Pub Date : 2024-04-25DOI: 10.1088/2051-672x/ad3fd0
Bingkui Wang, Renhuan Luo, Zhanhua Yang, Xiaoyu Zhou, Wang Li, Jiacheng Li, Qiankun Wei, Jun Chen, Guowang Wei, Jiubing Zhang, Zhongmin Wang and Weijiang Gan
A hydrophobic coating containing modified iron oxides was prepared for corrosion protection of aluminum alloy. The modified iron oxide particles were synthesized using the annealing method and the evaluation of the corrosion-resistant benefits of modified iron oxides as additive in the epoxy resin coating was conducted. The raw FeOOH phase can be transformed into the α-Fe2O3 phase by increasing the annealing temperature. The morphology, colors, and pore size of the modified iron oxide are controllably evolved via finely adjusting the annealing temperature, which is beneficial for the compatibility, dispersion, and stability with epoxy resin. Besides, modified α-Fe2O3 annealed at 700 °C exhibited elliptical morphology and good solubility in epoxy resin solvents to form a hydrophobic corrosion inhibition layer (TP700), which further improves the corrosion resistance. Findings of corrosion electrochemical measurements and salt spray test confirmed the existence of TP700 composite coating resulted in the best corrosion protective properties on aluminum alloy during the corrosion process with the minimum corrosion current of 7.75 × 10−10 A cm−2 and the maximum |Z|0.01Hz value of 1.80 × 108 Ω cm2, which both are about two orders of magnitude higher than the commercial Fe2O3. Our results suggest a new venue for preparing modified iron oxide pigment on the surface of aluminum alloy materials for enhanced anti-corrosion applications.
{"title":"Synthesis and characterization of modified iron oxide hydrophobic corrosion-resistant pigment for aluminum alloy coating","authors":"Bingkui Wang, Renhuan Luo, Zhanhua Yang, Xiaoyu Zhou, Wang Li, Jiacheng Li, Qiankun Wei, Jun Chen, Guowang Wei, Jiubing Zhang, Zhongmin Wang and Weijiang Gan","doi":"10.1088/2051-672x/ad3fd0","DOIUrl":"https://doi.org/10.1088/2051-672x/ad3fd0","url":null,"abstract":"A hydrophobic coating containing modified iron oxides was prepared for corrosion protection of aluminum alloy. The modified iron oxide particles were synthesized using the annealing method and the evaluation of the corrosion-resistant benefits of modified iron oxides as additive in the epoxy resin coating was conducted. The raw FeOOH phase can be transformed into the α-Fe2O3 phase by increasing the annealing temperature. The morphology, colors, and pore size of the modified iron oxide are controllably evolved via finely adjusting the annealing temperature, which is beneficial for the compatibility, dispersion, and stability with epoxy resin. Besides, modified α-Fe2O3 annealed at 700 °C exhibited elliptical morphology and good solubility in epoxy resin solvents to form a hydrophobic corrosion inhibition layer (TP700), which further improves the corrosion resistance. Findings of corrosion electrochemical measurements and salt spray test confirmed the existence of TP700 composite coating resulted in the best corrosion protective properties on aluminum alloy during the corrosion process with the minimum corrosion current of 7.75 × 10−10 A cm−2 and the maximum |Z|0.01Hz value of 1.80 × 108 Ω cm2, which both are about two orders of magnitude higher than the commercial Fe2O3. Our results suggest a new venue for preparing modified iron oxide pigment on the surface of aluminum alloy materials for enhanced anti-corrosion applications.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"28 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-04-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140803841","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-12DOI: 10.1088/2051-672x/ad3a82
Umesh Marathe, Jayashree Bijwe
This study encompasses the development of sandwich-structured adhesive reporting the synergism in the functioning of two kinds of nanoparticles (NPs)-SiC (Silicon carbide) and MWCNTs (multiwalled carbon nanotubes). Two adhesives using MWCNTs and NPs of SiC in selected amounts were developed using Polyaryletherketone (PAEK) thermoplastic polymer as a base matrix. Fabricated joints using these adhesives were characterized for degglomeration and dispersion of NPs, lap shear strength (LSS), and failure modes. Based on the data on the LSS, the advantages and disadvantages of using individual NPs were analyzed, and the third adhesive was designed in a sandwich manner, where positive points of both the NPs were expected to work synergistically. The sandwich adhesive showed higher LSS than the individual ones, i.e., an 8.6% and 26% improvement to SiC-based and MWCNT-based adhesives, respectively. It was concluded that the strengthening mechanism of MWCNTs of bulk polymer in the central portion was beneficial. The two outer layers of SiC NPs in PAEK interacting with the two steel surfaces of coupons proved helpful in increasing friction and, hence, synergistically increasing the LSS of sandwich adhesive.
