Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c9001447
A. Matting, R. Ziegler
Hydrogen embrittlement is the brittleness affecting copper and copper alloys containing oxygen which develops during heat treatment at temperatures of about 400 deg C (752 deg F) and above in an atmosphere containing hydrogen. The phenomenon of hydrogen embrittlement of copper and its alloys is illustrated by examples from practice and reference is made to data from recent publications on the subject. Embrittlement due to this cause can only be identified by microscopic examination because other modes of failure in copper; e.g., from heat cracking, mechanical overload, the formation of low melting point eutectics or corrosion; show a similar appearance when investigated on a macroscopic scale.
{"title":"Brittleness in Copper and Copper Alloys With Particular Reference to Hydrogen Embrittlement","authors":"A. Matting, R. Ziegler","doi":"10.31399/asm.fach.process.c9001447","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c9001447","url":null,"abstract":"\u0000 Hydrogen embrittlement is the brittleness affecting copper and copper alloys containing oxygen which develops during heat treatment at temperatures of about 400 deg C (752 deg F) and above in an atmosphere containing hydrogen. The phenomenon of hydrogen embrittlement of copper and its alloys is illustrated by examples from practice and reference is made to data from recent publications on the subject. Embrittlement due to this cause can only be identified by microscopic examination because other modes of failure in copper; e.g., from heat cracking, mechanical overload, the formation of low melting point eutectics or corrosion; show a similar appearance when investigated on a macroscopic scale.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"42 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"117229660","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c9001206
F. Naumann, F. Spies
A number of seamless pipe nipples of 70 mm diam and 3.5 mm wall thickness made of steel type 35.8 were oxyacetylene welded to collectors of greater wall thickness with a round bead. X-ray examination showed crack initiation in the interior of the nipples close to the root of the weld seam. The cracks only appeared where the originally deposited bead was remelted in the regions of overlap. Given the construction and welding technique used, it would have been preferable to make the nipples of a steel lower in sulfur content. However, by taking advantage of all the potential in shaping and welding technology, it should be possible to prevent crack formation with steel type 35.8 of normal composition.
{"title":"Cracking of Pipe Nipples in Welding","authors":"F. Naumann, F. Spies","doi":"10.31399/asm.fach.process.c9001206","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c9001206","url":null,"abstract":"\u0000 A number of seamless pipe nipples of 70 mm diam and 3.5 mm wall thickness made of steel type 35.8 were oxyacetylene welded to collectors of greater wall thickness with a round bead. X-ray examination showed crack initiation in the interior of the nipples close to the root of the weld seam. The cracks only appeared where the originally deposited bead was remelted in the regions of overlap. Given the construction and welding technique used, it would have been preferable to make the nipples of a steel lower in sulfur content. However, by taking advantage of all the potential in shaping and welding technology, it should be possible to prevent crack formation with steel type 35.8 of normal composition.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"173 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116414071","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c0048751
The presence of subsurface cracks in a longitudinal weld seam of an AISI type 316 stainless steel heat-exchanger shell was revealed by radiographic testing. Numerous intergranular cracks associated with the root pass of the weld, which had propagated both parallel and normal to the weld seam, were revealed by metallographic examination (hot shortness). It was indicated by energy-dispersive spectroscopy that type 316 electrode was not used for the root pass and instead a nickel-copper alloy electrode was employed. It was thus concluded that cracking was caused due to the use of an incorrect electrode for the root pass as these electrodes are crack sensitive if overheated. The weld seam was completely ground out and replaced with the correct electrode material as a corrective measure.
{"title":"Intergranular Cracking in Heat-Exchanger Welds Due to Hot Shortness","authors":"","doi":"10.31399/asm.fach.process.c0048751","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c0048751","url":null,"abstract":"\u0000 The presence of subsurface cracks in a longitudinal weld seam of an AISI type 316 stainless steel heat-exchanger shell was revealed by radiographic testing. Numerous intergranular cracks associated with the root pass of the weld, which had propagated both parallel and normal to the weld seam, were revealed by metallographic examination (hot shortness). It was indicated by energy-dispersive spectroscopy that type 316 electrode was not used for the root pass and instead a nickel-copper alloy electrode was employed. It was thus concluded that cracking was caused due to the use of an incorrect electrode for the root pass as these electrodes are crack sensitive if overheated. The weld seam was completely ground out and replaced with the correct electrode material as a corrective measure.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"115 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124013303","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c0047566
Handles welded to the top cover plate of a chemical-plant downcomer broke at the welds when the handles were used to lift the cover. The handles were fabricated of low-carbon steel rod; the cover was of type 502 stainless steel plate. The attachment welds were made with type 347 stainless steel filler metal to form a fillet between the handle and the cover. The structure was found to contain a zone of brittle martensite in the portion of the weld adjacent to the low-carbon steel handle; fracture had occurred in this zone. The brittle martensite layer in the weld was the result of using too large a welding rod and too much heat input, melting of the low-carbon steel handle, which diluted the austenitic stainless steel filler metal and formed martensitic steel in the weld zone. Because it was impractical to preheat and postheat the type 502 stainless steel cover plate, the low-carbon steel handle was welded to low-carbon steel plate, using low-carbon steel electrodes. This plate was then welded to the type 502 stainless steel plate with type 310 stainless steel electrodes. This design produced a large weld section over which the load was distributed.
