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Fracture Height Quantification from Vertical and Horizontal Section Fiber Measurements: A Comprehensive Study Using LF-DAS Measurements from HFTS-2 Data Set 从垂直和水平断面纤维测量中量化断裂高度:利用 HFTS-2 数据集中的 LF-DAS 测量数据进行综合研究
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219488-pa
Aishwarya Srinivasan, Joseph Mjehovich, K. Wu, G. Jin, Wen Wang, G. Moridis
Understanding fracture height growth is critical for optimizing hydraulic fracture treatments and field development. In recent years, low-frequency distributed acoustic sensing (LF-DAS) has become a popular tool for monitoring strain changes during hydraulic fracturing. While LF-DAS data from vertical monitoring wells (VMWs) can be used to determine fracture height, measurements from the vertical section of horizontal wells may have the potential to capture fracture height growth. The objectives of this study are (1) to apply three methods—(a) using the vertical section of horizontal fiber measurements, (b) using the vertical fiber measurements, and (c) using the horizontal section of horizontal fiber measurements—to determine the fracture height using the Hydraulic Fracturing Test Site 2 (HFTS-2) data set and (2) to demonstrate the reliability of using LF-DAS measurements from the vertical section of horizontal fibers for fracture height determination. In an effort to determine the fracture height from the HFTS-2 data set using the three methods, we demonstrate the reliability of the height prediction using strain measurements in the vertical section of the horizontal monitoring well (VS-HMW). First, we analyze the measurements from the vertical section of the horizontal fiber (B3H) during the stimulation of the heel-most stages of the horizontal wells (B1H, B2H, and B4H). Second, we analyze the measurements from the VMW (B5PH) during the stimulations of B1H, B2H, and B4H. Third, we use a geomechanical inversion algorithm to obtain height estimates from the horizontal section of the LF-DAS measurements at B3H during B1H, B2H, and B4H stimulations. The fracture height is determined based on the transition of the extension-compression zone in the LF-DAS measurements from the vertical sections. The height estimates obtained using the three methods are compared and found to be consistent in the six well pairs we analyzed. The LF-DAS measurements from the vertical well B5PH provide a complete height profile, while measurements from the vertical section capture fracture growth from the upper tip of the fracture to the landing depth of the horizontal well. The fracture height estimates obtained from our inversion algorithm represent the average height value of all fracture hits at the chosen stage. This study demonstrates the potential to determine fracture height growth using LF-DAS measurements in the vertical section of a horizontal well, thus avoiding the cost associated with drilling VMWs to obtain fracture heights.
了解压裂高度的增长对于优化水力压裂处理和油田开发至关重要。近年来,低频分布式声学传感(LF-DAS)已成为监测水力压裂过程中应变变化的常用工具。来自垂直监测井(VMW)的 LF-DAS 数据可用于确定压裂高度,而来自水平井垂直段的测量数据则有可能捕捉到压裂高度的增长。本研究的目标是:(1) 采用三种方法--(a) 使用水平纤维垂直段测量法;(b) 使用垂直纤维测量法;(c) 使用水平纤维水平段测量法--使用水力压裂试验场 2 (HFTS-2) 数据集确定压裂高度;(2) 证明使用水平纤维垂直段 LF-DAS 测量法确定压裂高度的可靠性。为了使用上述三种方法确定 HFTS-2 数据集的压裂高度,我们利用水平监测井垂直段(VS-HMW)的应变测量数据证明了高度预测的可靠性。首先,我们分析了水平井最跟部(B1H、B2H 和 B4H)刺激期间水平纤维垂直段(B3H)的测量结果。其次,我们分析了在 B1H、B2H 和 B4H 的刺激过程中来自 VMW(B5PH)的测量数据。第三,我们使用地质力学反演算法,从 B1H、B2H 和 B4H 激励期间 B3H 的 LF-DAS 测量水平剖面上获得高度估计值。裂缝高度是根据 LF-DAS 垂直剖面测量中延伸-压缩带的过渡来确定的。我们比较了三种方法得出的高度估计值,发现在我们分析的六对油井中,这三种方法得出的高度估计值是一致的。垂直井 B5PH 的 LF-DAS 测量提供了完整的高度剖面,而垂直剖面的测量则捕捉到了从裂缝上端到水平井着陆深度的裂缝生长情况。通过我们的反演算法获得的裂缝高度估计值代表了所选阶段所有裂缝的平均高度值。这项研究证明了利用水平井垂直段的 LF-DAS 测量来确定裂缝高度增长的潜力,从而避免了钻探 VMW 来获取裂缝高度所需的成本。
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引用次数: 0
Research on the Effects of an Electrode Drill Bit during the Rock Drilling Process by High-Voltage Electric Pulse 高压电脉冲对凿岩过程中电极钻头影响的研究
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219735-pa
Longchen Duan, Xianao Liu, Changping Li, Jifeng Kang, Di Zhang, Zhong Yuan