{"title":"Sandwich-structured nano-adhesive based on the synergistic action of two nanoparticles (SiC and MWCNTs)","authors":"Umesh Marathe, Jayashree Bijwe","doi":"10.1088/2051-672x/ad3a82","DOIUrl":"https://doi.org/10.1088/2051-672x/ad3a82","url":null,"abstract":"This study encompasses the development of sandwich-structured adhesive reporting the synergism in the functioning of two kinds of nanoparticles (NPs)-SiC (Silicon carbide) and MWCNTs (multiwalled carbon nanotubes). Two adhesives using MWCNTs and NPs of SiC in selected amounts were developed using Polyaryletherketone (PAEK) thermoplastic polymer as a base matrix. Fabricated joints using these adhesives were characterized for degglomeration and dispersion of NPs, lap shear strength (LSS), and failure modes. Based on the data on the LSS, the advantages and disadvantages of using individual NPs were analyzed, and the third adhesive was designed in a sandwich manner, where positive points of both the NPs were expected to work synergistically. The sandwich adhesive showed higher LSS than the individual ones, i.e., an 8.6% and 26% improvement to SiC-based and MWCNT-based adhesives, respectively. It was concluded that the strengthening mechanism of MWCNTs of bulk polymer in the central portion was beneficial. The two outer layers of SiC NPs in PAEK interacting with the two steel surfaces of coupons proved helpful in increasing friction and, hence, synergistically increasing the LSS of sandwich adhesive.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"100 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-04-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140617280","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-26DOI: 10.1088/2051-672x/ad2ec0
Edilson N Pollnow, Frantchescole B Cardoso, Ederson B das Neves, Rodrigo B Santos, Alice G Osorio
Owing to the global shortage of raw materials and an increase in their prices, there is a growing demand for engineering solutions to increase the lifespan and durability of equipment and components. Therefore, this study aims to combine surface engineering and welding engineering to produce a niobium-rich coating using submerged arc welding (SAW) deposition. SAW is a cost-effective technique that allows high deposition rates and technical simplicity, which can enhance mechanical properties and resistance to abrasive wear of components. This research involves the addition of a FeNbC powder alloy in percentages of 5, 10, and 15 wt% to a neutral commercial SAW flux, as an alternative to adding Nb to the microstructure of the deposited coating. The coating was characterized by optical microscopy to analyze the microstructure, such as the presence of phases; microhardness through a Vickers micro-durometer, and resistance to abrasive wear through the loss of mass using a rubber wheel-type abrasometer. The wear mechanisms were evaluated using scanning electron microscopy. The results showed that a Nb-rich coating can be deposited via SAW, and the coatings successfully increased microhardness by up to 110% and resistance to abrasive wear to values higher than the base metal used (microalloyed steel). The microstructure formed was rich in Fe2Nb and NbC, proving the formation of Nb-rich phases. Additionally, the mechanism of abrasive wear was predominantly plastic for the base metal and changed to micro-cutting and micro-plowing after the addition of up to 15% of FeNbC.
