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Synthesis and Chraracterization of Tin Sulfide Nanoparticles 硫化锡纳米颗粒的合成与表征
Pub Date : 2019-07-01 DOI: 10.22232/stj.2019.07.02.13
M. Upadhyay, A. Thakur, Mohan Daimary
In my present paper, Tin sulfide nanoparticles were successfully synthesized using wet chemical process and studied their structural properties. The prepared nanoparticles were characterized by X-Ray diffraction (XRD) and Raman spectroscopy. The XRD confirms the Tin Sulfide nanoparticles possessing orthorhombic structure having particle size is approx. 12.72 nm. The Raman spectrum shows the frequency of the phonon in these nanoparticles and the Raman modes of Tin Sulfide nanoparticles were found to shifts towards lower wave number side.
本文采用湿法合成了硫化锡纳米颗粒,并对其结构性质进行了研究。用x射线衍射(XRD)和拉曼光谱对制备的纳米颗粒进行了表征。XRD证实了硫化锡纳米颗粒具有正交结构,粒径近似。12.72纳米。拉曼光谱显示了这些纳米粒子中声子的频率,并且发现硫化锡纳米粒子的拉曼模式向低波数侧偏移。
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引用次数: 0
Potential of Iron Pillared Clay as Active Nanocatalyst for Rapid Decolorization of Methylene Blue 铁柱粘土作为亚甲基蓝快速脱色活性纳米催化剂的潜力
Pub Date : 2019-07-01 DOI: 10.22232/stj.2019.07.02.05
Lal hmunsiama, Seung-Mok Lee
In this study, the iron-pillared clay nanocatalyst (ICN) was employed as a nanocatalyst for decolorization of methylene blue (MB) in aqueous solutions without hydrogen peroxide. The changes in clay structure after the incorporation of iron-oxide particles was studied with the help of XRD analytical data. The SEM micrographs showed higher heterogeneous structure of ICN compared to pristine clay and the specific surface area of ICN (82.54 m2/g) is considerably higher than the unmodified clay (63.41 m2/g). Further, the EDX analytical data indicate the successful incorporation of iron-oxide into bentonite clay. Batch experiments showed that ICN could degrade MB within pH 3.0 to 11.0 and it is efficient even at higher concentrations. The degradation is very fast and more than 90% is removed within 30 mins. A small amount of ICN is effective for degradation of MB and the reusability test showed that ICN can be reuse for several times for the degradation of MB in aqueous solutions. The effect of scavengers studies indicate that the ·OH radicals generated from the ICN are responsible in the degradation of MB. This study indicates that ICN must be low cost and environmentally friendly active nanocatalyst for degradation of MB present in aquatic environment.
本研究采用铁柱粘土纳米催化剂(ICN)作为纳米催化剂,在无过氧化氢的水溶液中对亚甲基蓝(MB)进行脱色。利用XRD分析数据研究了氧化铁颗粒掺入后粘土结构的变化。SEM显微图显示,ICN的非均质结构高于原始粘土,ICN的比表面积(82.54 m2/g)明显高于未改性粘土(63.41 m2/g)。此外,EDX分析数据表明氧化铁成功掺入膨润土粘土中。批量实验表明,ICN在pH 3.0 ~ 11.0范围内可降解MB,在更高的浓度下也能有效降解MB。降解非常快,30分钟内可去除90%以上。少量ICN对MB的降解是有效的,可重复使用试验表明,ICN可多次重复使用以降解水溶液中的MB。清除剂的作用研究表明,ICN产生的·OH自由基参与了MB的降解,表明ICN必须是一种低成本、环保的活性纳米催化剂才能降解水生环境中的MB。
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引用次数: 0
Smart Automated Farming System using IOT and Solar Panel 使用物联网和太阳能电池板的智能自动化农业系统
Pub Date : 2019-07-01 DOI: 10.22232/stj.2019.07.02.03
Anita Shukla, Ankit Jain
Present work focuses on need of automation in farming by using IOT technology. Automation of farming envisages monitoring and controlling of various parameters which could be helpful in increasing productivity. The proposed system provides a technological solution to the various problems like, maintenance of water requirements, humidity level, maintenance of proper temperature, and proper availability of light for sophisticated plants, fire alert and to keep a check on unwanted entry in the farming lands including timely and sufficient supply of electricity. This hardware provides an effective and efficient solution to the defined problems in Indian farming system by using node MCU Wi-Fi module. Different sensors like humidity sensor, soil moisture sensor, PIR sensor, fire sensor, light sensor and temperature sensor have been used for monitoring and controlling of various problems technologically. In proposed system a Wi-Fi module has been used which automatically informs the farmer about the water requirement, site temperature, humidity and moisture, light, fire alert and about the unwanted occupancy or encroachment by displaying real time data which can be seen and accessed over internet using IOT technology from anywhere in the world. System is equipped with solar panel which provides power backup to the system even in the absence of power supply. We have used five different sensors on three different plants with different environmental conditions and the performances of different sensors are found to be upto the desired expectations.
