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Effect of CQ-amine ratio on the degree of conversion in resin monomers with binary and ternary photoinitiation systems cq -胺比对二元和三元光引发体系树脂单体转化率的影响
Pub Date : 2012-05-01 DOI: 10.5395/RDE.2012.37.2.96
Ho-Jin Moon, D. Shin
Objectives: This study evaluated the effect of camphorquinone (CQ)-amine ratio on the C=C double bond conversion of resins with binary and ternary photoinitiation systems. Materials and Methods: Two monomer mixtures (37.5 Bis-GMA/37.5 Bis- EMA/25 TEGDMA) with binary systems (CQ/DMAEMA in weight ratio, group A [0.5/1.0] and B [1.0/0.5]) and four mixtures with ternary system (CQ/OPPI/DMAEMA, group C [0.1/1.0/0.1], D [0.1/1.0/ 0.2], E [0.2/1.0/0.1] and F [0.2/1.0/0.2]) were tested: 1 : 2 or 2 : 1 CQ-amine ratio in binary system, while 1 : 1 ratio was added in ternary system. The monomer mixture was cured for 5, 20, 40, and 300 sec with a Demetron 400 curing unit (Demetron). After each exposure time, degree of conversion (DC) was estimated using Fourier transform infrared (FTIR) spectrophotometer (Nicolet 520, Nicolet Instrument Corp.). The results were analyzed by ANOVA followed by Scheffe test, with p = 0.05 as the level of significance. Results: DC (%) was expressed in the order of curing time (5, 20, 40, and 300 sec). Group A (, , , ); Group B (, , , ); Group C (, , , ); Group D (, , , ); Group E (, , , ); Group F (, , , ). Conclusion: All the monomers with ternary photoinitiation system showed higher DC than the ones with binary system, until 40 sec. Concerning about the effect of CQ-amine ratio on the DC, group A converted into polymer more than group B in binary system. However, there was no significant difference among groups with ternary system, except group C when cured for 5 sec only.
目的:研究脑醌与胺的比例对二元和三元光引发体系树脂C=C双键转化的影响。材料与方法:采用CQ/DMAEMA质量比为A组[0.5/1.0]和B组[1.0/0.5]的二元体系(37.5 Bis- gma /37.5 Bis- EMA/25 TEGDMA)和四种三元体系(CQ/OPPI/DMAEMA, C组[0.1/1.0/0.1],D组[0.1/1.0/ 0.2],E组[0.2/1.0/0.1]和F组[0.2/1.0/0.2])的单体混合物进行测试:二元体系中CQ-胺的比例为1:2或2:1,三元体系中CQ-胺的比例为1:1。将单体混合物用Demetron 400固化装置(Demetron)固化5,20,40和300秒。每次曝光后,使用傅里叶变换红外(FTIR)分光光度计(Nicolet 520, Nicolet Instrument Corp.)估计转换度(DC)。结果采用方差分析和Scheffe检验,p = 0.05为显著性水平。结果:DC(%)按固化时间(5、20、40、300秒)的顺序表示。A组(,,,);B组(,,,);C组(,,,);D组(,,,);E组(,,,);F组(,,,)。结论:在40秒前,三元光引发体系的单体均表现出高于二元体系的DC。在cq -胺比对DC的影响方面,二元体系中A基团转化为聚合物的速率高于B基团。除C组仅治疗5秒外,三元体系各组间无显著差异。
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引用次数: 8
Color and hardness changes in artificial white spot lesions after resin infiltration 树脂浸润后人工白斑病变的颜色和硬度变化
Pub Date : 2012-05-01 DOI: 10.5395/RDE.2012.37.2.90
Ji Hoon Kim, H. Son, Juhea Chang
Objectives: The purpose of this study was to determine the effect of resin infiltration technique on color and surface hardness of white spot lesion (WSL) with various degrees of demineralization. Materials and Methods: Ten human upper premolars were cut and divided into quarters with a window on the enamel surface. Each specimens were separated into four groups (n = 10) and immersed in demineralization solution to create WSL: control, no treatment (baseline); 12 h, 12 hr demineralization; 24 h, 24 hr demineralization; 48 h, 48 hr demineralization. Resin infiltration was performed to the specimens using Icon (DMG). color parameters of the enamel-dentin complex were determined using a spectroradiometer at baseline, after caries formation and after resin infiltration. Surface hardness was measured by Vickers Micro Hardness Tester (Shimadzu, HMV-2). The differences in color and hardness among the groups were analyzed with ANOVA followed by Tukey test. Results: Resin infiltration induced color changes and increased the hardness of demineralized enamel. After resin infiltration, there was no difference in color change () or microhardness among the groups (p