High-voltage electric pulse rock-breaking (HVEPB) has proved to be a novel and inexpensive method of breaking rock regardless of rock composition, but the design of the electrode drill bit lacks a theoretical basis. In this paper, we first establish a plasma channel model for electric breakdown and a numerical rock-breaking model for HVEPB, which can simulate the rock electrical breakdown plasma channel and the effect of different electrode drill bits on HVEPB. Second, we analyze the effects of different electrode arrangement structures and high-voltage electrode angles on plasma channels and the effects of internal cracks and rock-breaking processes through numerical simulation. Finally, we describe HVEPB experiments conducted using electrode drill bits with different electrode arrangement structures and high-voltage electrode angles, and with the boreholes reconstructed in three dimensions to analyze the effects of different electrode arrangement structures and high-voltage electrode angles on HVEPB drilling. The results show that the effects of the electrode drill bits on HVEPB are reflected mainly in the difference between the plasma channel and shock wave. Different electrode arrangement structures and high-voltage electrode angles result in different electric fields and energy utilization efficiencies within the rock, resulting in different shock waves and differences in the depth, shapes, and penetration of the plasma channels. The simulations and experimental studies in this paper can guide and optimize the design of the discharge tool to upgrade the drilling efficiency of HVEPB.
高压电脉冲破岩法(HVEPB)已被证明是一种新型、廉价的破岩方法,不受岩石成分的影响,但电极钻头的设计缺乏理论依据。本文首先建立了电击穿等离子体通道模型和 HVEPB 数值破岩模型,可以模拟岩石电击穿等离子体通道和不同电极钻头对 HVEPB 的影响。其次,我们通过数值模拟分析了不同电极排列结构和高压电极角度对等离子体通道的影响,以及内部裂缝和破岩过程的影响。最后,我们介绍了使用不同电极排列结构和高压电极角度的电极钻头进行的 HVEPB 实验,并对钻孔进行了三维重建,以分析不同电极排列结构和高压电极角度对 HVEPB 钻进的影响。结果表明,电极钻头对 HVEPB 的影响主要体现在等离子体通道和冲击波之间的差异上。不同的电极排列结构和高压电极角度会在岩石内部产生不同的电场和能量利用效率,从而产生不同的冲击波,等离子体通道的深度、形状和穿透力也不同。本文的模拟和实验研究可以指导和优化放电工具的设计,从而提高 HVEPB 的钻井效率。
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引用次数: 0
Experimental Study of the Effect of Molecular Collision Frequency and Adsorption Capacity on Gas Seepage Flux in Coal 分子碰撞频率和吸附容量对煤中瓦斯渗流通量影响的实验研究
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219733-pa
Yang Gao, Qingchun Yu
The differences in the transport behavior and adsorption capacity of different gases in coal play crucial roles in the evolution of coal permeability. Previous studies of coreflooding experiments failed to explain the mechanism of gas flow and have attributed the variation in gas seepage flux (flow rate) at the beginning of the experiment to the change in effective stress, while the differences in the microscopic properties of different gases, such as molar mass, molecular diameter, mean molecular free path, and molecular collision frequency, were ignored. To research the effect of these gas properties on seepage flux while circumventing the effective stress, coreflooding experiments with helium (He), argon (Ar), nitrogen (N2), methane (CH4), and carbon dioxide (CO2) were designed. The results show that the gas transport velocity in coal is affected by the combination of molecular collision frequency and dynamic viscosity, and the transport velocities follow the order of ν (CH4) > ν (He) > ν (N2) > ν (CO2) > ν (Ar). A permeability equation corrected by the molecular collision frequency is proposed to eliminate differences in the permeabilities measured with different gases. The adsorption of different gases on the coal matrix causes different degrees of swelling, and the adsorption-induced swelling strains follow the order of ε (CO2) > ε (CH4) > ε (N2) > ε (Ar) > ε (He). The reduction in seepage flux and irreversible alterations in pore structure caused by adsorption-induced swelling are positively correlated with their adsorption capacities. The gas seepage fluxes after adsorption equilibrium of coal follow the order of Q (He) > Q (CH4) >Q (N2) > Q (Ar) > Q (CO2). Like supercritical CO2 (ScCO2), conventional CO2 can also dissolve the organic matter in coal. The organic molecules close to the walls of the cleats along the direction of gas flow are preferentially dissolved by CO2, and the gas seepage flux increases when the dissolution effect on the cleat width is greater than that on adsorption swelling.