目前的工作重点是利用物联网技术实现农业自动化的需求。农业自动化设想监测和控制各种参数,这可能有助于提高生产力。拟议的系统为各种问题提供了技术解决方案,如维护水需求,湿度水平,维护适当的温度,为复杂的植物提供适当的照明,火灾警报和检查农田的非法进入,包括及时和充足的电力供应。该硬件通过节点MCU Wi-Fi模块为印度农业系统中定义的问题提供了有效和高效的解决方案。不同的传感器,如湿度传感器、土壤湿度传感器、PIR传感器、火灾传感器、光传感器和温度传感器,已经被用于各种问题的监测和控制技术。在拟议的系统中,使用了Wi-Fi模块,该模块通过显示实时数据自动通知农民有关用水需求,现场温度,湿度和湿度,光线,火灾警报以及不必要的占用或侵占,这些数据可以在世界任何地方使用物联网技术通过互联网看到和访问。系统配备了太阳能电池板,即使在没有电源的情况下也可以为系统提供备用电源。我们在三种不同环境条件下的不同植物上使用了五种不同的传感器,发现不同传感器的性能都达到了预期的水平。
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引用次数: 0
Electrodes for Estimation of Nimesulide Drug using Voltammetry Technique: A Revisit 用伏安法测定尼美舒利药物的电极:回顾
Pub Date : 2019-07-01 DOI: 10.22232/stj.2019.07.02.08
Abhik Chatterjee
Nimesulide is a pain-killer and falls in the category of non-steroidal anti-inflammatory drug. It can reduce different types of pain. Nimesulide is a safe drug but uncontrolled use of this medicine creates many problems. So detection and estimation of nimesulide is very important. Electro analytical methods are good choice for detection and estimation. Among them, voltammetry is one of the good method in this twenty-first century. In this review, different electrode materials for voltammetric study have been presented with detection limit.
尼美舒利是一种止痛药,属于非甾体类抗炎药。它可以减轻不同类型的疼痛。尼美舒利是一种安全的药物,但不加控制地使用这种药物会产生许多问题。因此尼美舒利的检测和评价具有重要意义。电分析方法是检测和估计的良好选择。其中,伏安法是二十一世纪较好的方法之一。本文综述了用于伏安研究的不同电极材料及其检出限。
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引用次数: 0
Interactive Color Image Segmentation using HSV Color Space 使用HSV色彩空间的交互式彩色图像分割
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.05
D. Hema, Dr. S. Kannan
The primary goal of this research work is to extract only the essential foreground fragments of a color image through segmentation. This technique serves as the foundation for implementing object detection algorithms. The color image can be segmented better in HSV color space model than other color models. An interactive GUI tool is developed in Python and implemented to extract only the foreground from an image by adjusting the values for H (Hue), S (Saturation) and V (Value). The input is an RGB image and the output will be a segmented color image.