{"title":"Impact of incorporating FeNbC into weld flux on the abrasive wear resistance of coatings produced by SAW in a microalloyed steel","authors":"Edilson N Pollnow, Frantchescole B Cardoso, Ederson B das Neves, Rodrigo B Santos, Alice G Osorio","doi":"10.1088/2051-672x/ad2ec0","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2ec0","url":null,"abstract":"Owing to the global shortage of raw materials and an increase in their prices, there is a growing demand for engineering solutions to increase the lifespan and durability of equipment and components. Therefore, this study aims to combine surface engineering and welding engineering to produce a niobium-rich coating using submerged arc welding (SAW) deposition. SAW is a cost-effective technique that allows high deposition rates and technical simplicity, which can enhance mechanical properties and resistance to abrasive wear of components. This research involves the addition of a FeNbC powder alloy in percentages of 5, 10, and 15 wt% to a neutral commercial SAW flux, as an alternative to adding Nb to the microstructure of the deposited coating. The coating was characterized by optical microscopy to analyze the microstructure, such as the presence of phases; microhardness through a Vickers micro-durometer, and resistance to abrasive wear through the loss of mass using a rubber wheel-type abrasometer. The wear mechanisms were evaluated using scanning electron microscopy. The results showed that a Nb-rich coating can be deposited via SAW, and the coatings successfully increased microhardness by up to 110% and resistance to abrasive wear to values higher than the base metal used (microalloyed steel). The microstructure formed was rich in Fe<sub>2</sub>Nb and NbC, proving the formation of Nb-rich phases. Additionally, the mechanism of abrasive wear was predominantly plastic for the base metal and changed to micro-cutting and micro-plowing after the addition of up to 15% of FeNbC.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"48 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140313000","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-21DOI: 10.1088/2051-672x/ad2ebe
P A Radi, L Vieira, P Leite, V J Trava-Airoldi, M Massi, D A P Reis
Metals and their alloys are very important for orthopedic applications, and the basic requirements for a successful implant are chemical stability, mechanical behavior, and biocompatibility in body fluids and tissues. For prosthesis applications, the corrosion resistance of metals is one of the major prerequisites to avoid impairment of the material properties due to degradation. The combined action of corrosion and wear on the material is called tribocorrosion and DLC (Diamond-Like Carbon) films have been extensively studied to increase prosthesis biocompatibility and to protect from corrosion. Additionally, DLC coatings can prevent the prosthesis to release toxic elements due to plastic deformation and corrosion. This paper is about tribocorrosion studies on DLC and DLC-Ag (DLC containing silver nanoparticles) on Ti-6Al-4V substrates. These films were obtained by PECVD (Plasma Enhanced Chemical Vapor Deposition) using hexane as a precursor. The tribocorrosion behavior of uncoated and coated samples was investigated in the reciprocating mode in Ringer’s lactate solution. From the polarization test results, the protective efficiency of the film was calculated. Silver nanoparticles improved the corrosion resistance of the films. The protective efficiency was 15 and 19% for DLC and DLC-Ag films, respectively.