不同气体在煤中的运移行为和吸附能力的差异对煤的渗透性演变起着至关重要的作用。以往的岩心充水实验研究未能解释气体流动的机理,将实验开始时气体渗流通量(流速)的变化归因于有效应力的变化,而忽略了不同气体微观性质的差异,如摩尔质量、分子直径、平均分子自由路径和分子碰撞频率等。为了在规避有效应力的同时研究这些气体特性对渗流通量的影响,设计了氦气(He)、氩气(Ar)、氮气(N2)、甲烷(CH4)和二氧化碳(CO2)的充芯实验。结果表明,煤中气体的运移速度受分子碰撞频率和动态粘度的共同影响,运移速度的顺序为 ν (CH4) > ν (He) > ν (N2) > ν (CO2) > ν (Ar)。提出了一个由分子碰撞频率校正的渗透率方程,以消除不同气体测量到的渗透率之间的差异。不同气体在煤基体上的吸附会引起不同程度的膨胀,吸附引起的膨胀应变遵循ε(CO2)>ε(CH4)>ε(N2)>ε(Ar)>ε(He)的顺序。吸附膨胀引起的渗流通量减少和孔隙结构的不可逆改变与吸附容量呈正相关。煤炭吸附平衡后的气体渗流通量按照 Q(He)>Q(CH4)>Q(N2)>Q(Ar)>Q(CO2)的顺序排列。与超临界 CO2(ScCO2)一样,常规 CO2 也能溶解煤中的有机物。沿气体流动方向靠近裂隙壁的有机分子优先被 CO2 溶解,当对裂隙宽度的溶解作用大于对吸附膨胀的溶解作用时,气体渗流通量会增加。
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引用次数: 0
Compact Viscosity Sensors for Downhole Enhanced Oil Recovery Polymer Fluid Degradation Monitoring 用于井下强化采油聚合物流体降解监测的紧凑型粘度传感器
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/209430-pa
Miguel Gonzalez, Subhash Ayirala, Lyla Maskeen, Abdulkareem AlSofi
There are currently no technologies available to measure polymer solution viscosities at realistic downhole conditions in a well during enhanced oil recovery (EOR). In this paper, custom-made probes using quartz tuning fork (QTF) resonators are demonstrated for measurements of viscosity of polymer fluids in the laboratory. The electromechanical response of the resonators was calibrated in simple Newtonian fluids and in non-Newtonian polymer fluids at different concentrations. The responses were then used to measure field-collected samples of polymer injection fluids. In the polymer fluids, the measured viscosity values by tuning forks were lower than those measured by the conventional rheometer at 6.8 s−1, closer to the solvent viscosity values. However, the predicted rheometer viscosity vs. QTF-measured viscosity showed a distinct exponential correlation (R2=0.9997), allowing for an empirical calibration between the two viscometers for fluids having the same solvent and polymer compositions. The QTF sensors produced acceptable viscosity measurements of polymer fluids within the required polymer concentration ranges used in the field and predicted field sample viscosities with less than 1–2 cp (or 10–20%) error from the rheometer data. Results were validated based on separate independent tests where the devices were used to measure the viscosity of Newtonian fluids and non-Newtonian polymer fluids in a series of consecutive dip tests, simulating more realistic usage. These devices can be used to measure either the “relative” viscosity changes from a polymer solution prior and post-injection or to measure a “calibrated” viscosity via empirical exponential correlation. The compact QTF sensors developed in this study can be easily integrated into portable systems for laboratory or wellsite deployment as well as logging tools for downhole deployment. This work also demonstrates the ability of these QTF devices to make sensitive viscosity measurements at high-frequencies, opening opportunities for their use in high-frequency rheology studies of EOR fluids.
