M P Selwood, D R Rusby, D N Fittinghoff, M P Hill, G J Williams
X-ray radiography is a ubiquitous diagnostic technique in high energy density (HED) physics, with point projection backlighting commonly used for characterizing static and dynamic objects at high spatial and temporal resolutions. These are typically constrained in attainable resolution by their decrease in brightness, which is a limiting factor for high-Z HED experiments, such as double-shell implosions at the National Ignition Facility (NIF) requiring MeV-scale bremsstrahlung sources at high (<50μm) resolution. Coded source imaging is a technique using multiple point-projection sources to produce multiple overlapping radiographs, which are then decoded as a function of the source positions in a process akin to coded aperture imaging. Here, we discuss a new approach to coded source generation using multiple individual small-diameter wire targets within the footprint of a defocused large-scale a0 ≃ 1 laser to produce an MeV-scale high-resolution bright combined source for x-ray radiography. We outline optimal source designs with NIF-Advanced Radiography Capability as the case study, highlight the need for iterative reconstruction decoding, and discuss the research required to demonstrate a robust physical proof-of-concept.
X 射线射线照相术是高能量密度(HED)物理学中一种无处不在的诊断技术,通常使用点投影背光源以高空间和时间分辨率描述静态和动态物体的特征。它们的分辨率通常受到亮度下降的限制,而亮度下降是高 Z HED 实验的限制因素,例如国家点火装置(NIF)的双壳内爆需要 MeV 级的轫致辐射源在高 (
{"title":"On the theory of multi-target coded sources for high-energy, high-resolution, and high-brightness x-ray radiography.","authors":"M P Selwood, D R Rusby, D N Fittinghoff, M P Hill, G J Williams","doi":"10.1063/5.0217711","DOIUrl":"https://doi.org/10.1063/5.0217711","url":null,"abstract":"<p><p>X-ray radiography is a ubiquitous diagnostic technique in high energy density (HED) physics, with point projection backlighting commonly used for characterizing static and dynamic objects at high spatial and temporal resolutions. These are typically constrained in attainable resolution by their decrease in brightness, which is a limiting factor for high-Z HED experiments, such as double-shell implosions at the National Ignition Facility (NIF) requiring MeV-scale bremsstrahlung sources at high (<50μm) resolution. Coded source imaging is a technique using multiple point-projection sources to produce multiple overlapping radiographs, which are then decoded as a function of the source positions in a process akin to coded aperture imaging. Here, we discuss a new approach to coded source generation using multiple individual small-diameter wire targets within the footprint of a defocused large-scale a0 ≃ 1 laser to produce an MeV-scale high-resolution bright combined source for x-ray radiography. We outline optimal source designs with NIF-Advanced Radiography Capability as the case study, highlight the need for iterative reconstruction decoding, and discuss the research required to demonstrate a robust physical proof-of-concept.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142133579","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
An experimental setup has been developed for the simultaneous measurement of the Hall coefficient (RH) and electrical conductivity (σ) of thermoelectric (TE) specimens in the temperature range of 300-700 K. The van der Pauw geometry is utilized for the RH and σ measurements. The sample holder geometry has been designed for diverse TE specimen dimensions and easy sample mounting. A special feature of the holder geometry is that the same sample can be used for other relevant thermoelectric measurements such as the Seebeck coefficient and thermal diffusivity. This minimizes measurement errors associated with compositional or doping inhomogeneities. In the absence of high temperature standard reference materials for Hall coefficient measurements, silicon samples with different doping concentrations have been used to verify the accuracy of the instrument. Additionally, the electrical conductivity data have been validated by measurements on the same samples in a calibrated setup. Repeat measurements indicate a maximum standard deviation of ±3% and ±0.5% for the RH and σ data in the studied temperature range. Furthermore, comparisons with the calibrated setup indicate deviations within ±3% for the σ data. The suitability of the measurement setup for TE specimens has been demonstrated using measurements on n-type (Mg2Sn) and p-type (Mg3Sb2) specimens with carrier concentrations in the range of 1019-1020 cm-3.