目的:研究树脂浸润技术对不同脱矿程度的白斑病变(WSL)颜色及表面硬度的影响。材料与方法:将10颗上颌前磨牙切成四等分,牙釉质表面开窗。每个标本分为4组(n = 10),浸泡在脱矿液中形成WSL:对照组,不处理(基线);12 h, 12 h脱矿;24h, 24h脱矿;48小时,48小时脱矿。用Icon (DMG)对标本进行树脂浸润。牙釉质-牙本质复合物的颜色参数在基线、龋形成后和树脂浸润后使用光谱仪测定。表面硬度采用维氏显微硬度计(Shimadzu, HMV-2)测定。采用方差分析和Tukey检验分析各组颜色和硬度的差异。结果:树脂浸润引起脱矿牙釉质颜色变化,硬度增加。经树脂浸润后,各组间颜色变化(p)、显微硬度(p)无显著差异
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引用次数: 5
Endodontic management of a maxillary lateral incisor with dens invaginatus and external root irregularity using cone-beam computed tomography 锥形束计算机断层对上颌侧切牙牙槽内陷和外根不规则的根管治疗
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.50
Y. Lim, S. Nam, Sung-Ho Jung, D. Shin, S. Shin, K. Min
Cone-beam computed tomography (CBCT) is a useful diagnostic tool for identification of both internal and external root configurations. This case report describes the endodontic management of a lateral incisor with both dens invaginatus and external root irregularity by using CBCT. Nonsurgical endodontic retreatment was performed on the lateral incisor with dens invaginatus. A perforation through the dens invaginatus and external concavity was repaired using mineral trioxide aggregate. After 18 mon of follow-up, there were no clinical symptoms. Recall radiographs appeared normal and showed healing of the periapical pathosis. The understanding of both internal root canal configuration and external root irregularity using CBCT can ensure predictable and successful results.
锥形束计算机断层扫描(CBCT)是一种有用的诊断工具,用于识别内部和外部根的结构。本病例报告描述了采用CBCT对侧切牙内凹和外根不规则的根管治疗。对侧切牙牙槽内陷进行非手术牙髓再治疗。使用三氧化二矿骨料修复牙槽内陷和外凹的穿孔。随访18个月,无临床症状。回忆x线片显示正常,并显示根尖周围病变愈合。利用CBCT对内根管形态和外根管不规则性的了解可以确保可预测和成功的结果。
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引用次数: 9
Evaluation of internal adaptation of dental adhesive restorations using micro-CT 显微ct评价牙粘接剂修复体的内适应性
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.41
Oh-Hyun Kwon, Sung-ho Park
Objectives: The internal adaptation of composite restorations with or without resin modified glass ionomer cement (RMGIC) was analyzed non-destructively using Microcomputed tomography (micro-CT). Materials and Methods: Thirty intact human teeth were used. The specimens were divided into 3 groups. In the control group, the cavities were etched with 10% phosphoric acid for 15 sec. Composite resin was filled into the cavity without adhesive. In group 1, light cured glass ionomer cement (GIC, Fuji II LC, GC) was applied as a base. The cavities were then etched, bonded, light cured and filled with composites. In group 2, the cavities were then etched, bonded, light cured and filled with composites without base application. They were immersed in a 25% silver nitrate solution. Micro-CT was performed before and after mechanical loading. One-way ANOVA with Duncan analysis was used to compare the internal adaptation between the groups before or after loading. A paired t-test was used to compare internal adaptation before and after mechanical loading. All statistical inferences were made within the 95% confidence interval. Results: The silver nitrate solution successfully penetrated into the dentinal tubules from the pulp spaces, and infiltrated into the gap between restoration and pulpal floor. Group 2 showed a lower adaptation than the control group and group 1 (p
目的:利用微计算机断层扫描(micro-CT)非破坏性分析树脂改性玻璃离子水门合剂(RMGIC)复合修复体的内部适应性。材料与方法:使用30颗完整的人牙。标本分为3组。对照组用10%磷酸蚀刻15秒,用复合树脂填充空腔,不粘接。第一组采用光固化玻璃离子水泥(GIC, Fuji II LC, GC)作为基底。这些空腔随后被蚀刻、粘合、光固化并填充复合材料。在第2组中,空腔被蚀刻、粘合、光固化并填充复合材料,而不使用基底。他们被浸泡在25%硝酸银溶液中。机械加载前后分别行Micro-CT检查。采用Duncan分析的单因素方差分析比较各组在加载前后的内部适应。采用配对t检验比较机械负荷前后的内适应。所有统计推断均在95%置信区间内进行。结果:硝酸银溶液成功地从牙髓间隙渗透到牙本质小管中,并渗入修复体与牙髓底之间的间隙。2组的适应能力低于对照组和1组(p
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引用次数: 12