{"title":"Tribocorrosion studies on DLC films with silver nanoparticles for prosthesis applications","authors":"P A Radi, L Vieira, P Leite, V J Trava-Airoldi, M Massi, D A P Reis","doi":"10.1088/2051-672x/ad2ebe","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2ebe","url":null,"abstract":"Metals and their alloys are very important for orthopedic applications, and the basic requirements for a successful implant are chemical stability, mechanical behavior, and biocompatibility in body fluids and tissues. For prosthesis applications, the corrosion resistance of metals is one of the major prerequisites to avoid impairment of the material properties due to degradation. The combined action of corrosion and wear on the material is called tribocorrosion and DLC (Diamond-Like Carbon) films have been extensively studied to increase prosthesis biocompatibility and to protect from corrosion. Additionally, DLC coatings can prevent the prosthesis to release toxic elements due to plastic deformation and corrosion. This paper is about tribocorrosion studies on DLC and DLC-Ag (DLC containing silver nanoparticles) on Ti-6Al-4V substrates. These films were obtained by PECVD (Plasma Enhanced Chemical Vapor Deposition) using hexane as a precursor. The tribocorrosion behavior of uncoated and coated samples was investigated in the reciprocating mode in Ringer’s lactate solution. From the polarization test results, the protective efficiency of the film was calculated. Silver nanoparticles improved the corrosion resistance of the films. The protective efficiency was 15 and 19% for DLC and DLC-Ag films, respectively.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"144 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312643","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-20DOI: 10.1088/2051-672x/ad31b4
Lunye Sun, Shanliang Shi, Zhenxing Li, Kamlakar P Rajurkar, Yonggang Hou, Peng Hai, Zhaofu Chu, Xianguo Li
Rare-earth gadolinium (Gd) is preferable for manufacturing regenerators of the core components of room-temperature magnetic refrigeration owing to its unique magnetocaloric and mechanical properties. However, the surface quality of the regenerator plays a crucial role in the heat transfer effect and service life of magnetocaloric systems during wire electrical discharge machining (WEDM) when fabricating rare-earth Gd array microstructure regenerators. In this study, different process parameters were used to conduct a process experiment of the WEDM of rare-earth Gd. First, the evolution of the surface microstructure and its causes were analyzed using a single-factor experiment, while a corrosion test was conducted on the samples. The analysis showed that the pulse-on time and open voltage considerably affected the surface quality of the processed samples, while the samples with better surfaces exhibited good corrosion resistance. Additionally, a Taguchi experiment was designed, and a regression analysis used to establish regression models between the process parameters (pulse-on time, pulse-off time, peak current, open voltage, and water pressure) and both surface roughness (SR) and material removal rate (MRR). The results showed that the average prediction errors of SR and MRR were only 5.34% and 5.48%, respectively.
{"title":"Research on microstructure evolution and surface quality of WEDM for magnetic refrigerant rare-earth gadolinium","authors":"Lunye Sun, Shanliang Shi, Zhenxing Li, Kamlakar P Rajurkar, Yonggang Hou, Peng Hai, Zhaofu Chu, Xianguo Li","doi":"10.1088/2051-672x/ad31b4","DOIUrl":"https://doi.org/10.1088/2051-672x/ad31b4","url":null,"abstract":"Rare-earth gadolinium (Gd) is preferable for manufacturing regenerators of the core components of room-temperature magnetic refrigeration owing to its unique magnetocaloric and mechanical properties. However, the surface quality of the regenerator plays a crucial role in the heat transfer effect and service life of magnetocaloric systems during wire electrical discharge machining (WEDM) when fabricating rare-earth Gd array microstructure regenerators. In this study, different process parameters were used to conduct a process experiment of the WEDM of rare-earth Gd. First, the evolution of the surface microstructure and its causes were analyzed using a single-factor experiment, while a corrosion test was conducted on the samples. The analysis showed that the pulse-on time and open voltage considerably affected the surface quality of the processed samples, while the samples with better surfaces exhibited good corrosion resistance. Additionally, a Taguchi experiment was designed, and a regression analysis used to establish regression models between the process parameters (pulse-on time, pulse-off time, peak current, open voltage, and water pressure) and both surface roughness (SR) and material removal rate (MRR). The results showed that the average prediction errors of SR and MRR were only 5.34% and 5.48%, respectively.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"34 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312790","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-08DOI: 10.1088/2051-672x/ad2ebf
Z A Zakletskii, Namik Gusein-Zade, A A Sorokin
In this paper, a procedure for estimating local fractal dimensionality values for greyscale images was developed. This procedure was tested on synthesised fractal and multifractal Brownian surfaces. The use of the method of detrended fluctuation analysis to determine the Hurst index for samples with a size not exceeding 2000 points was analysed. The optimal values of the sample size and the scale parameter have been obtained, allowing the Hurst index to be calculated with an error of less than 20%. The procedure was also tested on greyscale images, which are 8-bit representations of a synthesised fractal surface. The peculiarities of the application of the procedure for calculating the local fractal dimension for images obtained by scanning electron microscopy have been analysed. The values of the local fractal dimension of the oxide support MgAl2O4 are calculated using SEM images at different magnifications. It has been shown that, taking into account the fractal dimensionality calculation, different morphologies of the particle surface are observed at different scales of image magnification. At the highest magnification, the particle surface is found to consist of embedded smooth micron particles. The surface morphology of the MgAl2O4 particle depends on the micro- and mesopores between the embedded particles, this surface can be characterised by a fractal surface with FD2 = 2.3–2.4.