我们开发了一套实验装置,用于在 300-700 K 温度范围内同时测量热电(TE)试样的霍尔系数(RH)和电导率(σ)。样品支架的几何形状是针对不同的 TE 试样尺寸设计的,便于样品安装。样品架几何形状的一个特点是,同一样品可用于其他相关的热电测量,如塞贝克系数和热扩散率。这最大程度地减少了与成分或掺杂不均匀性相关的测量误差。由于缺乏用于霍尔系数测量的高温标准参考材料,我们使用了不同掺杂浓度的硅样品来验证仪器的准确性。此外,电导率数据还通过在校准装置中对相同样品的测量进行了验证。重复测量结果表明,在所研究的温度范围内,相对湿度和 σ 数据的最大标准偏差分别为 ±3% 和 ±0.5%。此外,与校准设置的比较表明,σ 数据的偏差在 ±3% 以内。通过对载流子浓度在 1019-1020 cm-3 范围内的 n 型(Mg2Sn)和 p 型(Mg3Sb2)试样进行测量,证明了该测量装置对 TE 试样的适用性。
{"title":"High temperature setup for measurement of Hall coefficient and electrical conductivity of thermoelectric materials.","authors":"B Agrawal, S Choudhary, P K Sahu, T Dasgupta","doi":"10.1063/5.0214582","DOIUrl":"https://doi.org/10.1063/5.0214582","url":null,"abstract":"<p><p>An experimental setup has been developed for the simultaneous measurement of the Hall coefficient (RH) and electrical conductivity (σ) of thermoelectric (TE) specimens in the temperature range of 300-700 K. The van der Pauw geometry is utilized for the RH and σ measurements. The sample holder geometry has been designed for diverse TE specimen dimensions and easy sample mounting. A special feature of the holder geometry is that the same sample can be used for other relevant thermoelectric measurements such as the Seebeck coefficient and thermal diffusivity. This minimizes measurement errors associated with compositional or doping inhomogeneities. In the absence of high temperature standard reference materials for Hall coefficient measurements, silicon samples with different doping concentrations have been used to verify the accuracy of the instrument. Additionally, the electrical conductivity data have been validated by measurements on the same samples in a calibrated setup. Repeat measurements indicate a maximum standard deviation of ±3% and ±0.5% for the RH and σ data in the studied temperature range. Furthermore, comparisons with the calibrated setup indicate deviations within ±3% for the σ data. The suitability of the measurement setup for TE specimens has been demonstrated using measurements on n-type (Mg2Sn) and p-type (Mg3Sb2) specimens with carrier concentrations in the range of 1019-1020 cm-3.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142294187","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Frank A F Winiberg, Mathieu Fradet, Rafal Krzysiak, Yangquan Chen, Kamjou Mansour, Aaron C Noell, J Kent Wallace, Lance E Christensen
Indium seals have been used extensively in ultra-high vacuum and cryogenic applications. Typically, these seals use indium alongside or in place of other metal gaskets in stainless-steel vacuum flanges, with some custom applications for flanges sealing directly with glass (optics or tubes). Here, we present the design and performance of three pressed indium seals (99.99% In) between aluminum and 0.5 in. diameter sapphire optics and aluminum and gold coated Kovar semiconductor packages (TO-66 and TO-39). Test fixtures were designed to mimic those of future tunable diode laser spectrometers for Earth, planetary, and manned spaceflight environmental monitoring applications. Successful high-hermeticity seals [<10-10 atm cc/s (He)] were achieved for all seals formed with sufficient pressure applied to allow indium to flow between mating surfaces. The hermeticity of the seals was maintained after temperature cycling (-10 to +80 °C, 20 cycles), with the optical seals surviving extended duration tests (-55 to +85 °C, per MIL-STD-883). Semiconductor packages (TO-39) subjected to these extended tests saw a moderate increase in leak rate [∼5 × 10-9 atm cc/s (He)]; however, further testing showed that either the glass-metal package seals or the indium were affected (the sample size was too small to draw firm conclusions for future applications). Overall, these results suggest long-term survivability of indium seals for Kovar-aluminum and sapphire-aluminum interfaces [>10 years at 10-10 atm cc/s (He)], where the coefficient of thermal expansion differs by approximately four times.