目前还没有任何技术可以测量强化采油(EOR)过程中油井在实际井下条件下的聚合物溶液粘度。本文展示了使用石英音叉(QTF)谐振器定制的探头,用于在实验室测量聚合物溶液的粘度。在简单牛顿流体和不同浓度的非牛顿聚合物流体中校准了谐振器的机电响应。然后利用这些响应测量现场采集的聚合物注射流体样本。在聚合物流体中,调谐叉测得的粘度值低于传统流变仪测得的 6.8 s-1,更接近溶剂粘度值。然而,预测的流变仪粘度与 QTF 测量的粘度之间呈现出明显的指数相关性(R2=0.9997),因此,对于具有相同溶剂和聚合物成分的流体,两种粘度计之间可以进行经验校准。在现场使用的聚合物浓度范围内,QTF 传感器对聚合物流体进行了可接受的粘度测量,预测的现场样品粘度与流变仪数据的误差小于 1-2cp(或 10-20%)。在一系列连续的浸渍试验中,这些设备被用来测量牛顿流体和非牛顿聚合物流体的粘度,模拟更真实的使用情况。这些装置既可用于测量聚合物溶液在注入前后的 "相对 "粘度变化,也可通过经验指数相关性测量 "校准 "粘度。本研究开发的 QTF 传感器结构紧凑,可轻松集成到便携式系统中,用于实验室或井场部署,也可集成到测井工具中,用于井下部署。这项工作还展示了这些 QTF 设备在高频率下进行灵敏粘度测量的能力,为它们在 EOR 流体的高频流变学研究中的应用提供了机会。
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引用次数: 0
The Investigation of Broad-Spectrum Sealing Drilling Fluid Based on Horsfield Close-Packing Theory 基于霍斯菲尔德封隔理论的广谱封隔钻井液研究
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219489-pa
Haoan Dong, Zhiyong Li, Xiangyu Meng, Xue Peng, Rongxin Ma, Haotian Cen, Ruixing Xu
In shale gas drilling operations, oil-based drilling fluids have proved to be effective in addressing the issue of shale reservoir hydration expansion, serving as the primary working fluid for complex subsurface shale formations. However, the presence of shale laminations and the development of microfractures with varying widths require drilling fluids with excellent sealing capabilities. In this study, a comprehensive investigation was conducted to develop a drilling fluid system with broad-spectrum high-sealing performance. The porosity of bridging particles was determined by using the Archimedean drainage method. The bridging particle size and quantity at each level were meticulously designed through leveraging the Horsfield close-packing theory. The incorporation of deformable nanoscale polymer sealing materials further enhanced the sealing performance of the drilling fluid system. Additionally, hydrophobic nanoscale silica particles were introduced as coemulsifier to prepare Pickering emulsions, thereby improving emulsion stability and enhancing particle-size distribution for improved sealing. Through formulation optimization, a drilling fluid system with broad-spectrum, high-sealing performance capabilities was developed. The study revealed a reduction in porosity of closely packed bridging particles from 35.36% to 11.38%. The drilling fluid system exhibited a remarkable sealing efficiency of 99.2% for microfractures in the 1–10 μm range and 95.8% for microfractures in the 30–50 μm range. Furthermore, it demonstrated excellent sedimentation stability, with a sedimentation factor of less than 0.52 after 48 hours of static sedimentation at 150°C. The drilling fluid system also exhibited favorable rheological, lubrication, and inhibition properties, thus meeting the demands of field applications.
在页岩气钻井作业中,油基钻井液被证明可以有效解决页岩储层水化膨胀问题,是复杂地下页岩层的主要工作液。然而,页岩层理的存在和不同宽度微裂缝的发育要求钻井液具有出色的密封能力。本研究进行了全面调查,以开发一种具有广谱高密封性能的钻井液体系。采用阿基米德排水法测定了架桥颗粒的孔隙率。利用霍斯菲尔德密堆积理论,对各层次桥接颗粒的大小和数量进行了精心设计。可变形纳米级聚合物密封材料的加入进一步提高了钻井液系统的密封性能。此外,还引入了疏水性纳米级二氧化硅颗粒作为助乳化剂来制备皮克林乳液,从而提高了乳液的稳定性,并改善了粒度分布,提高了密封性。通过配方优化,开发出了一种具有广谱、高密封性能的钻井液体系。研究显示,紧密堆积的架桥颗粒的孔隙率从 35.36% 降至 11.38%。该钻井液体系对 1-10 μm 范围内的微裂缝的封孔效率高达 99.2%,对 30-50 μm 范围内的微裂缝的封孔效率高达 95.8%。此外,它还具有出色的沉积稳定性,在 150°C 下静置沉积 48 小时后,沉积系数小于 0.52。该钻井液体系还具有良好的流变性、润滑性和抑制性,从而满足了现场应用的要求。
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引用次数: 0
Molecular Simulation of Competitive Adsorption of Hydrogen and Methane: Analysis of Hydrogen Storage Feasibility in Depleted Shale Gas Reservoirs 氢气和甲烷竞争吸附的分子模拟:枯竭页岩气藏中的储氢可行性分析
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/212218-pa
Fangxuan Chen, Shihao Wang, M. Dejam, H. Nasrabadi
As a clean energy carrier, hydrogen (H2) is considered an indispensable part of the energy transition roadmap. To meet increasing energy demand, extremely large storage capacities are required. Previous studies have focused on underground H2 storage in conventional depleted gas reservoirs, salt caverns, and saline aquifers. The increasing number of depleted shale gas reservoirs may be good candidates for H2 storage. In this work, we analyze the potential of H2 storage in depleted gas reservoirs using Monte Carlo (MC) simulations. The competitive adsorption of a methane-hydrogen (C1-H2) system under nanoscale conditions is investigated, including the effects of pore size, temperature, pressure, boundary material, and fluid composition. Our results show that C1 is preferentially adsorbed in a C1-H2 system. C1 forms the adsorption layer near the boundary surface, while H2 molecules are freely distributed in the pore. The fluid distribution indicates that H2 can be easily produced during H2 recovery processes, which contributes to H2 storage in depleted shale gas reservoirs. In addition, the effect of water on C1-H2 competitive adsorption is analyzed. The strong interactions between water and boundary atoms force C1 molecules away from the adsorbed region. This work provides a foundation for hydrogen storage in depleted shale gas reservoirs at a molecular level.