{"title":"Failure in Stainless Steel Welds Joining Low-Carbon Steel Handles to Type 502 Stainless Steel Covers Because of Martensite Zone in the Welds","authors":"","doi":"10.31399/asm.fach.process.c0047566","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c0047566","url":null,"abstract":"\u0000 Handles welded to the top cover plate of a chemical-plant downcomer broke at the welds when the handles were used to lift the cover. The handles were fabricated of low-carbon steel rod; the cover was of type 502 stainless steel plate. The attachment welds were made with type 347 stainless steel filler metal to form a fillet between the handle and the cover. The structure was found to contain a zone of brittle martensite in the portion of the weld adjacent to the low-carbon steel handle; fracture had occurred in this zone. The brittle martensite layer in the weld was the result of using too large a welding rod and too much heat input, melting of the low-carbon steel handle, which diluted the austenitic stainless steel filler metal and formed martensitic steel in the weld zone. Because it was impractical to preheat and postheat the type 502 stainless steel cover plate, the low-carbon steel handle was welded to low-carbon steel plate, using low-carbon steel electrodes. This plate was then welded to the type 502 stainless steel plate with type 310 stainless steel electrodes. This design produced a large weld section over which the load was distributed.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129967440","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c0090909
An injection-molded PVC water-filter housing fractured in service. 75x views and visual inspection supported the conclusion that failure occurred due to fatigue crack propagation, as indicated by the presence of discontinuous crack-growth bands and their evolution. However, an initial fissure was believed to have started first due to residual stresses developed during injection molding. No recommendations were made.
{"title":"Failure of a PVC Water-Filter Housing","authors":"","doi":"10.31399/asm.fach.process.c0090909","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c0090909","url":null,"abstract":"\u0000 An injection-molded PVC water-filter housing fractured in service. 75x views and visual inspection supported the conclusion that failure occurred due to fatigue crack propagation, as indicated by the presence of discontinuous crack-growth bands and their evolution. However, an initial fissure was believed to have started first due to residual stresses developed during injection molding. No recommendations were made.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"22 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125667316","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c9001207
F. Naumann, F. Spies
Pipes made of low-carbon Thomas steel had been welded longitudinally employing the carbon-arc process with bare electrode wire made for argon-shielded arc welding. Difficulties were encountered during the cutting of threads because of the presence of hard spots. Microstructural examination showed welding conditions were such that a carburizing atmosphere developed, which led to an increase in carbon content and hardening at certain locations such as terminal bells and lap joints. This explained the processing difficulties during the threading operation.
{"title":"Welded Pipes with Hard Spots","authors":"F. Naumann, F. Spies","doi":"10.31399/asm.fach.process.c9001207","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c9001207","url":null,"abstract":"\u0000 Pipes made of low-carbon Thomas steel had been welded longitudinally employing the carbon-arc process with bare electrode wire made for argon-shielded arc welding. Difficulties were encountered during the cutting of threads because of the presence of hard spots. Microstructural examination showed welding conditions were such that a carburizing atmosphere developed, which led to an increase in carbon content and hardening at certain locations such as terminal bells and lap joints. This explained the processing difficulties during the threading operation.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"201202 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"123362635","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c9001416
Hydraulic cylinders on three identical presses failed in a similar manner after approximately ten years' service life. The cylinder was a steel casting having a carbon content of the order of 0.3 to 0.4%. During machining of the internal surfaces, a sharp corner had been left at the junction of the head with the shell. From this stress raiser a fatigue crack had developed around the entire circumference of the cylinder to give a smooth crack of annular form. The use of a flat end to the cylinder, therefore, resulted in excessive stresses being introduced at the junction of the end with the cylinder.
{"title":"Fatigue Failure of Hydraulic Press Cylinders","authors":"","doi":"10.31399/asm.fach.process.c9001416","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c9001416","url":null,"abstract":"\u0000 Hydraulic cylinders on three identical presses failed in a similar manner after approximately ten years' service life. The cylinder was a steel casting having a carbon content of the order of 0.3 to 0.4%. During machining of the internal surfaces, a sharp corner had been left at the junction of the head with the shell. From this stress raiser a fatigue crack had developed around the entire circumference of the cylinder to give a smooth crack of annular form. The use of a flat end to the cylinder, therefore, resulted in excessive stresses being introduced at the junction of the end with the cylinder.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"114160442","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c9001520
Stuart M. Myron
Two types of chromium-plated hydraulic cylinders failed by cracking on their outer surfaces. In one case, the parts had a history of cracking in the nominally unstressed, as-fabricated condition. In another, cracks were detected after the cylinders were subjected to a pressure impulse test. Both part types were made of 15-5 PH (UNS S15500) precipitation hardening stainless steel. Hydrogen embrittlement cracking was the likely cause of failure for both part types. Cracking of the as-fabricated parts was ultimately prevented by changing the manufacturing procedure to allow for a reheat treatment. For parts that cracked after pressure testing, excessive dimensional changes precluded the inclusion of a reheat treatment as a manufacturing step, and further failure was averted by carefully employing proper machining practices, avoiding abusive machining.