{"title":"Design and performance of indium seals for size-constrained tunable laser spectrometers.","authors":"Frank A F Winiberg, Mathieu Fradet, Rafal Krzysiak, Yangquan Chen, Kamjou Mansour, Aaron C Noell, J Kent Wallace, Lance E Christensen","doi":"10.1063/5.0206815","DOIUrl":"https://doi.org/10.1063/5.0206815","url":null,"abstract":"<p><p>Indium seals have been used extensively in ultra-high vacuum and cryogenic applications. Typically, these seals use indium alongside or in place of other metal gaskets in stainless-steel vacuum flanges, with some custom applications for flanges sealing directly with glass (optics or tubes). Here, we present the design and performance of three pressed indium seals (99.99% In) between aluminum and 0.5 in. diameter sapphire optics and aluminum and gold coated Kovar semiconductor packages (TO-66 and TO-39). Test fixtures were designed to mimic those of future tunable diode laser spectrometers for Earth, planetary, and manned spaceflight environmental monitoring applications. Successful high-hermeticity seals [<10-10 atm cc/s (He)] were achieved for all seals formed with sufficient pressure applied to allow indium to flow between mating surfaces. The hermeticity of the seals was maintained after temperature cycling (-10 to +80 °C, 20 cycles), with the optical seals surviving extended duration tests (-55 to +85 °C, per MIL-STD-883). Semiconductor packages (TO-39) subjected to these extended tests saw a moderate increase in leak rate [∼5 × 10-9 atm cc/s (He)]; however, further testing showed that either the glass-metal package seals or the indium were affected (the sample size was too small to draw firm conclusions for future applications). Overall, these results suggest long-term survivability of indium seals for Kovar-aluminum and sapphire-aluminum interfaces [>10 years at 10-10 atm cc/s (He)], where the coefficient of thermal expansion differs by approximately four times.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142294184","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Shenghui Liu, Shichao Cheng, Yu Luo, Jianhe Zhu, Liangbao Liu, Hang Guo, Kunpeng Cui, Minfang An, Liangbin Li
A steel belt casting equipment, weighing approximately ∼6-7 tons and measuring ∼5 m in length, has been designed and developed for simulating the industrial processing of polymer films and being combined with synchrotron radiation in situ x-ray scattering measurements. Through modification of its modules, it is feasible to implement two distinct film casting modes, namely the wet and the dry casting processes. The speed of a steel belt can span from 0.5 to 8 m/min. The highest experimental temperature and drying wind speed are 300 °C and 6 m/s, respectively. All film casting parameters, such as extrusion speed, distance between die and steel belt, casting speed, temperature, and wind speed, can be adjusted independently. Especially, the control accuracy of the temperature and casting rate can reach ±0.1 °C and ±0.01 m/min, respectively. The feasibility of this equipment has been validated through in situ x-ray scattering tests at the BL10U1 industrial beamline of the Shanghai synchrotron radiation facility. With the assistance of this equipment, the understanding of the physical mechanism behind the film casting process should be improved so that the development of advanced functional polymer films.