Effect of different chlorhexidine application times on microtensile bond strength to dentin in Class I cavities 不同氯己定应用次数对ⅰ类牙本质微拉伸结合强度的影响
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.9
H. Kang, Ho-Jin Moon, D. Shin
Objectives: This study evaluated the effect of 2% chlorhexidine digluconate (CHX) with different application times on microtensile bonds strength (MTBS) to dentin in class I cavities and intended to search for ideal application time for a simplified bonding protocol. Materials and Methods: Flat dentinal surfaces with class I cavities () in 40 molar teeth were bonded with etch-and-rinse adhesive system, Adper Single Bond 2 (3M ESPE) after: (1) etching only as a control group; (2) etching + CHX 5 sec + rinsing; (3) etching + CHX 15 sec + rinsing; (4) etching + CHX 30 sec + rinsing; and (5) etching + CHX 60 sec + rinsing. Resin composite was builtup with Z-250 (3M ESPE) using a bulk method and polymerized for 40 sec. For each condition, half of the specimens were immediately submitted to MTBS test and the rest of them were assigned to thermocycling of 10,000 cycles between and before testing. The data were analyzed using two-way ANOVA, at a significance level of 95%. Results: There was no significant difference in bond strength between CHX pretreated group and control group at the immediate testing period. After thermocycling, all groups showed reduced bond strength irrespective of the CHX use. However, groups treated with CHX maintained significantly higher MTBS than control group (p
目的:本研究评价了2%二光酸氯己定(CHX)不同应用时间对I类牙本质微拉伸键合强度(MTBS)的影响,旨在为简化的键合方案寻找理想的应用时间。材料与方法:对40颗磨牙进行I类牙槽()的平面牙质面粘接,采用蚀刻-冲洗胶粘剂系统,Adper Single Bond 2 (3M ESPE)进行粘接:(1)仅作为对照组进行蚀刻;(2)蚀刻+ CHX 5秒+冲洗;(3)蚀刻+ CHX 15秒+冲洗;(4)蚀刻+ CHX 30秒+冲洗;(5)蚀刻+ CHX 60秒+冲洗。树脂复合材料用Z-250 (3M ESPE)用散装法构建,并聚合40秒。每种条件下,一半的样品立即提交给MTBS测试,其余样品在测试之间和测试前进行10,000次热循环。数据分析采用双向方差分析,显著性水平为95%。结果:CHX预处理组与对照组在直接测试期的粘结强度无显著差异。热循环后,与CHX的使用无关,所有组的结合强度都有所降低。然而,CHX治疗组的MTBS明显高于对照组(p
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引用次数: 5
Effect of fluoride concentration in pH 4.3 and pH 7.0 supersaturated solutions on the crystal growth of hydroxyapatite pH 4.3和pH 7.0过饱和溶液中氟浓度对羟基磷灰石晶体生长的影响
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.16
Haneol Shin, Sung-ho Park, Jeong-Won Park, Chan-Young Lee
Objectives: Present study was undertaken to investigate the crystal growth onto synthetic hydroxyapatite (HA) seeds in pH 4.3 and pH 7.0 supersaturated solutions with different fluoride concentrations. Materials and Methods: 8 groups of pH 4.3 and 7.0 calcium phosphate supersaturated solutions were prepared with different fluoride concentrations (0, 1, 2 and 4 ppm). Calcium phosphate precipitates yield crystal growth onto the HA seed surface while solutions flow. For evaluation of crystallizing process, the changes of , , concentrations of the inlet and outlet solutions were determined. The recovered solid samples were weighed to assess the amount of minerals precipitated, and finally determined their composition to deduce characteristics of crystals. Results: During the seeded crystal growth, there were significantly more consumption of , , in pH 4.3 solutions than pH 7.0 (p , , consumption in experimental solutions, weight increment of HA seed, and fluoride ratio in crystallized samples were increased. There were significant differences among the groups (p
目的:研究合成羟基磷灰石(HA)种子在pH 4.3和pH 7.0两种不同氟浓度的过饱和溶液中晶体的生长情况。材料与方法:制备了8组pH为4.3和7.0的磷酸钙过饱和溶液,氟浓度分别为0、1、2和4 ppm。当溶液流动时,磷酸钙沉淀在透明质酸种子表面生成晶体生长。为了评价结晶过程,测定了进口和出口溶液浓度的变化。对回收的固体样品进行称重,以评估沉淀的矿物数量,并最终确定它们的组成,以推断晶体的特征。结果:在种子晶体生长过程中,pH值为4.3的溶液比pH值为7.0的溶液消耗明显增加(p,),实验溶液消耗增加,HA种子增重增加,结晶样品含氟比增加。两组间差异有统计学意义(p
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引用次数: 1