{"title":"Hydrogen Embrittled Hydraulic Cylinders","authors":"Stuart M. Myron","doi":"10.31399/asm.fach.process.c9001520","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c9001520","url":null,"abstract":"\u0000 Two types of chromium-plated hydraulic cylinders failed by cracking on their outer surfaces. In one case, the parts had a history of cracking in the nominally unstressed, as-fabricated condition. In another, cracks were detected after the cylinders were subjected to a pressure impulse test. Both part types were made of 15-5 PH (UNS S15500) precipitation hardening stainless steel. Hydrogen embrittlement cracking was the likely cause of failure for both part types. Cracking of the as-fabricated parts was ultimately prevented by changing the manufacturing procedure to allow for a reheat treatment. For parts that cracked after pressure testing, excessive dimensional changes precluded the inclusion of a reheat treatment as a manufacturing step, and further failure was averted by carefully employing proper machining practices, avoiding abusive machining.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"85 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121718606","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c0047830
Textile-machine crankshafts forged from 4140 steel fractured transversely on one cheek during one to three years of service. The cause of failure for two forgings (one complete fractured forging and second a section that contained the shorter shaft fracture cheek) was determined. Indication of fatigue failure was revealed by visual examination of the fracture surfaces. Rough grooves from hot trimming of the flash were visible on the surface of the cheeks. The outer face of one cheek of the throw on the forging contained shallow surface folds. Slightly decarburized forged surface was identified around one of the folds and a fatigue crack initiated in the fold and propagated across the cheek. Properties representative of 4140 steel, quenched and tempered to a hardness of 20 to 22 HRC, were observed. Tempered bainite was revealed in the general microstructure. As a corrective measure, the forgings were normalized, hardened and tempered to 28 to 32 HRC before being machined to increase fatigue strength and extremely rough surfaces were removed by careful grinding.
{"title":"Fatigue Fracture of a 4140 Steel Forged Crankshaft Resulting From Stress Raisers Created During Hot Trimming","authors":"","doi":"10.31399/asm.fach.process.c0047830","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c0047830","url":null,"abstract":"\u0000 Textile-machine crankshafts forged from 4140 steel fractured transversely on one cheek during one to three years of service. The cause of failure for two forgings (one complete fractured forging and second a section that contained the shorter shaft fracture cheek) was determined. Indication of fatigue failure was revealed by visual examination of the fracture surfaces. Rough grooves from hot trimming of the flash were visible on the surface of the cheeks. The outer face of one cheek of the throw on the forging contained shallow surface folds. Slightly decarburized forged surface was identified around one of the folds and a fatigue crack initiated in the fold and propagated across the cheek. Properties representative of 4140 steel, quenched and tempered to a hardness of 20 to 22 HRC, were observed. Tempered bainite was revealed in the general microstructure. As a corrective measure, the forgings were normalized, hardened and tempered to 28 to 32 HRC before being machined to increase fatigue strength and extremely rough surfaces were removed by careful grinding.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"68 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116201177","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-06-01DOI: 10.31399/asm.fach.process.c0089793
During the final shop welding of a large armature for a direct-current motor (4475 kW, or 6000 hp), a loud bang was heard, and the welding operation stopped. When the weld was cold, nondestructive evaluation revealed a large crack adjacent to the root weld. Investigation showed the main crack had propagated parallel to the fusion boundary along the subcritical HAZ and was associated with long stringers of type II manganese sulfide (MnS) inclusions. This supported the conclusion that the weld failed by lamellar tearing as a result of the high rotational strain induced at the root of the weld caused by the weld design, weld sequence, and thermal effects. Recommendations included removing the old weldment to a depth beyond the crack and replacing this with a softer weld metal layer before making the main weld onto the softer layer.
{"title":"Failure During Fabrication of an Armature Because of Lamellar Tearing","authors":"","doi":"10.31399/asm.fach.process.c0089793","DOIUrl":"https://doi.org/10.31399/asm.fach.process.c0089793","url":null,"abstract":"\u0000 During the final shop welding of a large armature for a direct-current motor (4475 kW, or 6000 hp), a loud bang was heard, and the welding operation stopped. When the weld was cold, nondestructive evaluation revealed a large crack adjacent to the root weld. Investigation showed the main crack had propagated parallel to the fusion boundary along the subcritical HAZ and was associated with long stringers of type II manganese sulfide (MnS) inclusions. This supported the conclusion that the weld failed by lamellar tearing as a result of the high rotational strain induced at the root of the weld caused by the weld design, weld sequence, and thermal effects. Recommendations included removing the old weldment to a depth beyond the crack and replacing this with a softer weld metal layer before making the main weld onto the softer layer.","PeriodicalId":294593,"journal":{"name":"ASM Failure Analysis Case Histories: Processing Errors and Defects","volume":"56 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116296211","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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