{"title":"Determination of local fractal dimension of the catalyst support MgAl2O4 surface","authors":"Z A Zakletskii, Namik Gusein-Zade, A A Sorokin","doi":"10.1088/2051-672x/ad2ebf","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2ebf","url":null,"abstract":"In this paper, a procedure for estimating local fractal dimensionality values for greyscale images was developed. This procedure was tested on synthesised fractal and multifractal Brownian surfaces. The use of the method of detrended fluctuation analysis to determine the Hurst index for samples with a size not exceeding 2000 points was analysed. The optimal values of the sample size and the scale parameter have been obtained, allowing the Hurst index to be calculated with an error of less than 20%. The procedure was also tested on greyscale images, which are 8-bit representations of a synthesised fractal surface. The peculiarities of the application of the procedure for calculating the local fractal dimension for images obtained by scanning electron microscopy have been analysed. The values of the local fractal dimension of the oxide support MgAl<sub>2</sub>O<sub>4</sub> are calculated using SEM images at different magnifications. It has been shown that, taking into account the fractal dimensionality calculation, different morphologies of the particle surface are observed at different scales of image magnification. At the highest magnification, the particle surface is found to consist of embedded smooth micron particles. The surface morphology of the MgAl<sub>2</sub>O<sub>4</sub> particle depends on the micro- and mesopores between the embedded particles, this surface can be characterised by a fractal surface with FD<sub>2</sub> = 2.3–2.4.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"23 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312783","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-06DOI: 10.1088/2051-672x/ad2cb4
Mingxin Tan, Jin Cai, Jinglong Qu, Xingfei Xie, Shaomin Lv
This paper investigates the effects of ultrasonic shot peening (USP) on surface morphology, microstructure, and residual stress field distribution of TC17 alloy under different process parameters. The aim is to reveal the surface strengthening mechanism of TC17 alloy caused by USP. The results suggest that the use of the 2.5 mm projectile diameter leads to an increase in surface roughness, plastic deformation, and a deeper grain refinement layer compared to the 1.5 mm projectile diameter. Additionally, it results in a greater depth of the compressive residual stress layer and maximum compressive residual stress. The crack initiation sites under two projectile diameters are located below the compressive residual stress layer. The USP treatment introduces compressive residual stress on the surface, inhibiting the initiation of surface cracks, and the deeper compressive residual stress layer offsets the early fatigue failure caused by higher roughness.
{"title":"Effect of surface strengthening by ultrasonic shot peening on TC17 alloy","authors":"Mingxin Tan, Jin Cai, Jinglong Qu, Xingfei Xie, Shaomin Lv","doi":"10.1088/2051-672x/ad2cb4","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2cb4","url":null,"abstract":"This paper investigates the effects of ultrasonic shot peening (USP) on surface morphology, microstructure, and residual stress field distribution of TC17 alloy under different process parameters. The aim is to reveal the surface strengthening mechanism of TC17 alloy caused by USP. The results suggest that the use of the 2.5 mm projectile diameter leads to an increase in surface roughness, plastic deformation, and a deeper grain refinement layer compared to the 1.5 mm projectile diameter. Additionally, it results in a greater depth of the compressive residual stress layer and maximum compressive residual stress. The crack initiation sites under two projectile diameters are located below the compressive residual stress layer. The USP treatment introduces compressive residual stress on the surface, inhibiting the initiation of surface cracks, and the deeper compressive residual stress layer offsets the early fatigue failure caused by higher roughness.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"35 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312781","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-01DOI: 10.1088/2051-672x/ad2ba0
A Keksel, B Eli, M Eifler, J Seewig
Fitting standard geometric elements into measurement data using Least-Squares techniques is a common task in signal processing across various technical applications. However, the application of these well-established but purely data-based methods does not consider potentially available prior knowledge about the measurand of interest or the measuring device. Thus, up to this day, additional information is usually left unused beyond a few academic applications. By applying a Bayesian approach, this prior knowledge can be incorporated into the fitting task, potentially leading to a reduction in overall uncertainty and fragility of the evaluation result. In this study, Bayesian models are proposed for incorporating prior knowledge into circular, linear, and ellipse fitting tasks. The general approaches as well as specific results are compared to the established Total-Least-Squares method within the example of the application of the F-operator in surface texture measurement illustrating the practical benefits of the approach.