Coronal microleakage of four temporary restorative materials in Class II-type endodontic access preparations 四种临时修复材料在ⅱ类根管通路预备物中的冠状微渗漏
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.29
Sang-Mi Yun, L. Karanxha, Hee-Jin Kim, Sung-Ho Jung, Sujung Park, K. Min
Objectives: The purpose of this study was to evaluate the microleakage of 4 temporary materials in teeth with Class II-type endodontic access preparations by using a glucose penetration model. Materials and Methods: Glucose reaction test was performed to rule out the presence of any reaction between glucose and temporary material. Class II-type endodontic access preparations were made in extracted human premolars with a single root (n = 10). Each experimental group was restored with Caviton (GC), Spacer (Vericom), IRM (Dentsply-Caulk), or Fuji II(GC). Microleakage of four materials used as temporary restorative materials was evaluated by using a glucose penetration model. Data were analyzed by the one-way analysis of variance followed by a multiplecomparison Tukey test. The interface between materials and tooth were examined under a scanning electron microscope (SEM). Results: There was no significant reaction between glucose and temporary materials used in this study. Microleakage was significantly lower for Caviton and Spacer than for Fuji II and IRM. SEM observation showed more intimate adaptation of tooth-restoration interfaces in Caviton and Spacer than in IRM and Fuji II. Conclusions: Compared to IRM and Fuji II, Caviton and Spacer can be considered better temporary sealing materials in Class II-type endodontic access cavities.
目的:采用葡萄糖渗透模型,评价ⅱ类根管通路制剂中4种临时材料的微渗漏情况。材料和方法:进行葡萄糖反应试验,以排除葡萄糖与临时材料之间的任何反应。用拔除的单根前磨牙(n = 10)制备ⅱ类根管通路制剂。各实验组分别采用Caviton (GC)、Spacer (Vericom)、IRM (Dentsply-Caulk)或Fuji II(GC)进行修复。采用葡萄糖渗透模型对四种临时修复材料进行微渗漏评价。数据分析采用单因素方差分析和多因素比较Tukey检验。在扫描电子显微镜下观察了材料与牙齿的界面。结果:葡萄糖与本研究中使用的临时材料之间无明显反应。Caviton和Spacer的微泄漏明显低于富士II和IRM。扫描电镜观察表明,与IRM和Fuji II相比,Caviton和Spacer的修复界面适应性更强。结论:与IRM和Fuji II相比,Caviton和Spacer可以被认为是更好的II类根管通道临时密封材料。
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引用次数: 4
Effects of canal enlargement and irrigation needle depth on the cleaning of the root canal system at 3 mm from the apex 根管扩大和灌洗针深度对离根尖3mm处根管系统清洁的影响
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.24
Ho-Jin Moon, C. Hong
Objectives: The aim of this study was to test the hypothesis, that the effectiveness of irrigation in removing smear layer in the apical third of root canal system is dependent on the depth of placement of the irrigation needle into the root canal and the enlargement size of the canal. Materials and Methods: Eighty sound human lower incisors were divided into eight groups according to the enlargement size (#25, #30, #35 and #40) and the needle penetration depth (3 mm from working length, WL-3 mm and 9 mm from working length, WL-9 mm). Each canal was enlarged to working length with Profile.06 Rotary Ni-Ti files and irrigated with 5.25% NaOCl. Then, each canal received a final irrigation with 3 mL of 3% EDTA for 4 min, followed by 5 mL of 5.25% NaOCl at different level (WL-3 mm and WL-9 mm) from working length. Each specimen was prepared for the scanning electron microscope (SEM). Photographs of the 3mm area from the apical constriction of each canal with a magnification of , , , were taken for the final evaluation. Results: Removal of smear layer in WL-3 mm group showed a significantly different effect when the canal was enlarged to larger than #30. There was a significant difference in removing apical smear layer between the needle penetration depth of WL-3 mm and WL-9 mm. Conclusions: Removal of smear layer from the apical portion of root canals was effectively accomplished with apical instrumentation to #35/40 06 taper file and 3 mm needle penetration from the working length.