为模拟聚合物薄膜的工业加工过程,并结合同步辐射原位 X 射线散射测量,设计和开发了一种钢带浇注设备,重约 6-7 吨,长约 5 米。通过修改模块,可以实现两种不同的薄膜浇铸模式,即湿法和干法浇铸工艺。钢带的速度可以从 0.5 米/分钟到 8 米/分钟不等。最高实验温度和干燥风速分别为 300 °C 和 6 m/s。所有薄膜浇铸参数,如挤压速度、模具与钢带之间的距离、浇铸速度、温度和风速,均可独立调节。特别是温度和浇注速度的控制精度分别可达 ±0.1 ℃ 和 ±0.01 米/分钟。通过在上海同步辐射设施 BL10U1 工业光束线进行原位 X 射线散射试验,验证了该设备的可行性。在该设备的帮助下,人们对薄膜浇铸过程背后的物理机理的认识将得到提高,从而促进先进功能聚合物薄膜的开发。
{"title":"A versatile steel belt casting equipment for in situ synchrotron radiation x-ray scattering measurement of polymer films.","authors":"Shenghui Liu, Shichao Cheng, Yu Luo, Jianhe Zhu, Liangbao Liu, Hang Guo, Kunpeng Cui, Minfang An, Liangbin Li","doi":"10.1063/5.0219366","DOIUrl":"https://doi.org/10.1063/5.0219366","url":null,"abstract":"<p><p>A steel belt casting equipment, weighing approximately ∼6-7 tons and measuring ∼5 m in length, has been designed and developed for simulating the industrial processing of polymer films and being combined with synchrotron radiation in situ x-ray scattering measurements. Through modification of its modules, it is feasible to implement two distinct film casting modes, namely the wet and the dry casting processes. The speed of a steel belt can span from 0.5 to 8 m/min. The highest experimental temperature and drying wind speed are 300 °C and 6 m/s, respectively. All film casting parameters, such as extrusion speed, distance between die and steel belt, casting speed, temperature, and wind speed, can be adjusted independently. Especially, the control accuracy of the temperature and casting rate can reach ±0.1 °C and ±0.01 m/min, respectively. The feasibility of this equipment has been validated through in situ x-ray scattering tests at the BL10U1 industrial beamline of the Shanghai synchrotron radiation facility. With the assistance of this equipment, the understanding of the physical mechanism behind the film casting process should be improved so that the development of advanced functional polymer films.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142294180","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Providing a cloud service for optical quantum computing requires stabilizing the optical system for extended periods. It is advantageous to construct a fiber-based system, which does not require spatial alignment. However, fiber-based systems are instead subject to fiber-specific instabilities. For instance, there are phase drifts due to ambient temperature changes and external disturbances and polarization fluctuations due to the finite polarization extinction ratio of fiber components. Here, we report the success of measuring squeezed light with a fiber system for 24 h. To do this, we introduce stabilization mechanics to suppress fluctuations in the fiber system and an integrated controller to automatically align the entire system. The squeezed light at a wavelength of 1545.3 nm is measured every 2 min, where automated alignments are inserted every 30 min. The squeezing levels with an average of -4.42 dB are recorded with an extremely small standard deviation of 0.08 dB over 24 h. With the technologies developed here, we can build complicated optical setups with the fiber-based system and operate them automatically for extended periods, which is promising for cloud service of quantum computation.