使用最小二乘技术将标准几何元素拟合到测量数据中，是各种技术应用中信号处理的常见任务。然而，在应用这些成熟但纯粹基于数据的方法时，并没有考虑到有关测量对象或测量设备的潜在可用先验知识。因此，时至今日，除了少数学术应用外，额外的信息通常都被闲置。通过应用贝叶斯方法，可以将这些先验知识纳入拟合任务中，从而降低整体不确定性和评估结果的脆弱性。本研究提出了将先验知识纳入圆形、线形和椭圆拟合任务的贝叶斯模型。在表面纹理测量中应用 F 操作器的例子中，将一般方法和具体结果与既定的总最小二乘法进行了比较，以说明该方法的实际优势。
{"title":"Bayesian analysis of uncertainties in circle, straight-line and ellipse fitting considering a-priori knowledge − comparative analysis with total-least-squares approaches","authors":"A Keksel, B Eli, M Eifler, J Seewig","doi":"10.1088/2051-672x/ad2ba0","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2ba0","url":null,"abstract":"Fitting standard geometric elements into measurement data using Least-Squares techniques is a common task in signal processing across various technical applications. However, the application of these well-established but purely data-based methods does not consider potentially available prior knowledge about the measurand of interest or the measuring device. Thus, up to this day, additional information is usually left unused beyond a few academic applications. By applying a Bayesian approach, this prior knowledge can be incorporated into the fitting task, potentially leading to a reduction in overall uncertainty and fragility of the evaluation result. In this study, Bayesian models are proposed for incorporating prior knowledge into circular, linear, and ellipse fitting tasks. The general approaches as well as specific results are compared to the established Total-Least-Squares method within the example of the application of the F-operator in surface texture measurement illustrating the practical benefits of the approach.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"13 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312651","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-01DOI: 10.1088/2051-672x/ad2c33
Dorothee Hüser, Rudolf Meeß, Gaoliang Dai, André Felgner, Kai Hahm, Stefan Verhülsdonk, Carsten Feist, Sai Gao
In optical surface metrology, it is crucial to assess the fidelity of the topography measuring signals. One parameter to quantify this is the small-scale fidelity limit TFIL defined in ISO 25 178-600:2019. To determine this parameter, sinusoidal structures are generated, where the wavelengths are modulated according to a discrete chirp series. The objects are produced by means of ultra-precision diamond face turning. Planar areas and regions with slopes below 4° could be produced with form deviations of ≲10 nm. An initial estimate of the cutting tool’s nose radius resulted in a deviation that caused the ridges of the structures to be too narrow by approximately 150 nm, while the trenches were too wide. At the bottom of narrow trenches, deviations are observed in the form of elevations with heights of about 20 to 100 nm. The measurement standard investigated in this study has also been used to characterise optical instruments in a round-robin test within the European project TracOptic, which requires precise knowledge of the geometry of all structures. The geometry of the topography, cosine structures superimposed with form deviations, was measured using the Met. LR-AFM metrological long-range atomic force microscope of the German National Metrology Institute.
