080/09500839.2021.2024290
T. Teramoto, Momoko Narasaki, Katsushi Tanaka
ABSTRACT To elucidate the complex mechanism of solid-solution strengthening in high-entropy alloys (HEAs), it is necessary to determine the effective atomic radii of the constituent elements that are the sources of lattice strain. In the present study, the effective atomic radii of the constituent elements in CrMnFeCoNi HEA that are the basis of the atomic displacements, are evaluated from lattice parameters experimentally determined via θ–2θ X-ray diffraction measurements. The order of the evaluated atomic radii in the present study is different from that of the atomic radii determined via ab-initio calculations in previous studies. The results of the ab-initio calculations indicate a correlation between the yield stress of and the average atomic displacement in the HEA. However, no definite correlation is confirmed by the experimental results in the present study.
为了阐明高熵合金(HEAs)固溶强化的复杂机理,有必要确定作为晶格应变源的组成元素的有效原子半径。在本研究中,通过θ-2θ x射线衍射测量得到的晶格参数,计算了CrMnFeCoNi HEA中组成元素的有效原子半径,这是原子位移的基础。本研究中计算的原子半径的顺序与以往研究中通过从头计算确定的原子半径的顺序不同。从头算的结果表明,HEA的屈服应力与平均原子位移之间存在相关性。然而,本研究的实验结果并没有明确的相关性。
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引用次数: 2
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Philosophical Magazine Letters
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