作为一种清洁能源载体,氢气(H2)被认为是能源转型路线图中不可或缺的一部分。为了满足日益增长的能源需求,需要极大的储存能力。以往的研究主要集中在常规枯竭气藏、盐穴和含盐地下蓄水层中的地下氢气存储。越来越多的贫化页岩气藏可能是储存 H2 的理想场所。在这项研究中,我们利用蒙特卡罗(MC)模拟分析了在贫化气藏中封存 H2 的潜力。研究了纳米级条件下甲烷-氢(C1-H2)系统的竞争吸附,包括孔隙大小、温度、压力、边界材料和流体成分的影响。结果表明,C1 在 C1-H2 系统中优先被吸附。C1 在边界表面附近形成吸附层,而 H2 分子则在孔隙中自由分布。流体分布表明,在 H2 开采过程中很容易产生 H2,这有助于在枯竭页岩气藏中储存 H2。此外,还分析了水对 C1-H2 竞争吸附的影响。水与边界原子之间的强相互作用迫使 C1 分子远离吸附区域。这项研究从分子层面为贫化页岩气储层的氢气储存奠定了基础。
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引用次数: 0
A Generalized Method for Dynamic Fracture Characterization Using Two-Phase Rate Transient Analysis of Flowback and Production Data 利用回流和生产数据的两相速率瞬态分析进行动态断裂特征描述的通用方法
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/215213-pa
Guoqing Sun, Zhengxin Zhang, Changhe Mu, Chuncheng Liu, Chao Deng, Weikai Li, Weiran Hu
This study presents a comprehensive method for characterizing reservoir properties and hydraulic fracture (HF) closure dynamics using the rate transient analysis of flowback and production data. The proposed method includes straightline analysis (SLA), type-curve analysis (TCA), and model history matching (MHM), which are developed for scenarios of two-phase flow in fracture, stimulated reservoir volume (SRV), and nonstimulated reservoir volume (NSRV) domains. HF closure dynamics are characterized by two key parameters, which are pressure-dependent permeability and porosity controlled by fracture permeability modulus and compressibility. The above techniques are combined into a generalized workflow to estimate iteratively the five parameters (including four optional parameters and one fixed parameter) by reconciling data in different domains of time (single-phase water flow, two-phase flow, and hydrocarbon-dominated flow), analysis methods (SLA, TCA, and MHM), and phases (water and hydrocarbon phase). We used flowback and production data from a shale gas well in the US and a shale oil well in China to verify the practicability of the method. The analysis results of the field cases confirm the good performance of the newly developed comprehensive method and verify the accuracy in estimating the static fracture properties [initial fracture pore volume (PV) and permeability] and the HF dynamic parameters using the proposed generalized workflow. The accurate prediction of the decreasing fracture permeability and porosity, fracture permeability modulus, and compressibility demonstrates the applicability of the comprehensive method in quantifying HF dynamics. The field application results suggest a reduction of the fracture PV by 15% and 20%, and a reduction of the fracture permeability by 80% and 90% for shale gas and shale oil wells, respectively.