{"title":"Precision of diamond turning sinusoidal structures as measurement standards used to assess topography fidelity","authors":"Dorothee Hüser, Rudolf Meeß, Gaoliang Dai, André Felgner, Kai Hahm, Stefan Verhülsdonk, Carsten Feist, Sai Gao","doi":"10.1088/2051-672x/ad2c33","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2c33","url":null,"abstract":"In optical surface metrology, it is crucial to assess the fidelity of the topography measuring signals. One parameter to quantify this is the <italic toggle=\"yes\">small-scale fidelity limit T</italic>\u0000<sub>FIL</sub> defined in ISO 25 178-600:2019. To determine this parameter, sinusoidal structures are generated, where the wavelengths are modulated according to a discrete chirp series. The objects are produced by means of ultra-precision diamond face turning. Planar areas and regions with slopes below 4° could be produced with form deviations of ≲10 nm. An initial estimate of the cutting tool’s nose radius resulted in a deviation that caused the ridges of the structures to be too narrow by approximately 150 nm, while the trenches were too wide. At the bottom of narrow trenches, deviations are observed in the form of elevations with heights of about 20 to 100 nm. The measurement standard investigated in this study has also been used to characterise optical instruments in a round-robin test within the European project TracOptic, which requires precise knowledge of the geometry of all structures. The geometry of the topography, cosine structures superimposed with form deviations, was measured using the Met. LR-AFM metrological long-range atomic force microscope of the German National Metrology Institute.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"47 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312652","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-03-01DOI: 10.1088/2051-672x/ad2af3
Luis Miguel Ballesteros, David Cano, Camilo Andrés García, Laura Vanessa Giraldo, Luis Felipe Jiménez, Esteban Rave, J S Rudas, Cesar A Isaza M, Alejandro Toro
Patterned surfaces can be designed and engineered to control friction and wear resistance in various applications. In the present work, a comparative analysis of two contrasting manufacturing processes for surface texturing of polyamide, namely 3D printing by fused filament fabrication (FFF) and CNC micromachining (micro CNC) as additive and subtractive manufacturing techniques respectively was carried out. The analysis included the evaluation of the topography, roughness, mechanical properties, and tribological performance of the texturized surfaces. Both manufacturing routes were suitable for fabricating deterministic surfaces, being the micro CNC method the one that provided better repeatability and surface finishing as well as higher hardness. These factors influenced the tribological behavior of the polyamide when in contact with AISI 304 stainless steel. The effects of size, distribution and height of the texture elements and the manufacturing technique on the Coefficient of Friction (COF) were also discussed.
{"title":"Comparison of textured nylon surfaces manufactured by CNC micromachining and 3D printing","authors":"Luis Miguel Ballesteros, David Cano, Camilo Andrés García, Laura Vanessa Giraldo, Luis Felipe Jiménez, Esteban Rave, J S Rudas, Cesar A Isaza M, Alejandro Toro","doi":"10.1088/2051-672x/ad2af3","DOIUrl":"https://doi.org/10.1088/2051-672x/ad2af3","url":null,"abstract":"Patterned surfaces can be designed and engineered to control friction and wear resistance in various applications. In the present work, a comparative analysis of two contrasting manufacturing processes for surface texturing of polyamide, namely 3D printing by fused filament fabrication (FFF) and CNC micromachining (micro CNC) as additive and subtractive manufacturing techniques respectively was carried out. The analysis included the evaluation of the topography, roughness, mechanical properties, and tribological performance of the texturized surfaces. Both manufacturing routes were suitable for fabricating deterministic surfaces, being the micro CNC method the one that provided better repeatability and surface finishing as well as higher hardness. These factors influenced the tribological behavior of the polyamide when in contact with AISI 304 stainless steel. The effects of size, distribution and height of the texture elements and the manufacturing technique on the Coefficient of Friction (COF) were also discussed.","PeriodicalId":22028,"journal":{"name":"Surface Topography: Metrology and Properties","volume":"51 1","pages":""},"PeriodicalIF":2.7,"publicationDate":"2024-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140312650","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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