本研究的主要目标是通过分割提取彩色图像中必要的前景片段。该技术是实现目标检测算法的基础。HSV色彩空间模型比其他色彩空间模型能更好地分割彩色图像。Python开发了一个交互式GUI工具,通过调整H(色相),S(饱和度)和V(值)的值来实现仅从图像中提取前景。输入是一个RGB图像,输出将是一个分割的彩色图像。
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引用次数: 12
Avian Diversity in Mizoram University Campus, Aizawl, Mizoram 米佐拉姆邦Aizawl米佐拉姆大学校园的鸟类多样性
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.08
L. Sailo, G. Solanki, C. Lalhruaizela
We conducted an avian survey to assess the avian diversity of Mizoram University campus, Aizawl for a period of 24 months. During the study a total of 3,555 no of individuals of 189 species of birds belonging to 43 families were recorded. The family Muscicapidae represented the highest species composition with 28 species followed by family Timaliidae and of MZU campus and its adjacent area, 31 (16.4%) species are winter visitors, 15 (7.9%) species are summer visitor, and two species namely, Hooded pitta (Pitta sordid) and Forest wagtail (Dendronanthus indicus) are passer migrants. The variation calculated was 3.286 and species evenness index was 0.62. The detailed of avian fauna of campus recoded and the need of conservation actions are discussed in length.
本文对米佐拉姆大学艾扎尔校区进行了为期24个月的鸟类多样性调查。研究共记录鸟类43科189种3555只。以蝇科(28种)居多,其次是蝇科(28种)。在清华大学校园及其邻近地区,冬候鸟有31种(16.4%),夏候鸟有15种(7.9%),经候鸟有褐皮鼠(pitta sordid)和林摇尾(Dendronanthus indicus) 2种。变异数为3.286,物种均匀度指数为0.62。详细地讨论了校园鸟类区系的分类和保护措施的必要性。
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引用次数: 4
Impact of Optical Booster to Enhance the Gain Bandwidth for Dense Optical Communication System 光增强器对密集光通信系统增益带宽的影响
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.06
G. Kumar, C. Kumar
This paper explains how the combination of RAMAN and PARA-METRIC amplifier using non-linear fiber components increases the gain bandwidth. Two kinds of configuration of amplifier are demonstrated with gain associated and bit error rate is seen. 15 db gain is measured and flat gain of 5db is measured.
本文阐述了拉曼放大器与参数度量放大器的结合是如何利用非线性光纤元件提高增益带宽的。在增益相关的情况下,演示了两种放大器的配置,并观察了误码率。测量增益为15db,平坦增益为5db。
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引用次数: 1
Common Fixed Point Theorems on Multi-Valued Mappings in 2-Metric Space using T-Hardy Rogers Contraction Condition and F-Contraction 利用T-Hardy Rogers收缩条件和f -收缩的2-度量空间中多值映射的公共不动点定理
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.13
Dinanath Barman, Krishnadhan Sarkar, Kalishankar Tiwary
In this paper we have introduced multi valued 2 matrices on 2 matric space and have prove some fixed point theorems for multi-valued mappings on 2-metric space using T-Hardy and Rogers type contraction condition. We have also used F-contraction conditions, occasionally weakly compatible to prove the theorems.
本文引入了2矩阵空间上的多值2矩阵,利用T-Hardy和Rogers型收缩条件证明了2-度量空间上的多值映射的不动点定理。我们也用偶尔弱相容的f收缩条件来证明定理。
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引用次数: 0
Calorimetric Computation of Enthalpy of Formation of Trisacetylacetonato Chromium(III) [Cr(C5H7O2)3(c)] 三乙酰丙酮铬(III) [Cr(C5H7O2)3(c)]生成焓的量热计算
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.12
M. Pathak, Raghvendu Pathak
From thermochemical studies of organometallic compounds, a host of thermodynamic parameters viz., heat capacity, entropy, Gibbs energy etc., can be evaluated. The present communication deals with the evaluation of enthalpy of combustion and thereby estimation of enthalpy of formation of crystalline trisacetylacetonato chromium(III) [Cr (C5H7O2)3 (c)] or [Cr (acac)3 cH) and enthalpy of formation fH° –1 –1 respectively. Experimental data obtained are in good agreement with one another.