{"title":"Long-term stability of squeezed light in a fiber-based system using automated alignment.","authors":"Tomohiro Nakamura, Takefumi Nomura, Mamoru Endo, Atsushi Sakaguchi, He Ruofan, Takahiro Kashiwazaki, Takeshi Umeki, Kan Takase, Warit Asavanant, Jun-Ichi Yoshikawa, Akira Furusawa","doi":"10.1063/5.0203988","DOIUrl":"https://doi.org/10.1063/5.0203988","url":null,"abstract":"<p><p>Providing a cloud service for optical quantum computing requires stabilizing the optical system for extended periods. It is advantageous to construct a fiber-based system, which does not require spatial alignment. However, fiber-based systems are instead subject to fiber-specific instabilities. For instance, there are phase drifts due to ambient temperature changes and external disturbances and polarization fluctuations due to the finite polarization extinction ratio of fiber components. Here, we report the success of measuring squeezed light with a fiber system for 24 h. To do this, we introduce stabilization mechanics to suppress fluctuations in the fiber system and an integrated controller to automatically align the entire system. The squeezed light at a wavelength of 1545.3 nm is measured every 2 min, where automated alignments are inserted every 30 min. The squeezing levels with an average of -4.42 dB are recorded with an extremely small standard deviation of 0.08 dB over 24 h. With the technologies developed here, we can build complicated optical setups with the fiber-based system and operate them automatically for extended periods, which is promising for cloud service of quantum computation.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142352862","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
N Vanderloo, M Cufari, L Russell, T M Johnson, J Vargas, B C Foo, B I Buschmann, S G Dannhoff, A DeVault, T E Evans, J H Kunimune, Y Lawrence, J A Pearcy, B L Reichelt, C W Wink, M Gatu Johnson, R D Petrasso, J A Frenje, C K Li
Image plates (IPs) are a quickly recoverable and reusable radiation detector often used to measure proton and x-ray fluence in laser-driven experiments. Recently, IPs have been used in a proton radiography detector stack on the OMEGA laser, a diagnostic historically implemented with CR-39, or radiochromic film. The IPs used in this and other diagnostics detect charged particles, neutrons, and x-rays indiscriminately. IPs detect radiation using a photo-stimulated luminescence (PSL) material, often phosphor, in which electrons are excited to metastable states by ionizing radiation. Protons at MeV energies deposit energy deeper into the IP compared with x rays below ∼20 keV due to the Bragg peak present for protons. This property is exploited to discriminate between radiation types. Doses of mono-energetic protons between 1.7 and 14 MeV are applied to IPs using the MIT linear electrostatic ion accelerator. This paper presents the results from consecutive scans of IPs irradiated with different proton energies. The PSL ratios between subsequent scans are shown to depend on proton energy, with higher energy protons having lower PSL ratios for each scan. This finding is separate from the known energy dependence in the absolute sensitivity of IPs. The results can be compared to complimentary work on x rays, showing a difference between protons and x rays, forging a path to discriminate between proton and x-ray fluence in mixed radiation environments.
成像板(IP)是一种可快速恢复和重复使用的辐射探测器,通常用于测量激光驱动实验中的质子和 X 射线通量。最近,IP 被用于 OMEGA 激光器上的质子射线照相探测器堆栈,这是一种历史上使用 CR-39 或放射性变色胶片进行的诊断。在这种诊断和其他诊断中使用的 IP 可以不加区分地探测带电粒子、中子和 X 射线。IP 利用光致发光(PSL)材料(通常是荧光粉)检测辐射,其中电子被电离辐射激发至瞬态。由于质子存在布拉格峰,与 20 千伏以下的 X 射线相比,MeV 能量的质子会将能量沉积到 IP 的更深处。利用这一特性可以区分辐射类型。利用麻省理工学院的线性静电离子加速器,将 1.7 至 14 MeV 的单能质子剂量应用于 IP。本文介绍了用不同质子能量对 IPs 进行连续扫描的结果。结果表明,后续扫描之间的 PSL 比率取决于质子能量,能量越高的质子每次扫描的 PSL 比率越低。这一发现与已知的 IPs 绝对灵敏度的能量依赖性不同。该结果可与 X 射线的相关工作进行比较,后者显示了质子和 X 射线之间的差异,为在混合辐射环境中区分质子和 X 射线通量开辟了道路。
{"title":"Image plate multi-scan response to fusion protons in the range of 1-14 MeV.","authors":"N Vanderloo, M Cufari, L Russell, T M Johnson, J Vargas, B C Foo, B I Buschmann, S G Dannhoff, A DeVault, T E Evans, J H Kunimune, Y Lawrence, J A Pearcy, B L Reichelt, C W Wink, M Gatu Johnson, R D Petrasso, J A Frenje, C K Li","doi":"10.1063/5.0219547","DOIUrl":"10.1063/5.0219547","url":null,"abstract":"<p><p>Image plates (IPs) are a quickly recoverable and reusable radiation detector often used to measure proton and x-ray fluence in laser-driven experiments. Recently, IPs have been used in a proton radiography detector stack on the OMEGA laser, a diagnostic historically implemented with CR-39, or radiochromic film. The IPs used in this and other diagnostics detect charged particles, neutrons, and x-rays indiscriminately. IPs detect radiation using a photo-stimulated luminescence (PSL) material, often phosphor, in which electrons are excited to metastable states by ionizing radiation. Protons at MeV energies deposit energy deeper into the IP compared with x rays below ∼20 keV due to the Bragg peak present for protons. This property is exploited to discriminate between radiation types. Doses of mono-energetic protons between 1.7 and 14 MeV are applied to IPs using the MIT linear electrostatic ion accelerator. This paper presents the results from consecutive scans of IPs irradiated with different proton energies. The PSL ratios between subsequent scans are shown to depend on proton energy, with higher energy protons having lower PSL ratios for each scan. This finding is separate from the known energy dependence in the absolute sensitivity of IPs. The results can be compared to complimentary work on x rays, showing a difference between protons and x rays, forging a path to discriminate between proton and x-ray fluence in mixed radiation environments.