本研究提出了一种利用回流和生产数据的速率瞬态分析来描述储层特性和水力压裂(HF)闭合动态的综合方法。所提出的方法包括直线分析法(SLA)、类型曲线分析法(TCA)和模型历史匹配法(MHM),分别针对裂缝、受刺激储层体积(SRV)和非受刺激储层体积(NSRV)域中的两相流情况而开发。高频闭合动力学由两个关键参数表征,即由压裂渗透模量和可压缩性控制的与压力相关的渗透率和孔隙度。通过协调不同时间域(单相水流、两相水流和以碳氢化合物为主的水流)、分析方法(SLA、TCA 和 MHM)和相(水相和碳氢化合物相)的数据,将上述技术结合到一个通用的工作流程中,对五个参数(包括四个可选参数和一个固定参数)进行迭代估算。我们使用了美国一口页岩气井和中国一口页岩油井的回流和生产数据来验证该方法的实用性。现场案例的分析结果证实了新开发的综合方法的良好性能,并验证了使用所提出的通用工作流程估算静态裂缝属性(初始裂缝孔隙体积(PV)和渗透率)和高频动态参数的准确性。对递减的裂缝渗透率和孔隙度、裂缝渗透模量和压缩性的准确预测证明了综合方法在量化高频动态方面的适用性。现场应用结果表明,页岩气井和页岩油井的压裂PV值分别降低了15%和20%,压裂渗透率分别降低了80%和90%。
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引用次数: 0
Study on the Dispersion Stability and Sealing Performance of Nanoscale Plugging Materials for Shale Formations 页岩层纳米级封堵材料的分散稳定性和密封性能研究
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219736-pa
Haoan Dong, Zhiyong Li, Dong Xu, Lili Yan, Lihui Wang, Yan Ye
Nanoscale plugging materials are commonly used in the petroleum industry to seal microfractures and pores within shale formations, thereby maintaining wellbore stability and preventing drilling accidents caused by formation collapse. However, the influence of inorganic salts present in the formation and drilling fluids on the dispersion properties of nanoscale plugging materials often affects their sealing performance. In this study, we focus on investigating the influence of three commonly encountered inorganic salts in the drilling process—sodium chloride (NaCl), potassium chloride (KCl), and calcium chloride (CaCl2)—on the dispersibility and sealing performance of commonly used nanoscale plugging materials such as nanosilica and nanoemulsions in shale formations, exploring the dispersion and sealing mechanisms. Zeta potential is used as a characterization parameter, and molecular dynamics simulations are used to study the effects and mechanisms of inorganic salt ions on the dispersion of plugging materials. Filtration and pressure transmission experiments are conducted to investigate changes in their sealing performance. Scanning electron microscopy (SEM) is used to observe the microstructure of the formed filter cake, providing insights into the dispersion and sealing mechanisms. The results reveal that nanosilica agglomerates at zeta potentials ranging from −18 mV to −15.5 mV, resulting in an increase in filtration volume from 93.3 mL to 171.1 mL and downstream stable pressure transmission rising from 330.98 psi to 551.98 psi. Nanosilica (modified with KH570) agglomerates at zeta potentials of −10.3 mV to −9.9 mV, leading to an increase in filtration volume from 93.1 mL to 171 mL and downstream stable pressure transmission rising from 326.98 psi to 553.35 psi. The average gyration radius of the KH570 molecule decreases from 0.347 nm to 0.337 nm under the influence of inorganic salts. In contrast, the dispersion stability of nanoscale emulsions is independent of zeta potential; however, under the influence of inorganic salts, the filtration volume increases from 92.2 mL to 170.9 mL and downstream stable pressure transmission rises from 293.03 psi to 550.98 psi. The average gyration radius of nanoscale emulsion monomer molecules decreases from 0.340 nm to 0.336 nm under the influence of inorganic salts. Microscopic examination of filter-cake morphology shows that inorganic salts not only affect dispersion stability, leading to the aggregation of nanomaterials and influencing sealing performance, but also reduce the deformability of organic particles, thereby affecting sealing performance. The properties obtained in this study provide theoretical references for the sealing performance of nanomaterials in drilling fluids, offering significant value for researchers and field engineers in selecting nanoscale plugging materials for shale formations.
