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In-situpowder diffraction in high magnetic fields 强磁场中的原位粉末衍射
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.139
V. Pecharsky, Y. Mudryk, K. Gschneidner
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引用次数: 1
Synthesis and thermal decomposition of the oxalatho cuprates(II) – [M(NH3)4][Cu(C2O4)2]*3H2O, M = Pt, Pd 草酸铜酸盐(II) - [M(NH3)4][Cu(C2O4)2]*3H2O的合成与热分解,M = Pt, Pd
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKSU.2007.2007.SUPPL_26.289
K. Yusenko, E. Filatov, D. Vasilchenko, I. Baidina, A. Zadesenez, Y. Shubin
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引用次数: 10
Effect of interlayer cation and relative humidity on the hydration properties of a dioctahedral smectite 层间阳离子和相对湿度对二八面体蒙脱石水化性能的影响
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.417
W. Oueslati, M. Karmous, H. B. Rhaiem, B. Lanson, A. B. H. Amara
This paper aims at characterizing the structural evolution of a dioctahedral smec- tite (i.e. Wyoming montmorillonite) saturated by Na + , Cu 2+ or Pb 2+ . Hydration properties of the <2μm size fraction of Wyoming montmorillonite smectite (SWy) source clay (low charge i.e. 0.35) were studied by modelling of X-ray diffraction (XRD) patterns recorded under controlled relative humidity (RH) conditions on Na, Cu or Pb saturated specimens. The Cation Exchange Capacity (CEC) of the starting sample was first Na + saturated to guarantee better dispersion, followed by exchanges with the cations Cu 2+ or Pb 2+ . The resulting com- plexes were respectively labelled Wy- Na, Wy-Cu and Wy-Pb. The qualitative analysis of XRD patterns obtained under room pressure and temperature conditions showed that all complexes have one water layer hydration state. In order to highlight the specific hydration properties of each complex, we studied the XRD patterns under controlled relative humidity (%RH). The quantitative analysis of XRD patterns is achieved using an indirect method based on the comparison of experimental XRD patterns with calculated ones. This quantita- tive study showed that for Wy- Na, Wy-Cu and Wy-Pb at low RH (≈15%) the d001 spacing corresponds to a low hydration state characterized by one water layer, whereas for higher studied rates of relative humidity (75%), differences of hydration state can be distinguished for Wy-Na, Wy-Cu and Wy-Pb samples.
本文研究了一种以Na +、cu2 +或pb2 +为饱和的二八面体蒙脱石(即怀俄明蒙脱石)的结构演化特征。采用控制相对湿度(RH)条件下在Na、Cu或Pb饱和试样上记录的x射线衍射(XRD)模式,研究了怀俄明蒙脱石(SWy)源粘土(低电荷0.35)<2μm粒径组分的水化性能。起始样品的阳离子交换容量(CEC)首先是Na +饱和,以保证较好的分散性,然后与阳离子cu2 +或pb2 +交换。所得复合物分别被标记为Wy- Na、Wy- cu和Wy- pb。室温和常压条件下的XRD图谱定性分析表明,所有配合物均具有单一水层水化状态。为了突出每种配合物的具体水化性能,我们研究了在控制相对湿度(%RH)下的XRD图谱。通过对实验XRD图与计算XRD图的比较,采用间接法对XRD图进行了定量分析。定量研究表明,在低相对湿度(≈15%)条件下,Wy-Na、Wy- cu和Wy- pb样品的d001间距对应于一个水层的低水化状态,而在较高相对湿度(75%)条件下,Wy-Na、Wy- cu和Wy- pb样品的水化状态存在差异。
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引用次数: 19
New horizons for the structural characterization of stainless steel slags by X-ray powder diffraction 用x射线粉末衍射法表征不锈钢渣结构的新领域
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.61
B. Peplinski, B. Adamczyk, G. Kley, K. Adam, F. Emmerling, F. Simon
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引用次数: 1
Installation of the high resolution TOF diffractometer at the Budapest Research Reactor 布达佩斯研究堆高分辨率TOF衍射仪的安装
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.165
G. Káli, Zs. Sánta, H. Bleif, F. Mezei, L. Rosta, M. Szalók
The new TOF project started in 2000 in collaboration with the Hahn-Meitner- Institut. The spectrometer - previously tested on a cold beam - has been reinstalled to a radial thermal neutron beam at the Budapest Research Reactor. The TOF monochromator system consist of a double chopper with maximum rotation speed of 12000 rpm and the two single ones with 6000 rpm. The instrument will operate with a 2-dimensional detector of 80x100cm 2 in back scattering geometry, now He 3 tubes are used. The first test measurements we are presenting here show that the expected resolution Δd/d ~ 4x10 -4 can be achieved.