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142308528","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
F Goto, A Calloni, R Yivlialin, A Bossi, F Ciccacci, L Duò, J N O'Shea, G Bussetti
We present a system for the growth of molecular films in vacuum that exhibits high versatility with respect to the choice of molecular species. These can be either evaporated from powders or injected from solutions using an electrospray system, making it possible to handle particularly large and/or fragile molecules in a controlled environment. The apparatus is equipped with a reflectance anisotropy spectroscopy system for the in situ characterization of the optical response of the films and can be directly connected to a photoelectron spectrometer without breaking the vacuum. The system is conceived for the study and characterization of porphyrin films. Here, to showcase the range of possible analyses allowed by the experimental setup and test the operation of the system, novel results are provided on electrospray deposition on highly oriented pyrolytic graphite of Zn tetraphenyl porphyrins and Zn proto porphyrins, the latter featuring fragile side groups that make deposition from solution more attractive. In situ characterization is complemented by ex situ atomic force microscopy. Thanks to this multi-technique approach, changes in the film morphology and spectroscopic response are detected and directly related to the choice of the molecular moiety and growth method.
{"title":"A versatile system for the growth of porphyrin films via electrospray and molecular sublimation in vacuum and their multi-technique characterization.","authors":"F Goto, A Calloni, R Yivlialin, A Bossi, F Ciccacci, L Duò, J N O'Shea, G Bussetti","doi":"10.1063/5.0223459","DOIUrl":"https://doi.org/10.1063/5.0223459","url":null,"abstract":"<p><p>We present a system for the growth of molecular films in vacuum that exhibits high versatility with respect to the choice of molecular species. These can be either evaporated from powders or injected from solutions using an electrospray system, making it possible to handle particularly large and/or fragile molecules in a controlled environment. The apparatus is equipped with a reflectance anisotropy spectroscopy system for the in situ characterization of the optical response of the films and can be directly connected to a photoelectron spectrometer without breaking the vacuum. The system is conceived for the study and characterization of porphyrin films. Here, to showcase the range of possible analyses allowed by the experimental setup and test the operation of the system, novel results are provided on electrospray deposition on highly oriented pyrolytic graphite of Zn tetraphenyl porphyrins and Zn proto porphyrins, the latter featuring fragile side groups that make deposition from solution more attractive. In situ characterization is complemented by ex situ atomic force microscopy. Thanks to this multi-technique approach, changes in the film morphology and spectroscopic response are detected and directly related to the choice of the molecular moiety and growth method.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142120486","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Simon P H Vincent, Philippe Guittienne, Patrick Quigley, Cyrille Sepulchre, Rémy Jacquier, Robert Bertizzolo, Marcelo Baquero-Ruiz, Alan A Howling, Ivo Furno
A birdcage resonant helicon antenna is designed, mounted, and tested in the toroidal device TORPEX. The birdcage resonant antenna is an alternative to the usual Boswell or half-helical antenna designs commonly used for ∼10 cm diameter helicon sources in low temperature plasma devices. The main advantage of the birdcage antenna lies in its resonant nature, which makes it easily operational even at large scales, an appealing feature for the TORPEX device whose poloidal cross section is 40 cm in diameter. With this antenna, helicon waves are shown to be launched and sustained throughout the whole torus of TORPEX. The helicon waves can be launched at low power on a pre-existing magnetron-generated plasma with little effect on the density profiles. The birdcage antenna can also be used alone to produce plasma, which removes the constraint of a narrow range of applied magnetic fields required by the magnetron, opening the way to a new range of studies on TORPEX with the external magnetic field as a control parameter.