目的:本研究的目的是验证一个假设,即灌溉去除根管系统根尖三分之一涂抹层的有效性取决于灌溉针在根管中放置的深度和根管的扩大程度。材料与方法:将80个健全的人下切牙按放大尺寸(25、30、35、40)和入针深度(距工作长度3 mm, WL-3 mm和距工作长度9 mm, WL-9 mm)分为8组。采用Profile.06旋转镍钛锉将各管扩大至工作长度,并用5.25%的NaOCl灌水。然后,每根管最后用3 mL 3% EDTA冲洗4分钟,然后用5 mL 5.25% NaOCl按工作长度不同的水平(WL-3 mm和WL-9 mm)冲洗。每个样品都准备好进行扫描电子显微镜(SEM)。从每根根管的根尖狭窄处取3mm的照片,放大倍数为,,用于最后的评估。结果:当根管扩大到30 #以上时,WL-3 mm组去除涂抹层的效果有显著差异。针入深度WL-3 mm与WL-9 mm去除根尖涂抹层差异有统计学意义。结论:根尖预备至#35/40 06锥形锉,根管针尖距工作长度3mm,有效地完成了根管根尖部分涂片层的去除。
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引用次数: 1
Effects of matrix metallproteinases on dentin bonding and strategies to increase durability of dentin adhesion 基质金属蛋白酶对牙本质结合的影响及提高牙本质粘附持久性的策略
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.2
Jung-Hyun Lee, Juhea Chang, H. Son
The limited durability of resin-dentin bonds severely compromises the longevity of composite resin restorations. Resin-dentin bond degradation might occur via degradation of water-rich and resin sparse collagen matrices by host-derived matrix metalloproteinases (MMPs). This review article provides overview of current knowledge of the role of MMPs in dentin matrix degradation and four experimental strategies for extending the longevity of resin-dentin bonds. They include: (1) the use of broadspectrum inhibitors of MMPs, (2) the use of cross-linking agents for silencing the activities of MMPs, (3) ethanol wet-bonding with hydrophobic resin, (4) biomimetic remineralization of water-filled collagen matrix. A combination of these strategies will be able to overcome the limitations in resin-dentin adhesion.
树脂-牙本质结合的有限耐久性严重影响了复合树脂修复体的使用寿命。宿主来源的基质金属蛋白酶(MMPs)可能通过降解富水和树脂稀疏的胶原基质来降解树脂-牙本质键。这篇综述文章概述了MMPs在牙本质基质降解中的作用,以及延长树脂-牙本质键寿命的四种实验策略。它们包括:(1)MMPs的广谱抑制剂的使用,(2)使用交联剂沉默MMPs的活性,(3)乙醇与疏水性树脂的湿键,(4)充满水的胶原基质的仿生再矿化。这些策略的结合将能够克服树脂-牙本质粘连的局限性。
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引用次数: 0
Pulp necrosis following luxated injury to teeth in a patient with uncontrolled type II diabetes mellitus: a case report 2型糖尿病患者脱位后牙髓坏死1例报告
Pub Date : 2012-03-01 DOI: 10.5395/RDE.2012.37.1.61
Haneol Shin, Seung‐Jong Lee, I. Jung, Chan-Young Lee
Patients with diabetes mellitus show delayed wound healing and increased susceptibility to infection. Therefore, the effects of diabetes on pulpal and periodontal healing should be taken into consideration when treating diabetic dental traumatized patients. This case presents the treatment for dental traumatized 20 yr old female with uncontrolled type II diabetes. The traumatized upper central incisors had showed pulpal healing in early days. However, 7 mon after the trauma, the teeth had been diagnosed with pulp necrosis with apical abscess. Eventually, non surgical root canal treatment on the teeth had been performed.
糖尿病患者表现为伤口愈合延迟和感染易感性增加。因此,在治疗糖尿病牙外伤患者时,应考虑糖尿病对牙髓和牙周愈合的影响。本病例介绍20岁女性二型糖尿病患者牙外伤的治疗方法。创伤的上中切牙早期表现出牙髓愈合。然而,创伤后7个月,被诊断为牙髓坏死并根尖脓肿。最终,对牙齿进行了非手术根管治疗。
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引用次数: 0
期刊
Restorative Dentistry and Endodontics
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