新的TOF项目开始于2000年,与哈恩-迈特纳研究所合作。之前在冷束上测试过的光谱仪已经重新安装在布达佩斯研究反应堆的径向热中子束上。TOF单色仪系统由一个最大转速为12000转/分的双斩波器和两个转速为6000转/分的单斩波器组成。仪器将使用反向散射几何尺寸为80x100cm 2的二维探测器,现在使用He 3管。我们在这里介绍的第一个测试测量表明,可以实现预期的分辨率Δd/d ~ 4x10 -4。
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引用次数: 7
Reconstruction of high-temperature deformation process by texture of the low-temperature phase as applied to Zr-based alloys 利用低温相织构重建zr基合金高温变形过程
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.333
M. Isaenkova, Y. Perlovich, V. Fesenko, M. Grekhov
{"title":"Reconstruction of high-temperature deformation process by texture of the low-temperature phase as applied to Zr-based alloys","authors":"M. Isaenkova, Y. Perlovich, V. Fesenko, M. Grekhov","doi":"10.1524/ZKRI.2007.2007.SUPPL_26.333","DOIUrl":"https://doi.org/10.1524/ZKRI.2007.2007.SUPPL_26.333","url":null,"abstract":"","PeriodicalId":23897,"journal":{"name":"Zeitschrift Fur Kristallographie","volume":"10 1","pages":"333-338"},"PeriodicalIF":0.0,"publicationDate":"2007-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83690222","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Secondary extinction correction used in a novel method for improved XRD characterizations of textured materials: The case of thin films 二次消光校正用于改进织构材料的XRD表征的新方法:以薄膜为例
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.131
I. Tomov
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引用次数: 0
Size-related diffraction anomalies from strongly distorted nano-crystals 强畸变纳米晶体的尺寸相关衍射异常
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.117
M. Shevchenko
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引用次数: 0
X-ray diffraction analysis of an ε/γ' iron-nitride compound double layer ε/γ′氮化铁化合物双层的x射线衍射分析
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.223
T. Gressmann, A. Leineweber, E. Mittemeijer, E. Mittemeijer, M. Knapp
An -Fe3N/ -Fe4N double compound layer grown on -Fe was investigated by Xray diffraction analysis. The anisotropic diffraction-line broadening observed by highresolution synchrotron diffraction measurements and the diffraction-line shifts as measured for hexagonal layer can be quantitatively explained by the presence of both a lattice parameter gradient associated with a concentration gradient and a stress gradient within the layer. Investigation of the layer revealed an elastic anisotropy unusual for fcc type metals.
用x射线衍射分析研究了在-Fe表面生长的-Fe3N/ -Fe4N双复合层。高分辨率同步加速器衍射测量所观察到的各向异性衍射线展宽和六边形层的衍射线位移可以用层内与浓度梯度和应力梯度相关的晶格参数梯度的存在来定量解释。对该层的研究揭示了fcc型金属不同寻常的弹性各向异性。
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引用次数: 3
Rietveld refinements of SnO2ceramic powders doped with ZnO, WO3, CoO, Nb2O5and MoO3 ZnO、WO3、CoO、nb2o5和MoO3掺杂sno2陶瓷粉末的Rietveld细化
Q2 Chemistry Pub Date : 2007-11-01 DOI: 10.1524/ZKRI.2007.2007.SUPPL_26.467
J. G. Carrió, T. J. Masson, A. H. Munhoz, M. Jesus, L. Perazolli, Ubirajara Coleto, S. Gutierrez-Antonio, R. Marques, C. O. Paiva-santos
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引用次数: 1
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