{"title":"A birdcage resonant antenna for helicon wave generation in TORPEX.","authors":"Simon P H Vincent, Philippe Guittienne, Patrick Quigley, Cyrille Sepulchre, Rémy Jacquier, Robert Bertizzolo, Marcelo Baquero-Ruiz, Alan A Howling, Ivo Furno","doi":"10.1063/5.0212529","DOIUrl":"https://doi.org/10.1063/5.0212529","url":null,"abstract":"<p><p>A birdcage resonant helicon antenna is designed, mounted, and tested in the toroidal device TORPEX. The birdcage resonant antenna is an alternative to the usual Boswell or half-helical antenna designs commonly used for ∼10 cm diameter helicon sources in low temperature plasma devices. The main advantage of the birdcage antenna lies in its resonant nature, which makes it easily operational even at large scales, an appealing feature for the TORPEX device whose poloidal cross section is 40 cm in diameter. With this antenna, helicon waves are shown to be launched and sustained throughout the whole torus of TORPEX. The helicon waves can be launched at low power on a pre-existing magnetron-generated plasma with little effect on the density profiles. The birdcage antenna can also be used alone to produce plasma, which removes the constraint of a narrow range of applied magnetic fields required by the magnetron, opening the way to a new range of studies on TORPEX with the external magnetic field as a control parameter.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142120485","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
In photon-deficient, noncollective Thomson scattering diagnostics, filter polychromators are typically employed in the spectral analysis of Thomson-scattered signals to achieve acceptable signal-to-noise performance. Currently, the most common polychromator filter configuration employs a set of single-passband optical filters that define individual spectral channels. Here, we introduce a new spectral analysis method for Thomson scattering based on spectral filters with multiple passbands, referred to as Thomson scattering spectral multiplexing. Implementing multi-bandpass spectral filters on polychromators increases the achievable range of electron temperature measurement for a given number of filters employed. In addition, Thomson scattering spectral multiplexing reduces systematic measurement uncertainty, with fewer required spectral channels, thereby decreasing light loss from reduced optical element interactions. A multi-bandpass filter set, optimized by a genetic algorithm, has been successfully installed and tested on the Helically Symmetric eXperiment (HSX), demonstrating the benefits of the Thomson scattering spectral multiplexing method.