石油工业通常使用纳米级堵漏材料来封堵页岩地层中的微裂缝和孔隙,从而保持井筒稳定,防止地层坍塌造成钻井事故。然而,地层和钻井液中存在的无机盐对纳米级堵漏材料分散性能的影响往往会影响其密封性能。在本研究中,我们重点研究了钻井过程中常见的三种无机盐--氯化钠(NaCl)、氯化钾(KCl)和氯化钙(CaCl2)--对常用纳米级堵漏材料(如纳米二氧化硅和纳米乳液)在页岩层中的分散性和封堵性能的影响,探讨了其分散和封堵机理。采用 Zeta 电位作为表征参数,并利用分子动力学模拟研究无机盐离子对堵漏材料分散的影响和机理。还进行了过滤和压力传输实验,以研究其密封性能的变化。使用扫描电子显微镜(SEM)观察形成滤饼的微观结构,从而深入了解分散和密封机制。结果表明,纳米二氧化硅在 zeta 电位为 -18 mV 至 -15.5 mV 时聚结,导致过滤量从 93.3 mL 增加到 171.1 mL,下游稳定压力传输从 330.98 psi 上升到 551.98 psi。纳米二氧化硅(用 KH570 改性)在 zeta 电位为 -10.3 mV 至 -9.9 mV 时聚结,导致过滤量从 93.1 mL 增加到 171 mL,下游稳定压力传输从 326.98 psi 上升到 553.35 psi。在无机盐的影响下,KH570 分子的平均回旋半径从 0.347 nm 减小到 0.337 nm。相比之下,纳米级乳液的分散稳定性与 zeta 电位无关;然而,在无机盐的影响下,过滤体积从 92.2 mL 增加到 170.9 mL,下游稳定压力传输从 293.03 psi 上升到 550.98 psi。在无机盐的影响下,纳米级乳液单体分子的平均回旋半径从 0.340 nm 减小到 0.336 nm。滤饼形态的显微镜检查表明,无机盐不仅会影响分散稳定性,导致纳米材料聚集,影响密封性能,还会降低有机颗粒的变形能力,从而影响密封性能。本研究获得的性能为纳米材料在钻井液中的密封性能提供了理论参考,为研究人员和现场工程师选择页岩地层纳米级堵漏材料提供了重要价值。
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引用次数: 0
Prediction of Production-Inflow Profile of a Well Producing Single-Phase Flow of Slightly Compressible Fluid from Multilayer Systems by Temperature and/or Pressure Transient Data 通过温度和/或压力瞬态数据预测从多层系统生产单相轻微可压缩流体的油井的产量-流量曲线
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/214384-pa
C. Alan, Murat Cinar, Mustafa Onur
This study focuses on the prediction of the production-inflow profile of a well producing a single-phase flow of slightly compressible fluid (water or oil flow) in a multilayered system using the layer permeability and skin values estimated by history matching spatial and temporal temperature and/or pressure data sets along the completion interval. Such data may be acquired by wireline formation testing, production-logging-tool (PLT), or distributed temperature sensing (DTS) fiber-optic cables. We use an in-house thermal, transient coupled reservoir/wellbore simulator developed during this study. It solves transient mass, momentum, and energy conservation equations simultaneously for both reservoir and wellbore. The effects of the Joule-Thomson (J-T), adiabatic expansion, conduction, and convection are all included for predicting the flow profiles across the wellbore. The results from our in-house simulator are verified with the results from a commercial simulator for the single-phase fluid flow of a vertical well producing geothermal brine and oil in a two-zone multilayer system. We also compare the results from our rigorous transient coupled wellbore/reservoir model with the results from a model assuming steady-state thermal wellbore model used in the previous studies. We find that the steady-state thermal wellbore model used in the previous studies that ignore accumulation terms in mass, momentum, and thermal energy balances is a reasonably accurate model for predicting wellbore pressures and temperatures when it is coupled with a nonisothermal reservoir model for slightly compressible fluid because the transient effect in the wellbore is less important with the slightly compressible fluid. We investigate the nonlinear parameter estimation problem based on the use of single or multiple observed temperature and/or pressure (if available) profiles recorded spatially inside the wellbore and at the sandface. The purpose is to identify if the wellbore or sandface data profiles are more useful to accurately estimate the permeability and skin information and predict a production-inflow profile of the well depending on the representation of an actual multilayer system by a reduced-layered or fine-layered model. We show that using an upscaled-layered model (e.g., representing each heterogeneous layer with a lumped single layer with uniform permeability and skin) provides estimates that are more toward the thickness-average permeability and skin factors of the layers and may not provide a good prediction of the well’s production-inflow profile. We show that including the sandface temperature data in regression worsens, while the use of wellbore temperature data sets improves the quality of parameter estimation if an upscaled multilayered model is used. We also show that regressing on multiple temperature profiles, preferably at the sandface, alone could be used to predict the production-inflow profile accurately if a “fine” multilayered heterogeneous
