Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.375
F. Goetz-Neunhoeffer, J. Neubauer, R. Enderlé, M. Göbbels
{"title":"Investigation of the β'- to α-phase transformation temperature of (Ca1−xMgx)3(PO4)2solid solutions","authors":"F. Goetz-Neunhoeffer, J. Neubauer, R. Enderlé, M. Göbbels","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.375","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.375","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89099402","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.531
J. Maixner, A. Kloužková, M. Mrázová, M. Kohoutková
{"title":"X-ray phase analysis in leucite systems","authors":"J. Maixner, A. Kloužková, M. Mrázová, M. Kohoutková","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.531","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.531","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78666202","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.27
Jonathan P. Wright, A. Markvardsen, I. Margiolaki
{"title":"Likelihood methods with protein powder diffraction data","authors":"Jonathan P. Wright, A. Markvardsen, I. Margiolaki","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.27","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.27","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76859459","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.267
M. Quaas, I. Shyjumon, R. Hippler, H. Wulff
{"title":"Melting of small silver clusters investigated by HT-GIXRD","authors":"M. Quaas, I. Shyjumon, R. Hippler, H. Wulff","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.267","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.267","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76120873","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKSU.2007.2007.SUPPL_26.355
Y. Taran, J. Schreiber, A. Balagurov, U. Stuhr, H. Kockelmann, V. Zlokazov
The triaxial residual stresses in a composite tube from an austenitic stainless steel with a welded ferritic steel cladding were measured by the time-of-flight neutron diffraction method on the POLDI instrument at the PSI SINQ neutron pulsed facility. The POLDI results are compared to the results obtained by the destructive turning out and ring core methods and theoretical predictions of calculations by the finite element method. Only for the tangential component of the stress tensor the semiquantitative agreement of the all used methods was observed. There was a clear discrepancy between the results of the different methods in the axial component. For the radial component all methods reveal quite small stresses, however, with some distinct differences in their distributions.
{"title":"Triaxial residual stresses in composite tube from austenitic stainless steel with welded ferritic steel cladding","authors":"Y. Taran, J. Schreiber, A. Balagurov, U. Stuhr, H. Kockelmann, V. Zlokazov","doi":"10.1524/ZKSU.2007.2007.SUPPL_26.355","DOIUrl":"https://doi.org/10.1524/ZKSU.2007.2007.SUPPL_26.355","url":null,"abstract":"The triaxial residual stresses in a composite tube from an austenitic stainless steel with a welded ferritic steel cladding were measured by the time-of-flight neutron diffraction method on the POLDI instrument at the PSI SINQ neutron pulsed facility. The POLDI results are compared to the results obtained by the destructive turning out and ring core methods and theoretical predictions of calculations by the finite element method. Only for the tangential component of the stress tensor the semiquantitative agreement of the all used methods was observed. There was a clear discrepancy between the results of the different methods in the axial component. For the radial component all methods reveal quite small stresses, however, with some distinct differences in their distributions.","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75495487","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.273
E. Moroz, D. A. Zuyzin
{"title":"The use of RDF analysis in the study of powder samples: Zirconia complex supported by clay and pseudoboehmite","authors":"E. Moroz, D. A. Zuyzin","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.273","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.273","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75063726","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.569
T. González, A. Briceño, G. D. Delgado, J. M. Delgado
{"title":"Synthesis and structural characterization of mixed transition metal derivatives of maleic acid: (M2+0.5Fe2+0.5)(C4H3O4)-2• 4H2O (with M2+=Mn, Co, Ni, and Zn) using powder diffraction data","authors":"T. González, A. Briceño, G. D. Delgado, J. M. Delgado","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.569","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.569","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80038320","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKSU.2007.2007.SUPPL_26.477
W. Nowicki, J. Darul, P. Piszora, C. Baehtz, E. Wolska
Single phase spinel solid solutions of LixMn3-x-yFeyO4 series with range of 0.5≤x≤1.0 and 0.2≤y≤1.0, have been synthesized by a solid state reaction. By refining the high-resolution X-ray diffraction patterns with Rietveld profile analysis, the lattice parame- ters, interatomic distances and cation distribution were determined. The Fe-for-Mn substitu- tion increases the spinel unit cell constant from a = 8.27A to a = 8.38A, for the Fe/(Fe+Mn) mole ratio of 0.1 and 0.472, respectively. Evidence is given that the lithium ions occupy the tetrahedral sites exclusively, for the molar ratio 0� Fe/(Mn+Fe) � 0.3.
{"title":"Synchrotron X-ray diffraction study on the cation distribution in quaternary Li-Fe-Mn spinel oxides","authors":"W. Nowicki, J. Darul, P. Piszora, C. Baehtz, E. Wolska","doi":"10.1524/ZKSU.2007.2007.SUPPL_26.477","DOIUrl":"https://doi.org/10.1524/ZKSU.2007.2007.SUPPL_26.477","url":null,"abstract":"Single phase spinel solid solutions of LixMn3-x-yFeyO4 series with range of 0.5≤x≤1.0 and 0.2≤y≤1.0, have been synthesized by a solid state reaction. By refining the high-resolution X-ray diffraction patterns with Rietveld profile analysis, the lattice parame- ters, interatomic distances and cation distribution were determined. The Fe-for-Mn substitu- tion increases the spinel unit cell constant from a = 8.27A to a = 8.38A, for the Fe/(Fe+Mn) mole ratio of 0.1 and 0.472, respectively. Evidence is given that the lithium ions occupy the tetrahedral sites exclusively, for the molar ratio 0� Fe/(Mn+Fe) � 0.3.","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78710357","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKSU.2007.2007.SUPPL_26.283
E. Filatov, Y. Shubin, S. Korenev
{"title":"Study of nanoalloys formation mechanism from single-source precursors [M(NH3)5Cl](ReO4)2, M = Rh, Ir","authors":"E. Filatov, Y. Shubin, S. Korenev","doi":"10.1524/ZKSU.2007.2007.SUPPL_26.283","DOIUrl":"https://doi.org/10.1524/ZKSU.2007.2007.SUPPL_26.283","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77136965","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2007-11-01DOI: 10.1524/ZKSU.2007.2007.SUPPL_26.235
P. Angerer, P. Pessenda-Garcia, E. Neubauer, G. Nauer
{"title":"Texture and stress in nickel layers with incorporated zirconia particles","authors":"P. Angerer, P. Pessenda-Garcia, E. Neubauer, G. Nauer","doi":"10.1524/ZKSU.2007.2007.SUPPL_26.235","DOIUrl":"https://doi.org/10.1524/ZKSU.2007.2007.SUPPL_26.235","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87745155","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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