{"title":"Enhancing Thomson scattering polychromator performance with multi-pass spectral filters.","authors":"W R Goodman, B Geiger","doi":"10.1063/5.0219569","DOIUrl":"https://doi.org/10.1063/5.0219569","url":null,"abstract":"<p><p>In photon-deficient, noncollective Thomson scattering diagnostics, filter polychromators are typically employed in the spectral analysis of Thomson-scattered signals to achieve acceptable signal-to-noise performance. Currently, the most common polychromator filter configuration employs a set of single-passband optical filters that define individual spectral channels. Here, we introduce a new spectral analysis method for Thomson scattering based on spectral filters with multiple passbands, referred to as Thomson scattering spectral multiplexing. Implementing multi-bandpass spectral filters on polychromators increases the achievable range of electron temperature measurement for a given number of filters employed. In addition, Thomson scattering spectral multiplexing reduces systematic measurement uncertainty, with fewer required spectral channels, thereby decreasing light loss from reduced optical element interactions. A multi-bandpass filter set, optimized by a genetic algorithm, has been successfully installed and tested on the Helically Symmetric eXperiment (HSX), demonstrating the benefits of the Thomson scattering spectral multiplexing method.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142126498","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M Wappl, S A Bozhenkov, M N A Beurskens, S Bannmann, M D Kuczyński, H M Smith, K J Brunner, O P Ford, G Fuchert, J P Knauer, A Langenberg, N A Pablant, E Pasch, P Zs Poloskei, R C Wolf
Two novel web apps for W7-X are introduced: Profile Cooker and Power House. They are designed to streamline the workflow of profile fitting and power balance analysis while offering a graphical user interface that works in any common browser. This allows us to compile a comprehensive database of experimental power balance results. All fitting functions available in Profile Cooker are presented and compared on the basis of example profiles. The power balance equation assumed in Power House is established and its individual terms are discussed. The main focus of the power balance analysis is on the turbulent transport coefficients. A model for quick calculation of neutral beam power deposition based on experimental profiles is presented. Neoclassical root transition poses an issue for power balance analysis due to the uncertainty of the radial electric field. A global, neoclassical simulation with the code EUTERPE is performed for a set of experimental profiles to gain an understanding of the neoclassical root transition.
为 W7-X 引入两个新颖的网络应用程序:Profile Cooker 和 Power House。它们旨在简化剖面拟合和功率平衡分析的工作流程,同时提供可在任何普通浏览器中使用的图形用户界面。这使我们能够汇编一个全面的功率平衡实验结果数据库。Profile Cooker 中提供的所有拟合功能都以示例剖面为基础进行了介绍和比较。建立了 Power House 中假定的功率平衡方程,并对其各个项进行了讨论。功率平衡分析的重点是湍流传输系数。介绍了基于实验剖面的中性束功率沉积快速计算模型。由于径向电场的不确定性,新古典根转换对功率平衡分析提出了问题。使用 EUTERPE 代码对一组实验剖面进行了全局新古典模拟,以获得对新古典根过渡的理解。
{"title":"Web apps for profile fitting and power balance analysis at Wendelstein 7-X.","authors":"M Wappl, S A Bozhenkov, M N A Beurskens, S Bannmann, M D Kuczyński, H M Smith, K J Brunner, O P Ford, G Fuchert, J P Knauer, A Langenberg, N A Pablant, E Pasch, P Zs Poloskei, R C Wolf","doi":"10.1063/5.0225315","DOIUrl":"https://doi.org/10.1063/5.0225315","url":null,"abstract":"<p><p>Two novel web apps for W7-X are introduced: Profile Cooker and Power House. They are designed to streamline the workflow of profile fitting and power balance analysis while offering a graphical user interface that works in any common browser. This allows us to compile a comprehensive database of experimental power balance results. All fitting functions available in Profile Cooker are presented and compared on the basis of example profiles. The power balance equation assumed in Power House is established and its individual terms are discussed. The main focus of the power balance analysis is on the turbulent transport coefficients. A model for quick calculation of neutral beam power deposition based on experimental profiles is presented. Neoclassical root transition poses an issue for power balance analysis due to the uncertainty of the radial electric field. A global, neoclassical simulation with the code EUTERPE is performed for a set of experimental profiles to gain an understanding of the neoclassical root transition.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":null,"pages":null},"PeriodicalIF":1.3,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142294191","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}