从有机金属化合物的热化学研究,许多热力学参数,即热容,熵,吉布斯能等,可以评估。本文讨论了燃烧焓的计算,从而分别计算了三乙酰丙酮铬(III) [Cr (C5H7O2)3 (c)]或[Cr (acac) 3ch]晶体的生成焓和生成焓fH°-1 -1。得到的实验数据相互吻合良好。
{"title":"Calorimetric Computation of Enthalpy of Formation of Trisacetylacetonato Chromium(III) [Cr(C5H7O2)3(c)]","authors":"M. Pathak, Raghvendu Pathak","doi":"10.22232/stj.2019.07.01.12","DOIUrl":"https://doi.org/10.22232/stj.2019.07.01.12","url":null,"abstract":"From thermochemical studies of organometallic compounds, a host of thermodynamic parameters viz., heat capacity, entropy, Gibbs energy etc., can be evaluated. The present communication deals with the evaluation of enthalpy of combustion and thereby estimation of enthalpy of formation of crystalline trisacetylacetonato chromium(III) [Cr (C5H7O2)3 (c)] or [Cr (acac)3 cH) and enthalpy of formation fH° –1 –1 respectively. Experimental data obtained are in good agreement with one another.","PeriodicalId":22107,"journal":{"name":"Silpakorn University Science and Technology Journal","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2019-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85493183","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
New Taxon of Fungal Endophytes from Phrynium capitatum Willd: A Promising Ethnomedicinal Plant in Northeast India and its Systematic and Phylogenetic Analysis 印度东北部一种有发展前途的民族药用植物——野生头草真菌内生新分类群及其系统发育分析
Pub Date : 2019-01-01 DOI: 10.22232/stj.2019.07.01.04
Richa Sharma, S. Tangjang, A. C. Shukla
The findings of the current study deal with the first time report on the diversity of fungal endophyte from the ethnomedicinal plant- Phrynium capitatum Willd., (Marantaceae). The plant is growing wildly in the forest of Papum Pare, Arunachal Pradesh, India, and traditionally been used for anti-diabetic, antihyperglycemic or analgesic effects. During the investigation, samples of the plant parts, viz., leaves, stem, and roots were collected for isolation of endophytic spp. The endophytic spp were identified based on the morphological, cultural, and reproductive structures (hyaline, ellipsoidal, aseptate, pycnidia, beta conidia, perithecia, asci, and ascospores). Further, the phylogenetic analysis of the isolated species was made, using the sequences of 5.8S and 28S rDNA internal transcribed spacer sequence 1 and 4. The largest number of fungal endophytes (39%) were isolated from the leaves, followed by the roots (31%) and stems (30%). Overall 35 fungal species have been isolated, out of which, thirty-four belongs to the class Ascomycetes, and one from the class zygomycetes. The highest species richness and frequency of colonization were recorded in the leaf. The observations show that Pestalotiopsis longiseta was the most dominant endophytic species followed by Diplodina microsperma, Nodulisporium hinnuleum, Aspergillus flavus , Diaporthe sp., Nigrospora oryzae and Lasiodiplodia viticola. However, Pestalotiopsis neglecta, Sordaria fimicola, Diplodina microsperma, Fusarium incarnatum, Preussia sp., Diaporthe sp., Aureobasidium sp.were common fungal endophytes isolated from P. capitatum
本研究首次报道了民族药用植物头草真菌内生菌的多样性。(竹芋科)。这种植物广泛生长在印度** *的Papum Pare森林中,传统上被用于抗糖尿病、抗高血糖或镇痛作用。在调查过程中,采集植物的叶、茎、根等部分进行内生菌的分离,并根据其形态、培养和繁殖结构(透明状、椭球状、无菌状、柱头、分生孢子、周皮、子囊和子囊孢子)对内生菌进行鉴定。利用5.8S和28S rDNA内转录间隔序列1和4对分离种进行系统发育分析。从叶片中分离到的真菌内生菌最多(39%),其次是根(31%)和茎(30%)。共分离到35种真菌,其中34种属于子囊菌纲,1种属于接合菌纲。物种丰富度和定植频率均以叶片最高。结果表明,长拟盘多毛孢是最优势的内生菌种,其次是小精子双plodina hinnuleum、黄曲霉Aspergillus flavus、Diaporthe sp.、Nigrospora oryzae和Lasiodiplodia viticola。然而,忽略拟盘多毛孢、金缕索菌、小精子双plodina、incarnatum镰刀菌、Preussia sp.、Diaporthe sp.、Aureobasidium sp.是头藤中常见的内生真菌
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引用次数: 1
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Silpakorn University Science and Technology Journal
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