本研究的重点是预测多层系统中单相轻微可压缩流体(水流或油流)油井的产量-流量曲线,其方法是利用沿完井间隔的时空温度和/或压力数据集历史匹配估算的层渗透率和皮膜值。这些数据可以通过有线地层测试、生产记录工具(PLT)或分布式温度传感(DTS)光纤电缆获取。我们在这项研究中使用了内部开发的热瞬态耦合储层/井筒模拟器。它可同时求解储层和井筒的瞬态质量、动量和能量守恒方程。焦耳-汤姆森(J-T)、绝热膨胀、传导和对流的影响都包括在内,用于预测井筒的流动剖面。我们将内部模拟器的结果与商用模拟器的结果进行了验证,商用模拟器模拟的是在两区多层系统中生产地热卤水和石油的垂直井的单相流体流动。我们还将严格的瞬态井筒/储层耦合模型的结果与之前研究中使用的假定稳态热井筒模型的结果进行了比较。我们发现,以往研究中使用的稳态热井筒模型忽略了质量、动量和热能平衡中的累积项,当它与轻微可压缩流体的非等温油藏模型耦合时,是预测井筒压力和温度的相当准确的模型,因为轻微可压缩流体在井筒中的瞬态效应并不那么重要。我们利用井筒内和砂面空间记录的单个或多个观测温度和/或压力(如有)剖面,研究了非线性参数估计问题。目的是确定井筒或砂面数据剖面是否更有助于准确估算渗透率和表皮信息,并根据缩减层或精细层模型对实际多层系统的表示预测油井的产量-流量剖面。我们的研究表明,使用放大分层模型(例如,用具有均匀渗透率和表皮的集合单层来表示每个异质层)提供的估算结果更接近于各层的厚度平均渗透率和表皮系数,可能无法很好地预测油井的生产-流入剖面。我们的研究表明,如果使用放大的多层模型,在回归中加入砂面温度数据会使参数估计的质量下降,而使用井筒温度数据集则会提高参数估计的质量。我们还表明,如果使用 "精细 "多层异构模型,仅对多个温度曲线(最好是砂面温度曲线)进行回归,就能准确预测产量-流量曲线。我们还研究了在完井区间的非穿孔段加入或排除温度和/或压力测量值是否有助于改善参数估计问题。结果表明,如果对包括不同生产率下非射孔区段数据在内的多个温度剖面进行回归,则可以获得可靠的各层属性估计值,从而准确预测生产-流入剖面,尽管各层渗透率和集肤系数可能经常表现出较宽的 95% 置信区间以及它们之间的高度相关性。在历史匹配中,如果有砂面或井筒压力数据,将其添加到观测数据集中,总能提高参数估计的质量。
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引用次数: 0
The Effect of Gypsum/Bassanite on the Retardation of Ethylene Diamine Tetra(Methylene Phosphonic Acid) Sodium in Oil Well Cement Slurry 石膏/重晶石对油井水泥浆中乙二胺四乙酸钠缓凝剂的影响
IF 3.6 3区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-03-01 DOI: 10.2118/219728-pa
Jiamen Huang, Chunyu Wang, Xiao Yao, Chenzi Geng, Yiwei Zou, Yixin Wang
Organophosphonates are commonly used retarders to prolong the thickening time of oilwell cement slurry at medium and high temperatures. In this paper, the impact of calcium sulfate in cement on the retarding effect of ethylene diamine tetra(methylene phosphonic acid) sodium (EDTMPS) was explored. First, the thickening properties of cements from four different factories were studied in detail with varying additions of EDTMPS. The study revealed diverse thickening phenomena, including retarding, accelerating, and increasing the initial consistency of cement slurries. The heat flow of cement hydration was detected, and the mineral changes of cement slurries at the early stage (1–3 hours) were analyzed. Additionally, the effect of EDTMPS on the hydration of tricalcium aluminate (C3A) and gypsum (GP)/bassanite (BS) slurry was investigated through X-ray diffraction (XRD) and ion concentration test. Finally, two clinkers from the same cement factory were mixed with GP/BS of different dosages to study the effect of calcium sulfate type on the thickening properties of cement slurry with EDTMPS. The results revealed that EDTMPS slowed down the dissolution of GP while promoting the dissolution of C3A. The rapid hydration of C3A increased the consistency of cement slurry without the retarding effect of GP. However, EDTMPS promoted the dissolution of BS, which can retard the hydration of C3A. Therefore, EDTMPS is appropriate for cements containing BS.
有机膦酸盐是常用的缓凝剂,可延长油井水泥浆在中高温下的稠化时间。本文探讨了水泥中硫酸钙对乙二胺四甲苯膦酸钠(EDTMPS)缓凝效果的影响。首先,详细研究了四家不同工厂生产的不同 EDTMPS 添加量水泥的增稠性能。研究发现了多种增稠现象,包括延缓、加速和增加水泥浆的初始稠度。对水泥水化热流进行了检测,并分析了水泥浆早期(1-3 小时)的矿物变化。此外,还通过 X 射线衍射(XRD)和离子浓度测试研究了 EDTMPS 对铝酸三钙(C3A)和石膏(GP)/重晶石(BS)浆体水化的影响。最后,将来自同一水泥厂的两种熟料与不同掺量的 GP/BS 混合,研究硫酸钙类型对 EDTMPS 水泥浆稠化性能的影响。结果显示,EDTMPS 减慢了 GP 的溶解速度,同时促进了 C3A 的溶解。C3A 的快速水化增加了水泥浆的稠度,而 GP 却没有起到延缓作用。然而,EDTMPS 促进了 BS 的溶解,而 BS 会延缓 C3A 的水化。因此,EDTMPS 适用于含有 BS 的水泥。
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